Accessories Catalogue

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1 Accessories Catalogue For Perfect Freeze Drying

2 Accessories for Perfect Freeze Drying

3 Martin Christ Gefriertrocknungsanlagen GmbH An der Unteren Söse Osterode am Harz Phone +49 (0) Fax +49 (0)

4 1 Freeze Drying / Lyophilisation 5 2 Example Applications 9 3 Drying Chambers and shelves Drying chambers Unheated shelves Heated shelves LSC sealing device (wired) LSCplus sealing device (wireless) LSCplus shelves (wireless) LSC shelves (wired) Drying manifolds 46 4 Drying Accessories Product dishes Product sieves s, split s, not split Rubber valves Round-bottom flasks Filter inserts Wide-neck bottles Protective nets Ampoules Single vial sealing device Injection vials 73 5 Epsilon Accessories 77 6 Vacuum Vacuum pumps Vacuum pump oil Vacuum hoses Vacuum accessories 95 7 Process Data Acquisition Software and hardware Sensors Miscellaneous Cooling Baths and Freezing Equipment 107

5 Freeze Drying / Lyophilisation Freeze drying or lyophilisation takes place in the solid (frozen) state and is the preferred means for the long-term preservation of a wide variety of substances and for specimen preparation for modern analytic methods. It is also used in animal preparations and in museums to preserve the original material forms. Relatively new applications involve the drying of nanoparticles, where it is important to avoid the effects of capillary forces and surface tension. Freeze drying is used for more than 30 different substance categories or materials, with the pharmaceutical and biotechnology industries and food preservation being the most significant application areas.

6 1 Freeze Drying / Lyophilisation

7 6 Freeze Drying / Lyophilisation 1 Freeze Drying / Lyophilisation Freeze drying or lyophilisation is by far the gentlest way to remove moisture from materials. The physical phenomenon of sublimation means a direct transition from the solid state to the vapour state without passing through the liquid state. The frozen material is dried under vacuum without thawing. This method can be used for a wide variety of applications: Preserving the characteristics of original substances in products (e.g. pharmaceutical products or milk) Preserving the original form (e.g. animal preparations, archaeological objects or flowers) Conditioning the material (e.g. freeze-dried fruit in yoghurt) Chemical analyses (e.g. trace element analyses of foods, sludge or soil) Freeze dryers are generally divided into two categories: batch freeze dryers and continuous freeze dryers. Batch freeze dryers are available with capacities from 2 kg to approximately 1 tonne per batch. Christ specialises in this product category and is the only manufacturer worldwide offering products that cover the full spectrum from standard laboratory units to pilot freeze dryers and large production units.

8 Freeze Drying / Lyophilisation 7 Laboratory freeze dryer systems Ice condenser capacity 2 to 24 kg Mainly air-cooled chilling systems Broad range of accessories for a wide variety of applications Pilot freeze dryer systems Ice condenser capacity 6 to 16 kg Air-cooled or water-cooled chilling systems Freezing and drying in the drying chamber on shelves with liquid temperature control Production freeze drying systems Ice condenser capacity 20 to more than 1000 kg Water-cooled chilling systems Freezing and drying in the drying chamber on shelves with liquid temperature control One-chamber and two-chamber systems Special custom systems, SIP / H 2 O 2 disinfection, CIP, IQ/OQ, etc. Process integration (loading systems, auxiliary units)

9 Example Applications Accessories from Christ enable tailored solutions for individual applications. The modular system architecture makes adaptation to altered requirements easy, even a long time after the basic unit was acquired. The units in the Advanced series can be operated as one-chamber or two-chamber systems as desired with the appropriate accessories. Many accessories, such as acrylic chambers, can be used on basic units with capacities from 4 kg to 24 kg (ice capacity). A number of example systems are described below.

10 2 Example Applications

11 10 Example Applications Starter package Accessories for our smallest unit, Alpha 1 2 LDplus, for drying in round-bottom flasks, wide-neck bottles or ampoules or on unheated shelves. Starter product package with Alpha 1 2 LDplus Starter 3 shelves dia. 200 mm = 920 cm², distance between shelves 85 mm, additional ports for 8 flasks, round-bottom flasks and wide-neck bottles or distributor (Figure 3 in the Routine Processes folder) System Alpha 1-2 LDplus (item no ) Description Item number Quantity Page 1 Vacuum sensor Vacuum hose Base plate Three unheated shelves Acrylic drying chamber with 8 ports Rubber valves Vacuum pump RZ-2,5 (2.25 m³/h) Exhaust filter

12 Example Applications 11 Routine package Accessories for the Beta series for drying in round-bottom flasks, wide-neck bottles or vials or on unheated shelves with relatively high specimen volume. Routine product package with Beta 2 8 LDplus Routine Drying chamber with 24 ports for bottles, round-bottom flasks and wide-neck bottles or distributor for ampoules (Figure 12 in the Routine Processes folder) System Beta 2 8 LDplus (item no ) Description Item number Quantity Page 1 Vacuum sensor Vacuum pump RZ Exhaust filter Vacuum hose Base plate shelves with rim Acrylic drying chamber Extra acrylic drying chamber Rubber valve for connecting vessels Drip tray for acrylic drying chamber

13 12 Example Applications Pharmacy product package Accessories for the Alpha LSCplus series for carrying out the complete freeze drying process, including connection of crimp-seal vials under vacuum or inert gas. Pharmacy 1 product package with Alpha 2-4 LSCplus Pharmacy 1 Freezing and drying ice condenser chamber (method A) cooled shelves with sealing device (dia. 200 mm, total area m²) (Figure 2 in Advanced Processes folder) System Alpha 2-4 LSCplus (item no ) Description Item number Quantity Page 1 Extension unit HED-16 LSCplus Vacuum pump RZ-2,5 (2.25 m³/h) Exhaust filter Vacuum hose with standard flange couplings Electromagnetic pressure control and stop valve Sealing device integrated in acrylic lid

14 Example Applications 13 Dish Drying 1 product package Accessories for laboratory systems with LSCplus controller for drying relatively large specimen volumes in dishes or vessels (or in aluminium blocks if necessary). Dish Drying 1 product package with Alpha 1-4 LSCplus Dish Drying 1 10 heated shelves (dia. 200 mm; total area 0.31 m², distance between shelves 25 mm can be adjusted by removing shelves) System Alpha 1-4 LSCplus (item no ) Description Item number Quantity Page 1 Extension unit HED-16 LSCplus Vacuum pump RZ Exhaust filter Vacuum hose with standard flange couplings Electromagnetic pressure control and stop valve Base plate Frame for 10 shelves Shelves with rim, dia. 200 mm, with LyoBus-Modul Acrylic drying chamber

15 14 Example Applications Pharmacy 2 product package Accessories for laboratory systems with LSCplus controller for drying relatively large product volumes in crimp-seal vials, including connection under vacuum or inert gas. Pharmacy 2 product package with Alpha 2-4 LSCplus Pharmacy 2 4 heated shelves with sealing device (dia. 250 mm, total area 0.18 m², distance between shelves 50 mm can be adjusted by removing shelves) System Alpha 2 4 LSCplus (item no ) Description Item number Quantity Page 1 Extension unit HED-16 LSCplus Vacuum pump RZ Exhaust filter Vacuum hose with standard flange couplings Electromagnetic pressure control and stop valve Base plate Sealing device with 1 shelf Shelf with rim Acrylic drying chamber

16 Example Applications 15 Flask Drying / Solvent product package Accessories for the Gamma (and Delta) LSCplus series for drying in round-bottom flasks, wide-neck bottles or ampoules. Optionally also for aggressive solvents. Flask Drying / Solvent product package with Gamma 2 16 LSCplus Flask Drying / Solvent Drying manifold for 24 round-bottom flasks / wide-neck bottles or distributor for ampoules System Gamma 2 16 LSCplus (item no ) Description Item number Quantity Page 1 Vacuum pump RC Vacuum hose with standard flange couplings Electromagnetic pressure control and stop valve Solvent-resistant manifold with 24 rubber valves Drip tray

17 16 Example Applications Dish Drying 2 product package Accessories for the Delta (and Gamma) LSCplus series for drying very large specimen volumes (up to 16 litres) in dishes. Dish Drying 2 product package with Delta 1-24 LSCplus Dish Drying 2 8 heatable shelves (dia. 375 mm, total area 0.88 m², distance between shelves 48 mm) System Delta 1 24 LSCplus (item no ) Description Item number Quantity Page 1 Vacuum pump DUO 20 (20 m³/h) Exhaust filter Electromagnetic pressure control and stop valve Plate frame with 8 electrically heatable shelves Acrylic drying chamber Lifting hoist for acrylic drying chamber, electronic control

18 Example Applications 17

19 18 Freeze drying general Drying Chambers Drying chambers and manifolds are often desirable extensions to the basic unit for high specimen throughput. The chambers are recipients in which both heated and unheated shelves can be placed. Sealing devices can be used when long-term storage of the freeze-dried specimens under vacuum or under an inert gas atmosphere is desired. Stainless steel manifolds are the ideal solution for users who work exclusively with flasks or wide-neck bottles.

20 3 Drying chambers and shelves Alpha to Delta 3.1 Drying chambers Unheated shelves Heated shelves LSC sealing device LSCplus sealing device LSCplus shelves LSC shelves Drying manifolds 46

21 20 Drying chambers and shelves Alpha to Delta 3.1 Drying Chambers Drying chambers Ø 240 mm (for Alpha 1 2 LDplus) The drying chamber can be placed directly on top of any laboratory system. A base plate is additionally necessary when shelves and racks are used. Acrylic drying chamber Order number Clear height Weight approx. 240 mm 285 mm 3.6 kg With NS 45 / 40 ground joint stoppers Alpha 1-2 LDplus Acrylic drying chamber Order number Clear height Weight approx. 240 mm 285 mm 3.6 kg With 6 ports for individually closable rubber valves, including NS 45 / 40 ground joint stoppers Alpha 1-2 LDplus Acrylic drying chamber 240 mm Order number Clear height Weight approx. 285 mm 3.6 kg With 8 ports for individually closable rubber valves, including NS 45 / 40 ground joint stoppers Alpha 1-2 LDplus Overview Ø 240 mm only for Alpha 1 2 LDplus Item number [mm] Connections Weight [kg] Stainless steel drying chamber 240 mm Order number Clear height Weight 295 mm 8 kg With adapter ring, only usable in combination with glass lid Alpha 1-2 LDplus

