Scientific glass blowing

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2 Scientific glass blowing Normalab France S.A.S. is specialized in the scientific glass blowing since the beginning of the company in Thanks to this experience of more than fifty years and a team of nine glass-blowers accustomed to work with various techniques, Normalab s workshop is the French leader of scientific glass blowing specialized in the oil field. The activity and know-how are vast. The specialists share their time between: Standard production OEM manufacturing Custom-tailord design Repair From the beginning the workshop works with three types of glass: Sodocalcique (ordinary) Borosilicate (Duran ) Quartz The blowers master various techniques: Blowtorch works Turned glass The moulding Inactinic glass (scented with amber) Silvering Grinding and polishing Marking (engraving and transfer) Also in order to offer a complete service to its customers, Normalab proposes the checking and the calibration of various articles made of glass. With this intention the company is certified according to ISO Delivered certificates ensure a conformity with the international standards like ASTM, IP, EN, ISO, DIN, JIS, GOST Normalab s reputation is done, its distillation flasks and viscometer tubes* are impossible to circumvent in the oil laboratories. Their accuracy and solidity make a world wide reference of it. Quality, robustness, and accuracy of work is the daily objective of this historical workshop. * Find our full range starting from page 17

3 Table of Contents ASTM D p 3 ASTM D p 3 ASTM D p 3 ASTM D p 4 ASTM D p 5 ASTM D p 5 ASTM D p 5 ASTM D p 5 ASTM D p 5 ASTM D p 6 ASTM D p 5 ASTM D p 6 ASTM D p 6 ASTM D p 3 & 5 ASTM D p 18 to 25 ASTM D p 6 ASTM D p 7 ASTM D p 7 ASTM D p 7 ASTM D p 8 ASTM D p 8 ASTM D p 8 ASTM D p 9 ASTM D p 5 ASTM D p 9 ASTM D p 9 ASTM D P 4 ASTM D p 10 ASTM D p 10 ASTM D p 10 ASTM D p 11 ASTM D p 11 ASTM D p 11 ASTM D p 11 ASTM D p 6 ASTM D p 11 ASTM D p 11 ASTM D p 11 ASTM D p 12 ASTM D p 11 ASTM D p 18 & 25 ASTM D p 21 ASTM D p 7 ASTM D p 12 ASTM D p 12 ASTM D p 9 ASTM D p 12 ASTM D p 12 ASTM D p 6 ASTM D p 13 ASTM D p 12 ASTM D p 13 ASTM D p 8 ASTM D p 13 ASTM D p 8 ASTM D p 14 ASTM D p 13 ASTM D p 5 ASTM D p 9 ASTM D p 14 ASTM E p 5 ASTM E p 14 ASTM E p 4 DIN p 12 DIN p 6 DIN p 9 DIN p 8 DIN p 11 DIN p 8 DIN p 9 DIN p 15 DIN p 4 DIN p 9 DIN p 6 DIN p 6 DIN p 11 DIN p 5 EN p 15 EN p 15 EN p 16 EN p 3 EN p 12 IP p 7 IP p 6 IP p 12 IP p 6 IP p 3 IP p 6 IP p 5 IP 70.p 15 IP p 18 to 25 IP p 5 IP p 5 IP p 15 IP p 10 IP p 4 IP p 6 IP p 8 IP p 9 IP p 15 IP p 14 IP p 9 IP p 11 IP p 8 IP p 14 IP p 3 IP p 4 IP p 11 IP p 15 IP p 12 IP p 16 IP p 11 ISO p 11 ISO p 12 ISO p 6 ISO p 18 to 25 ISO p 18 to 25 ISO p 4 ISO p 5 ISO p 6 ISO p 11 ISO p 3 ISO p14 ISO p 12 ISO p 9 ISO p 3 ISO p 6 ISO p 9 ISO p 11 ISO p 7 ISO p 13 ISO p 14 ISO p 9 NF M p 7 NF M p 8 NF M p 11 NF M p 10 NF M p 14 NF M p 15 NF M p 16 NF M p 11 NF T p 7 NF T p 6 NF T p 5 & 14 NF T p 5 NF T p 15 NF T p 7 NF T p 8 NF T p 11 NF T p 13 NF T p 8 NF T p 5 NF T p 3 2

