LISA Inspectorate Estonia AS akrediteerimistunnistusele nr L029 ANNEX to the accreditation certificate No L029 of Inspectorate Estonia Ltd.

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1 LISA Inspectorate Estonia AS akrediteerimistunnistusele L029 ANNEX to the accreditation certificate No L029 of Inspectorate Estonia Ltd. 1. Akrediteerimisulatus on: Accreditation scope is: materjal või toode No Parameter Materials or products tested / tested 1. Tuha sisalduse määramine Ash determination 2. Broomiarvu määramine elektromeetrilise tiitrimisega Bromine number dmnetermination by electrometric titration 3. Leektäpi määramine Pensky-Martensi suletud nõus Determination of Flash-Point by Pensky-Martens closed cup 4. Vee määramine destilleerimisega Determination of water by distillation 5. Neto-ja kogupõlemissoojuse määramine Estimation of net and gross heat of combustion Kütteõli, bensiin, diislikütus Fuel oil, gasoline, gasoil Kütteõli, diislikütus, määrdeõli Fuel oil, diesel fuel, luboil Kütteõli, diislikütus, määrdeõli Fuel oil, diesel fuel, luboil Kütteõli, diislikütus, määrdeõli Fuel oil, diesel fuel, luboil Kütteõli, diislikütus, määrdeõli Fuel oil, diesel fuel, luboil D482; IP4; EN ISO 6245 D1159 D93; IP34;EN ISO 2719 D95; IP74; EN ISO 3733 D Tiheduse määramine hüdromeetrilisel meetodil Density determination by hydrometer method Kütteõli, bensiin, diislikütus, nafta, määrdeained Fuel oil, gasoline, gasoil, crude oil, lubricants D1298; IP160; ISO 3675 EN 7. Tiheduse määramine elektroonse mõõturiga Density determination by digital density meter 8. Väävli määramine fluoresentsröntgenspektroskoobiga Determination of sulphur by X-ray fluorescence spectroscopy 9. Metallide määramine AAS meetodil Determination of metals by AAS Kütteõli, bensiin, diislikütus, nafta, määrdeained Fuel oil, gasoline, gasoil, crude oil, lubricants Kütteõli, bensiin, diislikütus, nafta, määrdeained Fuel oil, gasoline, gasoil, crude oil, lubricants Kütteõli, bensiin, diislikütus, nafta, määrdeained Fuel oil, gasoline, gasoil, crude oil, lubricants D4052; IP 365; ISO D4294; IP 365; ISO 8754 IP 377; ISO 10478

2 Leht/Page 2/21 materjal või toode No Parameter Materials or products tested / tested 10. Leek- ja põlemistäpi määramine Clevelandi avatud nõus Flash point Cleveland. 11. Tahkete osiste määramine ekstraheerimismeetodiga 12. Kinemaatilise viskoossuse määramine Determination of kinematic viscosity 13. Hangumispunkti määramine Pour point Kütteõli, määrdeained Fuel oil, lubricants Kütteõli, diislikütus, nafta Fuel oil, gasoil, crude oil Kütteõli, diislikütus, nafta, määrded Fuel oil, gasoil, crude oil, lubricants Kütteõli, diislikütus, nafta, määrded Fuel oil, gasoil, crude oil, lubricants D92; IP36; EN ISO 2592 D473; IP53; 3735 ISO D445; IP 71; EN ISO 3104 D97; IP Asfalteenide määramine Determination of asphaltenes 15. Destillatsioon madaldatud rõhul Distillation at reduced pressure 16. Tahkete osiste määramine Determination of total sediment Kütteõli Fuel oil IP 143 Kütteõli Fuel oil Kütteõli Fuel oil D1160 D4870; IP375; Shell Mod.Stand Koksiarvu määramine Coadsoni järgi Determination of Coadson Carbon Residue 18. Stabiilsuse määramine Determination of stability and compatibility 19. Asfalteenide P-väärtuse määramine Determination of P-value of asphaltenes 20. Tolueeni ekvivalentpunkti määramine Determination of toluene equivalence point Kütteõli Fuel oil Kütteõli Fuel oil Kütteõli Fuel oil Kütteõli Fuel oil D189 D4740 Shell Mod.Stand Exxon AM-S Modifitseeritud ksüleeni- ekvivalendi katse Kütteõli Fuel oil BP 230 mod. Modified xylene equivalent test 22. Flokulatsiooni piirkond/ Flocculation ratio Kütteõli Fuel oil Shell Mod.Stand. 305

