Headspace Vials, Caps, and Septa Capillary Columns Syringes Hydrogen Generators

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1 PerkinElmer continues to drive innovation and performance in Gas Chromatography (GC) instrumentation and software, with a strong focus on making your lab more productive. Backed by our worldwide, world-class service and support team, PerkinElmer GC products are a great fit for your modern, fast-paced lab. PerkinElmer is the only GC supplier that manufactures and sells a complete single-vendor solution from sample handling to data handling. This means you will not struggle to find answers to applications and service questions one company provides the complete solution. Gas Chromatography

2 Gas Chromatography QUICK-FIND INDEX Page # Autosampler Accessories Vials, Caps and Septa 89 Autosampler Syringes 88 Capillary Columns Accessories 9 Capillary Columns 9 Capillary Injectors 50 Detectors Ferrules 9 Gas Purification Systems 6 Gas Sampling Supplies 6 Headspace Accessories and Supplies Filters and Traps 6 Headspace Vials, Caps, and Septa 8 Hydrogen Generators 65 Injector Liners 57 PerkinElmer offers a wide selection of superior quality products designed to work with your PerkinElmer instruments. Our precision-designed products deliver the peace of mind that comes from knowing that you ll get the results you need. The Quick Find Index to the left will help you find products fast. For your convenience, products are alphabetized by category, sub-category, and family. There is also a more complete Alphabetical INDEX on page 9 and a Part Number INDEX on page 07. Headspace Vials, Caps, and Septa PerkinElmer s patented vial and cap design incorporates pressure relief features which guarantee safe operation with the high pressure typically developed during thermostatting. These vials have a greater wall thickness and round base which enables them to withstand pressure up to 60 psig. PerkinElmer septa are designed for the patented pressure release cap to ensure safe operation at higher temperatures. Available pre-assembled into caps with starsprings. Page 8 Capillary Columns We use only the finest quality of high-strength fused silica in the manufacture of our columns. Each column is individually inspected and tested to guarantee you the highest performance and to maximize reproducibility. Page 9 Injector Septa 59 Ozone Precursor 80 PerkinElmer TotalChrom Software 7 Swagelok Fittings 95 Syringes 6 Thermal Desorber Stainless Steel and Glass Tubes 8 Thermal Desorber Traps and Fittings 8 Valves 68 Vial Crimping Tools 90 Syringes PerkinElmer Injector Syringes have been tested and optimized for use with a 7 cm needle. This is critical for depositing sample in the optimal zone. Syringes are individually inspected for accuracy and performance. Syringes for 0.5 μl to 50 μl capacity in two different point styles are available. PerkinElmer ultra micro volume syringes are recommended for sample injection of less than 5 μl. Page 6 Hydrogen Generators The patented DBS PG-H series of Hydrogen Pure Gas Generators is ideal for operation with gas analyzers as a source of pure hydrogen in plasma chambers and other isolated environments. Electrolytic membrane technology is preferred over alternative hydrogen generating techniques because it is clean, requires less maintenance, and there is no need to store chemicals to maintain operation. Page 65

3 Clarus GC Sleek design and easy touch screen revolutionize GC interaction Gas chromatography started in 95, with the seminal work of A.J.P. Martin and A.T. James and, within a few years, it became one of the most popular analytical techniques. PerkinElmer played a crucial role in the development of the technique: Clarus 500 GC Dual-channel, real-time signal display on the touch screen Flexible configurations with integrated mass spectrometry, headspace or thermal desorption and pyrolysis samplers Temperature-programmable inlets maximize reproducibility Pneumatic Pressure Controllers (PPC) provide accurate and highly reproducible gas controls GC analysis at your fingertips Easy setup/method development Multiple-language support Enhanced Solvent Purge mode Isolation mode High-pressure pulse injection Large-volume injection Petrochemical analysis from Hydrogen to Asphalt Ozone Precursors analysis Air Toxics analysis Food and Beverage quality control The sleek Clarus Gas Chromatograph from PerkinElmer offers a whole new approach to the way you interact with your GC instrument. An intuitive touchscreen interface features real-time signal display and eight-language support. Available in hundreds of configurations ranging from dedicated analyzers for petrochemical and air analysis to powerful mass spectrometer units, the Clarus GC is extremely flexible. For applications requiring mass spectrometer detection, the Clarus GC can be coupled to the industry s easiest-to-use and widestmass-range quadrupole mass spectrometer. The Clarus GC features the PerkinElmerexclusive PreVent operating mode. This powerful mode uses the combined features of the temperatureprogrammable PSS injector and the PPC, to increase analytical throughput, manage difficult samples, protect the column and chromatograph and lower detection limits PerkinElmer s award-winning datahandling software makes managing data easier than ever. Combine the Clarus GC with the Clarus Mass Spectrometer (MS), market-leading PerkinElmer TurboMatrix samplehandling accessories, flexible user-friendly TotalChrom software and world-class service and support for an integrated, complete analytical solution. The totally integrated Clarus autosampler provides flexibility and automation capability for the gas chromatograph. The autosampler accommodates three autosampler syringe sizes (0.5, 5.0, and 50 μl) and three injection speeds (slow, normal, and fast), for complete application flexibility. Unobstructed access to either injection port with one autosampler permits any combination of analyses for the most efficient utilization of the gas chromatograph. The Clarus MS features a wealth of innovative technology to provide the most complete characterization of samples. PerkinElmer Selected Ion and Full Ion (SIFI ) scanning technology and high scan speeds increase system accuracy. The mass spectrometer boasts a fast scanning speed with the widest mass range available for GC/MS, providing capability to analyze a greater scope of applications. The combination of a Clarus GC with a data-handling system provides a total laboratory solution from data collection and analysis to reporting and storage. 87

