1(10) 1. Akrediteerimisulatus on: Accreditation scope is: Objekt Object. Metoodika Method. Mõõtühik Unit. Saadus Product. Mõõteulatus Range. Nr.

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1 1(10) Nr. 1. Akrediteerimisulatus on: Accreditation scope is: Objekt Object Metoodika Method EESTI AKREDITEERIMISKESKUS LISA IsoTech OÜ laboratooriumi akrediteerimistunnistusele nr. L211 Saadus Product Mõõtühik Unit Mõõteulatus Range 1 Destillaatkütuste tsetaaniindeksi määramine Calculated Cetane Index of Distillate Fuels 2. Tiheduse määramine digitaalse tihedusmõõturiga Density by digital density meter 3. Vee määramine Karl Fischeri kulonomeetrilise tiitrimismeetodi abil Determination of water Coulometric Karl Fischer titration method Diislikütus Diesel fuel Autobensiin, diislikütus, kerge ja raske kütteõli, masuut, taimeõlid, biodiislikütus Gasoline, diesel fuel, light and heavy fuel oils, mazut, vegetable oils, biodiesel fuel Autobensiin Diislikütus, kerge ja raske kütteõli, taimeõlid, biodiislikütus, FAME kütteõli Gasoline, diesel light and heavy fuel oils, vegetable oils, biodiesel fuel, FAME heating oil indeks 32,5 56,5 kg/l 0,6 1,100 kg/m massi % 0,003 0,100

2 2 (10) 4. Destillatsiooni karakteristikute määramine atmosfäärirõhul Determination of distillation characteristics at atmospheric pressure 3405 Autobensiin Diislikütus, kerge ja raske kütteõli Gasoline,diesel fuel, light and heavy fuel oils mahu % lõpp: < 250 o C 5. Orgaaniliste hapnikuhendite ja hapniku üldsisalduse gaasikromatograafiline määramine Determination of organic oxygenates compounds and total organically bound oxygen content by gas chromatography EN Bensiin Gasoline massi % mahu % lõpp: < 400 o C 0, ,11 1,0 >1,0 3,0 >3,0 5,0 >5,0 7,0 >7,0 9,0 >9,0 11,0 >11,0 13,0 >13,0 15,0 Hapnik kuni 3,7 Oxygen up to 3,7 6. Aromaatsete süsivesinike tüübi määramine Determination of aromatic hydrocarbon types 7. Leekpunkti määramine Pensky- Martensi suletud tiiglis Flash Point by Pensky-Martens Closed Cup Tester EVS-EN Diislikütus Diesel fuel Diislikütus, raske ja kerge kütteõli, taimeõlid, biodiislikütus,fame kütteõli Diesel fuel, light and heavy fuel oils, vegetable oils, biodiesel fuel, FAME heating oil massi % 6 30 (MAH) 1 10 (DAH) 0 2 (T-AH) 1 12 (POLY-AH) 7 42(Total-AH) o C

3 3 (10) 8. Tuhasuse määramine naftasaadustes Ash from petroleum products 6245 massi % 0,001 0,079 0,080 0, Tahkete osiste määramine EVS-EN Diislikütus, kerge kütteõli mg/kg keskmistes destillaatides Determination of contamination in middle distillates Diesel fuel, light fuel oil 10. Korrosiivsus vaskplaadikatsel Vedelkütused klass 1-4 Corrosivenes by copper strip test 11. Kinemaatilise viskoossuse määramine Kinematic Viscosity of Transparent and Opaque Liquids 12. Külmfiltri ummistumispunkti määramine Determination of cold filter plugging point 13. Benseeni määramine pliivabas bensiinis Determination of benzene content in unleaded petrol EN Liquid fuels Diislikütus, raske ja kerge kütteõli, taimeõlid, biodiislikütus, FAME kütteõli, taimeõlid Diesel fuel, light and heavy fuel oils, biodiesel fuel, FAME heating oil, vegetable oils Diislikütus, raske ja kerge kütteõli, biodiislikütus, Diesel fuel, light and heavy fuel oils,biodiesel fuel Bensiin Gazoline mm 2 /s o C 10 (- 38) Mahu % (0,05 6,00)

