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2 BOLA-Flat Flange Distillation Apparatuses made of Fluoroplastic () with SAFE LAB-System 5 9 Suitable for the distillation of strong alkaline or acid products as well as aggressive solvents. All parts exposed to the medium are made of fluoroplastic. They can be heated by a thermostat or by an electric heating jacket, but the temperature in the flat flange reaction vessel should not exceed 00 C. Working under is also possible Since our distillation apparatus is equipped with the SAFE LABsystem, it represents the highest possible safety standard in the laboratory. This patented system allows two functions: both to connect two standard ground joints tightly and safely and to unlock and separate stuck standard ground joints. The whole trick consists of an additional thread and a stopper-loc nut. With just this stopper-loc nut one can either lock or unlock standard ground joints. Lock 5 Unlock +00 Capacity 500 ml 000 ml 000 ml 4000 ml 6000 ml Cat. No. B 80-0 B B B 80- B 80-5 Total dimensions (H x L), approx. 450x600 mm 550x700 mm 700x750 mm 750x980 mm 790x000 mm Reaction Vessel, Flat Flange NW 00 NW 00 NW 00 NW 50 NW 50 B 8-0 B 8-06 B 8-09 B 8- B 8-5 Gasket, Flat Flange NW 00 NW 00 NW 00 NW 50 NW 50 B 8-0 B 8-0 B 8-0 B 8-04 B 8-04 Lid, Flat Flange NW 00 NW 00 NW 00 NW 50 NW 50 B 8-0 B 8-0 B 8-0 B 8-04 B 8-04 Joining Piece, Flat Flange 4 NW 00 NW 00 NW 00 NW 50 NW 50 B 84-0 B 84-0 B 84-0 B B Dropping Funnel with Cone NS 9/ 5 5 ml 5 ml 50 ml 500 ml 500 ml B 85-0 B 85-0 B 85-0 B 85-0 B 85-0 Liebig Condenser 6 00 mm 450 mm 450 mm 600 mm 600 mm B 9-0 B 9-04 B 9-04 B 9-06 B 9-06 Distillation Thermometer 0/+50: C 7 B 90-0 B 90-0 B 90-0 B 90-0 B 90-0 Moon-shaped Stirrer Shaft 8 Ø0x50mm Ø0x450mm Ø0x50mm Ø0x600mm Ø0x600mm C 76- C 76-4 C 76-6 C 76-8 C 76-8 Thermometer for Flask 0/+50: C 9 B 87-0 B B B B Supporting Device for 0 B 86-0 B 86-0 B 86-0 B 86-0 B 86-0 Thermometer NS 9/ Standard Ground Joint Stirrer Bearing B 88-0 B 88-0 B 88-0 B 88-0 B 88-0 NS 9/ Distillation Head x NS 9/ B 89-0 B 89-0 B 89-0 B 89-0 B 98-0 Receiver Adaptor B 89-0 B 9-0 B 9-0 B 9-0 B 9-0 Vacuum Stopcock 4 B 9-0 B 9-0 B 9-0 B 9-0 B 9-0 Round Bottom Flask NS 9/ 5 00 ml 50 ml 500 ml 000 ml 000 ml or Distillate Bottle A A A B B Internet: info@bola.de
3 B 4 To protect your pump against aggressive gases, a scrubber bottle should be connected between the distillation apparatus and the pump. scrubber bottles we refer you to page. BOLA-Reaction Vessels, Flat Flange Made of fluoroplastic. Smooth interior surface. Cat. No. Capacity Flange Vessel O.D. Total height B ml NW 00 0 mm 0 mm B ml NW 00 0 mm 05 mm B ml NW mm 70 mm B ml NW mm 90 mm B ml NW 50 5 mm 0 mm BOLA-Gaskets, Flat Flange Made of fluoroplastic with silicone insert. Medium is only exposed to. Cat. No. flange B 8-0 NW 00 B 8-04 NW 50 BOLA-Joining Pieces, Flat Flange Joining pieces made of Silumin, very strong. Silumin Cat. No. Number of screws flange B NW 00 B NW 50 4 BOLA-Lids, Flat Flange Made of fluoroplastic. With standard ground joint necks. Cat. No. Flange Center socket Side sockets B 8-0 NW 00 NS 9/ x NS 9/ B 8-04 NW 50 NS 9/ x NS 9/ B 8-06 NW 50 NS 45/40 x NS 9/ Cleaning for Trace Analysis To prevent contaminations of cations and anions in trace analysis, the vessels should first be filled with a NHCL and HNO -solution. This solution should be allowed to stand for a maximum of 6 hours at room temperature. Afterwards, the vessel should be rinsed with clean, deionized!water. Internet: info@bola.de