22 Drying chambers and shelves Alpha to Delta 21 Connection ring, stainless steel 240 mm Order number Clear height Weight Connection 55 mm 2.7 kg With 8 ports for rubber valves including adapter ring; can only be used in combination with glass lid and stainless steel drying chamber For connecting vessels with DIN female ground joint NS29/32: 8x 100 ml, 8x 250 ml, 8x 500 ml, 8x 1000 ml, 8x 2000 ml round-bottom flasks 8x 75 ml, 8x 150 ml, 8x 300 ml, 8x 600 ml, 8x 1200 ml wide-neck filter bottles Alpha 1-2 LDplus Drying chambers Ø 300 mm (not for Alpha 1 2 LDplus) Acrylic drying chamber 300 mm Order number Clear height Weight approx. 295 mm 4.5 kg With stoppers For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber 300 mm Order number Clear height Weight approx. 460 mm 6 kg With stoppers For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber 300 mm Order number Clear height Weight approx. 600 mm 6.8 kg With stoppers For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber 300 mm Order number Clear height Weight approx. 515 mm 6.4 kg Suitable for hoist For all laboratory units except of Alpha 1-2 LDplus

23 22 Drying chambers and shelves Alpha to Delta Acrylic drying chamber 300 mm Order number Clear height Weight approx. Connection 295 mm 5.1 kg With 12 ports for individually closable rubber valves With stoppers For all laboratory units except of Alpha 1-2 LDplus Additional acrylic chamber Order number Clear height Weight approx. Connection 300 mm 295 mm 4.8 kg With 12 ports for individually closable rubber valves For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber 300 mm Order number Clear height Weight approx. Connection 460 mm 6 kg With 12 ports for individually closable rubber valves With stoppers For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber 300 mm Order number Clear height Weight approx. Connection 515 mm 6.6 kg With 12 ports for individually closable rubber valves With NS 45/40 standard ground joint For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber 300 mm Order number Clear height Weight approx. Connection 515 mm 6.6 kg With 12 ports for individually closable rubber valves Suitable for hoist For all laboratory units except of Alpha 1-2 LDplus

24 Drying chambers and shelves Alpha to Delta 23 Overview Ø 300 mm for Alpha to Delta Item number [mm] Connections Weight [kg] Stainless steel drying chamber 300 mm Order number Clear height Weight approx. 295 mm 5.4 kg Related items Only suitable for use with glass lid With adapter ring For all laboratory units except of Alpha 1-2 LDplus Stainless steel drying chamber 300 mm Order number Clear height Weight approx. 460 mm 8.6 kg Related items Only suitable for use with glass lid With adapter ring For all laboratory units except of Alpha 1-2 LDplus Conection ring, stainless steel Order number Weight Connection 300 mm 55 mm 2 kg For connecting vessels with DIN female ground joint NS29/32: 12x 100 ml, 12x 250 ml, 12x 500 ml, 12x 1000 ml, 12x 2000 ml round-bottom flasks 12x 75 ml, 12x 150 ml, 12x 300 ml, 12x 600 ml, 12x 1200 ml wide-neck filter bottles Related items Only usable for use with glass lid and stainless steel drying chamber or With adapter ring For all laboratory units except of Alpha 1-2 LDplus

25 24 Drying chambers and shelves Alpha to Delta Drying chambers Ø 457 mm (not suitable for use with Alpha 1 2 LDplus) Adapter flange item no required for Alpha 1 / 2 4 LDplus and Beta 1/2 8 LDplus Adapter flange item no required for Alpha 1 / 2 4 LSCplus and Beta 1/2 8 LSCplus Acrylic drying chamber 457 mm Order number Clear height Weight approx. 340 mm 12.7 kg With hoisting eye including connection for lifting device For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber 457 mm Order number Clear height Weight approx. 340 mm 12.7 kg With 18 individually closable rubber valves, hoisting eye including connection for lifting device For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber 457 mm Order number Clear height Weight approx. 460 mm 14.3 kg With hoisting eye including connection for lifting device For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber 457 mm Order number Clear height Weight approx. 460 mm 14.3 kg With18 ports for rubber valves, hoisting eye including connection for lifting device For all laboratory units except of Alpha 1-2 LDplus

26 Drying chambers and shelves Alpha to Delta 25 Acrylic drying chamber Order number Clear height Weight approx. 457 mm 565 mm 15.8 kg With hoisting eye including connection for lifting device For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber Order number Clear height Weight approx. 457 mm 565 mm 15.8 kg With 18 ports for rubber valves, with hoisting eye including connection for lifting device For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber Order number Clear height Weight approx. 457 mm 693 mm 17.6 kg With hoisting eye including connection for lifting device For all laboratory units except of Alpha 1-2 LDplus Acrylic drying chamber 457 mm Order number Clear height Weight approx. 693 mm 17.6 kg With 18 ports for rubber valves, hoisting eye including connection for lifting device For all laboratory units except of Alpha 1-2 LDplus

27 26 Drying chambers and shelves Alpha to Delta Overview Ø 457 mm for Alpha to Delta Item number [mm] Connections Weight [kg] Stoppers for acrylic chambers NS 45 / 40 Order number Colour Black Also usable with acrylic lid (121401) and glass lid (121411) Rubber stoppers Colour For closing ports in acrylic chambers Grey Order number Silicone cap For ports of acrylic chambers Order number

28 Drying chambers and shelves Alpha to Delta Unheated shelves Shelves for LDplus controller 3 aluminium shelves with rim 200 mm Order number Heating/cooling Unheated Spacing between shelves 80 mm Only for Alpha 1 2 LDplus 3 aluminium shelves with rim 265 mm Order number approx. Heating/cooling 270 mm Unheated Spacing between shelves 79 mm 5 aluminium shelves with rim 265 mm Order number Heating/cooling Unheated Spacing between shelves 79 mm 5 aluminium shelves Order number Heating/cooling 360 mm Unheated Spacing between shelves 70 mm Not for Alpha 1 2 LDplus 1 aluminium shelf with rim and feet Order number Spacing Heating/cooling 33 mm 265 mm Unheated Stackable up to 10 high Not for Alpha 1 2 LDplus 1 aluminium shelf with rim and feet Order number Heating/cooling 200 mm Unheated For use with Alpha 1 2 LDplus and other laboratory freeze dryers

29 28 Drying chambers and shelves Alpha to Delta Number of drying vessels per shelf, order number and Order number of drying vessels ID code Nominal capacity (ml) Dimensions Ø (mm) Dimensions height (mm) Content with 1 cm layer Number Min. necessary spacing Static (ml) Dynamic (ml) * ml (sh. f.) ml (sh. f.) ml (sh. f.) R R R R H (sp. f.) H (sp. f.) (sp. f.) (sp. f.) * sh.f. = shell freezing; sp.f. = spin freezing (see introduction) Rack Order number Clearance Dimensions To hold 10 (11) microtiter plates (no deep-well plates) 20 mm Anodised aluminium plate holders and stainless steel spacers If the microtiter plates are placed in this rack for freezing (externally), the specially formed anodised aluminium plate holders act as cold buffers, which prevents partial or full thawing of the specimens at the start of the process Use base plate for Alpha to Delta mm, depth 97.5 mm, width mm Rack Clearance To hold 1 deep-well plate or 1 microtiter plate 50 mm Order number Anodised aluminium plate holders and stainless steel spacers If the microtiter plates are placed in this rack for freezing (externally), the specially formed anodised aluminium plate holders act as cold buffers, which prevents partial or full thawing of the specimens at the start of the process. Shelves can be stacked up to 5 high For Alpha to Delta

30 Drying chambers and shelves Alpha to Delta 29 Rack Order number Clearance To hold 6 microtiter plates or 6 deep-well plates 85 mm Anodised aluminium with stainless steel spacers in three levels Not stackable Also for Alpha 1 2 LDplus Rack Clearance Dimensions To hold 5 microtiter plates 25 mm Stainless steel with PDVF feet Racks can be stacked up to 3 high Also for Alpha 1 2 LDplus 137 mm, depth mm, width 89.5 mm Order number Sealing devices for LDplus controller Sealing device with 2 shelf with rim Order number Temperature control system Extension 200 mm None Shelves, separation 70 mm; with just one shelf 152 mm Only in combination with base plate Hood For Alpha 1 2 LDplus or can be used Sealing device with 1 shelf with rim 250 mm Order number Temperature control system None Extension Can be extended to 2 shelves (max.) with shelf Hood For Alpha 1/2 4 LDplus and Beta 1/2-8 LDplus or can be used Sealing device with 1 shelf with rim 250 mm Order number Temperature control system None Extension Can be extended to max. 4 shelves (120959) Hood For Alpha 1/2 4 LD plus and Beta 1/2-8 LD plus or can be used

31 30 Drying chambers and shelves Alpha to Delta 3.3 Heated shelves Sealing devices for LSC system controller (wired) Sealing device integrated into acrylic lid Ø 300 mm Order number Temperature control system Weight approx. For sealing injection vials, sealing distance adjustable, under vacuum or inert gas with 1 shelf with rim Ø 200 mm Heatable with integrated PT 100 sensor 6 kg For Alpha with LSC system controller Number of drying vessels per shelf, order number and Order number of drying vessels ID code Nominal capacity (ml) Dimensions Ø (mm) Dimensions height (mm) Content with 1 cm layer Static (ml) Dynamic (ml) * R R R R H (sp. f.) * sh. f. = shell freezing; sp. f. = spin freezing (see introduction) Number Sealing device with 1 shelf with rim Order number Temperature control system 250 mm For sealing injection vials with serrated rubber stoppers under vacuum or inert gas Electrical heating with built-in sensor PT 100 Extension Can be extended to max. 2 shelves (120960) Weight approx. of pressure plate is adjustable 9 kg For Alpha to Delta with LSC controller Options for order number and Shelf arrangement Clearance between shelves (mm) Usable shelf area (cm 2 ) to x 45 to

32 Drying chambers and shelves Alpha to Delta 31 Sealing device with 1 shelf 250 mm Order number Temperature control system For sealing injection vials with serrated rubber stoppers under vacuum or inert gas Electrical heating with built-in sensor PT 100 Extension Can be extended to max. 4 shelves (120960) Weight approx. of pressure plate is adjustable 10 kg For Alpha to Delta with LSC controller Options for order number and Shelf arrangement Clearance between shelves (mm) Usable shelf area (cm 2 ) to & 3 2x 135 to , 2 & 3 3x 83 to to 4 4x 50 to shelf with rim 250 mm Order number Temperature control system None Use For and shelf with rim Order number Temperature control system 250 mm Electrical heating Use For and shelf with rim Order number Temperature control system 250 mm Electrical heating with built-in sensor PT 100 Use For and