3 Leht/Page 3/21 No Parameter Materials or products tested / tested 23. Fraktsioonkoostise määramine Determination of distillations Nafta, bensiin, diislikütus, lennukikütus Crude oil, gasoline, gasoil, aviation fuels D86; IP123; EN-ISO Vee määramine destilleerimisega Determination of water by distillations 25. Vee määramine potentsiomeetrilise Karl Fischeri tiitrimisega Determination of water by potentiometric Karl Fischer titration 26. H 2 S määramine Determination of H 2 S 27. Merkapaanväävli määramine potentsiomeetrilise meetodiga Determination of mercaptan sulphur by potentiometric method 28. Korrosioon vaskplaadil Copper corrosion by copper strip tarnish test Toornafta Crude oil Toornafta Crude oil Toornafta, bensiin, naftaleen, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoils Toornafta, bensiin, naftaleen, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoils Toornafta, bensiin, naftaleen, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumgaasiõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoils D4006; IP74 D4377; DIN United Org. of Petrol. 163/Mobil D3227; IP342 D130; IP 154; EN ISO 2160

4 Leht/Page 4/21 No Parameter Materials or products tested / tested 29. Tiheduse määramine Digitaalmõõturiga Density and Relative Density of Crude Oils by Digital Density Meter 30. Oksüdatsiooniline stabiilsus Oxidation Stability of Gasoline (Induction Period ) 31. Aromaatsete süsivesinike määramine keskmistes destillaatides Determination of aromatic hydrocarbon types in middle distillates. High performance liquid chromatography(hplc) method with refractive index detection Toornafta, bensiin, solvent nafta, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumgaasiõli aviation fuels, kerosene, gasoil, fuel oil, vacuum gasoils Toornafta, bensiin, naftaleen, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoils Toornafta, bensiin, naftaleen, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoils D5002 D 525 EN ISO 7536 IP Väävli sisalduse määramine ultraviolettfluoresentsmeetodil. Determination of sulfur content of automotive fuels. Ultraviolet fluorescence method Toornafta, bensiin, naftaleen, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli IP 490 EN ISO aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoils 33. Vaikude sisaldus. Gum Content in Fuels by Jet Evaporation Toornafta, bensiin, naftaleen, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoils D 381 EN ISO 6246

5 Leht/Page 5/21 materjal või toode No Parameter Materials or products tested / tested 34. Vaba vee ja tahkete osiste määramine destilleeritud kütuses visuaalselt Visual inspection of free water and particulate contamination in distillate fuels 35. Hägustumispunkti määramine Determination of cloud point 36. Külmfiltreeritavuspunkti määramine Determination of cold filter plugging point CFPP 37. värvuse määramine Determination of Colour 38. Arvutatud tsetaanindeks Calculated cetane index by four variable equation Toornafta, bensiin, solvent nafta, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoil Toornafta, bensiin, solvent nafta, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoil Toornafta, bensiin, solvent nafta, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoil Toornafta, bensiin, solvent nafta, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoil Toornafta, bensiin, solvent nafta, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoil D4176 D2500; IP219 IP309 D1500; IP196 D4737; IP380;

6 Leht/Page 6/21 materjal või toode No Parameter Materials or products tested / tested 39. Aniliinpunkti määramine Determination of aniline point 40. Diisli indeksi määramine Determination of diesel index Toornafta, bensiin, solvent nafta, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoil Toornafta, bensiin, solvent nafta, lennukikütus, petroleum, diislikütus, kütteõli ja vaakuumõli aviation fuels, kerosene, gasoil, fuel oil and vacuum gasoil D611; IP2 41. Happearvu määramine Determination of acid number Määrdeained, bensiin Lubricants,gasoline D664; D974; IP139; 42. Saybolti värvuse määramine Determination of Saybolt colour Bensiin Gasoline D156