4 BOLA-Dropping Funnels Made of fluoroplastic (FEP). Equipped with SAFE LABsystem,, with fine adjustment stopcock and standard ground joint cone made of fluoroplastic (). FEP Cat. No. Capacity Cone B ml NS 9/ B ml NS 9/ B ml NS 9/ 6 BOLA-Liebig Condensers, Transparent Connections made of fluoroplastic (). With cone and socket, equipped with SAFE LAB-system. The thin-walled cooling tube is made of translucent and gastight fluoroplastic (), the outer cooling jacket is made of glass (borosilicate glass). The medium is exposed only to fluoroplastic. Cat. No. Length Cone Socket B mm NS 9/ NS 9/ B mm NS 9/ NS 9/ B mm NS 9/ NS 9/ 7 BOLA-Distillation Thermometers Fluoroplastic-coated. Calibrated for immersion depth of 50 mm. -0 Cat. No. reaction vessel Temperature range C Length O.D. B ml 0/+50: 00 mm 7,5 mm 8 BOLA-Moon-Shaped Stirrer Shafts Fluoroplastic-coated stainless-steel shafts. The moon-shaped stirrer blade with double-sided groove and the access for the stirrer blade are made of solid fluoroplastic. The stirrer blade tilts and can therefore be inserted through a standard ground joint. Cat. No. reaction vessel standard ground joint Shaft dia. Length C ml NS 9/ 0 mm 50 mm C ml NS 9/ 0 mm 450 mm C ml NS 9/ 0 mm 50 mm C /6000 ml NS 9/ 0 mm 600 mm C /6000 ml NS 45/40 6 mm 600 mm 9 BOLA-Thermometers for Flasks Fluoroplastic-coated. -0 Cat. No. reaction vessel Temperature range C Length O.D. B ml 0/+50: 450 mm 7 mm B ml 0/+50: 50 mm 7 mm B /4000/6000 ml 0/+50: 600 mm 7 mm 4 4 Internet: info@bola.de
5 4 B 0 Lock 0 BOLA-Supporting Devices for Thermometers Made of fluoroplastic. Equipped with SAFE LAB-system, with adjustable special gasket made of /FPM. You will find suitable PT 00 probes coated with on pages 8 to 0. Cat. No. Ground Joint dia. B 86-0 NS 9/ 8 mm Unlock BOLA-Standard Ground Joint Stirrer Bearings Made of fluoroplastic. Equipped with SAFE LAB-system, with adjustable special gasket. Cat. No. Cone Bearing dia. B 88-0 NS 9/ 0 mm B NS 45/40 6 mm BOLA-Distillation Heads Made of fluoroplastic. Equipped with SAFE LABsystem, with two ground joint cones NS 9/ and integrated supporting device for thermometers with a diameter of 8 mm. Cat. No. Cone dia. B 89-0 x NS 9/ 8 mm BOLA-Receiver Adaptors Made of fluoroplastic. Equipped with SAFE LABsystem, with cone and socket NS 9/, with connection for stopcock NS 9/6. Cat. No. B BOLA-Vacuum Stopcocks Made of fluoroplastic. Equipped with SAFE LAB-system. Cat. No. Cone Stopcock Connection bore dia. for tube O.D. B 9-0 NS 9/6 mm 8 mm Assembled by: Mueller-Scherr,Graz Internet: info@bola.de 5 5
6 with supporting device BOLA-Distillation Heaters 0V/50Hz, consisting of: Heating Jacket: Encapsulated in a solid metal mantle / with integrated protection against excess temperature (+00 C) / with supporting device Relay: Infinitely variable output regulation / indicator of heating phase and signal lamp / connection for contact thermometer Step Switch: Heater bands can be triggered separately / with equipment-on indicator lamp Cat. No. reaction vessel Heating capacity Number of heater bands B ml 500 Watt B ml 700 Watt B ml 000 Watt 4 B ml 400 Watt 4 BOLA-Liebig Condensers, Vertical The thin-walled cooling tube consists of translucent and gastight corrugated tube with a large