33 32 Drying chambers and shelves Alpha to Delta Sealing devices for LSCplus controller (wireless) Sealing device with 1 shelf 200 mm For sealing injection vials with serrated rubber stoppers under vacuum or inert gas Order number Temperature control system Weight approx. Electrical heating with built-in sensor PT 100 and LyoBus-Modul 6.5 kg Max. vessel height 70 mm; for LSCplus controller Fan Weight approx. 200 mm For circulation of cold air Order number For LSCplus controller; integrated into , and Number of drying vessels per shelf, order number and Order number of drying vessels ID code Nominal capacity (ml) Dimensions Ø (mm) Dimensions height (mm) Content with 1 cm layer Static (ml) Dynamic (ml) * R R R R H (sp. f.) * sh. f. = shell freezing; sp. f. = spin freezing (see introduction) Number Sealing device with max. 2 shelves 250 mm Order number For sealing injection vials with serrated rubber stoppers under vacuum or inert gas Temperature control system Electrical heating with built-in sensor PT 100 and LyoBus-Modul Extension Can be extended to max. 2 shelves (120830) Weight approx. 8 kg For LSCplus controller Options Shelf arrangement Clearance between shelves (mm) Usable shelf area (cm 2 ) to x 45 to

34 Drying chambers and shelves Alpha to Delta 33 Sealing devices for LSCplus controller (wireless) Sealing device with max. 4 shelves 250 mm Order number For sealing injection vials with serrated rubber stoppers under vacuum or inert gas Temperature control system Electrical heating with built-in sensor PT 100 and LyoBus-Modul Extension Can be extended to max. 4 shelves (120830) Weight approx. of pressure plate is adjustable 8.4 kg For LSCplus controller Options Shelf arrangement Clearance between shelves (mm) Usable shelf area (cm 2 ) to x 135 to x 83 to x 50 to Shelf Order number Temperature control system 250 mm Electrical heating with built-in sensor PT 100 and LyoBus-Modul Use For item and Fan Order number Weight approx. 250 mm For circulation of cold air 1.1 kg For LSCplus controller; integrated into and

35 34 Drying chambers and shelves Alpha to Delta Number of drying vessels per shelf order number , and Order number of drying vessels ID code Nominal capacity (ml) Dimensions Ø (mm) Dimensions height (mm) Content with 1 cm layer Number Min. necessary shelf area and Static (ml) Dynamic (ml) * spacing ml (sh. f.) ml (sh. f.) ml (sh. f.) R R R R H (sp. f.) H (sp. f.) (sp. f.) (sp. f.) * sh. f. = shell freezing; sp. f. = spin freezing (see introduction)

36 Drying chambers and shelves Alpha to Delta 35 Shelves for single-chamber method ( inside ) for LSCplus controller Shelves with integrated acrylic lid 200 mm Order number Temperature control system Weight, black anodised Electrical heating with built-in sensor PT 100 and LyoBus-Modul Max. vessel height 70 mm; for LSCplus controller Shelves with integrated acrylic lid 200 mm Order number Temperature control system, black anodised Electrical heating with built-in sensor PT 100 and LyoBus-Modul Weight Max. vessel height 140 mm; only usable with , for LSCplus controller Adapter / distance ring 300 mm Order number PET Fan Weight 200 mm For circulation of cold air Order number For LSCplus controller; integrated into , and Support frame Use approx. Weight To hold max. 5 shelves Ø 200 mm Inside the ice condenser chamber 295 mm 2 kg Order number Suitable for Gamma and Delta with LSCplus controller Variations Shelf arrangement Clearance between shelves (mm) Usable shelf area (cm 2 ) , x to 5 4x

37 36 Drying chambers and shelves Alpha to Delta Shelves for single-chamber method ( inside ) for LSCplus controller Support frame Use approx. Weight To hold max. 10 shelves Ø 200 mm Inside the ice condenser chamber 514 mm 3.3 kg Suitable for Delta with LSCplus controller Order number Variations Shelf arrangement Clearance between shelves (mm) Usable shelf area (cm 2 ) , x x x to 10 9x Shelf Temperature control system Weight approx. Control 200 mm, black anodised Electrical heating with built-in sensor PT 100 and LyoBus-Modul 2.3 kg For LSCplus controller Order number Shelves for double-chamber method ( outside ) for LSCplus controller Base plate Control 300 mm The base plate is necessary when shelves are used For LSCplus controller Order number Adapter flange 457 mm For mounting drying chamber Ø 457 mm Only for Alpha and Beta with LSCplus controller Order number

38 Drying chambers and shelves Alpha to Delta 37 Shelves for double-chamber method ( outside ) for LSCplus controller Support frame Use approx. Weight Control To hold max. 5 shelves Ø 200 mm Outside of ice condenser chamber 295 mm 2 kg For LSCplus controller Order number Variations Shelf arrangement Clearance between shelves (mm) Usable shelf area (cm 2 ) x to 5 4x Support frame Use approx. Weight Control To hold max. 10 shelves Ø 200 mm Outside of ice condenser chamber 514 mm 3.3 kg For LSCplus controller Order number Variations Shelf arrangement Clearance between shelves (mm) Usable shelf area (cm 2 ) x x x to 10 9x Shelf Temperature control system Weight approx. Control 200 mm, black anodised Electrical heating with built-in sensor PT 100 and LyoBus-Modul 2.3 kg For LSCplus controller Order number

39 38 Drying chambers and shelves Alpha to Delta Shelves for double-chamber method ( outside ) for LSCplus controller Intermediate valve Control 300 mm For LSCplus controller Base plate is necessary Order number LyoCube Base frame Dimensions 424 x 334 x 360 mm (H x W x D) Order number Weight Control Stainless steel Approx. 3 kg For LSCplus controller Shelf Dimensions Temperature control system Weight approx. Control 256 x 300 mm, black anodised Electrical heating with built-in sensor PT 100 and LyoBus-Modul Approx. 2.5 kg For LSCplus controller Order number Plate frame with 3 shelves, 86 mm between shelves Plate frame with 5 shelves, 67 mm between shelves Plate frame with 8 shelves, 48 mm between shelves 375 mm Order number Order number Order number Temperature control system Control, black anodised Electrical heating with built-in sensor PT 100 and LyoBus-Modul For LSCplus controller Spacer Spacing Shelf spacing:48 mm Order number Spacer Spacing Shelf spacing:58 mm Order number

40 Drying chambers and shelves Alpha to Delta Heated shelves Heated shelves for LSC controller Plate frame with 5 electrically heatable shelves Order number Spacing Extension Weight 375 mm Shelf spacing 67 mm Each shelf is equipped with a base heater, precision connector, connecting cable and LED display for checking operation Can be extended to max. 8 shelves Suitable for Alpha, Gama and Delta with LSC controller ~ 30 kg Plate frame consisting of 3 electrically heatable shelves Order number Heating/cooling Extension Weight 375 mm, black anodised Each shelf equipped with base heater and PT 100 sensor Precision connector, connecting cable, LED display for checking operation, distance adjustable with spacers (see page 32) Can be extended to max. 8 shelves with LSC controller Suitable for Gamma and Delta ~ 19 kg Shelves Heating/cooling Order number mm, black anodised Equipped with base heater LED display for checking operation Extension For extension of plate frame Weight ~ 5 kg Select a drying chamber order no. to to and select spacers according to number of shelves and shelf spacing Order number Order no / 515 Clear height: 340 Spacing Number of shelves Order number Order no / 521 Clear heigh: 460 Spacing Number of shelves Order number Order no / 527 Clear heigh: 565 Spacing Number of shelves Order number Order no / 531 Clear heigh: 693 Spacing Number of shelves Usable shelf area Ø 375 (cm²) * * * Standard * *

41 40 Drying chambers and shelves Alpha to Delta Heated shelves for LSC controller Stainless steel spacers (1 set) Order number Spacing Weight approx. Shelf spacing: 48 mm 0.3 kg Stainless steel spacers (1 set) Order number Spacing Weight approx. Shelf spacing: 53 mm 0.3 kg Stainless steel spacers (1 set) Order number Spacing Weight approx. Shelf spacing: 60 mm 0.4 kg Stainless steel spacers (1 set) Order number Spacing Weight approx. Shelf spacing: 86 mm 0.5 kg Stainless steel spacers (1 set) Order number Spacing Shelf spacing: 92 mm Stainless steel spacers (1 set) Order number Spacing Shelf spacing: 114 mm Stainless steel spacers (1 set) Order number Spacing Shelf spacing: 124 mm

42 Drying chambers and shelves Alpha to Delta 41 Heated shelves for LSC controller Number of drying vessels per shelf Ø 375 mm in combination with drying chamber order numbers to Order number of drying vessels ID code / nominal capacity (mm) Dimensions (mm) Content with 1 cm layer Freezing Static (ml) Dynamic* (ml) a Number b Minimum necessary shelf spacing (mm) ml (sh. f.) ml (sh. f.) ml (sh. f.) R R R R H (sp. f.) H (sp. f.) * sh. f. = shell freezing; sp. f. = spin freezing (see introduction) a = without thermoblock; b = with thermoblock Shelf rack Order number Shelf holder To hold max. 5 shelves Ø 200 mm Temperature control system approx. Control Heated (including two connecting cables) 295 mm For LSC controller : Variations Shelf arrangement Clearance between shelves (mm) Usable shelf area (cm 2 ) to 5 4x

43 42 Drying chambers and shelves Alpha to Delta Heated shelves for LSC controller Shelf rack Order number Shelf holder To hold max. 10 shelves Ø 200 mm Temperature control system approx. Control Heated (including two connecting cables) 435 mm For LSC controller : Variations Shelf arrangement Clearance between shelves (mm) Usable shelf area (cm 2 ) x x x to 10 9x Connecting cable for rack Order number Length 700 mm Connecting cable for rack Order number Length 500 mm Connecting cable for rack Order number Length 700 mm Teflon encapsulated Extension cable with precision connector Order number Length 500 mm For feeding the plug-and-socked connection through the base plate of the intermediate valve For connection of an electrically heated shelf Extension cable with precision connector Order number Length 500 mm For feeding the connector through the base plate of the intermediate valve for connection of a process sensor (124802)

44 Drying chambers and shelves Alpha to Delta 43 Extension cable with precision connector Order number Length 500 mm For power supply to shelves with electric heaters Connection For connection of rack no or of sealing device or and plate frame Extension cable with precision connector Order number Length Connection 500 mm Teflon encapsulated For feeding the plug-and-socked connection through the base plate of the intermediate valve For connection of an electrically heated shelf shelf with rim Order number Temperature control system Connection Control 200 mm Electrical heating with built-in sensor PT 100 and connecting cable In the absence of a rack, the shelf can be placed directly on the floor of the ice condenser chamber For LSC controller shelf with rim Order number Temperature control system 200 mm Electrical heating with base heater Usable with rack and

