A SURVEY OF OUR KNOW-HOW : PETROLEUM GLASSWARE VISCOMETER TUBES

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1 N O R M A L A B A N A L I S A SURVEY OF OUR KNOW-HOW : PETROLEUM GLASSWARE VISCOMETER TUBES NORMALAB ANALIS FRANCE S.A. 14, rue des Lilas LINTOT - FRANCE Tel : (33) Fax : (33) Web : http : // Page 1

2 PETROLEUM GLASSWARE INDEX OF TEST METHODS ASTM ASTM D p 3 ASTM D p 3 ASTM D p 3 ASTM D p 3 ASTM D p 3 ASTM D p 4 ASTM D p 4 ASTM D p 4 ASTM D p 4 ASTM D p 4 ASTM D p 4 ASTM D p 4 ASTM D p 5 ASTM D p 3 ASTM D p 13 à 21 ASTM D p 5 ASTM D p 5 ASTM D p 5 ASTM D p 5 ASTM D p 5 ASTM D p 6 ASTM D p 6 ASTM D p 6 ASTM D p 4 ASTM D p 6 ASTM D p 6 ASTM D p 3 ASTM D p 7 ASTM D p 7 ASTM D p 7 ASTM D p 7 ASTM D p 7 ASTM D p 6 ASTM D p 8 ASTM D p 4 ASTM D p 8 ASTM D p 8 ASTM D p 8 ASTM D p 8 ASTM D p 8 ASTM D p ASTM D p 15 ASTM D p 5 ASTM D p 8 ASTM D p 9 ASTM D p 6 ASTM D p 9 ASTM D p 9 ASTM D p 4 ASTM D p 9 ASTM D p 9 ASTM D p 4 ASTM D p 4 ASTM D p 9 ASTM D p 9 ASTM D p 6 ASTM D p 6 ASTM D p 11 ASTM D p 4 ASTM D p 6 ASTM D p 11 ASTM E p 4 ASTM E p 11 ASTM E p 3 DIN DIN p 9 DIN p 4 DIN p 6 DIN p 6 DIN p 8 DIN p 6 DIN p 6 DIN p 10 DIN p 3 DIN p 6 DIN p 5 DIN p 5 DIN p 7 DIN p 4 CEN EN p 10 EN p 10 EN p 10 EN p 3 EN p 10 EN p 9 EN p 9 EN p 9 IP IP p 5 IP p 4 IP p 9 IP p 4 IP p 3 IP p 5 IP p 3 IP p 13 à 20 IP p 4 IP p 4 IP p 10 IP p 7 IP p 3 IP p 5 IP p 6 IP p 10 IP p 6 IP p 7 IP p 6 IP p 3 IP p 3 IP p 8 IP p 8 IP p 10 IP p 8 ISO ISO p 8 ISO p 9 ISO p 4 ISO p 13 à 20 ISO p 13 à 20 ISO p 3 ISO p 4 ISO p 5 ISO p 7 ISO p 3 ISO p 9 ISO p 6 ISO p 3 ISO p 9 ISO p 9 ISO p 5 ISO p 6 ISO p 7 ISO p 7 ISO p 5 ISO p 11 ISO p 6 AFNOR NF M p 5 NF M p 4 NF M p 5 NF M p 7 NF M p 10 NF M p 10 NF M p 8 NF T p 5 NF T p 4-11 NF T p 3 NF T p 10 NF T p 5 NF T p 6 NF T p 7 NF T p 6 NF T p 4 NF T p 11 NF T p 3 NF T p 7 Page 2

3 ASTM D 20 - D AFNOR T IP ml Flask Receiver 100 ml ASTM D 36 - EN ISO Standardized beaker for manual or automatic softening point apparatus ASTM D 70 - ISO IP Density bottle A - 24/30 ml Density bottle B - 24/30 ml Density bottle C - 24/30 ml Density bottle D - 24/30 ml ASTM D 86 - D E EN ISO 3405 IP IP DIN ml distillation flask ml distillation flask ml distillation flask ml distillation flask Distillation receiver 100 ml Distillation receiver 200 ml Complete receiver 100 ml with metal foot for automatic distillation Distillation receiver 100 ml with glass foot Spare graduated glass tube ml distillation flask black bottom ml distillation flask black bottom ml distillation flask with shank and holed cork for probe ml distillation flask with shank and holed cork for probe Male/Female shank for condenser tube entry ASTM D 87 - AFNOR T IP Test tube Page 3