surface made of fluoroplastic. The outer cooling jacket is made of glass (borosilicate glass). The medium is exposed only to fluoroplastic. Cat. No. Length Cone Socket B mm NS 9/ NS 9/ B mm NS 9/ NS 9/ BOLA-Links Made of fluoroplastic. Equipped with SAFE LAB-system, for vertical positioning of the Liebig condenser. Cat. No. Cone Socket B 0-0 NS 9/ NS 9/ BOLA-Ground Joint Distributors Made of fluoroplastic. With cone and socket, equipped with SAFE LAB-system. Cat. No. Socket Cone Length x Width x Total height B 0-0 x NS 9/ x NS 9/ mm x 40 mm x 05 mm B 0-04 x NS 9/ x NS 9/ 60 mm x 40 mm x 05 mm 6 6 Internet: info@bola.de
7 OLA-SAFE LAB Replacement Stopper-Loc Nuts Made of glass-fibre reinforced. locking and unlocking cones. Cat. No. Suitable for ground joint K NS 9/6 K 49-0 NS 9/ K 49-6 NS 45/40 Lock B Unlock BOLA-Stoppers Made of fluoroplastic. With standard ground joint, with knurled or hexagonal ribs. Now new with turned, circular sealing ribs easily removable prevents sticking together of the ground joints improved sealing reduced danger of breaking Cat. No. Rib-ø Ground joint H mm NS 9/6 H mm NS 9/ H mm NS 45/40 BOLA-Distillate Bottles Made of fluoroplastics. Non-porous, with a standard ground joint adaptor NS 9/, not suitable for. FEP Cat. No. Capacity Bottle dia. Total height, approx. B ml 59 mm 60 mm B ml 7 mm 90 mm B ml 9 mm 5 mm BOLA-Round Bottom Flasks Made of fluoroplastic. With standard ground joint, non-porous. Suitable for a rotary evaporation, e.g. at 0 mbar and a temperature of 50 C. Cat. No. Capacity Ground Joint Height Max. O.D. flask A ml NS 9/ 7 mm 67 mm A ml NS 9/ 49 mm 88 mm A ml NS 9/ 77 mm 07 mm In chapter A on page 6 you will find a choice of round bottom flasks with two or three necks in different versions, like for example with standard ground joint or GL side necks. Internet: info@bola.de 7 7
8 BOLA-Standard Ground Joint Tube Fittings Made of fluoroplastic. Equipped with SAFE LAB-system, for connecting tubes and tubing. Now new with turned, circular sealing ribs easily removable prevents sticking together of the ground joints improved sealing reduced danger of breaking Cat. No. Cone tubing Ground Joint I.D. x O.D. B 04-0 NS 9/6 4,0 x 6,0 mm B 04-6 NS 9/,6 x, mm B 04-0 NS 9/ 4,0 x 6,0 mm B 04- NS 9/ 6,0 x 8,0 mm B 04-4 NS 9/ 8,0 x 0,0 mm BOLA-Micro Reaction Vessels Ideal for reactions of small volumes of reactants. The integral GL thread fittings, when used together with our laboratory screw joints, allow assembly with tubing, glass or metal tubes, thermometers, sensors or probes of wide range of diameters. Any unused GL thread fittings can be blocked off by means of GL screw caps. We recommend to heat these micro-reaction vessels by a thermostat. (Supplied without laboratory screw joint and thermometer.) Low pressure Cat. No. Capacity GL fittings I.D. Height, O.D. Total inside height B ml x GL 8 45,5 mm 40 mm 50 mm 79 mm B ml x GL 8 45,5 mm 58 mm 50 mm 97 mm B ml x GL 4 45,5 mm 58 mm 50 mm 96 mm and x GL 8 B ml x GL 8 60,0 mm 86 mm 66 mm 0 mm and x GL 5 B ml x GL 5 80,0 mm 09 mm 85 mm 58 mm You will find suitable laboratory screw joints on page. Example for application BOLA-Liebig Condensers, Vacuum Suitable for. With a solid and one-piece cooling tube made of (not ), for other dimensions see cat. no. B 9-.. on page 4. Cat. No. Length Cone Socket B mm NS 9/ NS 9/ B mm NS 9/ NS 9/ B mm NS 9/ NS 9/ Any technical questions? Simply call our technical hotline. We will be glad to help you. Technical Hotline: y +49(0)946 / Internet: info@bola.de