45 44 Drying chambers and shelves Alpha to Delta Number of drying vessels per shelf order number and Order number of drying vessels ID code / nominal capacity (mm) Dimensions (mm) Content with 1 cm layer Freezing Static (ml) Dynamic* (ml) Number Minimum necessary shelf spacing (mm) ml (sh. f.) ml (sh. f.) ml (sh. f.) R R R R H (sp. f.) H (sp. f.) * sh. f. = shell freezing; sp.f. = spin freezing (see introduction) a = without thermoblock; b = with thermoblock a b Base plate Order number mm The accessory base plate is necessary when shelves are used Only for Alpha 1 2 LDplus Base plate Order number mm The accessory base plate is necessary when shelves are used Alpha to Delta Base plate for 10 microtiter plate rack Order number mm To hold 6 racks no in combination with transition flange no Only for Alpha and Beta Base plate 423 mm With large hood; Gamma and Delta Order number Adapter flange Order number For mounting drying chamber Ø 457 For Alpha 1/2 4 LDplus and Beta 1 8/2 8 LDplus

46 Drying chambers and shelves Alpha to Delta 45 Drip tray for manifold Order number mm For protection of the freeze dryer; collects the condensation water dripping from the drying vessels Alpha to Gamma, for manifolds , and Drip tray for drying chamber Order number Inside diameter 575 mm 260 mm For protection of the freeze dryer; collects the condensation water dripping from the drying vessels For Alpha 1 2 LDplus Drip tray Weight approx. Order number mm For protection of the freeze dryer; collects the condensation water dripping from the drying vessels 2 kg Suitable for drying chamber Ø 300 mm Drip tray Order number For protection of the freeze dryer; collects the condensation water dripping from the drying vessels Suitable for drying chamber Ø 457 mm, outside 800 mm Glass lid 240 mm Order number With central DIN female ground joint NS 45 / 40 and stopper NS 45 / 40 Only for Alpha 1 2 LDplus Acrylic lid Weight approx. 300 mm 3.1 kg Order number With central DIN female ground joint NS 45 / 40 and stopper NS 45 / 40 Thickness 40 mm Safety glass lid 300 mm Order number Solvent resistant, with central stainless steel DIN female ground joint NS 45 / 40 and stopper Thickness 19 mm

47 46 Drying chambers and shelves Alpha to Delta 3.4 Drying manifolds Drying manifolds Vertical manifold Order number Stainless steel with DIN male ground joint NS 45 / 40 Width 372 mm 1030 mm For connection to acrylic or glass lid with female ground joint and 12 rubber valves, for substances containing solvents Connections For connecting vessels with DIN female ground joint NS 29 / 32: 12x 100 ml, 12x 250 ml, 12x 1000 ml, 12x 2000 ml round-bottom flasks, 12x 75 ml, 12x 150 ml, 12x 300 ml, 12x 600 ml, 12x 1200 ml, 8x 2000 ml wide-neck filter bottles The connections can be shut off individually and the drying vessels can be vented individually Three levels with four connections each; Alpha 1-2 LDplus, Alpha 1 / 2 4, Beta 1 / 2 8, Gamma 1 / 2 16 and Delta 1 / 2 24 Vertical manifold Order number Stainless steel with DIN male ground joint NS 45 / 40 Width Weight approx. Connections 650 mm 1170 mm 18 kg With flange-mounted glass lid Ø 300 mm and 24 rubber valves, for aqueous solutions For connecting vessels with DIN female ground joint NS29/32: 24x 100 ml, 24x 250 ml, 24x 500 ml, 24x 1000 ml, 16x 2000 ml round-bottom flasks, 24x 75 ml, 24x 150 ml, 24x 300 ml, 24x 600 ml, 24x 1200 ml, 8x 2000 ml wide-neck filter bottles The connections can be shut off individually and the drying vessels can be vented individually Three levels with eight connections each; Alpha 1 / 2 4, Beta 1 / 2 8, Gamma 1 / 2 16 and Delta 1 / 2 24 Vertical manifold Order number Stainless steel with DIN male ground joint NS 45 / 40 Width Connections 380 mm 755 mm For connection to acrylic or glass lid with female ground joint and 8 rubber valves, for substances containing solvents For connecting vessels with DIN female ground joint NS29/32: 8x 100 ml, 8x 250 ml, 8x 500 ml, 8x 1000 ml, 4x 2000 ml round-bottom flasks, 8x 75 ml, 8x 150 ml, 8x 300 ml, 8x 600 ml, 8x 1200 ml, 4x 2000 ml wide-neck filter bottles The connections can be shut off individually and the drying vessels can be vented individually Two levels with four connections each; Alpha 1 2 LDplus, Alpha 1/2-4, Beta 1 / 2 8, Gamma 1 / 2 16, Delta 1 / 2 24 and Epsilon 2 6 D LSC/ LSCplus

48 Drying chambers and shelves Alpha to Delta 47 Vertical manifold Order number Stainless steel with DIN male ground joint NS 45 / 40 Width 650 mm 946 mm With flange-mounted glass lid Ø 300 mm and 24 rubber valves, for substances containing solvents With DIN10KF connector for hot water defrosting Connections For connecting vessels with DIN female ground joint NS 29 / 32: 24x 100 ml, 24x 250 ml, 24x 500 ml, 24x 1000 ml, 8x 2000 ml round-bottom flasks, 24x 75 ml, 24x 150 ml, 24x 300 ml, 24x 600 ml, 16x 1200 ml, 8x 2000 ml wide-neck filter bottles The connections can be shut off individually and the drying vessels can be vented individually Three levels with eight connections each; Alpha 1 / 2 4, Beta 1 / 2 8, Gamma 1 / 2 16 and Delta 1 / 2 24 Vertical manifold Order number Width Stainless steel 650 mm 903 mm With flange-mounted glass lid Ø 300 mm and 16 rubber valves, for substances containing solvents With DN 10 KF connector for hot water defrosting Connections For connecting vessels with DIN female ground joint NS 29 / 32: 16x 100 ml, 16x 250 ml, 16x 500 ml, 16x 1000 ml, 16x 2000 ml round-bottom flasks, 16x 75 ml, 16x 150 ml, 16x 300 ml, 16x 600 ml, 16x 1200 ml, 8x 2000 ml wide-neck filter bottles The connections can be shut off individually and the drying vessels can be vented individually Three levels with eight connections each; Alpha 1 / 2 4, Beta 1 / 2 8, Gamma 1 / 2 16 and Delta 1 / 2 24 Vertical manifold Width Stainless steel 650 mm 1129 mm Order number With flange-mounted glass lid Ø 300 mm and 16 rubber valves, for substances containing solvents With DN 10 KF connector for hot water defrosting Connections For connecting vessels with DIN female ground joint NS 29 / 32: 16x 100 ml, 16x 250 ml, 16x 500 ml, 16x 1000 ml, 16x 2000 ml round-bottom flasks, 16x 75 ml, 16x 150 ml, 16x 300 ml, 16x 600 ml, 16x 1200 ml, 16x 2000 ml wide-neck filter bottles The connections can be shut off individually and the drying vessels can be vented individually Three levels with eight connections each; Alpha 1 / 2 4, Beta 1 / 2 8, Gamma 1 / 2 16 and Delta 1 / 2 24

49 48 Drying chambers and shelves Alpha to Delta Vertical manifold Order number Stainless steel with DIN male ground joint NS 45 / 40 Width Weight 108 mm 450 mm 3 kg For connection to acrylic or glass lid with female ground joint and 48 rubber valves, for aqueous solutions, for connecting vials The connections can be shut off individually and the drying vessels can be vented individually Alpha 1 2 and 1 / 2 4, Beta 1 / 2 8, Gamma 1 / 2 16 and Delta 1 / 2 24 Vertical manifold Stainless steel with DIN male ground joint NS 45 / 40 Order number Width 108 mm 440 mm For connection to acrylic or glass lid with female ground joint and 60 rubber valves, for substances containing solvents, for connection of ampoules The connections can be shut off individually and the drying vessels can be vented individually Alpha 1/2 4, Beta 1 / 2 8, Gamma 1 / 2 16 and Delta 1 / 2 24 Vertical manifold Width Weight Stainless steel with DIN KF 40 connection 520 mm 770 mm Approx. 10 kg Order number For connection to acrylic or glass lid and 96 rubber hoses, for aqueous solutions, for connection of ampoules The connections can be shut off individually and the drying vessels can be vented individually Alpha 1/2 4, Beta 1 / 2 8, Gamma 1 / 2 16 and Delta 1 / 2 24

50 Drying chambers and shelves Alpha to Delta 49 Overview Vertical manifolds Item number Connections Solvent Water Mounting Width (mm) (mm) Weight (kg) Connections 1 Systems Yes Yes Ground joint stubs x 2000 ml round-bottom flasks and wide-neck bottles Alpha Epsilon Yes Yes Ground joint stubs Yes Yes Glass lid Ø 300 mm x 2000 ml wide-neck bottles Beta Delta x 2000 ml wide-neck bottles Alpha Delta Yes Acrylic lid Ø 300 mm Yes Yes Glass lid Ø 300 mm Yes Yes Glass lid Ø 300 mm x 2000 ml round-bottom flasks and 8x wide-neck bottles x 2000 ml round-bottom flasks and wide-neck bottles x 2000 ml round-bottom flasks and wide-neck bottles Alpha Delta Alpha Delta Alpha Delta Yes Ground joint stubs Yes Yes Ground joint stubs Yes Connection over KF Ampoules Alpha Delta Ampoules Alpha Delta Ampoules Alpha Delta with individually closable rubber valves for connection of round-bottom flasks and wide-neck bottles with DIN female ground joint NS 29 / 32 1 The maximum number of large-volume vessels Horizontal manifold (T shape) Order number Width Weight approx. Connections Stainless steel 1070 mm 550 mm 6 kg With flange-mounted glass lid Ø 300 mm and 16 rubber valves, for aqueous solutions For connecting vessels with DIN female ground joint NS29/32: 16x 100 ml, 16x 250 ml, 16x 500 ml, 8x 1000 ml, 8x 2000 ml round-bottom flasks 16x 75 ml, 16x 150 ml, 16x 300 ml, 16x 600 ml, 16x 1200 ml, 16x 2000 ml wide-neck filter bottles The connections can be shut off individually and the drying vessels can be vented individually Alpha 1/2 4, Beta 1 / 2 8, Gamma 1 / 2 16 and Delta 1 / 2 24 Horizontal manifold (T shape) Order number Stainless steel with DIN male ground joint NS 45 / 40 Width Weight approx. Connections 687 mm 320 mm 5.7 kg For connection to acrylic or glass lid with female ground joint and 20 rubber valves, for aqueous solutions Injection vials The connections can be shut off individually and the drying vessels can be vented individually Alpha 1 2 LDplus, Alpha 1 / 2 4, Beta 1 / 2 8, Gamma 1 / 2 16 and Delta 1 / 2 24

