Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005

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1 Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005 Period of validity: to Holder of certificate: Haltermann Carless Deutschland GmbH Qualitätssicherungs-Labor Werk Hamburg at the locations: Schlengendeich 17, Hamburg Joachim-Becher-Str. 1, Speyer Tests in the fields: chemical and physical-chemical testing of mineral oil and related products, selected properties of gasoline fuel, diesel fuels, diesel fuels from fatty acid methyl ester (FAME); printing ink distillates Abbreviations used: see last page Within the fields marked with * the testing laboratory is permitted, without being required to inform and obtain prior approval from DAkkS, the following: usage of different versions of standard test s granted here. The testing laboratory maintains a current list of all testing s within the flexible scope of accreditation. This document is a translation. The definitive version is the original German annex to the accreditation certificate. 1/19

2 Location Hamburg: 1. Fuels 1.1 Gasoline* Density DIN Testing of mineral oils and related materials - Determination of density procedure 3 (withdrawn) DIN EN ISO ASTM D 4052 Crude petroleum and petroleum products - Determination of density - Oscillating U-tube Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter Distillation Characteristics DIN EN ISO ASTM D Petroleum products - Determination of distillation characteristics at atmospheric pressure Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure Vapor Pressure ASTM D DIN EN Standard Test Method for Vapor Pressure of Petroleum Products (Mini Method) Vapor Pressure part 1: Determination of air saturated vapor pressure (ASVP) and calculation of equivalent to dry vapor pressure (DVPE) Period of validity: to Translation - 2/19

3 Content of Lead DIN EN ASTM D Determination of low contents lead by atomic absorption spectroscopy Standard Test Method for Lead in Gasoline by Atomic Absorption Spectroscopy Content of sulphur DIN EN ISO ASTM D 5453 Determination of sulfur content of automotive fuels - Ultraviolet fluorescence Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultra-violet Fluorescence evaporation residue DIN EN ISO ASTM D DIN Evaporation residue of volatile and middle distillate fuels - jet evaporation Standard Test Method for Gum Content in Fuels by Jet Evaporation Solvents for coating materials- determination of evaporation residue corrosiveness DIN EN ISO Petroleum products - Corrosiveness to copper - Copper strip test - corrosiveness to copper - copper strip test Period of validity: to Translation - 3/19

4 ASTM D Standard Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test content of benzene DIN EN DIN EN ISO ASTM D Determination of the benezene content by infrared spectrometry Determination of hydrocarbon types and oxygenates in automotive-motor gasoline and in ethanol (E85) automotive fuel - Multidimensional gas chromatography Standard Test Method for Hydrocarbon Types, Oxygenated Compounds and Benzene in Spark Ignition Engine Fuels by Gas Chromatography Oxygenates ASTM D b DIN EN ISO MTBE, ETBE, TAME, DIPE, tertiary-amyl Alcohol and C1 to C4 Alcohols in Gasoline by Gas Chromatography Determination of hydrocarbon types and oxygenates in automotive-motor gasoline and in ethanol (E85) automotive fuel - Multidimensional gas chromatography Period of validity: to Translation - 4/19

5 ASTM D ASTM D (reapproved ) Standard Test Method for Hydrocarbon Types, Oxygenated Compounds and Benzene in Spark Ignition Engine Fuels by Gas Chromatography Ethanol and Methanol Content in Fuels containing greater 20 % Ethanol by Gas Chromatography Hydrocarbon types DIN EN ISO ASTM D ASTM D ISO Corrigendum Determination of hydrocarbon types and oxygenates in automotive-motor gasoline and in ethanol (E85) automotive fuel - Multidimensional gas chromatography Standard Test Method for Hydrocarbon Types, Oxygenated Compounds and Benzene in Spark Ignition Engine Fuels by Gas Chromatography Standard Test Method for Hydrocarbon Types in Liquid Petroleum Products by Fluorescent Indicator Adsorption Liquid petroleum products - Determination of hydro-carbon types -fluorescent indicator adsorption Neutralization number ASTM D Standard Test Method for Acid and Base Number by Color-Indicator Titration Period of validity: to Translation - 5/19

6 n-heptane, i-octane und toluene ASTM D (reapproved 2013) ASTM D Standard Test Method for Analysis of High- Purity n-heptane and Isooctane by Capillary Gas Chromatography Standard Test Method for Trace Impurities in Mono-cyclic Aromatic Hydrocarbons by Gas Chromatography water content DIN EN ISO ASTM D 6304 ASTM E 1064 Determination of water - Coulometric Karl Fischer titration Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration Calculation of net heat of combustion ASTM D 3338/D 3338M 2009 (reapproved: 2014) Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels Calculation of hydrogen content ASTM D 3343 Standard Test Method for Estimation of Hydrogen Content of Aviation Fuels Refractive Index Measurement DIN measurement of relative refractive index by precision refractometer Period of validity: to Translation - 6/19