4 Autosampler Accessories Syringes and Accessories Autosampler Replacement Parts Description Gas Chromatography Autosampler Accessories Replacement Vial Locator (may require N608 service installation, not included) Spring (pkg. )* N608 Shoulder Screw (pkg. )* * Requires two for complete installation. See illustration. Miscellaneous Accessories Autosampler Starter Kit Includes: 5 μl x 0.6 mm o.d. syringe, ml clear sample vials (00), ml amber sample vials (00), blue crimp caps with septa (00), green crimp caps with septa (00), red crimp caps with septa (00), septa for waste/wash vials (00), crimper mm, decapper mm, ml vial rack. Each Autosampler Thermostatting Accessory Allows thermostatting of Autosampler tray from 0 to 50 C. Accessory includes: tubing, tie wraps, clamp, and instructions. (Circulating bath not included.) N AutoSystem XL Autosampler Add-On Accessory (White Color) Note: Cannot be installed on an AutoSystem. Service installation is required. Spare Autosampler Tray N N ( ) N μl Syringe for Autosampler N6090 Syringes Replacement Needles for 0.5 μl Syringes 0.5 μl Syringes Needle o.d. 0.7 N N Recommended Use Needle o.d. Low injection volume. 0.5 capillary 0.7 N605 0 on-column injection. Plunger type: Metal Plunger in needle type Low injection volume analyses 0.6 N605 0 Plunger type: Metal Plunger in needle type 5 μl Syringes Recommended Use Needle o.d. 0.5 capillary on-column injection 0.7 N6080 Plunger type: metal. Plunger in barrel Routine analyses. Plunger type: metal 0.6 N605 0 Plunger in barrel Routine analyses. Shipped standard 0.6 N6090** 0 with instrument. Plunger type: metal Plunger in barrel with Teflon -tipped seal ** Shipped standard with instrument 50 μl Syringe Recommended Use Needle o.d. Metal plunger in barrel type 0.7 N90799 Metal plunger in barrel type 0.6 N

5 Autosampler Accessories Vials, Caps, and Septa Crimp Caps and Septa Screw Top Sample Vials and Caps Crimp Caps Aluminum crimp caps and septa for mm sample vial, Teflon /rubber. Description Blue Crimp Caps and Septa (pkg. 00) N90686 Green Crimp Caps and Septa (pkg. 00) N Red Crimp Caps and Septa (pkg. 00) N Silver Crimp Caps and Septa (pkg. 00) N Viton Septa Crimp Caps These Viton septa caps are recommended for applications that require work with chloroform. Crimp Top Sample Vials Amber ( mm) vial for photosensitive samples, ml volume. Caps and septa not included. Low-Volume Sample Inserts N μl low volume glass inserts for crimp cap sample vials. Supports required but not included. Description Insert (pkg. 000) N Support (pkg. 500) N Clear ( mm) sample vial, ml volume. Caps and septa not included. (pkg. 00) N90680 N These vials are custom designed for the AutoSystem Series and Clarus GC. (Not to be used with low-volume insert.) Description Cap, for Screw Top Vial (pkg. 00) N90 0 Septa for Screw Top Cap (pkg. 00) N90 PTFE-Coated Butyl Rubber Vial, Clear Glass Screw Top (pkg. 00) N9095 Vial Holder Racks Keep your samples organized and tip proof! These rugged, plastic vial racks are great for holding vials while you load and cap your samples. They stack away neatly when done. Description 6 vial capacity, 0 mm N vial capacity, mm N900 Waste Vials Description Cap for Waste and Wash Vials (5 mm), (pkg. ) 0990 Clear Waste and Wash Vial ml (5 mm), (pkg. ) 0990 Septa for Waste Wash Vials N For use with viscous or toxic samples Diffusers for Waste and Wash Vials Diffusers are sold exclusively by PerkinElmer. The conical shape allows the needle to penetrate into solvent or waste. Reduces spillage and large losses through evaporation. N6076 Autosampler Accessories Gas Chromatography See page for ordering information. For the most current product listing, visit 89

6 Autosampler Accessories Vial Crimping Tools Crimping Tools Gas Chromatography Autosampler Accessories Benchtop Crimper N66006 Electronic Crimper N90567 (0 V) Benchtop Crimper Sturdy, rugged stand will accept three size jaws. Jaws required but not included. Jaws for Benchtop Crimpers Description AutoSystem GC Vials, mm N Headspace Vials, 0 mm N66009 Electronic Crimpers Electronic crimpers and decappers are easy to use and fully rechargeable. Ergonomically designed to alleviate the potential for Carpal Tunnel Syndrome and provide a consistent crimp pressure numerous times. The unit comes with a standard Black and Decker VersaPak Gold battery and charger, and will crimp several hundred vials on one charge. Crimping pressure is fully adjustable for precision control. Description mm Electronic Crimper 0V N90567 mm Electronic Crimper 00V N mm Electronic Crimper 0V N mm Electronic Crimper 0V N mm Electronic Decapper 0V N90575 mm Electronic Decapper 00V N mm Electronic Decapper 0V N mm Electronic Decapper 0V N Electronic Crimper Replacement Battery N90585 Hand Crimpers Description.5 ml (AutoSystem GC sample vials), mm ml and 0.0 ml (headspace vials), 0 mm N Economy Cap Removal Tool N Description mm Autosampler Crimp Caps N mm Headspace Crimp Caps N

7 Capillary Columns Capillary Columns Capillary Columns Top 0 Reasons to Buy PerkinElmer Elite Series Capillary Columns Finest quality of high-strength fused silica Each column individually inspected and tested Reproducible results Crosslinked and bonded stationary phase 5 Robust column cage 6 Superior resolution 7 Wide selection of stationary phases available 8 Reduced baseline bleed 9 Lower baseline noise 0 Column lengths from 5 to 05 m Why choose fused silica? Many factors influence the quality of a column. Fused silica is considered to be the purest form of glass, with fewer metal oxides (Lewis acid sites) and hydrogen bonding (surface silanol) groups. The stationary phase is cross linked (polymerized) and also bonded to the surface of the column to provide a high degree of stability, resulting in lower bleeding of the stationary phase at elevated temperatures. The superior inertness of the column means that acidic and basic compounds can be analyzed on the same column. Selecting the right stationary phase The inherent efficiency (large number of theoretical plates) of capillary columns allows you to choose from relatively few types of phases, compared to the many varieties of packed columns previously required. Perhaps more importantly, because capillary columns are more efficient, you will see superior resolution resulting in narrower, taller peaks that allow easier integration from your data system. Identification of small peaks are facilitated by a reduced baseline bleed and lower baseline noise. Non-polar Elite- columns from PerkinElmer will preferentially retain non-polar compounds, whereas the PerkinElmer Elite-00 column phase provides high selectivity for analytes containing lone pair electrons, such as nitro and carbonyl groups. Elite-WAX polyethylene glycol columns are highly selective toward polar compounds such as alcohols. What length do I need? Typically, capillary columns are available in lengths from 5 to 05 meters. The longer the column the more resolving power, but this also increases the analysis time. Doubling a column length only increases resolution by approximately 0% but, under isothermal conditions, will double the analysis time. If using a temperature programmed analysis, retention times are more dependent on the temperature than on the column length. PerkinElmer provides columns in the most popular lengths of 5, 0,, 5, 5, 0, 50, 60, 75, 00, and 05 m depending upon the column i.d. 9