7 Leht/Page 7/21 No Parameter Materials or products tested / tested 43. Väävli avastamine Doctor testiga Detection of sulphur by Doctor test 44. Määrimisomadused Evaluating Lubricity 45. Asfalteenide määramine Asphaltene Determination in Petroleum Distillates/ Residues by Visible Spectrophotometry 46. Bakterioloogiline test Bacteriological Test 47. Põlemissoojuse määramine Heat of Combustion Bensiin Gasoline Bensiin Gasoline Naftasaadused Petroleum products Naftasaadused Petroleum products Naftasaadused Petroleum products IP30 ISO ; D 6079 Total 642/89E IP 385 D Vesiniksulfiidi määramine Hydrogen Sulphide in Fuel Oil Naftasaadused Petroleum products IP Nikli, vanaadiumi, naatriumi ja raua sisalduse määramine AAS meetodiga Determination of Nickel, Vanadium, Iron and Sodium in Crude Oils and Residual Fuels by Flame AAS 50. Lämmastiku sisalduse määramine modifitseeritud Kjeldahli meetodil Total Nitrogen in Lubricating Oils and Fuel by Modif Kjeldahl 51. Hangumispunkti määramine Pour Point of Crude Oils Naftasaadused Petroleum products Naftasaadused Petroleum products Naftasaadused Petroleum products D 5863 D 3228 D Üldniiskussisalduse määramine Total Moisture Determination 53. Tuhasisalduse määramine Ash content Kivisüsi, koks ja puidupelletid Coal, coke and wooden pellets Kivisüsi, koks ja puidupelletid Coal, coke and wooden pellets ISO 589 ISO 331 ISO 687 ISO Väävlisisalduse määramine Sulfur content Kivisüsi, koks ja puidupelletid Coal, coke and wooden pellets D Lenduvainete määramine Volatile matter content Kivisüsi, koks ja puidupelletid Coal, coke and wooden pellets ISO 562

8 Leht/Page 8/21 materjal või toode No Parameter Materials or products tested / tested 56. Põlemissoojuse määramine kalorimeetrilise pommi meetodiga ja arvutamine. Determination of cross calorific value by calorimeter bomb method and calculation of net calorific value 57. Kloori määramine Chlorine Determination 58. Tuha sulamine Ash Fusion/ Fusibility determination (coal and coke ash) Kivisüsi, koks ja puidupelletid Coal, coke and wooden pellets Kivisüsi, koks ja puidupelletid Coal, coke and wooden pellets Kivisüsi, koks ja puidupelletid Coal, coke and wooden pellets ISO 1928 D 2361 D Lämmastiku määramine Determination of Nitrogen in the analysis sample of Coal and Coke (Kjeldahl-Gunning ) 60. Tuha määramine AAS meetodiga Determination of Ash Elements (major and minor) in Coal and Coke ash by AAS 61. Üldfosfori määramine IA meetodiga Determination of Total Sulphur in Coal and Coke using a High-Temperature Tube Furnace Combustion with Infrared Absorption 62. Oksüdatsiooniline stabiilsus Oxidation Stability of Distillate Fuel Oil (Accelerated ) 63. Vahasisaldus Wax Content 64. Juhtivus Conductivity Kivisüsi, koks ja puidupelletid Coal, coke and wooden pellets Kivisüsi, koks ja puidupelletid Coal, coke and wooden pellets Kivisüsi, koks ja puidupelletid Coal, coke and wooden pellets Toornafta, bensiin, naftaleen, diislikütus, kütteõli ja vaakuumiõli gasoil, fuel oil and vacuum gasoils Toornafta Crude oil Toornafta, bensiin, naftaleen, diislikütus gasoil D3179 D3682 D 5016 D a UOP