4 4 (10) 14. Naftasaaduste hägustumispunkti määramine Cloud Point of Petroleum Products EN Diislikütus, kerge kütteõli, biodiislikütus, Diesel fuel, light fuel oil, biodiesel o C 49 (-38) 15. Rasvhapete metüülestrite (RME) sisalduse määramine keskmistes destillaatides. Infrapunase spektroskoopia meetodil. Determination of fatty acid methyl esters(fame) in middlde distillates. Infrared spectroscopy method 16. Erimärgistusaine Solvent Yellow 124 määramine Determination of marker Solvent Yellow Värvaine Automate Blue kontsentratsiooni määramine. Determination of marker Automate Blue. 18. Oksüdatsioonilise stabiilsuse määramine. Determination of the oxidation stability of middle-distillate fuels 19. Naftasaaduste koksiarvu määramine mikromeetodil. Determination of carbon residue Micro method 20. Diislikütuse määrimisomadused (HFRR) Lubricity of Diesel Fuel (HFRR)- Part1, Method B EN VV määrus 148/2014 (lisa 1) VV määrus 148/2014 (lisa 3) EVS-EN ISO fuel Diislikütus Diesel fuel Diislikütus,kerge kütteõli Diesel fuel, light fuel oil Diislikütus,kerge kütteõli Diesel fuel, light fuel oil Diislikütus Diesel fuel Diislikütus Diesel fuel mahu % (0,05 3) mahu % (% v/v) (3 20) mahu % (% v/v) mg/dm 3 0,1 10 mg/dm 3 0,1 15 g/m massi % 0,10 30,0 μm ( ) μm

5 5 (10) 21. Küllastunud aururõhu määramine. Mini meetod Vapor Pressure of Petroleum Products (MiniMethod). EN kpa Aurulukuindeks, VLI (VLI=10VP + 7E70) Vapour Lock Index 23. Kergete ja keskmiste destillaatkütuste vaigusisalduse määramine jugaaurutusmeetodil -Gum content of light and middle distillate fuels -Jet evaporation method EN Index mg/100ml 0, Bensiini oksüdatsioonikindluse määramine induktsiooniperioodi meetodil. Determination of oxidation stability of gasoline Induction period method 7536 min >15

6 6 (10) Väävlisisaldus (energiat dispergeeriv röntgenikiirguse fluorestsentsspetroskoopia) Determination of sulfur content Energy dispersive X -ray fluorescence spectrometric method EVS mg/kg Väävlisisaldus (energiat dispergeeriv röntgenkiirguse fluorestsentsspetroskoopia) Determination of sulfur content Energy dispersive X -ray fluorescence spectrometric method EVS massi % (m/m) 0,03 5, Vee määramine naftasaadustes ja bituminoossetes materjalides destilleerimismeetodil. and bituminous materials Determination of water Distillation method ISO 3733 massi % (m/m) < 30

7 Nr. LISA IsoTech OÜ laboratooriumi akrediteerimistunnistusele nr. L211 Tegevused väljapool laborit / Activities outside the laboratory Objekt Object 1 Koguste määramine/arvu tamine Quantity measurements Metoodika Method API MPMS Chapter 12.1 Calculation of Static Petroleum Quantities, Upright Cylindrical Tanks and Marine Vessel IsoTech Tööjuhend: K Saadus Product Autobensiin, diislikütus, kerge ja raske kütteõli, masuut. Gasoline, diesel fuel, light and heavy fuel oil, mazut, Mõõteulatus Mõõtühik Range, unit kg m 3 7 (10) Mõõtevõime Measurement capability U=0,5 % (k=2) mõõtetulemusest 2 Nivoo mõõtmine mahutites Tank Gauging 3 Proovivõtmine Sampling API MPMS Chapter 3 - Tank Gauging. Section 1A-Standard Practice for the Manual.Gauging of Petroleum and Petroleum Product. K API MPMS Ch.8 Sampling Sec.1 - Manual Sampling of Petroleum and Petroleum Products ISO 3170 Petroleum liquids-manual sampling ASTM D 4057 Petroleum and petroleum products. Manual sampling. EVS-EN Automotive fuels Assessment of petrol and diesel fuel quality Sampling from retail site pumps and commersial site fuel dispensers IsoTech Tööjuhend: K Autobensiin, diislikütus, kerge ja raske kütteõli, masuut, taimeõlid, biodiislikütus (rasvhapete metüülestrid) Vedelikud (Metanool,o-ksüleen,p-ksüleen, m- ksüleen,benseen,tolueen,mtbe,atsetoon, glütserool Gasoline, diesel fuel, light and heavy fuel oil, mazut, vegetable oils, biodiesel (FAME) Liquid products(methanol, o-xylene,p-xylene,m-xylene, benzene, toluene, MTBE, acetone Glycerol Autobensiin, diislikütus, kerge ja raske kütteõli, masuut. Gasoline, diesel fuel, light and heavy fuel oil, mazut, (0 25) m U=2 mm (k=2)