8 Capillary Column Accessories Adapter Kits Gas Chromatography Capillary Column Accessories Adapter Kit Accessories Detector Receiver /8 to /6 in. detector receiver for use when using capillary columns with FID, ECD, NPD, and FPD. Flow Accessory 0-0 ml For use when converting an AutoSystem flow controller to low-flow operation. Flow Accessory 0-00 ml Shipped as standard with instrument. Injector/Detector Adapter for Fused-Silica Capillary Columns This /8 to /6 in. stainless steel reducer can be easily installed. For use when installing capillary columns on the /8 in. split/splitless injector and all /8 in. detector fittings. The reducer allows the use of /6 in. graphite/vespel ferrules rather than the larger /8 in. ferrule. (Not compatible with AutoSystem or Clarus Series.) N Wafer Scribe The ceramic wafer scribe is inexpensive and ideal for cutting polyimide fused-silica capillary columns. The scribe is easy to hold and simple to use. All four sides can be used. (pkg. 0) Wide-Bore Adapter Kit AutoSystem GC Adapter Kit N N N N The 0.5 mm Capillary Column Adapter Kit from PerkinElmer contains all the parts necessary to adapt packed column injectors quickly and easily for use with wide-bore capillary columns. For accurate control of the low flows used in wide-bore capillary columns (down to ml/min.). Kit includes 0-0 ml/min. flow controller element, wide-bore adapter with /6 in. fitting, wide-bore glass liner and column support hanger. May be used in both on-column or off-column modes. (For AutoSystem GC Series only.) N Wide-Bore Kit Replacement Parts Column Nut /6 in. Replacement /6 in. column nut. Connects capillary column to adapter. Graphite/Vespel /6 in. Ferrule /6 in. x 0.8 mm i.d. For connecting capillary columns to adapter liner. Graphite/Vespel / in. Ferrule For installing adapter liner into injector. Graphite Ferrule Reverse ferrules used to connect 0.5 mm capillary columns to wide-bore adapter kit. /6 in. fitting. Reverse ferrule /6 in. x 0.8 mm i.d. (pkg. 0) Graphite/Vespel Ferrule Reverse ferrules used to connect 0.5 mm capillary columns to wide-bore adapter kit. /6 in. fitting. Reverse ferrule /6 in. x 0.8 mm i.d. (pkg. 0) Wide-Bore Quartz Liner AutoSystem GC wide-bore replacement quartz liner. Wide-Bore Glass Liner Replacement glass liner (untreated) for use with the wide-bore adapter kit (0.5 mm columns) N600 N

9 Capillary Column Accessories Connectors and Supplies Column Connectors Union Connectors Column i.d. (mm) Qty. 0.5* pkg. 0 N * pkg. 0 N pkg. 5 N * pkg. 0 N907 6 pkg. 5 N907 Reducing Connectors Column i.d. (mm) Qty. 0. to 0.5* pkg. 0 N to 0.5* pkg. 0 N to 0.* pkg. 0 N90 6 pkg. 5 N90 * Note: These connectors are not recommended for use with aluminum-clad columns. Tools Pin Vise and Drill Bits For enlarging ferrule i.d. for capillary columns. Kit includes a double-ended pin vise and a set of drill bits, sizes No. 6 (0.99 mm) through No. 80 (0. mm). N906 5 Pin Vise and Drill Bit Kit N906 Uncoated Deactivated Fused-Silica Capillary Tubing High-quality, uncoated fusedsilica tubing is available in standard capillary sizes. Deactivated tubing is perfect for making guard columns and replacement Transfer Lines in HS and TD samplers retention gaps; available in 5 m lengths. Use our SPLITTERS and CONNECTORS to attach tubing to your polyimide-coated columns. Polyimide-Uncoated Deactivated Tubing Tube i.d. (mm) Length m N m N m N m N m N Capillary Column Support for PerkinElmer GCs Column supports delicate fused-silica columns in the proper oven location for optimum chromatographic performance. Description AutoSystem Series/Clarus N Universal Connectors Allows for fast, leak-free connections of fused-silica columns. The new fused-silica tapered design allows connection of any size column and it s easy to use. (0. to 0.5 mm columns can be used.) Description Polyimide Sealing Resin* (5 g) N90 9 Universal Connector* (pkg. 5) N909 8 Universal Y Splitter* (pkg. ) N * Note: These connectors are not recommended for use with aluminum-clad columns. Universal Connector N909 Capillary Column Accessories Gas Chromatography See page for ordering information. For the most current product listing, visit 9