4 A B ASTM D 88 - D E Saybolt flask 60 ml B Graduated cylinder ml A ASTM D 91 - D 96 - D D D D D 4007 AFNOR M T IP 75 - DIN A Cone-shaped tube 100 ml (203 mm) A ml pear-shaped centrifuge tube 100 ml B ,5 pear-shaped centrifuge tube 100 ml B ASTM D 95 - AFNOR T IP 74 - ISO Round bottom flash CN 24/29 (500 ml) Liebig condenser CN 24/29 (400 mm) Dean stark trap (10 ml x 0,1 ml) ml : 1/5 dean stark with conical bottom ASTM D 97 - D ISO IP Test jar for manual apparatus Pour test tube for automatic apparatus Cloud test tube for automatic apparatus ASTM D IP 23 - DIN ml flask - CN 24/ Réfrigérant Liebig 400 mm CN 24/ Piège gradué - CN 24/29 Page 4

5 ASTM D ISO IP DIN ml Beaker ASTM D ISO IP 53 - DIN Glass conical flask 1 L Sintered cartridge made of alundun Glass water cup ASTM D AFNOR T IP Heat resistant glass coking bulb ASTM D ISO M Glass sample container with cover Cover for container ASTM D D AFNOR T Test tube ASTM D AFNOR M07021 Méthode II Test tube Jacket tube ml pipet ml pipet Manual stirrer Page 5

6 ASTM D D AFNOR T IP 135 DIN ml beaker ASTM D D AFNOR T IP 158 DIN Filter stick (24/24) Filter stick (35/20) ASTM D ISO IP DIN Borosilicate glass jar L graduated cylinder for foam test Diffuser stone calibrated Stainless steel diffuser stone (without certificat) ASTM D D DIN Lipkin pycnometer ASTM D D D ISO DIN Glass condenser Oxygen inlet tube Oil test tube Iron / copper catalyst packed in glass tube Page 6

7 ASTM D ISO Column with condenser Flask with thermowell Jacketed receiver Cold trap ASTM D AFNOR T Dewar freezing tube (200 ml) ASTM D AFNOR M IP ml flask (non aromatic products) ml flask (aromatic products) Burner for non-aromatic samples Burner for aromatic samples Chimney Absorber Spray trap ASTM D ISO IP 156 DIN FIA true bore column - 1/100 mm precision Upper S28/12 ground joint for accuracy column Low S12/2 ground joint for accuracy column Upper part of standard column Analyser part of standard column (pack of 25) ASTM D AFNOR T ISO Glass graduated cylinder (100 ml) Page 7

8 ASTM D ISO IP 196 DIN Standard glass sample tube ASTM D D AFNOR M IP ml weathering receiver ASTM D Depentanization apparatus ASTM D Complete adsorption column for low olefinic concentration ASTM D High efficiency column Spherical grount joint with nipple ASTM D IP Borosilicate glass sample container Copper catalyst packed in a plastic container with drying stopper Page 8

9 ASTM D ml trace sediment tube ASTM D D NF EN ISO Quartz combustion chamber Absorber with fritted plate Trap ASTM D ISO IP 16 DIN Jacketed sample tube (double walls) Unsilvered dewar flask ASTM D D ISO ISO 5164 EN EN Burettes for reference fluids : ml buret without bulb nor stopcock ml buret without bulb nor stopcock ml buret with bulb without stopcock ml buret with bulb without stopcock Buret 400 ml automatic filing with stopcock, graduations in % each 0,5 % and in ml (each 2 ml) ml buret for measuring dilute tetraethyllead ml buret for measuring dilute tetraethyllead ASTM D Borosilicate glass sample conbainer for RTFOT test Page 9

10 AFNOR M EN 13 - EN 41 - IP ml complete flask without CN ml complete flask with CN Protective glass tube ml flask with electric heating resistance and cock, with RIN 29/ Reflux condenser with RIN 29/ Separating funnel with RIN 29/32 AFNOR T IP DIN CAT N ml conical flask with ground joint (24/29) Reflux extractor (CN 24 / CN 34) Condenser ml conical flask with ground joint (29/34) Reflux extractor (CN 29 / CN 34) IP AFNOR M EN 116 CAT N Pipette for manual method without spherical joint Pipette for manual method with Spherical joint Pipette for automatic method without spherical joint Pipette for automatic method with spherical joint Supply connection with S joint CEN test tube CFPP EN 1428 CAT N ml round bottom flask, 29/32 ground joint ml : 1/10 dean stark, 29/32 ground joint Condenser, effective length 400 mm 29/32 ground joint Page 10

11 ASTM D 4006 CAT N Dessicant tube Liebig CN Dean-stark CN L flask, joint 24/40 ASTM D ISO CAT N ml borosilicate glass crucible ml borosilicate glass crucible ml quartz crucible ml quartz crucible ASTM E NFT CAT N Dean-stark 5 ml - CN 24/ Dean-stark 10 ml - CN 24/ Dean-stark 10 ml with conical bottom CN 24/29 NFT CAT N CNOMO TEST Foaming tendency of aqueous cutting fluids - Silicone tube (2 m) (cat. n 14094) - Small three-pronged clamp maide of laboral alloy (cat. n 16254) - Stand with rod diameter 12 mm x 800 mm length (cat. n 16324) - Universal boss (cat. n 16329) - Jacketed cylinder 2000 ml (cat. n 23340) - Upper tip for cylinder (cat. n 23341) - Flowmeter L/h for water or soluble oil having a density of 1,02 and a viscosity of 1 Cp, pyrex tube, stainless steel float with stand and fitting for rubber tube (cat. n 23344) - Centrifuge pump type RM-PP-VKKK-5/35-30 (15) (cat. n 27557) - Frequency variator for pump (cat. n 27558) Page 11