51 50 Drying chambers and shelves Alpha to Delta Horizontal manifold (T shape) Order number Stainless steel with DIN male ground joint NS 45 / 40 Width 301 mm 611 mm For connection to acrylic or glass lid with female ground joint and 40 rubber valves, for substances containing solvents, for connection of ampoules The connections can be shut off individually and the drying vessels can be vented individually Alpha 1 2 LD plus, Alpha 1 / 2 4, Beta 1 / 2 8, Gamma 1 / 2 16 and Delta 1 / 2 24 Horizontal manifold (T shape), multi-row Note Wall fastening necessary Order number Stainless steel with DIN male ground joint NS 45 / 40 Width Connections 1076 mm 1327 mm Connection over clamp joint stubs DN65 ISO, S and 20 rubber valves, for substances containing solvents For connecting vessels with DIN female ground joint NS29/32: 20x 100 ml, 20x 250 ml, 20x 500 ml, 20x 1000 ml, 11x 2000 ml round-bottom flasks 20x 75 ml, 20x 150 ml, 20x 300 ml, 20x 600 ml, 20x 1200 ml, 14x 2000 ml wide-neck filter bottles The connections can be shut off individually and the drying vessels can be vented individually Delta 2 24 LSC Horizontal manifold (T shape) Stainless steel with DIN male ground joint NS 45 / 40 Order number Width Connections 860 mm 1054 mm For connection to glass lid and 21 rubber valves, for aqueous solutions For connecting vessels with DIN female ground joint NS29/32: 21x 100 ml, 21x 250 ml, 21x 500 ml, 21x 1000 ml, 21x 2000 ml round-bottom flasks 21x 75 ml, 21x 150 ml, 21x 300 ml, 21x 600 ml, 21x 1200 ml wide-neck filter bottles The connections can be shut off individually and the drying vessels can be vented individually Gamma 1 / 2 16 LSC and Delta 1 / 2 24 LSC Horizontal manifold (T shape), multi-row Stainless steel Order number Width Connections 865 mm 918 mm Connection over clamp joint stubs DN 50 ISO, S and 24 rubber valves, for substances containing solvents For connecting vessels with DIN female ground joint NS29/32: 24x 100 ml, 24x 250 ml, 24x 500 ml, 24x 1000 ml round-bottom flasks 24x 75 ml, 24x 150 ml, 24x 300 ml, 24x 600 ml, 24x 1200, 12 x 2000 ml wide-neck filter bottles The connections can be shut off individually and the drying vessels can be vented individually Gamma 1 / 2 16 LSC and Delta 1 / 2 24 LSC; requires connection kit

52 Drying chambers and shelves Alpha to Delta 51 Overview Horizontal manifolds Item number Connections Solvent Water Mounting Width (mm) Yes Acrylic lid Ø 300 mm Yes Ground joint stubs (mm) Weight (kg) Connections x 1000 ml round-bottom flasks, 8x 2000 ml round-bottom flasks Systems Alpha Delta Injection vials Alpha Delta Yes Yes Ground joint stubs Yes Yes Wall attachment, clamp joint stubs Yes Ground joint stubs Ampoules Alpha Delta Multi-row Delta Multi-row Gamma Delta Yes Yes Clamp nipples Multi-row 12x 2000 ml wide-neck bottles Gamma Delta With individually closable rubber valves for connection of round-bottom flasks and wide-neck bottles with DIN female ground joint NS 29 / 32 1 The maximum number of large-volume vessels Distributor for ampoules Order number Connections 15 Ball tap with small flange DN 10KF and accessories Order number For hot water defrosting

53 52 Freeze drying general Drying Accessories Here you can find the commonly used small items that can be essential for good results in your daily work with freeze dryers. For example, product sieves can prevent the loss of very light or fine-grain material. Wide-neck filter bottles allow the equipment to be used almost continuously by connection to rubber valves, which act as three-way taps. Ampoules and injection vials are containers for long-term storage without contact with oxygen.

54 4 Drying Accessories 4.1 Product dishes Product sieves s, split s, not split Rubber valves Round-bottom flasks Filter inserts Wide-neck filter bottles Protective nets Ampoules Individual sealing device Injection vials 73

55 54 Drying Accessories 4.1 Product dishes Product dishes Product dish Order number Rim height Stainless steel 65 mm 20 mm Product dish Order number Rim height Stainless steel 75 mm 20 mm Product dish Order number Rim height Stainless steel 200 mm 18 mm Product dish Order number Rim height Stainless steel 360 mm 32 mm Product dish Order number Rim height Stainless steel, acrylic rim 340 mm 35 mm With removable bottom Product dish, Teflon coated Order number Rim height Teflon-coated stainless steel 65 mm 20 mm Product dish, Teflon coated Order number Rim height Teflon-coated stainless steel 75 mm 20 mm

56 Drying Accessories 55 Product dish, Teflon coated Order number Rim height Teflon-coated stainless steel 200 mm 18 mm Product dish, Teflon coated Order number Rim height Teflon-coated stainless steel 360 mm 32 mm 4.2 Product sieves Product sieves Product sieve Order number Mesh size 200 mm 0.2 mm Product sieve Mesh size 200 mm 0.25 mm Order number Product sieve Mesh size 360 mm 0.2 mm Order number Product sieve Mesh size 360 mm 0.25 mm Order number product dishes Product dish Rim height 63 mm 20 mm Order number Product dish Rim height 140 mm 18 mm Order number

57 56 Drying Accessories Product dish Order number Rim height 200 mm 18 mm Product dish Order number Rim height 360 mm 32 mm 4.3 s, split thermoblocks for sealing device, Ø 195 mm Form 195 mm 37 mm Two-piece Order number For holding a total of 100 vessels Ø x mm with round bottom Form 195 mm 33 mm Two-piece For holding a total of 72 vessels Ø x mm with flat bottom Order number Form 195 mm 30 mm Two-piece Order number For holding a total of 92 vessels Ø x mm with flat bottom

58 Drying Accessories 57 thermoblocks for sealing device, Ø 195 mm Form 195 mm 30 mm Two-piece Order number For holding a total of 70 vessels Ø 16 x 35 mm (2R vials) Form 195 mm 41 mm Two-piece Order number For holding a total of 34 vessels Ø x mm (6R/8R vials) Form 195 mm 45 mm Two-piece Order number For holding a total of 14 vessels Ø 27.5 x 57 mm with flat bottom Form 192 mm 30 mm Two-piece Order number For holding a total of 64 vessels Ø 16 x 35 mm (2R vials) For sealing device (units with LSC controller) Form 192 mm 41 mm Two-piece Order number For holding a total of 32 vessels Ø 22.5 x 45 mm (6R/8R vials) For sealing device (units with LSC controller) Form 192 mm 33 mm Two-piece For holding a total of 72 vessels Ø 14.8 x 35.5 mm For sealing device (units with LSC controller) Order number

59 58 Drying Accessories for shelves inside ice condenser chamber (120761) Form 195 mm 70 mm Two-piece Order number For a total of 24 vessels Ø x mm (50 ml flask) Only in combination with distance ring for sealing device Ø 240 mm Form 240 mm 20 mm Two-piece For holding a total of 136 vessels Ø 12 x 30 mm Order number Form 240 mm 30 mm Two-piece Order number For holding a total of 94 vessels Ø x mm (2R vials) Form Order number mm 30 mm Two-piece For holding a total of 48 vessels Ø x mm with flat bottom Form 240 mm 36 mm Two-piece Order number For holding a total of 48 vessels Ø x mm (10R vials)

60 Drying Accessories 59 for sealing device Ø 240 mm Order number Form 240 mm 36 mm Two-piece For holding a total of 198 vessels Ø x mm with flat bottom Form Order number mm 41 mm Two-piece For holding a total of 112 vessels Ø x mm (6R/8R vials) Form 240 mm 43 mm Two-piece Order number For holding a total of 32 vessels Ø x mm (20R vials) Overview thermoblocks Item number Block diameter (mm) Number of vials Vial diameter (mm) Comments x with round bottom x with flat bottom x with flat bottom x 35 2R vials x R/8R vials x 57 with flat bottom x ml flask x x R vials x with flat bottom x R vials x with flat bottom x R/8R vials x R vials

61 60 Freeze Drying drying Accessories general 4.4 s, not split thermoblocks Ø 195 mm 195 mm 30 mm Order number For holding a total of 70 vessels Ø x mm or 27 vessels Ø x mm 30 mm Order number For holding a total of 79 vessels Ø x mm with flat bottom 195 mm 30 mm Order number For holding a total of 118 vessels Ø x mm with round bottom 195 mm 33 mm Order number For holding a total of 50 vessels Ø x mm with round or flat bottom or 50 vessels Ø x mm with flat or round bottom 195 mm 30 mm Order number For holding a total of 104 vessels Ø x mm with flat or round bottom

62 Freeze Drying drying Accessories general 61 thermoblocks Ø 195 mm Order number mm 30 mm For holding a total of 86 vessels Ø x mm 195 mm 30 mm For holding a total of 44 vessels Ø x mm with flat bottom Order number Order number mm 70 mm For holding a total of 22 vessels Ø x mm (designed for flasks or Eppendorf) or 21 vessels Ø x mm or 22 vessels Ø x mm Order number mm 31 mm For holding a total of 69 vessels Ø x mm Order number mm 32 mm For holding a total of 50 vessels Ø x mm with flat bottom Order number mm 40 mm For holding a total of 16 strips with 8 tubes per strip

63 62 Drying Accessories thermoblocks Ø 195 mm Order number mm 35 mm For holding a total of 85 vessels Ø x mm with flat bottom Order number mm 50 mm For holding a total of 43 vessels Ø x mm 195 mm 50 mm For holding a total of 44 vessels Ø x mm (injection vials with crimp seal Ø 23 mm) Order number Order number mm 38 mm For holding a total of 140 vessels Ø x mm 195 mm 40 mm For holding a total of 93 vessels Ø x mm with flat bottom Order number mm 45 mm Order number For holding a total of 37 vessels Ø x mm with flat bottom

64 Drying Accessories 63 thermoblocks Ø 195 mm 195 mm 41.5 mm Order number For holding a total of 36 vessels Ø x mm (10H vials) 195 mm 45 mm Order number For holding a total of 58 vessels Ø x mm (Eppendorf caps) two pieces not for sealing device 195 mm 44 mm Order number For holding a total of 36 vessels Ø x mm (10R / 15R vials) Order number mm 46 mm For holding a total of 23 vessels Ø x mm (20H vials) Order number mm 55 mm For holding a total of 36 vessels Ø x mm (30R vials) 195 mm 58 mm For holding a total of 86 vessels Ø x mm with round bottom (ampoules) Order number

65 64 Drying Accessories thermoblocks Ø 195 mm 195 mm 60 mm Order number For holding a total of 79 vessels Ø x mm with round bottom 195 mm 70 mm Order number For holding a total of 20 vessels Ø x mm with round bottom 195 mm 60 mm Order number For holding a total of 100 vessels Ø x mm with round bottom 195 mm 60 mm Order number For holding a total of 91 vessels Ø x mm with flat bottom 195 mm 70 mm Order number For holding a total of 22 vessels Ø x mm or 22 vessels Ø x mm 195 mm 61 mm Order number For holding a total of 13 vessels Ø x mm (50H vials)

