CRYO FTIR.

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1 FTIR Cryostats

2 Cryostats for FTIR Experiments Cryo Industries Variable Temperature Continuous Flow Cryostas (Models RC-102 and RC-152) are an excellent choice for Fourier Transform Infra-Red (FTIR) spectroscopy experiments. Model RC-102 (sample in vacuum) and Model RC-152 (sample in vapor) are superior, versatile flow cryostats that offer fast cooldown with high efficiency. Linear Drive Knob All Models come standard with a multiple position sample holder, mounting flange to fit spectrometer and a high efficiency cryogen transfer line. Model RC-102 allows sample rotation with scale and Model RC-152 via a top-loading rotatable, adjustable sample positioner. ellows to allow linear travel Available Options Include: Remotely controlled linear manipulator and/ or rotary stage IR window materials (wedged or plane parallel) Operate with either LHe or LN2 Electrical access to sample Complete systems available: temperature controller, pumping stations and storage dewars. Operating temperature range: RC-102: 2 K to 325 K RC-152: 1.5 K to 325 K Optional sample rotation feature w/graduated 360 rotation indication dial Rotatable O-ring seal Sample and radiation shield both move in linear direction together inside (rotational movement is optional) Model RC-102 with Linear Rotation

3 THE INFORMATION CONTAINED IN THIS DRAWING IS THE SOLE PROPERTY OF CRYO INDUSTRIES OF AMERICA, INC., S WILLOW STREET MANCHESTER, N.H ANY REPRODUCTION IN PART OR WHOLE WITHOUT THE WRITTEN PERMISSION OF CRYO INDUSTRIES IS STRICTLY PROHIITED CRYO Model RC-102 with Linear Rotation for FTIR 0.75 I.D. S/S FLEX HOSE X 72 LG WITH NW-25 FLange QUICK DISCONNECT FOR TRANSFER LINE/WORK STATION SEPARATION HELIUM VENT WITH NW25 ADAPTER 1.37 O.D. VALVE CONTROL KNO LINEAR MOTION STAGE (SHOWN MID-TRAVEL) STORAGE DEWAR INSERT LEG 3.20 (TOTAL TRAVEL IS 2.20 TO 4.20) DRUM DIAL ROTATIONAL SEAL HOUSING (3) LANK PORTS (1) 10 PIN ELECTRICAL FEEDTHROUGH.050 O.D. LIQUID HELIUM VALVE CONTROL TUE APPROX QUICK DISCONNECT FOR SAMPLE ACCESS SECTION I.D O.D. FTIR SAMPLE COMPARTMENT COVER NW25 FLANGE ACTIVATED CHARCOAL CRYOPUMP HELIUM TRANSFER LINE ANTI VIRATION CONCENTRICITY SPACER 1.25 DIA. COPPER SAMPLE MOUNT WITH HEATER, PROVISION FOR TEMP. SENSOR AND (8) #4-40 TAPPED HOLES HELIUM INLET WITH FLOW CONTROL VALVE WITH FILTER DIA. COPPER SAMPLE HOLDER WITH (3) 0.19 (5mm) DIA. CLEAR VIEW PORTS Cryo Model: FTIR (4) 1/4-20 TAPPED MOUNTING HOLES ON A 3.50 DIA..C. PROPRIETARY INFORMATION CRYO INDUSTRIES of America Inc S. Willow St., Manchester N.H TITLE: MODEL RC102 FTIR OPTICAL CRYOGENIC WORKSTATION System Features Cryo Reference Drawing No.: FTIR <2K to 325K operating temperature range Operates with liquid helium or liquid nitrogen Operates in Push or Pull modes (4) 1.62 inch diameter clear view CFQ windows 1.25 inch diameter OFHC copper sample mount Hi Power Heater installed on sample mount Anti vibration and location concentricity spacer for sample mount Gold Plated optical OFHC copper T-Style Sample holder w/provision to hold (3) samples 360 degree drum dial with rotational housing seal for sample rotation 2 inch (5 cm) linear motion travel stage for linear sample movement (1) 10-pin electrical feedthrough with mate (3) spare blank feedthrough ports NW25 vapor pumping port Evacuation valve with NW25 interface flange Safety pressure relief Flexible stainless steel helium transfer line with flow control valve included Model CD-12A Silicon Diode Temperature Sensor - bolt on style - installed on sample mount (Sensor is removable or movable)

4 Model RC-102 Compact with Sample Rotation 0.75 I.D. S/S FLEX HOSE X 72 LG WITH NW-25 FLange QUICK DISCONNECT FOR TRANSFER LINE/WORK STATION SEPARATION 1.37 O.D. HELIUM VENT WITH NW25 ADAPTER VALVE CONTROL KNO 360 DRUM DIAL ROTATIONAL SEAL HOUSING ALLOWS SAMPLE MOUNT RADIATION SHIELD TO E ROTATED STORAGE DEWAR INSERT LEG (3) LANK PORTS APPROX SAFETY PRESSURE (1) 10 PIN ELECTRICAL FEEDTHROUGH.050 O.D. LIQUID HELIUM VALVE CONTROL TUE 2.25 O.D MAIN ANTI VIRRATION AND ROTATION CONCENTRICITY SPACER SECTION - NW25 FLANGE DIA. COPPER SAMPLE MOUNT WITH HEATER, PROVISION FOR TEMP. SENSOR AND (4) #4-40 TAPPED HOLES ACTIVATED CHARCOAL CRYOPUMP 1.25 HELIUM TRANSFER LINE DIA. COPPER C-STYLE 90 DUAL SAMPLE HOLDER (4) #8-32 TAPPED MOUNTING HOLES OPTIONAL SECONDARY ANTI VIRATION AND ROTATION CONCENTRICITY SPACER (INSTALLED ONLY IF NEEDED) HELIUM INLET WITH FLOW CONTROL VALVE WITH FILTER Cryo Model: CLR System Features PROPRIETARY INFORMATION THE INFORMATION CONTAINED IN THIS DRAWING IS THE SOLE PROPERTY OF CRYO INDUSTRIES OF AMERICA, INC., S WILLOW STREET MANCHESTER, N.H ANY REPRODUCTION IN PART OR WHOLE WITHOUT THE WRITTEN PERMISSION OF CRYO INDUSTRIES IS STRICTLY PROHIITED TITLE: CRYO INDUSTRIES of America Inc S. Willow St., Manchester N.H COMPACT MODEL RC102 ROTATIONAL SAMPLE OPTICAL Ref. Cryo Drawing: CLR <2K to 325K operating temperature range Operates with liquid helium or liquid nitrogen Compact 1.50" square window block design (2) 0.93 inch diameter clear view CFQ o-ring sealed windows (Removable) 0.75 inch diameter copper sample mount Gold Plated Copper C-style optical sample holder(as Per sketch) Hi Power Heater installed on sample mount (1) 10-pin electrical feedthrough with mate (3) Spare blank feedthrough ports NW25 vapor pumping port Evacuation valve with NW25 interface flange Safety pressure relief on vacuum space Flexible stainless steel transfer line with flow control valve Silicon Diode Temperature Sensor (SD) style installed on sample mount Rotational sample mount design includes: degree drum dial with rotational o-ring housing seal 1 degree graduations Anti vibration concentricity spacer Design allows external control to rotate sample mount and radiation shield together inside of outer windows

5 Cryo Industries of America, Inc South Willow Street Manchester, NH Ph: (603) Fax: (603)

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