10 Capillary Column Accessories Ferrules Gas Chromatography Capillary Column Accessories Graphite and Vespel Ferrules Graphite Ferrules This is the ferrule of choice for high-temperature applications. Of the three ferrule types available, graphite is the softest, making it less damaging to capillary columns when overtightened. Graphite seals easily and does not stick to glass columns. Recommended for use with capillary columns. Temperature limit is 50 C. Nut Size (in.) Ferrule i.d. (in.) Qty. /6 /6 pkg /8 /8 pkg / / pkg Graphite/Vespel Ferrules Graphite/vespel ferrules (5% graphite/85% polyimide) are recommended for use with GC/MS systems. Best choice for glass columns and polyimide-coated, fused-silica capillary columns. Can usually be removed easily from column. Temperature limit is 50 C. Nut Size (in.) Ferrule i.d. (in.) Qty. /6 /6 pkg /8 /8 pkg. N / / pkg Vespel Packed Stainless Steel Column Ferrules Vespel ferrules are not reusable; they tend to stick to columns after use at upper temperature limit. Not recommended for fused-silica capillary columns. Use these vespel ferrules on /6 in. metal tubing and glass-lined receivers (heated or ambient). Temperature limit is 50 C. Nut Size (in.) Ferrule i.d. (in.) Qty. /8 /8 pkg. 0 N / / pkg. 0 N Capillary Column Ferrules Package quantity: 0 Nut Size Column Ferrule Graphite Graphite/Vespel (in.) i.d. (mm) i.d.(mm) / N/A / / (-hole) N N / / (-hole) N/A / N/A / (-hole) N/A / N/A Note: mm i.d. columns require 0.5 mm i.d. ferrules; 0.5 mm i.d. columns require 0.8 mm i.d. ferrules. SilTite Metal Ferrules Nut and Ferrules Kit SilTite Metal Nut and Ferrules provide a continuous leak-free connection and are perfect for connecting your column to a GC/MS. From the SilTite drawing it can be seen that the taper of the inner nut is designed specifically for the angle of the SilTite ferrule. This ensures an even closure of the ferrule around the whole column to eliminate leaks. Features and Benefits: No need to re-tighten the nut Eliminate contamination Reusable nut Leak-free seal Starter kit contains SilTite nuts and 0 ferrules The metal SilTite ferrule and nut are manufactured from the same material and will therefore not expand and contract at different coefficient rates. The base of the SilTite ferrule forms a perfect seal with the MS interface, covering the whole transfer interface. SilTite metal ferrules have a temperature limit well above the temperature capacity of the injector, MS interface or GC oven. Description Qty. SilTite Ferrules Starter Kit 0. mm pkg. 0 N SilTite Ferrules Starter Kit 0.5 mm pkg. 0 N SilTite Ferrules Starter Kit 0.8 mm pkg. 0 N SilTite Ferrules 0. mm pkg. 0 N SilTite Ferrules 0.5 mm pkg. 0 N SilTite Ferrules 0.8 mm pkg. 0 N SilTite Nuts pkg. 5 N

11 Capillary Column Accessories Fittings Swagelok Fittings Swagelok TM Fittings Swagelok fittings from PerkinElmer are available in brass and stainless steel. The patented advanced-geometry back ferrule design provides a leak-tight tube connection on all Swagelok stainless steel tube fittings, in sizes / to / in., and 6 to mm. Leak-tight seals that will withstand high-pressure, vibration, vacuum and temperature changes depend upon close tolerances and consistent, exacting quality control in conjunction with good design principles. Ease of installation Back ferrule axially advances the front ferrule Vibration fatigue resistance Wide variety of configurations Brass Stainless Steel Product Qty. Size Bulkhead Adapter pkg. / in. to / in. tube N Back Ferrule pkg. 5 /6 in. N90000 N /8 in. N N / in. N N9000 Cross Union pkg. /8 in. N Front Ferrule pkg. 5 /6 in. N9000 N /8 in. N N / in. N N9000 Male Adapter pkg. / in. tube to /8 in. NPT N Tube to Pipe Male Connector pkg. /8 in. to /8 in. NPT N905 9 /8 in. to / in. NPT N905 9 / in. to /8 in. NPT N / in. to / in. NPT N Nut pkg. 5 /6 in. N N /8 in. N N / in. N N Plug pkg. /6 in. N /8 in. N N90006 / in. N N90 7 Union pkg. /6 in. N90008 N /8 in. N N / in. N Union Tee pkg. /6 in. N90 7 /8 in. N90 7 / in. N90 7 Reducing Union pkg. /8 in. to /6 in. N N905 7 / in. to /8 in. N N906 6 / in. to /6 in. N907 Capillary Column Accessories Gas Chromatography See page for ordering information. For the most current product listing, visit 95

12 Capillary Columns Application Index Environmental Subject Column Page No. Forensic/Clinical Toxicology Subject Column Page No. Gas Chromatography Capillary Columns Amines and Phenols Elite-5Amine 99 EPA Method 508 Pesticides Elite-5 99 EPA Method 508 Organochlorine Pesticides Elite-CLPesticides 00 Elite-CLPesticides 00 EPA Method 5. Elite-6 (GC/MS) 0 EPA Method 55. Elite-5 0 EPA Method 55. Chlorinated Disinfection Byproducts Elite-00 0 EPA Method 80 Volatile Organics Elite-Volatiles 0 EPA Method 808 Pesticides Elite-5 0 EPA Method 808A Organochlorine Pesticides Elite-CLPesticides 0 Elite-CLPesticides 0 EPA Method 860B Volatile Organics Elite-VMS 05 EPA Method 860B Volatile Organics Elite-VMS 06 EPA Method 870 Semi-Volatile Organics Elite-5 ms 07 Essential Oils Citronella Java Oil Elite- 08 Nitrogen Containing Herbicides Elite-5 08 Pesticides Elite-5 09 Synthetic Essential Oil Elite- 09 Food and Flavors Subject Column Page No. Brewing Beer Elite-BAC 0 Essential Oils Lemon Oil Elite-5 0 Essential Oils Native Spearmint Oil Elite-WAX ETR Essential Oils Synthetic Mushroom Aroma Elite-WAX ETR Sugars As Alditol Acetates Elite-5 TCA in Wine Elite-5 ms Anabolic Steroids Underivatized Elite-5 Blood Alcohol Elite-BAC Cannabinoids TMS Derivatives Elite-5 Cocaine and Metabolites Elite-5 5 Sympathomimetic Amines HFBA Derivatives Elite-5 5 Industrial Chemicals Subject Column Page No. Alcohols and Aldehydes Elite-WAX ETR 6 Alcohol Mixtures Elite-WAX ETR 6 Aldehydes Elite-WAX 7 Amines & Phenols Elite-5Amine 7 Aromatics Elite-WAX ETR 8 Industrial Solvents Elite-MWAX 8 Industrial Solvents Elite-WAX ETR 8 Petroleum Subject Column Page No. Prudhoe Bay Crude Oil Elite-GC-79 9 Volatile Hydrocarbons Elite-Q PLOT 9 96