66 Drying Accessories 65 thermoblocks Ø 195 mm Order number mm 43 mm For holding a total of 7 vessels Ø x mm (100H vials) 195 mm 85 mm Order number For holding a total of 124 vessels Ø x mm or 124 vessels Ø x mm Order number mm 85 mm For holding a total of 37 vessels Ø x mm with round bottom 195 mm 80 mm Order number For holding a total of 190 vessels Ø x mm with round bottom 195 mm 85 mm Order number For holding a total of 37 vessels Ø x mm with flat bottom 195 mm 100 mm Order number For holding a total of 37 vessels Ø x mm with flat bottom

67 66 Freeze Drying drying Accessories general. not split Ø 195 mm, stackable 195 mm 30 mm Order number For holding a total of 354 vessels Ø x mm (Eppendorf caps) Total height of three stacked blocks = 200 mm Space between thermoblocks 55 mm Order number mm 45 mm For holding a total of 58 vessels Ø x mm (Eppendorf caps) Max. stacking height 4 blocks; spacers required (item no ) Space between thermoblocks 30 mm 195 mm 70 mm Order number For holding a total of 72 vessels Ø x mm (15 ml flask); spacers required (item no ) 195 mm 70 mm Order number For holding a total of 27 vessels Ø x mm (50 ml flask); spacers required (item no ). not split Ø 360 mm Order number mm 150 mm For holding a total of 12 vessels Ø x mm

68 Drying Accessories 67 Order number mm 220 mm For holding a total of 6 vessels Ø x mm Overview thermoblocks Item number Block Number of Vial diameter (mm) Comments diameter (mm) vials / x x x with flat bottom x with round bottom x x Eppendorf caps x Round or flat bottom x with flat bottom x with flat bottom / x x x x with flat bottom Tube strips x with flat bottom x x Injection vials x with flat bottom x with flat bottom x with flat bottom x H vials x Eppendorf caps/two pieces x R/15R vials x H vials x R vials x Ampoules x with round bottom x with round bottom x with round bottom x with flat bottom x x H vials x H vials x x with round bottom x with round bottom x with flat bottom x with flat bottom

69 68 Drying Accessories 4.5 Rubber valves Rubber valves Rubber valve Order number For connection to drying chamber or as spare rubber valve for drying manifold The rubber valve is equipped with a DIN male ground joint NS29/32 for connection of round-bottom flasks, etc.; ml injection vials or wide-neck filter bottles can be connected after removing the rubber ground joint from the valve Sterilisation Fully sterilisable at +121 C Rubber valve Order number Rubber valve with stainless steel shut-off knob, solvent resistant version For connecting vessels with DIN female ground joint 29 / 32 Replacement rubber and piece For rubber valve, NS 29 / 32 Order number Sterilisation Sterilisable at +121 C Screw stopper Connection Sterilisation Plastic For rubber valve Sterilisable at +121 C Order number Shut-off knob Connection Sterilisation Stainless steel For rubber valve Sterilisable at +121 C Order number Adapter Connection For rubber valve, NS 14.5 Order number Adapter and filter Connection For rubber valve NS Order number

70 Drying Accessories Round-bottom flasks Round-bottom flasks Round-bottom flask Order number Size 100 ml Round-bottom flask Order number Size 250 ml Round-bottom flask Order number Size 500 ml Round-bottom flask Size 500 ml Order number With glass shard protection Round-bottom flask Size 1000 ml Order number Round-bottom flask Size 2000 ml Order number Filter inserts Filter inserts and spare parts for filter inserts Filter insert With fine filter for rubber valves Order number Filter insert Stainless steel With fine filter for rubber valves (solvent resistant) Order number Filter paper 18 mm Order number Quantity 100 For retention filter

71 70 Drying Accessories 4.8 Wide-neck filter bottles Wide-neck filter bottles Wide-neck filter bottle Order number Size 75 ml Wide-neck filter bottle Order number Size 150 ml Wide-neck filter bottle Order number Size 300 ml Wide-neck filter bottle Order number Size 600 ml Wide-neck filter bottle Order number Size 1200 ml Wide-neck filter bottle Order number Size 2000 ml Order number of drying vessels Nominal capacity (ml) Dimensions Ø outside (mm) Dimensions height (mm) Bottle opening Ø Content with 1 cm layer Static (ml) Dynamic (ml) * Spare rubber cap Order number Size For Ø 75 ml to Ø 300 ml Spare rubber cap Size For Ø 600 ml to Ø 2000 ml Order number

72 Drying Accessories 71 Filter paper Order number Size Ø 30 mm Quantity 100 Pore size 70 µm Use For wide-neck filter bottles 75 ml to 300 ml Filter paper Order number Size Ø 47 mm Quantity 100 Pore size 70 µm Use For wide-neck filter bottles 600 ml to 2000 ml 4.9 Protective nets Protective nets Protective net Vessel Ø Length mm For round-bottom flasks and wide-neck filter bottles 250 mm Order number Protective net Vessel Ø Length mm For round-bottom flasks and wide-neck filter bottles 250 mm Order number Protective net Vessel Ø Length mm For round-bottom flasks and wide-neck filter bottles 250 mm Order number

73 72 Drying Accessories 4.10 Ampoules Ampoules Long-neck ampoules Order number Capacity Overall length Neck diameter Neck length 2 ml 12 mm 121 mm 8 mm 90 mm Quantity 100 Long-neck ampoules Capacity 5 ml Order number Overall length Neck diameter 12 mm 156 mm 8 mm Quantity 100 Long-neck ampoules Capacity 10 ml Order number Overall length Neck diameter 16 mm 156 mm 8 mm Quantity 100 Ampoule sealing torch Order number For connection to gas and oxygen or to gas, air and oxygen The torch has a special flame stabilisation system, which allows it to be operated with a high air ratio to cool the flame Single vial sealing device Screw bottles Screw bottles Order number For screw bottles compliant with ISO 11418, with round fitting 18 x 3.0 For connection to rubber valve

74 Drying Accessories Injection vials Injection vials (crimp seal vials), DIN/ISO compliant Injection vials Order number Type 2 R Quantity 352 Injection vials Type 6 R Order number Quantity 192 Injection vials Type 10 R Order number Quantity 160 Injection vials Type 20 R Order number Quantity 99 Injection vials Type 50 H Order number Quantity 130 Injection vials Type 100 H Order number Quantity 88 Vial type Maximum capacity (ml) (mm) (mm) Capacity with 1 cm fill level (ml) 2 R R R R R R R R R H H H H H H H H H H

75 74 Drying Accessories Serrated rubber stopper Order number mm For injection vials 2 R Quantity 100 Serrated rubber stopper Order number mm For injection vials 6 R 100 H Quantity 100 Crimp caps Order number Dimensions Ø 13 x 6.8 mm For injection vials 2 R Quantity 100 Crimp caps Order number Dimensions Ø 20 x 7.5 mm For injection vials 6 R 100 H Quantity 100 Hand crimper Order number For 2 R Hand crimper Order number For 6 R 100 H Decrimper Order number For 2 R Decrimper Order number For 6 R 100 H

76 Drying Accessories 75

77 Epsilon Accessories Systems with rectangular drying chambers are traditionally designated Epsilon at Christ. The shelves are usually heated or cooled, depending on the process step. Here as well it is important to choose the right accessories. The available options include product dishes for bulk goods, frames for direct contact between shelf surfaces and crimp vials, and drying manifolds for drying in flasks or wide-neck bottles on Epsilon systems.

78 5 Epsilon Accessories

79 78 Epsilon Accessories 5 Epsilon Accessories Product dishes Product dish Order number Size (mm) Stainless steel 225 x 300 x 30 (W x D x HD) For Epsilon 2-6 D Product frame Size (mm) Stainless steel 225 x 300 x 30 (W x D x HD) For Epsilon 2-6 D Order number Product base sheet Stainless steel Order number Size (mm) 225 x 300 For product frame For Epsilon 2-6 D Product sieve Size (mm) 225 x 300 Order number Mesh size 0.2 mm Product dish Size (mm) Rim height Stainless steel 227 x 400 x 20 (W x D x HD) 20 mm For Epsilon 1 4 / 2 4 D Order number Product frame Size (mm) Stainless steel 227 x 400 x 20 (W x D x HD) For Epsilon 1 4 / 2 4 D Order number Product base sheet Stainless steel Order number Size (mm) 227 x 400 For product frame For Epsilon 1 4 / 2 4 D

80 Epsilon Accessories 79 Product dish Size (mm) Stainless steel 227 x 400 x 20 (W x D x HD) For Epsilon 1 4 / 2 4 D Order number Product dish Size (mm) Weight approx. Stainless steel 350 x 450 x 30 (W x D x HD) 2.3 kg For Epsilon 2-12 D Order number Product dish Size (mm) Weight approx. Stainless steel 350 x 400 x 30 (W x D x HD) 2.3 kg For Epsilon 2-12 D Order number Product frame Size (mm) Weight approx. Stainless steel 350 x 450 x 30 (W x D x HD) 1.5 kg For Epsilon 2-12 D Order number Product base sheet Stainless steel Order number For product frame Weight approx. 1.8 kg For Epsilon 2-12 D Overview Product dishes Item number Size in mm Nominal volume Layer thickness 1 cm Device x ml Epsilon 1-4/2-4 and Epsilon x ml Epsilon x ml Epsilon x ml Epsilon 2-10 D x ml Epsilon 2-12 D x ml Production systems x ml Production systems x ml Production systems

81 80 Epsilon Accessories Product sensor Order number Model PT 100 Cable length approx. 0.8 m Product sensor Model PT 100 Order number Cable length approx. 2 m Product sensor Model 2x PT 100 Order number Product sensor Model PT 100 Mini-Epsilon Order number Horizontal drying manifold Width 575 mm Order number Connection 753 mm Stainless steel With connection to rear wall of system via 2x DN 40 KF-37 and 12 rubber valves, for substances containing solvents For connecting vessels with DIN female ground joint NS29/32: 12x 100 ml, 12x 250 ml, 12x 500 ml, 12x 1000 ml, 8x 2000 ml round-bottom flasks 12x 75 ml, 12x 150 ml, 12x 300 ml, 12x 600 ml, 12x 1200 ml, 6x 2000 ml wide-mouth filter bottles The connections can be shut off individually and the drying vessels can be vented individually Epsilon 1 / 2 6 D Vertical manifold Width Connection 400 mm 524 mm Stainless steel Flange mounted directly on drying chamber, with 4 rubber valves, for substances containing solvents For connecting vessels with DIN female ground joint NS29/32: 4x 100 ml, 4x 250 ml, 4x 500 ml, 4x 1000 ml, 4x 2000 ml round-bottom flasks 4x 75 ml, 4x 150 ml, 4x 300 ml, 4x 600 ml, 4x 1200 ml wide-mouth filter bottles The connections can be shut off individually and the drying vessels can be vented individually 1 level; only for Epsilon 1 / 2 4 LSC Order number Drip tray Size 30 x 138 x 525 mm For drying manifolds Order number For Epsilon 1 6 and 2 6