9 Leht/Page 9/21 materjal või toode No Parameter Materials or products tested / tested 65. Parafiini, nafteeni ja aromaatsete süsivesinike tüübi määramine MD gaasikromatograafia meetodil Paraffin, naphtene and Aromatic Hydrocarbon type analyses. 66. Oksügenaadid ja parafiin, olefiin, nafteen ja aromaatsed ühendid gaasikromatograafia meetodil Oxygenates and Paraffin, Olefin, Naphtene, Aromatic (O-PONA) Types GC 67. Vees lahustuvad happed ja leelised Water Soluble acids and alkalis 68. Üldsaastatus Total contamination Bensiin, solvent nafta Gasoline, naphta Bensiin, solvent nafta Gasoline, naphta Toornafta, bensiin, naftaleen, diislikütus, kütteõli ja vaakuumiõli gasoil, fuel oil and vacuum oils Toornafta, bensiin, naftaleen, diislikütus, kütteõli ja vaakuumiõli gasoil, fuel oil and vacuum oils D5443 D6839 GOST IP Tina sisaldus Lead Content Toornafta, bensiin, naftaleen, diislikütus, kütteõli ja vaakuumiõli IP Elavhõbeda ja arseeni sisaldus Mercury, Arsenic content 71. Erimärgistusaine Solvent, Red, Blue, Yellow gasoil, fuel oil and vacuum oils Toornafta, bensiin, naftaleen, diislikütus, kütteõli ja vaakuumiõli gasoil, fuel oil and vacuum oils Toornafta, bensiin, solvent nafta, diislikütus, kütteõli ja vaakuumiõli gasoil, fuel oil and vacuum oils Cold vapour method by AAS VV No. 194

10 Leht/Page 10/21 materjal või toode No Parameter Materials or products tested / tested 72. Arseeni määramine Arsenic content determination Toornafta, bensiin, naftaleen, diislikütus, kütteõli ja vaakuumiõli EN ISO fuel oil and vacuum oils gasoil, 73. Mineraalväetiste õli imavus Determination of oil retention of mineral 74. Mineraalväetiste vastupanu lõhkemisele Determination of resistance to detonation of mineral 75. Süsinikuna väljendatavad lõhkevad aineosad Combustible ingredients expressed as Carbon EC Regulation 2003/2003 Annex III Art.3, 2 EC Regulation 2003/2003 Annex III Art.4, EC Regulation 2003/2003 Annex ph EC Regulation 2003/ Granulomeetria Granulometry <1 mm <0,5mm III Annex III 4 EC Regulation 2003/2003 Annex Kloor Chlorine EC Regulation 2003/2003 III Annex III 6

11 Leht/Page 11/21 Määratav näitaja No Parameter 79. Vask Copper (Cu) 80. Nitraati sisaldavate väetiste eksotermiline lagunemine Trough test for determination of the selfsustaining exothermic decomposition of fertilizers containing nitrates 81. Test for Oxidizing Solids Test 0.1: Materials or products tested / tested EC Regulation 2003/2003 Annex III 7 Test method Sec 38, UN Manual of tests and Criteria Section 34 of UN Manual of Tests and Criteria, 2015 (Recom. on the Transport of Dangerous Goods)

12 Leht/Page 12/21 No Parameter Materials or products tested / tested 82. UN Gap Test 83. Koenen Test 84. UN Time/Pressure Test 85. Korrodeerivuskatse Test C.1: Test for determining the corrosive properties of liquids and solids that may become liquid during transport 86. Kaadmiumi määramine väetistes Cadmium content determination in fertilizers 87. Kroomi määramine Chromium content determination 88. Tihedus Density Test series 1 & 2, type 1 (a) and type 2 (a) as per Section 11 & 12 of UN Manual of Tests and Criteria (Recom. on the Transport of Dangerous Goods) Test Series 1 & 2, test 1 (b) & 2 (b) as per Section 11 & 12 of UN Manual of Tests and Criteria (Recom. on the Transport of Dangerous Goods) Test Series 1 & 2, test 1 (c)(i) & 2 (c)(i) as per Section 11 & 12 of UN Manual of Tests and Criteria (Recom. on the Transport of Dangerous Goods) Section 37 of the UN Manual of Tests and Criteria (Recom. on the Transport of Dangerous Goods) EN EN D 4052 (mod) D Üldlämmastik Total Nitrogen ТУ GOST Ammoniumnitraadi sisaldus Ammonium Nitrate content 91. Lämmastik Nitrogen in the form of Ammonium Nitrate Nitrogen in the form of Urea 92. Ammoniumnitraat Urea/Ammonium Nitrate ТУ ТУ ТУ