8 8 (10) 4 Koguste mõõtmine API MPMS Ch.3 Tank gauging Section 2 Autobensiin, diislikütus, kerge ja raske U=1,5 % (k=2) raudtee mahutites Standard kütteõli, masuut, taimeõlid, biodiislikütus Mõõtetulemusest kg Gauging in rail tank Practice for Gauging Petroleum and Petroleum (FAME) m 3 from measurement result cars Products in Tank Cars Gasoline, diesel fuel, light and heavy fuel oil, Таблица калибровки железнодорожных mazut, vegetable oils, biodiesel (FAME) цистерн. Москва, Транспорт Koguste mõõtmine laevamahutites Quantity measurement on Board Tank Vessel 6 Arvestiga mõõtmine ja arvutus mahule 15 o C juures. Calculation ofpetroleum Quntities Using Dynamic Measurement Methods API MPMS. Chapter 17 - Marine Measurement. Section 2 -Measurement of Cargoes On Board Tank Vessels API MPMS Ch 17 Sec 4 Method for Quantification of Small Volumes on Marine Vessels (OBQ/ROB). IsoTech Tööjuhend: K API MPMS Chapter 12.2 Calculation of Petroleum Quantities Using Dynamic Measurement Methods and Volumetric Correction Factors API MS Ch 5 Metering Autobensiin, diislikütus, kerge ja raske kütteõli, masuut, taimeõlid, biodiislikütus (FAME) Gasoline, diesel fuel, light and heavy fuel oil, mazut, vegetable oils, biodiesel (FAME) kg m 3 U=0,5 % (k=2) Mõõtetulemusest from measurement result m 3 U= 0,7 % Mõõtetulemusest from measurement result

9 9 (10) 7 Temperatuuri mõõtmine elektroonilise termomeetriga Static temperature determination using portable electronic thermometers API MPMS Ch.7 - Temperature Determination. IsoTech Tööjuhend: K Autobensiin, diislikütus, kerge ja raske kütteõli, masuut, taimeõlid, biodiislikütus, FAME kütteõli Gasoline, diesel fuel, light and heavy fuel oil, mazut, vegetable oils, biodiesel fuel, FAME heating oil ( ) o C U=0.3 o C (k=2) 8 Tükikauba koguse mõõtmine quantitative measurementof piece goods EVS 746 Tükikauba koguse mõõtmine. Mõõtemetoodika / Piece goods quantity measurement. Measurement method Tiheduse määramine digitaalse tihedusmõõturiga Density by digital density meter Autobensiin, diislikütus, kerge ja raske kütteõli, masuut. Gasoline, diesel fuel, light and heavy fuel oils, mazut. (0,600 1,100) kg/l ( ) kg/m 3 U=0,0005 kg/m 3 (k=2)

10 2. Firma juriidiline aadress / Legal address of firm: Pae 41-39, Tallinn, Eesti Labori asukoht / Laboratory address: Fosforiidi 8, Maardu, Eesti 10 (10) 3. Labor on akrediteeritud standardi EVS-/IEC 17025:2006 nõuete suhtes Laboratory is accredited against the requirements of standard EVS-/IEC 17025:2006 Märkus: käesolev lisa asendab välja antud lisa seoses akrediteerimisulatuse täpsustamisega. This annex was issued due to specification of accreditation scope and replaces annex issued on Kristiina Saarniit EAK juhataja Director of EAK Tallinnas, Kalju Anni Peaassessor Lead Assessor

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