9 4 BOLA-Distillation Apparatuses, Transparent Suitable for the distillation of strong alkaline or acid products as well as aggressive solvents. In addition, it can also be used for the distillation of pure liquids which should not come into contact with glass. One important advantage of this apparatus is the reaction vessel with a large opening and a very smooth interior surface. The reactions, such as vaporization, boiling or bubbling as well as the filling height are visible in this reaction vessel. B These apparatuses can be heated by a thermostat, by an electric heating jacket or on a hotplate, but the temperature in the reaction vessel should not exceed 00 C. Stirring with a -coated magnetic stirring bar is possible when using a hotplate. The medium is exposed only to. is resistant to virtually all chemicals and can be used at temperatures from 00 C to +60 C. BOLA-Transparent Reaction Vessels, Flat Flange Made of fluoroplastic. With a smooth and non-porous surface and a flat bottom. BOLA-Gaskets, Flat Flange Made of fluoroplastic with silicone insert. Medium is only exposed to. Cat. No. Cat. No. Capacity Height Vessel O.D. Flange B ml 50 mm 50 mm 70/46 Flange B -0 70/46 Do you need technical assistance such as professional advice or dimensions? Simply call us! Technical Hotline: y +49(0)946 / BOLA-Lids, Flat Flange Made of fluoroplastic. Cat. No. Center socket Side sockets Flange B -0 NS 9/ x NS 9/ 70/46 BOLA-Joining Pieces, Flat Flange Made of aluminum. Cat. No. 4 Flange B -0 70/46 Internet: info@bola.de 9 9
10 BOLA-Micro Distillation Apparatuses 4 made of Fluoroplastic () This micro distillation apparatus is made of a fluoroplastic material (). It is suitable for and for the distillation of smaller liquid quantities. This apparatus can be heated by a thermostat or by an electric heating jacket, but the temperature in the distillation vessel should not exceed 00 C. The connections are gastight screw fittings. The distillation vessel (90 ml) is connected with the collecting vessel (60 ml) by means of a condenser (glass pipe with a tube inside). The second connection on both the distillation vessel and the collecting vessel may be used, for example, to introduce an inert gas, to connect a source, to make a metered addition, to take a sample, to provide a filtered vent or to insert a fluoroplastic-jacketed thermometer. The medium to be distilled (e.g. strong alkalis, acids or aggressive solvents) is exposed only to pure fluoroplastics (/). Low pressure BOLA-Micro Distillation Apparatuses, Complete Made of fluoroplastic (). Cat. No. Capacity of Capacity of distillation vessel collecting vessel B ml 60 ml BOLA-Distillation Vessels with Screw Cap Made of fluoroplastic (). Cat. No. Capacity With connections for tube B ml 0 mm and 8 mm BOLA-Collecting Vessels with Screw Cap Made of fluoroplastic (). Cat. No. Capacity With connections for tube B ml 0 mm and 8 mm BOLA-Distillation Liebig Condensers Made of fluoroplastic ()/glass (borosilicate glass). Cat. No. Tube O.D. Length, approx. Hose connector dia. B mm 0 mm 9 mm BOLA-Distillation Thermometers Fluoroplastic-coated. Cat. No. 4 Temperature range C Length B /+50: 00 mm 0 0 Internet: info@bola.de
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