13 Leht/Page 13/21 No Parameter Materials or products tested / tested 93. Vaba ammoonium Free Ammonia content Mineral ТУ Dünaamiline viskoossus Viscosity Dynamic 95. Tahkestumispunkt Solidification Point Mineral Mineral D 445 D 2500 (mod.) 96. Külmumispunkt Freezing Point Mineral D 97 (mod) 97. Corrosion Inhibitor content (CORBLOK 9140) 98. Ammooniumi massiprotsent Mass Fraction of Ammonia, NH Lämmastiku massiprotsent Mass Fraction of Nitrogen 100. Vee massiprotsent Mass Fraction of Water, H 2 O 101. Ammooniumi õli sisaldus Oil Content in Ammonia 102. Raua sisaldus Iron (Fe) Mineral Mineral Mineral Mineral Mineral Mineral ACRON in-house method GOST GOST GOST GOST GOST Üldkloori sisaldus Total Chlorine Content Mineral GOST

14 Leht/Page 14/21 No Parameter Materials or products tested / tested 104. Süsinikoksiidi massiosa Mass Fraction of Carbon Oxide (IV) 105. Inertsete gaaside mahuosa Volume Fraction Conditional Inert Gases in Ammonia (Gaseous Ph) Naftasaaduste koguste määramine/arvutamine Petroelum products quantity measurement 107. Naftasaaduste proovivõtmine Sampling of Petroleum Products 108. Naftasaaduste temperatuuri mõõtmine elektroonilise termomeetriga Static Temperature Determination Using Portable Electronic Thermometers 109. Naftasaaduste sügavuste mõõtmine mahutites Gauging of Petroleum Products 110. Naftasaaduste koguste mõõtmine raudtee mahutites Gauging Petroleum Products in Tank Cars Mineral Mineral Naftasaaduste koguse määramine Measurement of quantity of petroleum products Naftasaaduste koguse määramine Measurement of quantity of petroleum products Naftasaaduste koguse määramine Measurement of quantity of petroleum products Naftasaaduste koguse määramine Measurement of quantity of petroleum products Naftasaaduste koguse määramine Measurement of quantity of petroleum products GOST STAs 6 (AS Nitrofert) IP 201/64 Calculation of oil quantities. Petroleum measurement manual. Part I API MPMS Chapter 12.1 Calculation of Static Petroleum Quantities in Upright Cylindrical Tanks and Marine Vessel API Manual of Petroleum Measurement Standards Chapter 8 Sampling Section 1 - Manual Sampling of Petroleum and Petroleum Products, API Manual of Petroleum Measurement Standards. Chapter 7 - Temperature Determination. Section 3 - Static Temperature Determination Using Portable Electronic Thermometers API Manual of Petroleum Measurement Standards Chapter 3 - Tank Gauging. Section 1A- Standard Practice for the Manual.Gauging of Petroleum and Petroleum Product API Manual of Petroleum Measurement Standards Chapter 3 Tank gauging Section 2 Standard Practice for Gauging Petroleum and Petroleum Products in Tank Cars Инструктивные указания по определению веса наливных грузов в цистернах. Утв.гл.упр. вагонного хозяйства МПС 2003

15 Leht/Page 15/21 No Parameter Materials or products tested / tested 111. Naftasaaduste koguste määramine laevamahutites. Petroelum products quantity measurement on Board Tank Vessels 112. Kauba massi mõõtmine kaalumisega Mass measurement by weighing 113. Tükikauba koguse mõõtmine Piece goods measurement (tally survey) 114. Kauba massi mõõtmine laeval süvisemärkide järgi Quantity measurement by draft survey 115. Metsamaterjali mõõtmine Timber quantities measurement 116. Saematerjali koguse mõõtmine Saw quantity measurement 117. Puistekaupade koguse mõõtmine Bulk s quantity measurement 118. Vedelike, va naftasaadused, koguste mõõtmine. Liquid exl petroleum products, quantity measurement 119. Koguste mõõtmine lineaarmõõtmete abil Quantity measurement using linear parameters Naftasaaduste koguse määramine Measurement of quantity of petroleum products Kauba ja materjali Quantity measurement of s and goods Kauba ja materjali Quantity measurement of s and goods Kauba ja materjali Quantity measurement of s and goods Kauba ja materjali Quantity measurement of s and goods Kauba ja materjali Quantity measurement of s and goods Kauba ja materjali Quantity measurement of s and goods Kauba ja materjali Quantity measurement of s and goods Kauba ja materjali Quantity measurement of s and goods API Manual of Petroleum Measurement Standards. Chapter 17 - Marine Measurement. Section 2- Measurement of Cargoes On Board Tank Vessels EVS 745 Kauba ja materjali massi mõõtmine kaalumisega EVS 746 Tükikauba koguse mõõtmine Inspectorate Estonia M "Kauba massi mõõtmine laeval süvisemärkide järgi" Inspectorate Estonia M Inspectorate Estonia M Inspectorate Estonia M Puistekaupade koguse mõõtmine Inspectorate Estonia M Inspectorate Estonia M