4 ASTM D 20 - D402 - AFNOR T IP Graduated cylinder with neck (100 ml) Distillation flask (500 ml) ASTM D 36 - NF EN ISO Calibrated beaker ASTM D Calibrated beaker ISO 1427 ASTM D 70 - NF EN ISO IP Pycnometer A - 24/30 ml (Hubbard model) Pycnometer B - 24/30 ml (Bingham model) Pycnometer C - 24/30 ml (Warden model) Pycnometer D - 24/30 ml (Capillary-stopper)

5 ASTM D 86 - D E NF EN ISO IP IP DIN Nomenclature Distillation flask (100 ml) Distillation flask (125 ml) Distillation flask (200 ml) Distillation flask (250 ml) Graduated receiver (100 ml) Cylinder 200 ml Distillation receiver with brass foot (100 ml) for auto version (Brasse base ref 12921, cylinder ref 12919, joint ref 30187N) Graduated receiver glass with foot (100 ml) Nomenclature Distillation flask (125 ml) Receiver 100 ml for manual version ml distillation flasj with shank & holed cork for probe ml distillation flask with shank & holed cork for probre M/F shank for condenser tube entry Graduated receiver glass with foot (100 ml) with NORMALAB no condensation treatment Graduated receiver (5 ml) Simax 0,4ml Graduated cylinder (5 ml) Schott 0.9 ml 12609EC Graduated cylinder economic (5 ml) Simax 100ml 100 ml 90 5ml

6 ASTM D 87 - D402 - AFNOR T IP Test tube with paraffin (3ml) ASTM D 88 - D E Graduated receiver ml Saybolt flask (60 ml) ASTM D 91 - D 96 - D D D NF ISO T IP 75 - DIN " cone-shaped tube (100 ml) Pear shaped tube (100 ml) with 3 ml graduated tip Pear shaped tube (100 ml) with 1.5 ml graduated tip ASTM D 95 - AFNOR T IP 74 - ISO Round bottom flask CN24/29 (500 ml) Liebig condenser CN24/29 (400 mm) Dean Stark trap (10ml in 0.1) ml : 1/5 Dean Stark with conical bottom 5

7 ASTM D 97 - D AFNOR T IP 15 - ISO Test tube for manual apparatus Test Tube for Pour Point Test tube with glass mirror for Cloud and Pour Point Test Tube with platinum mirror for Cloud and Pour Point ASTM D IP 23 - DIN Nomenclature Round bottom flask CN24/29 (1 l) Liebig condenser CN24/29 (400 mm) Trap CN24/29 (5 ml) ASTM D ISO IP DIN Nomenclature Test cell (100 ml) ASTM D ISO IP 53 - DIN Water cup with glass hook Extraction thimble, alundum Extraction flask (1 litre)

8 ASTM D AFNOR T IP Heat-resistant glass coking bulb ASTM D NF EN ISO M Glass test container without cover Glass test container with cover Cover for container ASTM D D AFNOR T Dropping point test tube 7

9 ASTM D AFNOR M07021 Méthode II stroke pipette (5 ml) stroke pipette (10 ml) Test tube 25x150mm Jacket Manual stirring ASTM D D AFNOR T IP DIN Beaker (400 ml) ASTM D D AFNOR T IP DIN Complete filter assembly CN Complete filter assembly with certificate

10 ASTM D NF ISO IP DIN Graduated cylinder (1 liter) Diffuser stone, calibrated (with certificate) Stainless steel diffuser stone Borosilicate glass tank ASTM D D IP DIN Lipkin pycnometer ASTM D D D NF EN ISO DIN Test container Mushroom condenser Oxygen delivery tube (D 943) Mushroom condenser (D2274) Oxidation cell (D 943/D 2893) Oxidation cell (D 2274 / D 4310)

11 23239 Dewar freezing tube ASTM D 1177 ASTM D Bingham density bottle (25 ml) ASTM D AFNOR M IP Absorber Chimney Burner for nonaromatic samples Spray trap Flask (25 ml) for nonaromatic samples Burner for aromatic samples Flak (25 ml) for aromatic samples