82 Epsilon Accessories 81 Thermblocks for Epsilon Order number Dimensions (mm) x 85.8 x 30 (L x W x H) For holding a total of 30 vessels Ø x mm with flat bottom or holding a total of 20 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.8 x 48 (L x W x H) For holding a total of 40 vessels Ø x mm with flat bottom and crimp rim Ø 12.2 Order number Dimensions (mm) x 85.7 x 31.5 (L x W x H) For holding a total of 40 vessels Ø x mm with bail crimp Order number Dimensions (mm) x 85.8 x 43 (L x W x H) For holding a total of 30 vessels Ø x mm (Eppendorf caps) Order number Dimensions (mm) x 85.8 x 23 (L x W x H) For holding a total of 48 vessels Ø x mm Order number Dimensions (mm) x 85.8 x 72 (L x W x H) For holding a total of 48 vessels Ø x mm with round bottom

83 82 Epsilon Accessories Thermblocks for Epsilon Order number Dimensions (mm) x 85.8 x 50 (L x W x H) For holding a total of 35 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.7 x 21 (L x W x H) For holding a total of 35 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.8 x 38 (L x W x H) For holding a total of 35 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 86 x 28 (L x W x H) For holding a total of 35 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.8 x 45 (L x W x H) For holding a total of 12 vessels Ø x mm with flat bottom Order number Dimensions (mm) 198 x 99 x 35 (L x W x H) For holding a total of 50 vessels Ø 15 x 45 mm with round or flat bottom

84 Epsilon Accessories 83 Thermblocks for Epsilon Order number Dimensions (mm) x 85.8 x 72 (L x W x H) For holding a total of 24 vessels Ø x mm with round bottom Order number Dimensions (mm) x 85.8 x 44 (L x W x H) For holding a total of 24 vessels Ø x mm with round bottom Order number Dimensions (mm) x 85.8 x 35 (L x W x H) For holding a total of 24 vessels Ø x mm Order number Dimensions (mm) x 85.8 x 72 (L x W x H) For holding a total of 24 vessels Ø x mm with round bottom Order number Dimensions (mm) x 85.8 x 30 (L x W x H) For holding a total of 24 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.8 x 38 (L x W x H) For holding a total of 18 vessels Ø x mm with flat bottom

85 84 Epsilon Accessories Thermblocks for Epsilon Order number Dimensions (mm) x 85.7 x 25 (L x W x H) For holding a total of 18 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.8 x 61 (L x W x H) For holding a total of 12 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.8 x 38 (L x W x H) For holding a total of 12 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.7 x 31.5 (L x W x H) For holding a total of 12 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.7 x 31 (L x W x H) For holding a total of 10 vessels Ø x mm with flat bottom Order number Dimensions (mm) x x 20 (L x W x H) For holding a total of 35 vessels Ø 24 x 45 mm with flat bottom (10R vials)

86 Epsilon Accessories 85 Thermblocks for Epsilon Order number Dimensions (mm) x 85.8 x 38 (L x W x H) For holding a total of 10 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.8 x 61 (L x W x H) For holding a total of 10 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 93 x 65 (L x W x H) For holding a total of 12 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.8 x 63 (L x W x H) For holding a total of 11 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.8 x 38 (L x W x H) For holding a total of 8 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.8 x 44 (L x W x H) For holding a total of 6 vessels Ø x mm with flat bottom

87 86 Epsilon Accessories Thermblocks for Epsilon Order number Dimensions (mm) x 85.8 x 61 (L x W x H) For holding a total of 6 vessels Ø x mm with round bottom Order number Dimensions (mm) x 85.8 x 66.5 (L x W x H) For holding a total of 4 vessels Ø x mm with flat bottom Order number Dimensions (mm) x 85.8 x 42 (L x W x H) For holding a total of 2 vessels Ø x mm with flat bottom

88 Epsilon Accessories 87 Overview Item number Block dimensions (mm) Number of vials Vial diameter (mm) (mm) Epsilon 1-4 LSCplus Epsilon 2-4 LSCplus 270 x 400 mm (W x L) Number of thermoblocks per shelf Epsilon 2-6D LSCplus 225 x 300 mm (W x L) Epsilon 2-10D LSCplus 350 x 400 mm (W x L) Epsilon 2-12D 350 x 400 mm (W x L) x 85.8 x x x 85.8 x x x 85.7 x x x 85.8 x x x 85.8 x x x 85.8 x x x 85.8 x x x 85.7 x x x 85.8 x x x 86 x x x 85.8 x x x 99 x x x 85.8 x x x 85.8 x x x 85.8 x x x 85.8 x x x 85.8 x x x 85.8 x x x 85.7 x x x 85.8 x x x 85.8 x x x 85.7 x x x 85.7 x x x x x x 85.8 x x x 85.8 x x x 93 x x x 85.8 x x x 85.8 x x x 85.4 x x x 85.8 x x x 85.8 x x

89 88 Epsilon Accessories s for Epsilon 2-4 / 2-10 Order number Dimensions (mm) 400 x 99 x 25 (L x W x H) For holding a total of 150 vessels Ø x mm with round or flat bottom 6-row block Order number Dimensions (mm) 400 x x 32 (L x W x H) For holding a total of 100 vessels Ø x mm or a total of 190 vessels Ø x mm Two-sided, designed for two vessel sizes Order number Dimensions (mm) 400 x 63 x 45 (L x W x H) For holding a total of 50 vessels Ø x mm (Eppendorf caps) Order number Dimensions (mm) 400 x x 45 (L x W x H) For holding a total of 100 vessels Ø x mm (Eppendorf caps) Vials placed stepwise at an angle of 60 in four rows Order number Dimensions (mm) 296 x 219 x 5 (L x W x H) For holding a total of 88 vessels Ø x mm Order number Dimensions (mm) 200 x 270 x 30 (L x W x H) For holding a total of 108 vessels Ø 16 x 35 mm with flat bottom (2R vials)

90 Epsilon Accessories 89 Order number Dimensions (mm) 225 x 300 x 30 (L x W x H) For holding a total of 130 vessels Ø 16 x 35 mm with flat bottom (2R vials) Order number Dimensions (mm) 400 x 80 x 62 (L x W x H) For holding a total of 11 vessels Ø x mm (50 ml flask) 1-row block Overview Item number Block dimensions (mm) Number of vials Vial diameter (mm) (mm) Epsilon 1-4 LSCplus Epsilon 2-4 LSCplus 270 x 400 mm (W x L) Number of thermoblocks per shelf Epsilon 2-6D LSCplus 225 x 300 mm (W x L) Epsilon 2-10D LSCplus 350 x 400 mm (W x L) Epsilon 2-12D 350 x 400 mm (W x L) x 99 x x x x x x 63 x x x x x x 219 x x x 270 x x x 300 x x x 80 x x s for Epsilon 2-12D Order number Dimensions (mm) x 89.2 x 90 (L x W x H) For holding a total of 75 vessels Ø ,2 x mm Order number Dimensions (mm) x 80 x 85 (L x W x H) For holding a total of 44 vessels Ø 16 x 100 mm with round bottom

91 90 Freeze drying general Vacuum The best drying results are obtained with the right vacuum. For aqueous media or media with low solvent content, oil-sealed rotary vane pumps are typically used, although oil-free dry-running pumps are increasingly being used. Their advantage is that there is no need for oil changes or disposal of used oil. Where specimens containing solvents or specimens fully dissolved in organic substances such as DMSO, acetonitryl or tertiary butanol are used, pumps that can withstand these chemicals must be used. The state of the art here is chemistry hybrid pumps, which consist of a rotary vane pump with an auxiliary diaphragm pump that evacuates the oil space. This reduces the condensation of aggressive solvents in the vacuum pump oil. The vacuum range that pump systems for freeze drying must be able to achieve in practice is to 0.01 millibar (hpa). Most vacuum sensors used for process control are hot-wire types (Pirani sensors; see the general information section) and are also available in chemical-resistant versions.

92 6 Vacuum 6.1 Vacuum pumps Vacuum pump oil Vacuum hoses Vacuum accessories 95

93 92 Vacuum 6.1 Vacuum pumps Vacuum pumps Chemical hybrid vacuum pump Order number Model Suction capacity Power CV 12 D 11 m 3 / h 115/230 V, 50 / 60 Hz With small flange coupling DN 25/25 Final vacuum 2 x 10-3 mbar Chemical hybrid vacuum pump Order number Model Suction capacity Power CV 23 D 16 m 3 / h 230 V; 50/60 Hz With small flange coupling DN 25/25 Final vacuum 2 x 10-3 mbar Chemical hybrid vacuum pump Order number Model RC 6 Suction capacity Power 5.9 m 3 / h 230 V, 50 / 60 Hz With small flange coupling DN 16 Final vacuum 2 x 10-3 mbar Chemical hybrid vacuum pump Order number Model RC 6 Suction capacity Power Emissions condenser and trap, for substances containing solvents 5.9 m 3 / h 230 V, 50 / 60 Hz With small flange coupling DN 16 Final vacuum 2 x 10-3 mbar Vacuum pump (chemical-resistant rotary-vane pump) Model Pascal 2010 C1 Order number Suction capacity Power 10 m 3 / h 230 V, 50 / 60 Hz With small flange coupling DN 16 Final vacuum 2 x 10-3 mbar

94 Vacuum 93 Vacuum pump (chemical-resistant rotary-vane pump) Order number Model Suction capacity Power Pascal 2021 C1 21 m 3 / h 230 V, 50 / 60 Hz With small flange coupling DN 25 Final vacuum 2 x 10-3 mbar Vacuum pump (rotary-vane pump) Model RZ 2,5 Order number Suction capacity Power 2.3 m 3 / h 230 V, 50 / 60 Hz With small flange coupling DN 16 Final vacuum 2 x 10-3 mbar Vacuum pump (rotary-vane pump) Model RZ 6 Order number Suction capacity Power 5.7 m 3 / h 230 V, 50 / 60 Hz With small flange coupling DN 16 Final vacuum 2 x 10-3 mbar Vacuum pump: Model DUO 10 Order number Suction capacity Power 11.1 m 3 / h 230 V, 50 / 60 Hz With small flange coupling DN 25/25 Final vacuum 2 x 10-3 mbar Vacuum pump: Model DUO 20 Order number Suction capacity Power 20 m 3 / h 230 V, 50 / 60 Hz With small flange coupling DN 25/25 Final vacuum 2 x 10-3 mbar Vacuum pump: Model Suction capacity Power nxds 10i 11.4 m 3 / h V, 50 / 60 Hz Final vacuum <0,01 mbar Order number With small flange coupling DN 25/25