16 Leht/Page 16/21 No Parameter Materials or products tested / tested 120. Koguste mõõtmine ja arvutamine kalda ja laeva mahutites Quantity measurement and calculation in tanks and marine vessels Põlevkiviõli toodete Measurement of quantity of shale oil products 121. Proovivõtmine Sampling Põlevkiviõli toodete Measurement of quantity of shale oil products Inspectorate Estonia AS meetod OP-16 Inspectorate Estonia AS meetod OP Sügavuste mõõtmine mahutites. Gauging in tanks 123. Temperatuuri mõõtmine elektroonse termomeetriga. Temperature measurement using portable electronic thermometer 124. Koguste mõõtmine ja arvutamine raudtee mahutites Quantity measurement and calculation in railway tanks 125. Fosforisisaldus. Ferrochrome. for determination of phosphorus 126. Süsinikusisaldus. Ferroalloys, metal chromium and metal manganese. for determination of carbon 127. Üldsüsiniku sisaldus. Steel and iron. Determination of total carbon content. Infrared absorption method after combustion in an induction furnace 128. Väävli sisaldus. Ferroalloys, metal chromium and metal manganese. for determination of sulfur Põlevkiviõli toodete Measurement of quantity of shale oil products Põlevkiviõli toodete Measurement of quantity of shale oil products Põlevkiviõli toodete Measurement of quantity of shale oil products Inspectorate Estonia AS meetod OP-16 Inspectorate Estonia AS meetod OP-16 Inspectorate Estonia AS meetod OP-16 Инструктивные указания по определению веса наливных грузов в цистернах. Утв.гл.упр. вагонного хозяйства МПС 2003 GOST GOST ISO9556:2003 GOST

17 Leht/Page 17/21 No Parameter Materials or products tested / tested 129. Väävli sisaldus. Steel and iron. Determination of sulfur content. Infrared absorption method after combustion in an induction furnace 130. Räni sisaldus. Ferrochrome. for determination of silicon 131. Räni sisaldus. Ferrosilicon, ferrosiliconmanganese and ferrosilicochromium. Determination of silicon content. Gravimetric method 132. Titaani sisaldus. Ferrosilicon. for determination of titanium 133. Kroomi sisaldus. Ferrochrome. for determination of chromium 134. Niiskuse veeldumispiir. Determination of flow moisture limit. Flow moisture table test and transportable moisture limit 135. Raua sisalduse määramine Determination of total iron content -Part 1: Titrimetric method after tin(ii) chloride reduction 136. Metallipuru tiheduse määramine heelium- püknomeetriga Standard Test for Metal Powder Skeletal density by Helium Pycnometry 137. Ammoniumlämmastiku määramine Determination of ammoniacal nitrogen content ISO4935:1990 GOST ISO 4158:1978 GOST GOST ISO IMSBC Code 2016 ISO B EC Regulation 2003/2003 Annex IV 2.1 EN 15475