12 ASTM D AFNOR M IP ISO DIN Standard wall tubing (lower part) FIA True Bore adsorption column Upper connection RIS 28/ Outlet for true bore column (S12/2) Standard adsorption column (upper part) Low parts for FIA standard column (pack of 25) ASTM D AFNOR T ISO Borosilicate glass graduated cylinder (100 ml) ASTM D ISO IP196 - DIN Glass sample jar ASTM D D AFNOR M IP Graduated weathering cylinder (100 ml) Set of glassware for depentanization ASTM D 2001 ASTM D 2002 Nomenclature Complete adsorption column (method B) 11

13 ASTM D Spherical ground joint with nipple High efficiency column ASTM D IP Sample container, made of borosilicate glass Catalyst copper coil (ready to use) ASTM D Bulb glass cone-shaped capillary 100 ml ASTM D NF EN ISO Quartz combustion chamber Absorber with fritted plate Trap ASTM D NF EN ISO IP 16 - DIN Jacketed sample tube Dewar flask (double wall)

14 ASTM D 2623 Burette for reference mixture Lead burette (3 ml) Lead burette (4 ml) Burette (100 ml) without ball nor valve Burette (400 ml) auto-fill with tap, graduated in 0.5% and 2 ml Burette (200 ml) without ball nor valve Burette 100 ml with ball valvle without stopcock Burette (400 ml) with ball without valve ASTM D Standardized glass container RTFOT ASTM D NF ISO T Complete sample glassware Plunger (5 ml) Plunger (10 ml) Complete Impinger graduated receiver ASTM D Condenser CN 24/40 down Drying tube Dean Stark (5 ml) CN 24/ CN 24/40 ball (1 liter) round bottom 13

15 ASTM D ISO For normalab device Borosilicate glass sample vials (2 ml) - Pack of Borosilicate glass sample vials (16 ml) - Pack of Quartz sample vial ash content (2 ml) Quartz sample vial ash content (16 ml) Vials (4 ml) ISO x Vials (16 ml) single use x Vials (2 ml) single use x 144 ASTM E NF T Dean-Stark (10 ml) cone-shaped - CN 24/ Dean-Stark (5 ml) - CN 24/ Dean-Stark (10 ml) - CN 24/40 ISO IP Standard sulfonation flask (10 ml) Precision sulfonation flask (10 ml) Precision sulfonation flask (5 ml) Flask methode II - M07016 AFNOR Plugged test tube (100ml) - CN 24/ Flask (20 ml) - CN 24/ Distillation column with cap Condenser with CN 14/23 AFNOR M IP

16 AFNOR M EN 13 - EN 41 - IP Protection tube Complete glassware without CN Complete glassware with CN Flask (500 ml) with resistance and CN Hopkins condenser with CN Separatory funnel with CN AFNOR T IP DIN Condenser CN 34/ Conical flask (500 ml) CN Reflux extractor CN29/ Conical flask (500 ml) CN Reflux extractor CN24/34 IP Redwood flask (50 ml) IP Complete condenser kit (amber glass) Cradle (amber glass) Test tube (amber glass) Cold-finger condenser (amber glass) Complete condenser kit Test tube Cold-finger condenser 15

17 IP NF EN AFNOR M RIS Automatic pipette CFPP test tube RIS Pipette for manual apparatus RIS male tip CFPP pipette Pipette for manual apparatus without RIS

18 Viscometer Tubes Introduction The following pages presents the various types of viscometric tubes we have been manufacturing for years in our factories and calibration laboratory. Construction Normalab s voscometric tubes are made out of low-expanding Duran 50 glass. The tubes are made with high accuracy capillaries (+/ mm). Scores and figures are marked using an indelible process instread of the conventional engraving method. The viscometers result less fragiles (less breakages due to score discontinuities). Each viscometric is dedicated a serial number and supplied in carefully studied single packing. The standard capillary viscometers are delivered without any engraved constant. This may be archieved on customer s special request against small additional cost. Calibration 3 options are available for most of the models: a) Without certificate b) «Factory» certificate The constant is obtained by using only one pure mineral oil grade of which viscosity has been previously determined with viscometer tube calibrated by «Laboratoire National d Essais» or using a Cannon calibrated tube. Any type of viscometer may be manufactured with the constant required by customers and providing 10% accuracy or better if requested at the ordering time. c) Calibration certificate Normalab viscometers are calibrated in our laboratory using reference viscometers calibrated by the French «Laboratoire National d Essais» (National Testing Laboratory). Those viscometers are checked at regular intervals by means of viscosity oil standards. Normalab has been assessed and registered as meeting the requirements of ISO 9001 for laboratory and associated services of repair, calibation and verification of laboratories devices. 17