95 94 Vacuum 6.2 Vacuum pump oil Vacuum pump oil Pump oil Contents Pumps 1 l bottle RZ / RC / DUO Order number Pump oil Contents Pumps 5 l cannister RZ / RC / DUO Order number Pump oil Contents Pumps 20 l cannister RZ / RC / DUO Order number Vacuum hoses Vacuum hoses Vacuum hose Order number Length 1 m With standard flange couplings DN 16 / DN 25 Vacuum hose Length 1.5 m Order number With standard flange couplings DN 16 / DN 25 Vacuum hose Order number Length 1 m With standard flange couplings DN 25 / DN 25 Vacuum hose Order number Length 1.5 m With standard flange couplings DN 25 / DN 25

96 Vacuum Vacuum accessories Vacuum accessories Micro aeration valve With hose fitting Order number Micro vent valve With hose fitting and pipe bend, DN25 / DN25 Order number Electromagnetic pressure control valve Order number For installation in the suction line of the vacuum pump With DN 25 / DN25 Alpha and Beta LDplus, as well as Alpha to Gamma systems with LSC and Epsilon 1 4 / 2 4 Manual stop valve For the vacuum hose between LDplus series freeze dryer systems and the vacuum pump (in place of the solenoid pressure control valve ) With standard flange DN 25 / DN25 Order number Exhaust filter Order number For vacuum pumps / Replacement filter cartridge Order number For

97 96 Vacuum Exhaust filter Order number Model ONF 25 L With automatic oil return Exhaust filter Order number Model ONF 25 L Without automatic oil return Replacement filter cartridge Order number For and Vacuum sensor Order number Model Connection Measuring range Measuring principle Warranty Note A VSP 63 MV SW With integrated signal processing for direct connection to the freeze drying system mbar Pirani With connecting cable, clamping/centring and T fitting 6 months These sensors are wear parts whose service life is largely dependent on the proper use and handling of the freeze dryer Replacement sensor Order number Model Warranty A VSP 62 MV SW 6 months Vacuum sensor Model Connection Measuring range Measuring principle Warranty Type 722 A Preferably for pilot systems mbar (or lower with reduced accuracy) Capacitive and piezoelectric With Jumo pressure sensor d trans p30 6 months Order number Note These sensors are wear parts whose service life is largely dependent on the proper use and handling of the freeze dryer

98 Vacuum 97 Vacuum sensor Order number Model Type VSP 3000 Connection Measuring range Measuring principle Warranty Note with integrated signal processing for direct connection to the freeze drying system mbar Pirani With connecting cable, clamping/centring and T fitting 6 months These sensors are wear parts whose service life is largely dependent on the proper use and handling of the freeze dryer Chemical-resistant vacuum sensor Model TPR 281 Order number Connection Measuring range Measuring principle Warranty Note With integrated signal processing for direct connection to the freeze drying system mbar Pirani Complete with connecting cable, two centring and clamping rings and T fitting DN 25 / 25 ISO-KF 6 months These sensors are wear parts whose service life is largely dependent on the proper use and handling of the freeze dryer Replacement sensor Model TPR 281 Order number Connection Warranty Note For connection to system controller; chemical resistant 6 months These sensors are wear parts whose service life is largely dependent on the proper use and handling of the freeze dryer High-vacuum grease Order number

99 98 Freeze drying general Process Data Acquisition Our unique software for process documentation is described in this section. It is available in two versions: a basic version for data logging and a full version with extensive additional control functions. A software module for recipe generation and an extension unit for the utilisation of heated shelves are also available. The related hardware accessories include product probes for temperature and electrical resistance, data cables, etc.

100 7 Process Data Acquisition 7.1 Software and hardware Sensors Miscellaneous 102

101 100 Process Data Acquisition 7.1 Software and hardware Software and hardware Program selection module Order number Model Control PGM-30 LSCplus system controller extension module for 30 user-defined individual programs Control of temperature and pressure profiles and individual process steps (freezing, primary drying, secondary drying) Very easy to use thanks to integration into system controller and guided data entry; supports entry and deletion of individual steps LyoControlplus Note Order number Determination of eutectic point Includes sensors for temperature and resistance For use in combination with LSCplus system controller and LyoLogplus documentation software Documentation software LyoLogplus Order number Windows-based software for logging relevant process parameters: ice condenser temperature, product temperature, shelf temperature, vacuum, and/or Lyo-Rx (depending on freeze dryer configuration) Supports export in PDF and Excel file formats Extension kit Serial interface for LD plus Order number USB Model Includes Order number Process data logging for equipment with LSCplus system controller For graphical process display USB stick, LyoLogplus installation CD

102 Process Data Acquisition 101 LPCplus process visualisation Order number Model Includes Note LPCplus Software for standard PCs for data transfer and freeze drying system monitoring in combination with LSCplus system controller LPC software on diskettes, 1 connecting cable, installation and operation manual, PC with operating system, colour monitor and colour graphic printer PC hardware included 7.2 Sensors Sensors Product sensor Order number Model PT 100 Cable length approx. 0.8 m With precision connector for use with LSC controller Alpha Delta Product sensor Order number Model PT 100 Cable length approx m With precision connector for use with LSCplus controller

103 102 Process Data Acquisition Product sensor Order number Model PT 100 Cable length approx. 0.8 m With precision connector Epsilon Product sensor Model PT 100 Order number Cable length approx. 1.3 m With precision connector Epsilon Product sensor Model PT 100 Order number Cable length approx. 2 m With precision connector Epsilon Sensor for temperature and resistance Order number Cable lenght For LyoControlplus With precision connector for use with LSCplus system controller 0,26 m Sensor for temperature and resistance For LyoControlplus Order number Cable lenght With precision connector for use with LSCplus system controller 0,8 m Sensor for temperature and resistance For LyoControl and LyoControlplus Order number Cable lenght Epsilon 0,8 m 7.3 Miscellaneous Interface cable Model USB-RS 232 Order number

104 Process Data Acquisition 103

105 104 Freeze drying general Cooling Baths and Freezing Equipment The accessories in this section can be used for routine external freezing of specimens in round-bottom flasks or wide-mouth bottles prior to drying. Freezing under rotation to form relatively thin frozen layers dramatically reduces drying time (see separate booklet "Principles and Applications of Freeze Drying"). Suitable media for cooling baths are also available.

106 8 Cooling Baths and Freezing Equipment

107 106 Chilling Baths and Freezing Equipment 8 Cooling Baths and Freezing Equipment Cooling Baths and Freezing Equipment Cooling bath Order number Model CB Dimensions (mm) 410 x 450 x 460 Bath depth 200 mm Bath opening (mm) 300 x 327 (W x L) Characteristics Capacity Air cooled Stainless steel tank with integrated condensate drain, digital display and actual ice condenser temperature indication 18 litres Bath temp. Approx. -40 C Power Note 230 V, 50 / 60 Hz For connection of 1 or 2 rotators Non-halogenated chilling media Rotator with support rod Order number Weight approx. Power For freezing liquids in round-bottom flasks 3.8 kg 230 V, 50 Hz Speed continuously variable from 60 to 2000 rpm Horizontal roller rotator Order number Weight approx. Application Power Stainless steel 11.5 kg For 1 or ml wide-neck filter bottles 220 V, 50 Hz Speed continuously variable from 60 to 2000 rpm Therminol D12 Order number Quantity 5 l cannister Therminol D12 Order number Quantity 10 l cannister Therminol D12 Order number Quantity 20 l cannister

108 Chilling Baths and Freezing Equipment 107

109 108 Service Service and Representatives Christ systems are marketed in more than 70 countries worldwide. To enable support for our customers at all times, we have an international network of representatives for advice and service. At the national level, support and advice are provided by our representatives and by our trained system specialists directly from our head office. We are there for you all the time. Vancouver San Diego Montreal Tonawanda New York Helsingborg Oslo Kopenhagen Moskau Brüssel Warschau London Osterode Kiew Prag Paris Budapest Basel Wien Madrid Rom Istanbul Lissabon Athen Tunis Peking Seoul Tokio Kairo Delhi Shanghai Mexico City Riyadh Dubai Mumbai Dhaka Hong Kong Madras Bangkok Bogota Singapur Lima Johannesburg Sao Paolo Santiago Buenos Aires Perth Sydney Adelaide Auckland Selected international Christ representatives For information about our international representatives and contact data, visit

110 Service 109 Questionnaire for requesting advice or a quotation Your name and address 1 What is the maximum quantity (kilograms or litres) to be dried each day? 2 Are there any particular requirements regarding batch size? If so, please specify. 3 What has to be dried? 4 What is the ratio (weight percentage) of the dry substance to the initial overall mass? 5 What is the consistency of the substance to be dried (low viscosity, high viscosity, pasty, solid)? If solid, how big are the pieces? 6 Does the substance to be dried contain solvents other than water? If so, which ones and in what percentages? 7 What residual moisture level in the dried substance is considered acceptable? 8 If you already have experience with freeze drying, of the substance concerned, what is your opinion of: a) the quality of the dried substance? b) the equipment used? 9 What vessels are to be used for drying? What are the shapes and sizes of the vessels? Can you provide samples? How much undried substance should be present in each vessel? How many vessels per batch are necessary? (Note: These details are particularly important to help us determine the proper choice of freeze drying equipment for your application.) 10 Will the substance be stored in the drying vessels, or is transfer necessary? 11 Is sealing under vacuum necessary?

111 110 Service 12 Is preservation under nitrogen necessary? 13 Available power: AC V Hz 3-phase AC V Hz 14 Do you have any other specific wishes or requirements? A laboratory is available for carrying out tests of drying methods. Date Signature Martin Christ Gefriertrocknungsanlagen GmbH A der Unteren Söse Osterode am Harz Phone +49 (0) Fax +49 (0)

112 Service 111 Vapour pressure above ice mbar Vapour pressure C Temperature 1 mbar =ˆ 1 hpa = 10 2 Pa 1 mbar =ˆ 10 5 Pa = 0.1 N / mm 2 1 Pa = 1 N / m 2 1 Torr = mbar

113 112 Conversion table Conversion table Conversion table for vapour pressure above ice (ice temperature in C and corresponding pressure in mbar) C =^ mbar C =^ mbar C =^ mbar C =^ mbar

114 Our Product Spectrum With our unique and broad spectrum of equipment and accessories, we supply freeze drying systems and vacuum concentrators for every application. Let us show you what we can do! Freeze drying systems for industrial production with ice condenser capacities from 20 to 500 kg; custom system engineering including loading and unloading systems. 2 Pilot freeze drying systems for process development or optimisation with ice condenser capacities from 4 to 12 kg. 3 Freeze drying systems for routine applications or R&D with ice condenser capacities from 2 to 24 kg. 4 Rotation vacuum concentrators for applications ranging from routine operations to evaporation concentration in advanced pharmaceutical research

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