13 Capillary Columns U.S. EPA Methods U.S. EPA Drinking Water Test Methods U.S. EPA Organic Chemical Analysis Waste Water Methods Method Column Recommendations Method Column Recommendations 50. Elite-6 0 m x.5 mm i.d.,.00 μm N Elite-6 0 m x.5 mm i.d.,.00 μm N Elite-6** 75 m x.5 mm i.d.,.00 μm N Elite-6** 75 m x.5 mm i.d.,.00 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-Volatiles** 75 m x.5 mm i.d.,.55 μm N969 7 Elite-Volatiles** 75 m x.5 mm i.d.,.55 μm N969 7 Elite m x.5 mm i.d.,.00 μm N Elite m x.5 mm i.d.,.00 μm N Elite-6* 0 m x.5 mm i.d.,.00 μm N Elite-6** 0 m x.5 mm i.d.,.00 μm N Elite-6** 75 m x.5 mm i.d.,.00 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-Volatiles 0 m x.5 mm i.d.,.55 μm N Elite m x.5 mm i.d.,.00 μm N Elite-Volatiles** 75 m x.5 mm i.d.,.55 μm N Elite-6 0 m x.5 mm i.d.,.00 μm N Elite m x.5 mm i.d.,.00 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-6 0 m x.5 mm i.d.,.00 μm N Elite-5ms** 0 m x.5 mm i.d.,.50 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite- 5 m x.5 mm i.d.,.50 μm N Elite-* 0 m x. mm i.d., 0.5 μm N Elite-5 0 m x.5 mm i.d.,.50 μm N Elite-6** 0 m x.5 mm i.d.,.00 μm N Elite-5ms** 0 m x.5 mm i.d.,.50 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-608** 0 m x.5 mm i.d., 0.8 μm N Elite-* 0 m x. mm i.d.,.00 μm N Elite-5 0 m x.5 mm i.d.,.50 μm N Elite-7 0 m x. mm i.d., 0.50 μm N Elite-5ms** 0 m x.5 mm i.d.,.00 μm N Elite-5* 0 m x.5 mm i.d., 0.5 μm N Elite-5 0 m x. mm i.d., 0.5 μm N Elite-5ms** 0 m x.5 mm i.d., 0.5 μm N968 6 Elite-5ms** 0 m x. mm i.d., 0.5 μm N Elite-70* 0 m x.5 mm i.d., 0.5 μm N Elite-5 5 m x.5 mm i.d.,.50 μm N Elite-5* 0 m x.5 mm i.d., 0.5 μm N Elite-5ms** 5 m x.5 mm i.d.,.50 μm N9699 Elite-5ms** 0 m x.5 mm i.d., 0.5 μm N Elite- 0 m x. mm i.d.,.00 μm N Elite-608** 0 m x. mm i.d., 0.50 μm N Elite-5ms** 0 m x.5 mm i.d.,.00 μm N968 6 Elite-70* 0 m x.5 mm i.d., 0.5 μm N Elite-5ms 60 m x.5 mm i.d., 0.0 μm N Elite-5ms 60 m x.5 mm i.d., 0.0 μm N Elite-5ms** 60 m x. mm i.d., 0.0 μm N Elite-5ms 60 m x. mm i.d., 0.0 μm N Elite-608** 0 m x.5 mm i.d., 0.8 μm N Elite-* 0 m x. mm i.d., 0.5 μm N Elite-70 0 m x.5 mm i.d.,.00 μm N Elite-5* 0 m x. mm i.d., 0.5 μm N Elite-7 0 m x.5 mm i.d.,.00 μm N Elite-5ms** 0 m x. mm i.d., 0.5 μm N Elite-5** 0 m x.5 mm i.d.,.00 μm N965 7 Elite-70* 0 m x. mm i.d., 0.5 μm N Elite-5ms** 0 m x.5 mm i.d.,.50 μm N Elite-6* 0 m x.5 mm i.d.,.0 μm N Elite-6 0 m x.5 mm i.d.,.0 μm N Elite-6* 0 m x.5 mm i.d.,.00 μm N Elite-6 0 m x.5 mm i.d.,.00 μm N Elite-6* 75 m x.5 mm i.d.,.00 μm N Elite-6 75 m x.5 mm i.d.,.00 μm N Elite-5* 0 m x. mm i.d.,.00 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-5ms** 0 m x.5 mm i.d.,.00 μm N968 6 Elite-Volatiles** 75 m x.5 mm i.d.,.55 μm N969 7 Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite m x.5 mm i.d.,.00 μm N Elite-Volatiles** 75 m x.5 mm i.d.,.55 μm N Elite-5ms** 0 m x. mm i.d., 0.5 μm N Elite-5* 0 m x. mm i.d., 0.5 μm N Elite-5* 0 m x. mm i.d., 0.5 μm N Elite-5ms** 0 m x.5 mm i.d.,.00 μm N968 6 Elite-5ms** 0 m x. mm i.d., 0.5 μm N Elite-5* 0 m x.5 mm i.d., 0.5 μm N Elite- 0 m x.5 mm i.d.,.50 μm N Elite-5* 0 m x. mm i.d., 0.5 μm N Elite-608** 0 m x.5 mm i.d., 0.8 μm N Elite-5ms** 0 m x.5 mm i.d., 0.5 μm N968 6 Elite-70 0 m x.5 mm i.d.,.00 μm N Elite-5ms** 0 m x. mm i.d., 0.5 μm N Elite-6 75 m x.5 mm i.d.,.55 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-6** 75 m x.5 mm i.d.,.00 μm N Elite-* 0 m x. mm i.d.,.00 μm N Elite-5* 0 m x.5 mm i.d., 0.5 μm N Elite-5ms** 0 m x.5 mm i.d.,.00 μm N968 6 Elite-5ms** 0 m x.5 mm i.d., 0.5 μm N Elite-70* 0 m x. mm i.d., 0.5 μm N Elite-5* 0 m x. mm i.d., 0.5 μm N * Specified in EPA method. Elite-5ms** 0 m x. mm i.d., 0.5 μm N ** This column is highly recommended by PerkinElmer for this EPA method. The choice of column for this purge-and-trap method may depend on your sample concentrator to GC interface. Capillary Columns Gas Chromatography See page for ordering information. For the most current product listing, visit 97