19 CANNON-FENSKE routine viscometers for transparent liquids ASTM D IP 71 - ISO A: without certificate B: with factory certificate C: with calibration certificate Size Approx. constant Viscosity (cst) A B C to to to to to to to to to to to to to to

20 CANNON-FENSKE reverse flow viscometers for opaque liquids ASTM D D IP 71 - ISO A: without certificate B: with factory certificate C: with calibration certificate Size Approx. constant Viscosity (cst) A B C to to ,6 to to to to to to to to to to to to

21 UBBELOHDE viscometers for transparent liquids ASTM D IP 71 - ISO A: without certificate B: with factory certificate C: with calibration certificate Size Approx. constant Viscosity (cst) A B C to C to B to A 0.007/8 1.5 to to C to B to to C to B to A 0.7/ to ,0 200 to C 3,0 600 to B 5, to to C to B to to

22 HOUILLON viscometers for transparent liquids B: with factory certificate C: with calibration certificate Size Approx. constant Viscosity (cst) B C to to to to to to to to to Viscometer tubes CANNON-MANNING VACUUM ASTM D 2171 A: without certificate C: with calibration certificate Size Approx. Cst Bulb B Approx. Cst Bulb C 21 Viscosity (P) A C 4 0,002 0, to ,006 0, to ,02 0, to ,06 0, to ,2 0, to ,6 0,2 12 to ,6 36 to to to to to

23 BS / IP SL viscometers for transparent liquids ASTM D IP 71 - ISO A: without certificate B: with factory certificate C: with calibration certificate Size Approx. constant Viscosity (cst) A B C to A to to A to to A to to A to to BS / IP U RF viscometers for opaque liquids ASTM D D IP 71 - ISO A: without certificate B: with factory certificate C: with calibration certificate Size Approx. constant Viscosity (cst) 22 A B C to to to to to to to to to to to

24 SIL viscometers for transparent liquids ASTM D IP 71 - ISO A: without certificate C: with calibration certificate Size Approx. constant Viscosity (cst) A C 0C to to C to to C to to C to to CANNON-UBBELOHDE viscometers for AVS - for transparent liquids ASTM D IP 71 - ISO A: without certificate B: with factory certificate Size Approx. constant A B 0C A C C C

25 BAUME VIGNERON viscometers for transparent liquids A: without certificate C: with calibration certificate Viscosity (cst) A C

26 CANNON-UBBELOHDE viscometer for AVS - with screwed end - for transparent liquids - ASTM D IP 71 - ISO A: without certificat B: with factory certificate Size Approx. constant A B 0C A C C C

27 ORSAT Device Smoke analyzer used to dose the component of a gas by absorption into the bells to liquid reagents (carbon dioxide,unsaturated hydrocarbons, oxgen) and determination of hydrogen by combustion of copper oxide, methane and ethanecombustion on spiral platinum position device for dosing CO, CO 2, O 2, delivered in hard case with carrying handle. Complete booklet (no reagent) Absorber Rubber gas bulb Jacket Burette 0-30% at 1/5% and 50-90% at 1% Bottle Drying tube position ramp with tap Rubber stopper for top cover (pack of 2) Rubber stopper for bottom cover (pack of 2) 26

28 KUMAGAWA Extractor (borosilicate glass) 12280* Complete extractor, 125 ml capacity 12284* Complete extractor, 250 ml capacity 12288* Complete extractor, 500 ml capacity Spare flask (250 ml) for Spare flask (500 ml) for Spare flask (1000 ml) for Spare extractor tube (125 ml) Spare extractor tube (250 ml) Spare extractor tube (500 ml) Spare condenser RIN male 50/ Spare condenser RIN male 60/ Spare condenser RIN male 85/70 * The capacity of an extractor is the one of the extractor tube and not the capacity of the flask. 27

