Test Report. on Type Testing of Diaphragm Gland Seal Valves Type RWH-03 according to EN ISO 10297:2014

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1 HBAM Test Report Bundesanstalt für Materialforschung und -prüfung on Type Testing of Diaphragm Gland Seal Valves Type RWH-03 according to EN ISO 10297:2014 Reference /2015 DGA reference DGA Copy 1sl copy of 2 copies Customer tekno valves Natun Rasta, Bilkanda 24 Parganas (N) Kolkata India Order date 14 June 2014 Receipt of order 14 June 2014 Type of testing Initial testing Receipt of samples 19 x TV/DR-2922/2014 (samples with aluminium and plastic handwheels and PA 6.6 and PCTFE seat) for testing the mechanical properties between August 2014 and February x TV/DR-3248/2015 for testing the mechanical properties on Test period Marchto July 2015 Test location Division 2.1 "Gases, Gas Plants" Working Group Pressure Equipment - Accessories" Building 44 Test procedure according to EN ISO 10297:2014 This test report consists of page 1 to 5 and enclosures to procedure /2015. The pressures indicated in the test report are over-pressures in bar. This lest report may only be published in MI wordmg and without any additions A revocable written consent shall be obtained (rom BAMbeforehand for any amended reproduction or the publication of any excerpts. The content of the test report refers exclusively to the objects tested x Safely in technology and chemistry

2 BAM Test Report page 2 of 5 pages / Description of valves and documentation 1.1 Description of valves Figure 1: TV/DR-2922/2014 The valves (see Figure 1) consist of a valve body, a sealing system for internal and external tightness (five metallic diaphragms with a spring loaded non-metallic seat) and an operating mechanism with handwheel. They are optionally equipped with a pressure relief device (bursting disc or combined bursting disc with fusible plug), see 1.2 Documentation. The valves having a maximum valve test pressure of 250 bar are intended for gas cylinders for technical gases and for a total package mass of more than 111 kg have to be used with a valve protection according to ADR. 1.2 Documentation Drawings Assembly drawing TV/DR-2922/2014/Amd with integrated parts list Assembly drawing TV/DR-3248/ with integrated parts list Further documents List of gases Annexure T List of pressure relief devices TV/DR/CE-2176/ BAM Test Report on PRDs DG BAM Test Report on PRDs DGA

3 BAM Test Report page 3 of 5 pages /2015 Performed tests and test results Requirement/Test (note) General according to EN ISO no. 5.1 Materials according to EN ISO no. 5.2 Dimensions according to EN ISO no. 5.3 Test result (note) (Valve body material according to 5.2 a).) (The valves are not of the pin-index type for medical service.) (The valves are not intended to be protected by a valve protection cap according to Figure 1 of EN ISO 11117:2008.) Valve connections according to EN ISO no. 5.4 Mechanical strength according to EN ISO no. 5.5 Valve operating mechanism according to EN ISO no. 5.6 (See 3 Summary.) (See tests no. 6.9 and Annex A.) The requirements are fulfilled or partiy not applicable (see below). (See tests no. 6.11, 6.12, 6.13, 6.14 and Annex B.) Valve operating device according to EN ISO no. 5.7 Leakage according to EN ISO no. 5.8 Resistance to ignition according to EN ISO no. 5.9 (See test no ) (See test no ) (The valves are not intended to be used for oxygen or other oxidizing gases.) (See test Annex C.) General according to EN ISO no. 6.1 Documents according to EN ISO no. 6.2 Hydraulic burst pressure test according to EN ISO no. 6.9 (Pi/w = 469 bar, t > 2 min) All requested documents have been provided. carried out on TV/DR-2922/2014 and TV/DR-3248/2015

4 BAM Test Report page 4 of 5 pages /2015 Requirement/Test (note) Flame impingement test according to EN ISO no (t>1 min, 0 = 800 C C) Excessive torque test according to EN ISO no (T0 = 20 Nm; T, = 25 Nm according to the handwheel diameter of 65 mm) Test result (note) (Tc determined = 6.0 Nm.) Tightness tests according to EN ISO no (pw = 0,5 bar, 10 bar and 250 bar at 0 = -40 C -20 C, RT and +65 C with helium) (In addition to the requirements the valves were also tested for external tightness at -40 C.) Endurance test according to EN ISO no (Prt = 250 bar, 2000 cycles with 7"e.sfart = 7 Nm: Te.end = 7 Nm) Visual examination according to EN ISO no Marking according to EN ISO no. 7 Impact test according to EN ISO Annex A ( = 400 J, valving torque = 200 Nm) subsequent hydraulic burst pressure test {Pvbt = 469 bar, t > 2 min) subsequent internal tightness test (pw = 250 bar, 0 = RT with air) All required markings are existent. (The identification of further inlet and outlet connec tions in addition to the ones given in 3 Summary has to be marked.) (Valves with a total package mass of more than 111 kg require a valve protection according to ADR.) (The test results are transferrabie to inlet connections 25E according to EN ISO and 3/4-14 NGT according to CGA V-1.) carried out on valves with inlet thread 1"according to BS 341 of TV/DR-2922/2014 and TV/DR-3248/2015 (The number of protruding threads after the valving procedure amounted to 2.) Test for acetylene valves according to EN ISO Annex B (pvb, = 909 bar, pvl = 60 bar) Oxygen pressure surge test according to EN ISO Annex C

5 BAM Test Report page 5 of 5 pages / Summary The diaphragm gland seal valves type RWH-03 manufactured by the Company tekno valves, India with the common features Type Gas Classification Drawing number Design Inlet connection Outlet connection Material of valve body Sealing against atmosphere Sealing in the seat Lubricant Nominal diameter Handwheel diameter Tightness tested with Strength tested with Total package mass Impact test carried out with RWH-03 see Annexure T TV/DR-2922/2014 TV/DR-3248/2015 handwheel operated diaphragm gland seal valve 25EtoEN ISO /4-14 NGTtoCGAV-1 1"toBS341 CGA 660 to CGA V-1 or as per any other regional/national/international Standards CW722R, EN 12165:1998 metallic diaphragm PA 66 / PCTFE Krytox GPL mm 65 mm p = 0.5 bar, 10 bar and 250 bar at t= -40 C, -20 C, +20 C and +65 C 469 bar 111 kg 400 J, intended for gas cyiinders to be used with a valve protection according to ADR (for a total package mass of more than 111 kg) fulfil the requirements of EN ISO 10297:2014. The use of the valves is restricted to the above mentioned gases as well as inlet connections. BAM Federal Institute for Materials Research and Testing Berlin, 7 August 2015 Division 2.1 "Gases, Gas Plants" by order M UV B. Eng. Andreas Woitzek Study Director "Pressure Equipment - Accessories" The BAM Division 2 1.Gases, Gas Plants" is mcluded in the accreditation of the BAM Certification Body granted by the Deutsche Akkreditierungsstelle GmbH (DAkkS) according to DIN EN ISO/IEC The accreditation applies for the inspection procedures itemized in the accreditation certificate (D-IS ). (( DAkkS Deutsche Akkreditierungsstelle D-IS Test results of non-accredited test methods are marked (with an asterisk). Distribution list: 1sl copy: tekno valves 2nd copy: BAM - Division 2.1 Gases, Gas Plants" Enclosures: Drawings and documents stamped with procedure number

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