14 Capillary Columns U.S. EPA Methods U.S. EPA Solid Waste Test Methods Gas Chromatography Capillary Columns Method Column Recommendations 800 Elite-6 75 m x.5 mm i.d.,.00 μm N Elite-Volatiles** 75 m x.5 mm i.d.,.55 μm N Elite-6 0 m x.5 mm i.d.,.00 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-6 0 m x.5 mm i.d.,.00 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-6 0 m x.5 mm i.d.,.00 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-5ms 0 m x.5 mm i.d.,.50 μm N Elite- 5 m x.5 mm i.d.,.50 μm N Elite-608** 0 m x.5 mm i.d., 0.8 μm N Elite-5* 0 m x.5 mm i.d.,.50 μm N Elite-608** 0 m x.5 mm i.d., 0.8 μm N Elite-70* 0 m x.5 mm i.d.,.00 μm N Elite-5 0 m x.5 mm i.d.,.50 μm N Elite-5ms** 0 m x.5 mm i.d.,.50 μm N Elite-5 0 m x. mm i.d., 0.5 μm N Elite-5ms** 0 m x. mm i.d., 0.5 μm N Elite- 0 m x. mm i.d.,.00 μm N Elite-5ms** 0 m x.5 mm i.d.,.00 μm N968 6 Elite-5ms** 0 m x. mm i.d.,.00 μm N Elite- 0 m x.5 mm i.d.,.50 μm N Elite-70** 0 m x.5 mm i.d.,.00 μm N Elite-5* 5 m x.5 mm i.d.,.50 μm N Elite-5ms** 0 m x.5 mm i.d.,.50 μm N Elite-5** 0 m x.5 mm i.d., 0.50 μm N Elite-608** 0 m x.5 mm i.d., 0.8 μm N Elite-70 0 m x.5 mm i.d.,.00 μm N Elite-6 0 m x.5 mm i.d.,.00 μm N Elite-6 75 m x.5 mm i.d.,.00 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-Volatiles** 75 m x.5 mm i.d.,.55 μm N Elite-5 0 m x.5 mm i.d.,.50 μm N Elite-5ms** 0 m x.5 mm i.d.,.50 μm N Elite-5* 0 m x. mm i.d.,.00 μm N Elite-6* 0 m x.5 mm i.d.,.00 μm N Elite-6 75 m x.5 mm i.d.,.00 μm N Elite-Volatiles** 0 m x.5 mm i.d.,.55 μm N Elite-Volatiles** 75 m x.5 mm i.d.,.55 μm N969 7 Elite-5ms** 0 m x.5 mm i.d.,.00 μm N B Elite-Volatiles** 0 m x.5 mm i.d.,.0 μm N Elite-5* 0 m x. mm i.d.,.00 μm N Elite-5ms** 0 m x.5 mm i.d., 0.50 μm N Elite-5* 0 m x.5 mm i.d., 0.5 μm N Elite-5ms** 0 m x.5 mm i.d.,.00 μm N968 6 * Specified in EPA method. ** This column is highly recommended by PerkinElmer for this EPA method. The choice of column for this purge-and-trap method may depend on your sample concentrator to GC interface. 98

15 Capillary Column Applications Environmental Amines and Phenols U.S. EPA Method 508 Pesticides. Etridiazole (50 pg/μl). Chlorneb (000 pg/μl). Propachlor (000 pg/μl). Trifluralin (50 pg/μl) 5. a-bhc (0 pg/μl) 6. Hexachlorobenzene (0 pg/μl) 7. b-bhc (0 pg/μl) 8. g-bhc (0 pg/μl) 9. PCNB (impurity) (00 pg/μl) 0. PCNB (IS) (00 pg/μl). d-bhc (0 pg/μl). Chlorothalonil (50 pg/μl). Heptachlor (0 pg/μl). Aldrin (0 pg/μl) 5. DCPA (50 pg/μl) 6. DCB (SS) (5000 pg/μl) 7. Heptachlor Epoxide (0 pg/μl) 8. g-chlordane (0 pg/μl) 9. Endosulfan I (0 pg/μl) 0. a-chlordane (0 pg/μl) Column: Elite-5 Dimensions: 0 m, 0.5 mm i.d., 0.5 μm Sample:.0 μl splitless injection of a pesticide mix Splitless Hold: 0.75 min. Oven Temperature: 60 C to 00 C/min. (hold 0 min.) Injector: 50 C Detector: ECD, 0 C Carrier Gas: 0 cm/sec. N TIME (MIN.). Dieldrin (0 pg/μl). Endrin (0 pg/μl). Endosulfan II (0 pg/μl). Chlorobenzilate (000 pg/μl) 5. P, P'-DDD (50 pg/μl) 6. Endrin Aldehyde (50 pg/μl) 7. Endosulfan Sulfate (0 pg/μl) 8. P, P'-DDD (0 pg/μl) 9. Methoxychlor (00 pg/μl) 0. cis-permethrin (000 pg/μl). trans-permethrin (000 pg/μl) TIME (MIN.) Diethylamine. Pyridine. Morpholine. Phenol 5. Aniline 6. -Chlorophenol 7. Diethylenetriamine 8. Octylamine 9. -Methyl--Pyrrolidinone 0. -Nitrophenol., 6-Dimethylaniline. Nicotine. -Nitroaniline Column: Elite-5Amine Dimensions: 0 m, 0. mm i.d.,.0 μm Sample:.0 μl split injection of miscellaneous amines and phenols in water On-Column Conc.: ng Oven: 0 C to 0 0 C/min. Injector & Detector: 05 C Carrier Gas: Hydrogen Linear Velocity: 8 cm/sec. 0 C FID Sensitivity: 6. x 0- AFS Split Ratio: 5: N Capillary Column Applications Gas Chromatography See page for ordering information. For the most current product listing, visit 99