18 Leht/Page 18/21 No Parameter Materials or products tested / tested 138. Ammonium- ja nitraatlämmastiku määramine Devarda järgi. Determination of nitric and ammoniacal nitrogen content according to Devarda 139. Fosfori määramine gravimeetrilisel kinoliin fosfomolübdaat meetodil Phosphorus in mineral fertilizers. Gravimetric method using quinoline phosphomolybdate 140. Niiskusesisalduse määramine. Gravimeetrilisel meetodil kuivatamisega alarõhul. Determination of moisture content Gravimetric method by drying under reduced pressuure Veeslahustuva kaaliumi määramine tetrafenüülboraadiga. Water soluble potassium using tetraphenylborate 142. Mineraalhappes lahustuvate sulfaatide määramine gravimeetriliselt Determination of sulphates. Gravimetric method 143. Kogulämmastiku määramine karbamiidis Determination of total nitrogen in urea EC Regulation 2003/2003 Annex IV EN EC Regulation 2003/2003 Annex IV 3.1.4/ EN 15920; EN 15959; EN 15957; ISO 6598 EVS EN 12049:2000 AOAC EC Regulation 2003/2003 Annex IV 4.1 EN EC Regulation 2003/2003 Annex IV 8.9 EN EC Regulation 2003/2003 Annex IV EN Spektrofotomeetriline biureedi määramine karbamiidis Spectrophoto-metric determination of biuret in urea EC Regulation 2003/2003 Annex IV 2.5 EN 15479

19 Leht/Page 19/21 No Parameter Materials or products tested / tested 145. Sõelanalüüs Sieving test EN 1235:2000/A1:2003 ISO Niiskusesisalduse määramine (105±2) o C juures kuivatamisega Determination of moisture content. Gravimetric method by drying at (105±2) o C 147. Al, Si, V, Ni, Fe, Na, Ca, Zn, P sisalduse määramine ICP-OES meetodil. Determination of Al, Si, V, Ni, Fe, Na, Ca, Zn, P in residual fuel oil by ashing fusion and inductively coupled plasma emission spectrometry 148. Niiskusesisalduse määramine. Üldniiskus Determination of moisture content. Total moisture 149. Tuhasuse määramine. Determination of ash content 150. Kütteväärtuse määramine Determination of calorific value Kütteõli Fuel oil Biokütused pelletid/ Solid biofuels pellets Biokütused pelletid/ Solid biofuels pellets Biokütused pelletid/ Solid biofuels pellets EN IP 501 EN ISO :2015 EN ISO 18122:2015 EN 14918:2009

20 Leht/Page 20/21 No Parameter Materials or products tested / tested 151. Üldise süsiniku-,vesiniku-ja lämmastikusisalduse määramine. Determination of total content of C, H and N 152. Üldise väävli-ja kloriididesisalduse määramine. Determination of total content of S and Cl 153. Proovide ettevalmistus. Sample preparation 154. Mikroelementide As (CV-AAS) ja Cd,Co,Cr,Cu,Hg,Mn,Mo,Ni,Pb, Sb,V ja Zn (ICP-OES) määramine Determination of minor elements- As(CV-AAS) and Cd,Co,Cr,Cu,Hg,Mn,Mo,Ni,Pb, Sb,V, Zn (ICP-OES) 155. Spetsifikatsioonid ja klassifitseerimine - Osa 2 Fuel specifications and classes Part Koksiarv mikromeetodil. Determination of Carbon residue, micro method Biokütused pelletid/ Solid biofuels pellets Biokütused pelletid/ Solid biofuels pellets Biokütused pelletid/ Solid biofuels pellets Biokütused pelletid/ Solid biofuels pellets Biokütused pelletid/ Solid biofuels pellets Naftasaadused, FAME. Petroleum products FAME EN ISO 16948:2015 EN ISO 16994:2016 EN 14780:2017 EN ISO 16968:2015 EVS-EN ISO :2014 EN ISO D Hardgrove Grindability Index Kivisüsi Coals, antracites D409/D409M Niiskuspunkti määramine. Läbivustest. Proctor-Fagerberg test Determination of flow moisture point and transportable moisture limit. Penetration test. Proctor-Fagerberg test, modified Proctor-Fagerberg test including coals ( 50 mm nts) 159. Lõikekatse. Proovivõtmine Cut test. Sampling Metalli ja mineraalide kontsentraadid, kivisüsi Metals and minerals, coals, metal concentrates, ores, fines Kakaooad Cocoa beans IMSBC Code 2016 ISO 2292 Sampling ISO 1114 Cut test FCC Quality Rules ( )

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