29 SOXHLET Extractor Complete extractor, 60 ml capacity Complete extractor, 125 ml capacity Complete extractor, 200 ml capacity Complete extractor, 500 ml capacity Complete extractor, 1000 ml capacity Spare flask (100 ml) for Spare flask (250 ml) for Spare flask (500 ml) for Spare flask (1000 ml) for Spare flask (2000 ml) for Spare extractor tube (60 ml) Spare extractor tube (125 ml) Spare extractor tube (200 ml) Spare extractor tube (500 ml) Spare extractor tube (1000 ml) Condenser 4 balls RIN 24/ Condenser 4 balls RIN 29/ Condenser 6 balls RIN 29/ Condenser 8 balls RIN 29/

30 MAIN PRODUCTS 1 NDI 450 ASTM D 86, ISO 3405, IP 123, DIN Automated atmospheric Distillation unit 2 NPM 450 ASTM D 93, ISO 2719, IP 34, DIN Fully automatic Pensky Martens Flash Point tester 3 NTE 450 ASTM D 97 & 2500, ISO 3015 & 3016, IP 15& Automated Cloud and Pour Point instrument CP PP 4 NTL 450 ASTM D 6371, IP Automated Cold Filter Plugging Point instrument CFPP 5 NPN TECH ASTM D 5, D 217, D 937, D 1321, D 1403, IP 49, ISO 3997, DIN Automatic Penetrometer NABLEND ASTM D 613 & 2699 & 2700, ISO 5163 & 5164, IP 41 & 236 & 237,, DIN Automatic Blending Unit for octan and cetan reference fuel (Blending) 29