16 Capillary Column Applications Environmental Gas Chromatography Capillary Column Applications U.S. EPA Method 508 Organochlorine Pesticides TIME (MIN.) Column: Elite-CLPesticides Dimensions: 0 m, 0. mm i.d., 0.50 μm, Elite-CLPesticides (N9666) Dimensions: 0 m, 0. mm i.d., 0.5 μm, Elite-CLPesticides (N9666) EPA 508. list w/added compounds Oven: 0 C (hold min.) to 00 9 C/min. (hold 0 min.) Injector: Direct, Uniliner inlet liner, 00 C Dead Time:.797 (Elite-CLPesticides),.66 (Elite-CLPesticides) Head Pressure: psi (constant) Carrier Gas: Helium Flow:. 0 C 0,, 5,6 7 8,9 N9666 N ,9 6, 7, , Hexachloropentadiene. Etridiazole. Chlorneb. Hexachlorobenzene 5. Propachlor 6. a-bhc 7. Simazine 8. g-bhc 9. Atrazine 0. Trifluralin. Pentachloronitrobenzene. b-bhc. d-bhc. Metribuzin 5. Heptachlor 6. Aldrin 7. Chlorothalonil 8., '-Dibromobiphenyl 9. Alachlor , Metalachlor. DCPA (Dacthal ). Heptachlor Epoxide. g-chlordane. Cyanazine 5. a-chlordane 6., '-DDE 7. Endosulfan I 8. Dieldrin 9. Endrin 0. Chlorobenzilate., '-DDD. Endosulfan II., '-DDT. Endrin Aldehyde 5. Methoxychlor 6. Endosulfan Sulfate 7. cis-permethrin 8. trans-permethrin TIME (MIN.) 6 8, ,

17 Capillary Column Applications Environmental U.S. EPA Method 5. Column: Elite-6 (GC/MS) Dimensions: 75 m, 0.5 mm i.d.,.0 μm Sample: 0 ppm of 50. Standards Calibration Mixes -6 Oven: 5 C (hold 8 min.) to 0 C at 0 C/min. (hold min.) Detector: MS, 50 C Scan Range: 5-00AMU Purge: min. Purge and Trap: Tenax, Silica Gel, charcoal Desorb Preheat: 0 C, min. desorb at 5 C Desorb Flow Rate: 0 ml/min. Standards used are 5 Volatiles Kit:. Dichlorodifluoromethane. Chloromethane. Vinyl Chloride. Bromomethane 5. Chloroethane 6. Trichlorofluoromethane 7., -Dichloroethene 8. Methylene Chloride 9. trans-, -Dichloroethene 0., -Dichloroethane. cis-, -Dichloroethene., -Dichloropropane. Bromochloromethane. Chloroform 5.,, -trichloroethane 6. Carbon Tetrachloride U.S. EPA Method 55. N , -Dichloropropene 8. Benzene 9., -Dichloroethane 0. Trichloroethene., -Dichloropropane. Dibromomethane. Bromodichloromethane. cis-, -Dichloropropene 5. Toluene 6. trans-, -Dichloropropene 7.,, -Trichloroethane TIME (MIN.) , 8. Tetrachloroethene 9., -Dichloropropane 0. Dibromochloromethane., -Dibromoethane. Chlorobenzene.,,, -tetrachloroethane. Ethylbenzene 5. m-xylene 6. p-xylene 7. o-xylene 8. Styrene 6, , ,6 7,8 9. Bromoform 0. Isopropylbenzene. Bromobenzene.,,, -Tetrachloroethane.,, -Trichloropropane. Propylbenzene 5. -Chlorotoluene 6.,, 5-Trimethylbenzene 7. -Chlorotoluene 8. tert-butylbenzene 9.,, -Trimethylbenzene,, TIME (MIN.) Chloroform.,, -Trichloroethane. Carbon Tetrachloride. Trichloroacetonitrile 5. Trichloroethylene 6. Bromodichloromethane 7. Chloral Hydrate 8. Dichloroacetonitrile 9., -Dichloro--Propanone 0.,, -Trichloroethane. Chloropicrin , sec-butylbenzene 5., -Dichlorobenzene 5. p-isopropyltoluene 5., -Dichlorobenzene 5. n-butylbenzene 55., -Dichlorobenzene 56., -Dibromo--Chloropropane 57.,, -Trichlorobenzene 58. Hexachlorobutadiene 59. Naphthalene 60.,, -Trichlorobenzene. Dibromochloromethane., -Dibromoethane (EDB). Tetrachloroethylene 5. Bromochloroacetonitrile 6.,, -trichloro--propanone 7. Bromoform 8. Dibromoacetonitrile 9.,, -Trichloropropane 0. -Bromofluorobenzene (I.S.).,-Dibromo--Chloropropane (DBCP) Column: Elite-5 Dimensions: 0 m, 0.5 mm i.d.,.0 μm Sample:.0 μl split injection, ng on-column concentration Oven: 5 C (hold min.) to 00 C at 0 C/min. Injector: 00 C Detector: ECD, 90 C Carrier: Helium at 0 cm/sec. Split Ratio: 0: N96077 Capillary Column Applications Gas Chromatography See page for ordering information. For the most current product listing, visit 0

18 Capillary Column Applications Environmental Gas Chromatography Capillary Column Applications U.S. EPA Method 55. Chlorinated Disinfection Byproducts U.S. EPA Method 808 Pesticides Column: Elite-5 Dimensions: 0 m, 0. mm i.d., 0.50 μm Oven Temperature: 0 C (hold min.) to C/min. (hold 6 min.) Injector: 00 C Detector: ECD, 00 C Carrier Gas: Helium 5,6 8, 7 9 N967 0,.,,5,6-tetrachloro-m-xylene. a-bhc. g-ghc (lindane). b-bhc 5. d-bhc 6. Heptachlor 7. Aldrin 8. Heptachlor Epoxide 9. g-chlordane 0. a-chlordane.,'-dde Endosulfan I. Dieldrin. Endrin 5.,'-DDT 6. Endosulfan II 7.,'-DDD 8. Endrin Aldehyde 9. Methoxychlor 0. Endosulfan Sulfate. Endrin Ketone. Decachlorobiphenyl 8,9 0. Chloroform.,,-Trichloroethane. Carbon Tetrachloride. Trichloroacetonitrile 5. Trichloroethylene 6. Bromodichloromethane 7. Chloral Hydrate 8. Dichloroacetonitrile 9.,-Dichloro--Propanone 0.,, -Trichloroethane. Chloropicrin TIME (MIN.). Dibromochloromethane., -Dibromoethane (EDB). Tetrachloroethylene 5. Bromochloroacetonitrile 6.,,-Trichloro--Propanone 7. Bromoform 8. Dibromoacetonitrile 9.,, -Trichloropropane 0. -Bromofluorobenzene (IS)., -Dibromo--Chloropropane (DBCP) Column: Elite-00 Dimensions: 0 m, 0.5 mm i.d.,.0 μm Sample:.0 μl split injection, ng on-column concentration Oven: 5 C (hold min.) to 00 0 C/min. Injector/Detector: 00 C/90 C Carrier Gas: Helium Linear Velocity: 0 50 C ECD Sensitivity: 0 khz full scale Split Ratio: 0: TIME (MIN.) N