12 VISCOMETER TUBES INTRODUCTION The following pages present the various types of viscometers we have been manufacturing for years in our workshop and our calibration laboratory MANUFACTURING Normalab Analis viscometers are made out of low-expanding DURAN 50 glass. The tubes are made with high accuracy capillaries (+/- 0,01 mm). Scores and figures are marked using computerized engraving or indelible process. The viscometer result less fragilit (less breakages due to score discontinuities). The standard capillary viscometers are delivered without any engraved constant. This may be achieved on customer s special request when ordering. CALIBRATION 2 options are available for most of our models : A: Without certificate These Normalab Analis viscometers are made of calibrated glass tubes. The mentioned constant (s) assume on aproximate value for the coefficient of thermal expansion typical to that for hydrocarbons.the uncertainty of the mentioned constant is more than 0,2 %. An additional calibration with at least two viscosity oil standards is then to be conducted in your laboratory. B-C : With calibration certificate Normalab Analis viscometers are calibrated within our air conditionned laboratory using reference viscometers calibrated by the french National Testing Laboratory. These viscometer tubes are checked at regular intervals by means of certified viscosity oil standards. Normalab Analis has been assessed and registered as meeting the requirements of ISO 9002 for laboratory and associated services of repair, calibration and verification of laboratories devices by SGS and the COFRAC. Page 12

13 CANNON FENSKE OPAQUE ASTM D D IP 71 - ISO For Opaque liquids VISCOMETER TUBES 25 0,002 0,3 1, ,004 0,8 3, ,008 1,6 6, , , , , , , , UBBELOHDE 0 0,001 0, C 0,003 0, B 0, A 0,007/8 1, , C 0, B 0, , C 0, B 0, A 0,7/0, , C 3, B 5, C B Page 13

14 VISCOMETER TUBES CANNON FENSKE ROUTINE 25 0,002 0, ,004 0, ,008 1, , , , , , , , HOUILLON Size Nominal Viscosity cst C Code Constant REF. 50 0,016 0,8 3, ,032 1,6 6, , , , , Page 14

15 VISCOMETER TUBES CANNON MANNING VACUUM ASTM D 2171 For bitumens 4 0,002 0,0006 0,036 0, ,006 0,002 0,12 2, ,02 0,006 0, ,06 0,02 1, ,2 0,06 3, ,6 0, , BS / IP SL 1 0,01 3, A 0, , A 0, , A 3, , A 30, , Page 15

16 VISCOMETER TUBES BS / IP U RF ASTM D D IP 71 - ISO For Opaque Liquids 1 0,003 0, , , , , , , , , , , S.I.L. 0C 0,003 0, , C 0, , C 0, C Page 16

17 VISCOMETER TUBES BAUME VIGNERON Viscosity cst A C REF. REF. 0, , , , CANNON UBBELOHDE without washer connection B - With calibration certificate Size Nominal A B 0C 0, A 0, , C 0, , C 0, C Page 17

18 VISCOMETER TUBES CANNON UBBELOHDE with washer connection B - With calibration certificate Size Nominal A B 0C 0, A 0, , C 0, , C 0, C CANNON MANNING SEMI - MICRO 25 0,002 0, ,004 0, ,008 1, , , , , , , , Page 18

19 VISCOMETER TUBES CANNON UBBELOHDE DILUTION 25 0,002 0, ,004 0, ,008 1, , , , , , , , CANNON UBBELOHDE SEMI-MICRO 25 0,002 0, ,004 0, ,008 1, , , , , , , , Page 19

20 VISCOMETER TUBES BS / IP SL - S 1 0,0008 1,05 mini ,003 2, ,01 3, , , , BS / IP SL - MSL MICRO UBBELOHDE 1 0,003 0, , , , , ZEITFUCHS For Transparent and Opaque Liquids 1 0,003 0, , , , , Page 20

21 VISCOMETER TUBES U. F. Viscosity cst A C REF. REF. 0, , , , ASTM D Constant temperature viscosity bath «ROUTINE» (max. 100 C) with glass jar of 20 liters, thermometer for temperature reading and 5 places for common viscometers (support not included) Constant temperature viscosity bath «ROUTINE» (max 200 C) with glass jar of 20 liters, digital temperature display and 5 places for commun viscometers (support not included) Page 21

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