31 Designation ASTM AFNOR ISO EN IP DIN Designation ASTM AFNOR ISO EN IP DIN Penetration of bitumous material D Density and relative density of viscous materials by bingham pycnometer D1480 Loss on heating of oil and asphaltic compounds D6 T ASTM color of petroleum products (ASTM color scale) D Softening point of bitumen (ring and ball) D Sulfur in petroleum products (high-temperature method) D1552 M Flash point by tag closed tester D Density or relative density of light hydrocarbons by pressure thermohydrometer D Density of semi-solid bitumous materials (Pycnometer method) D /190 ENGLER specific viscosity of tar products D Distillation of petroleum products D Determination of water in liquid petroleum products by Karl Fischer reagent D Saybolt viscosity D88 Effects of heat and air on asphatic materials (Thin-film oven test) D1754 Precipitation number of lubricating oil D91 Water and sediment in fuel oils by the centrifuge méthod (laboratory procedure) D Flash and fire points by Cleveland open cup D / 403 Roll stability of lubricating grease D1831 Flash point by Pensky-Martens closed cup D / Volatility of liquefied petroleum (LP) Gases D1837 M Water in petroleum products and bitumous materials by ditillation D95 T Copper strip corrosion by liquefied petroleum (LP) Gases D Water and sediment in crude oil by centrifuge method D96 Filter bloquing tendency of distillate fuel oils D Pour point of petroleum products D97 T Residues in liquefied petroleum (LP) Gases D Ductibility of bituminous materials D113 T Dropping point of lubricating grease over wide temperature range D Sulfur in petroleum products (general bomb method) D Oxidation stability of steam turbine oils by rotating bomb D Detection of copper corrosion from petroleum products D Trace sediment in lubricating oils D2273 Saybolt color of petroleum products D156 M Oxidation stability of distillate fuel oil (accelerated methode) D Conradson carbon residue of petroleum products D Freezing point of aviation fuels D Cone penetration of lubricating grease D217 T Hydrogen sulfide in liquefied petroleum (LP) gases (lead acetate method) D Heat of combustion of liquid hydrocarbon fuels by calorimeter D240 Oxidation stability of mineral insulating oil D2440 Standard test methods and practices for emulsified asphalts D244 Cloud point of petroleum products D2500 T API gravity of crude petroleum and petroleum products (hydrometer method) D Apparent viscosity of engine oils using the cold-cranking simulator D Vapor pressure of petroleum products (Reid method) D / 402 Hydrolytic stability of hydraolic fluids (beverage bottle method) D2619 Existent gum in fuels by jet evaporation D Electrical conductivity of aviation and distillate fuels D Kinematic viscisity of transparent and opaque liquids D Knock characteristics of motor by the research method D Sediment incrude ooils and fuels by the extraction method D Knock characteristics of motor and aviation fuels by the motor method D Ash from petroleum products D482 4 Demulsibility characteristics of lubricating oils D2711 Ramsbottom carbon residue of petroleum products D524 T Sulfur in liquefied petroleum gases (oxy-hyrogen burner or lamp method) D2784 M Oxidation stability of gasoline (induction period method) D * Effect of heat and air on a moving film of asphalt (RTFOT) D2872 Dropping point of lubricating greases D566 T Oxidation characteristics of extreme pressure lubricating oils D2893 Aniline point and mixed aniline point of petroleum products and hydrocarbon solvents D611 M Low-temperature viscosity of autumotive fluid lubricants (Brookfield viscisimeter) D2983 T and check fuel blending for octane and cetane measurement D Salts in crude oil (electrometric method) D Acide number of petroleum products by potentiometric titration D Solvent extractables in petroleum waxes D3235 Rust-preventing characterstics of inhibited mineral oil in presence of water D665 T Flash point of liquids by Setaflash-closed-cup apparatus D3278 Oil content of petroleum waxes D721 T Air release properties of petroleum oils D Oxidation stability of aviation fuels (potential residue méthod) D873 M Flash point by small scale closed tester D Sulfated ash from libricting oils and additives D Water separation characteristics of aviation turbine fuels by portable separometer D3948 Dielectric breakdown voltage of insulating fluids D Water and sediment in crude oil by the centrifuge method (laboratory procedure) D4007 Foaming caracteristics of lubrocating oils D Manual sampling of pétroleum and petroleum products D Insolubles in used lubricating oils D893 T High-shear viscosity using the ICI cone / plate viscosimeter D4287 Cone penetration of petrolatum D937 T Sulfur in oil analyzer D Density and relative density of liquids by lipkin bicapillary pycnometer D Water in crude oils by potentimetric Karl Fischer D Oxidation stability of lubricating greases (oxygen vessel method) D Determination of carbon residue (MCRAT) D Oxidation characteritics of inhibited mineral oils D Low sulfur & nitrogen analyzer for light hydrocarbon products D Evaporation loss of lubricating greases and oils D972 Free water and particulate contamination in mid-distillate fuels (Clear and bright rating) D4860 Distillation of volatile organic liquids D Vapor pressure of petroleum products (mini method) D5191 Water vapor content of gaseous fuels by mesurement of dew-point temperature D1142 Distillation du pétrole brut Distillation of petroleum products at reduced pressure D Apparent viscosity of engine oils using the cold-cranking simulator D5293 Freezing point antifreeze products D1177 T Low sulfur & nitrogen analyzer for light hydrocarbon products D Determining the water washout characteritics of lubricating greases D ,part2 Cloud and Pour Point D5773 Sampling liquefied petroleum (LP) gases (manual method) D Evaporation loss of lubricating oils by the Noack method D5800 T Gauge vapor pressure of liquefied petroleum gases (LP-Gas method) D / 410 Portable gasoline analysis with mid-ftir D5845 API gravity of crude petroleum and liquid petroleum products by hydrometer D Cloud and Pour Point D5949 Hydrocarbon types in liquid petroleum products by fluorescent indicator adsorption D1319 M * Freeze Point D5972 Needle penetration of petroleum waxes D1321 T High temperature foaming characteritics of lubricating oils D6082 Smoke point of kerosine and aviation turbine fuel D1322 M Portable gasoline analysis with mid-ftir D6277 Water separability of petroleum oils and synthetics fluids D Vapore pressure of gasoline D6377 Cone penetration of lubricating grease using 1/4 and 1/2 scale cone equipment D1403 T Vapor pressure of gasoline D6378

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