7 DIN Testing of mineral oils part 2: measurement of relative refractive index by abberefractometer GC-Composition DIN ASTM D ASTM D Testing of mineral oil hydrocarbons, similar liquids and solvents for paints and varnishes - Analysis by gas chromatography - General working principles Benzene, Toluene, Ethylbenzene, p/m- Xylene, o-xylene, C9 and Heavier Aromatics, and Total Aromatics in Finished Gasoline by Gas Chromatography Standard Test Method for Detailed Analysis of Petroleum Naphthas through n-nonane by Capillary Gas Chromatography (Benzene- and n-hexane- Content) Miscellaneous ISO ASTM D ASTM D General for determination of chloride ions - Potentiometric Standard Test Method for Hydroperoxide Number of Aviation Turbine Fuels, Gasoline and Diesel Fuels Standard Test Method for Oxidation Stability of Spark Ignition Fuel - Rapid Small Scale Oxidation Test (RSSOT) DIN ISO Clear liquids - Estimation of colour by the platinum-cobalt colour scale (withdrawn) Period of validity: to Translation - 7/19

8 1.2 Diesel Fuel * Density DIN Testing of mineral oils and related materials - Determination of density - procedure 3 DIN EN ISO ASTM D 4052 Crude petroleum and petroleum products - Determination of density - Oscillating U-tube Standard Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter Distillation Characteristics DIN EN ISO ASTM D Petroleum products - Determination of distillation characteristics at atmospheric pressure Standard Test Method for Distillation of Petroleum Products at Atmospheric Pressure Viscosity DIN EN ISO ASTM D a Petroleum products - Transparent and opaque liquids - Determination of kinematic viscosity and calculation of dynamic viscosity Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids (and Calculation of Dynamic Viscosity) (withdrawn standard) Period of validity: to Translation - 8/19

9 Flash Point ASTM D 93 a DIN EN ISO Standard Test Methods for Flash Point by Pensky-Martens Closed Cup Tester (withdrawn standard) Determination of flash point - Pensky- Martens closed cup Sulphur Content DIN EN ISO ASTM D Determination of sulfur content of automotive fuels - Ultraviolet fluorescence Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultraviolet Fluorescence Cold Filter Plugging Point (CFPP) ASTM D DIN EN Standard Test Method for Cold Filter Plugging Point of Diesel and Heating Fuels Determination of cold filter plugging point - Stepwise cooling bath Cloud Point DIN EN ISO ASTM D 2500 b Petroleum products - determination of cloud point Petroleum products - Determination of cloud point Standard Test Method for Cloud Point of Petroleum Products Period of validity: to Translation - 9/19

10 Pour Point DIN ISO ASTM D a ASTM D (reapproved: 2014) Petroleum products - Determination of pour point Standard Test Method for Pour Point of Petroleum Products Standard Test Method for Pour Point of Petroleum Products (Robotic Tilt Method) Carbon Residue DIN EN ISO ASTM D Determination of carbon residue - Micro Carbon Residue (Micro Method) Water Content DIN EN ISO ASTM D 6304 ASTM E 1064 Determination of water - Coulometric Karl Fischer titration Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl Fischer Titration Standard Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration Neutralization Number ASTM D Standard Test Method for Acid and Base Number by Color-Indicator Titration Period of validity: to Translation - 10/19

11 Cetane Index DIN EN ISO ASTM D (reapproved ) ASTM D (reapproved 2011) Calculation of cetane index of middledistillate fuels by the four-variable equation Standard Test Method for Calculated Cetane Index by Four Variable Equation in Verbindung mit: und Standard Test Method for Calculated Cetane Index of Distillate Fuels Corrosiveness DIN EN ISO ASTM D Petroleum products - Corrosiveness to copper - Copper strip test (ISO 2160:1998) Standard Test Method for Corrosiveness to Copper from Petroleum Products by Copper Strip Test Total Contamination DIN EN Determination of total contamination in middle distillates, diesel fuels and fatty acid methyl esters Lubricity DIN ISO ASTM D (reapporved ) Assessment of lubricity using the highfrequency reciprocating rig (HFRR) - Part 1: Test Standard Test Method for Evaluating Lubricity of Diesel Fuels by the High- Frequency Reciprocating Rig (HFRR) Period of validity: to Translation - 11/19

12 Cetane and 1-Methylnaphthalene DIN Determination of purity by gaschromategraphy - part 2: cetane and 1-methylnaphthalene Aromatic Hydrocarbons DIN EN Determination of aromatic hydrocarbon types in middle distillates - High performance liquid chromatography with refractive index detection FAME DIN EN Determination of fatty acid methyl ester (FAME) content in middle distillates - Infrared spectrometry Calorific Value ASTM D 3338/D 3338M 2009 (reapproved: 2014) Standard Test Method for Estimation of Net Heat of Combustion of Aviation Fuels Hydrogen Content ASTM D 3343 Standard Test Method for Estimation of Hydrogen Content of Aviation Fuels Oxidation Stability DIN EN Fatty acid methyl ester (FAME) fuel and blends with diesel fuel - Determination of oxidation stability by accelerated oxidation Period of validity: to Translation - 12/19

13 DIN EN ISO DIN EN ASTM D ASTM D Determination of the oxidation stability of middle-distillate fuels Middle distillates and fatty acid methyl ester (FAME) fuels and blends - Determination of oxidation stability by rapid small scale oxidation Standard Test Method for Oxidation Stability of Middle Distillate Fuels - Rapid Small Scale Oxidation Test (RSSOT) Standard Test Method for Oxidation Stability of Distillate Fuel Oil (Accelerated Method) Conductivity ASTM D DIN Standard Test Methods for Electrical Conductivity of Aviation and Distillate Fuels Determination of electrical conductivity part 1: laboratory Refractive Index Measurement DIN DIN measurement of relative refractive index by precision refractometer Testing of mineral oils part 2: measurement of relative refractive index by abberefractometer Period of validity: to Translation - 13/19

14 GC-Composition DIN Testing of mineral oil hydrocarbons, similar liquids and solvents for paints and varnishes - Analysis by gas chromatography - General working principles Aniline Point DIN ISO Determination of aniline point and mixed aniline point Peroxid Number ASTM D DIN EN Anhang C Standard Test Method for Hydroperoxide Number of Aviation Turbine Fuels, Gasoline and Diesel Fuels Calculation of saturated monoglycerides content in diesel fuels by EN 590 in combination with: DIN EN DIN EN Determination of monoglyceridecontent Determination of cloudpoint FAME Period of validity: to Translation - 14/19

15 1.3 Diesel Fuel from Fatty Acid Methylester (FAME) * Ester Content DIN EN Determination of ester and linolenic acid methyl ester contents Density DIN EN ISO DIN Crude petroleum and petroleum products - Determination of density - Oscillating U-tube Testing of mineral oils and related materials - Determination of density procedure 3 Viscosity DIN EN ISO Petroleum products - Transparent and opaque liquids - Determination of kinematic viscosity and calculation of dynamic viscosity Sulphur Content DIN EN ISO ASTM D 5453 Determination of sulfur content of automotive fuels - Ultraviolet fluorescence Total Sulfur in Light Hydrocarbons, Spark Ignition Engine Fuel, Diesel Engine Fuel, and Engine Oil by Ultra-violet Fluorescence Period of validity: to Translation - 15/19

16 Water Content DIN EN ISO Determination of water - Coulometric Karl Fischer titration Total Contamination DIN EN Determination of total contamination in middle distillates, diesel fuels and fatty acid methyl esters Corrosiveness DIN EN ISO corrosiveness to copper - copper strip test Oxidation Stability DIN EN Determination of oxidation stability (accelerated oxidation test) Acid DIN EN Determination of acid value Iodine Value DIN EN DIN EN Determination of iodine value Determination of iodine value in fatty acid methyl esters (FAME) - Calculation from gas chromatographic data Period of validity: to Translation - 16/19

17 Methanol DIN EN Determination of methanol content Content of free and total Glycerol and Mono-, Di-, Triglyceride / / DIN EN Determination of free and total glycerol and mono-, di-, triglyceride contents Cold Filter Plugging Point (CFPP) DIN EN Determination of cold filter plugging point Cloud Point DIN EN DIN EN Anhang C Petroleum products; determination of cloud point Calculation of saturated monoglycerides content in FAME in combination with: DIN EN Determination of monoglyceride content DIN EN Determination of cloudpoint FAME Period of validity: to Translation - 17/19

18 2. Printing Ink Distillates * Density DIN EN ISO Crude petroleum and petroleum products - Determination of density - Oscillating U-tube Aniline Point DIN ISO Determination of aniline point and mixed aniline point Period of validity: to Translation - 18/19

19 Location Speyer: 3. Fuels 3.1 Gasoline * ASTM D Benzene, Toluene, and Total Aromatics in Finished Gasolines by Gas Chromatography/ Mass Spectrometry Abbreviations used: ASTM FAME ISO Process-Matrix- American Society for Testing and Materials fatty acid methyl ester (Fettsäuremethylester) International Organization for Standardization Number of the characteristics within the Process-Matrix for Mineral Oel (72 FB Version 1.2, August 2017) Period of validity: to Translation - 19/19

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