19 Capillary Column Applications Environmental U.S. EPA Method 808A Organochlorine Pesticides 6, , TIME (MIN.) TIME (MIN.) Dibromochloropropane. Hexachlorocyclopentadiene.,, 5, 6-Tetrachloro-m-Xylene. Hexachlorobenzene 5. cis-diallate 6. a-bhc 7. trans-diallate 8. g-bhc 9. b-bhc 0. d-bhc. Heptachlor. Aldrin. Isodrin. Heptachlor Epoxide 5. g-chlordane 6. a-chlordane 7., '-DDE 8. Endosulfan I 9. Dieldrin 0. Chlorobenzilate. Endrin.,'-DDD. Endosulfan II., '-DDT 5. Endrin Aldehyde 6. Methoxychlor 7. Endosulfan Sulfate 8. Endrin Ketone 9. Decachlorobiphenyl Column: Elite-CLPesticides and Elite-CLPesticides Dimensions: 0 m, 0. mm i.d., 0.50 μm, Elite-CLPesticides (N9666) Dimensions: 0 m, 0. mm i.d., 0.5 μm, Elite-CLPesticides (N96670) On-Column Conc.: 6 60 pg Oven: 80 C (hold min.) to 00 0 C/min. (hold 5 min.) Injector: Direct, Uniliner inlet liner Detector: ECD, 00 C, with Anode Purge Dead Time:.9 min. Head Pressure: 8.7 psi (constant) Flow Rate: 0 C N9666 N96670 Capillary Column Applications Gas Chromatography See page for ordering information. For the most current product listing, visit 0

20 Capillary Column Applications Environmental Gas Chromatography Capillary Column Applications U.S. EPA Method 80 Volatile Organics Column: Elite-Volatiles Dimensions: 0 ppb in 5 ml of RO Water. 75 m, 0.5 mm i.d.,.55 μm Concentrator: Purge and Trap Trap: Vocarb 000 Purge: min. at 0 ml/min. Dry Purge: min. at 0 ml/min. (MCS bypassed with Silcosteel tubing) Desorb Preheat: 5 C Desorb: 50 C for min. Bake: 60 C for 8 min. Interface: direct Transfer Line: 0. mm i.d. Oven: 5 C (hold min.) to 60 C at 5 C/min. (hold min.) to 0 C at 7 C/min. (hold min.) Carrier: Helium at 9 ml/min. Detectors: PID/ELCD PID: makeup 7 ml/min., purge 7 ml/min., set at 0.5 mv base temp 00 C ELCD: Reaction Gas 5mL/min. Reaction Temp.: 90 C, propanol flow 70 μl/min. PID 7 N969. Dichlorodifluoromethane. Chloromethane. Vinyl Chloride. Bromomethane 5. Chloroethane 6. Trichlorofluoromethane 7., -Dichloroethene 8. Methylene Chloride 9. Freon 0. trans-, -Dichloroethene. Methyl-tert-Butyl-Ether., -Dichloroethane. cis-, -Dichloroethene. Bromochloromethane 5. Chloroform 6., -Dichloropropane 7., -Dichloroethane 8.,, -Trichloroethane 9., -Dichloropropene 0. Carbon Tetrachloride. Benzene. Fluorobenzene. Dibromomethane., -Dichloropropane 5. Trichloroethene 6. Bromodichloromethane 7. -Chloroethylvinylether 8. cis-, -Dichloropropene 9. trans-, -Dichloropropene 0.,, -Trichloroethane 0. Toluene., -Dichloropropane. Dibromochloromethane., -Dibromoethane 5. Tetrachloroethene 6.,,, -Tetrachloroethane 7. Chlorobenzene 8. Ethyl Benzene 9. m-xylene 0. p-xylene. Bromoform. Styrene., -Dichlorobutane.,,, -Tetrachloroethane 5. o-xylene 6.,, -Trichloropropane 7. Isopropyl Benzene 8. Bromobenzene 9. n-propyl Benzene 50. -Chlorotoluene 5. -Chlorotoluene 5.,, 5-Trimethylbenzene 5. tert-butylbenzene 5.,, -Trimethylbenzene 55. sec-butylbenzene 56., -Dichlorobenzene 57., -Dichlorobenzene 58. p-isopropyl Toluene 59., -Dichlorobenzene 60. n-butylbenzene , -Bromo--Chloropropane 6. -Bromo--Chlorobenzene 6.,, -Trichlorobenzene 6. Naphthalene 65. Hexachlorobutadiene 66.,, -Trichlorobenzene ELCD TIME (MIN.) / enlarged view from PID

21 Capillary Column Applications Environmental U.S. EPA Method 860B Volatile Organics , TIME (MIN.). Carbon Dioxide. Dichlorodifluoromethane. Freon. Chloromethane 5. Vinyl Chloride 6. Bromomethane 7. Chloroethane 8. Trichlorofluoromethane 9. Ethanol 0. Diethyl Ether.,-Dichloroethene. Lodomethane. Carbon Disulfide. Freon 5. Acrolein 6. Allyl Chloride 7. Methylene Chloride 8. Acetone 9. trans-,-dichloroethene 0. Methyl Acetate. Methyl tert-butyl Eether. tert-butyl Alcohol Column: Elite-VMS Dimensions: 0 m, 0.8 mm i.d.,.0 μm Conc.: 5 ppb each in 5 ml of RO water Trap: Vocarb 000 Purge: 0 ml/min. Dry Purge: 0 ml/min. (MCS by-passed with Silcosteel Tubing) Desorb Preheat: 5 C Desorb: 50 C Desorb Flow Rate: 5 ml/min. Helium Bake: 8 60 C Interface: Plumbed through injection port N TIME (MIN.). Acetonitrile. Diisopropyl Ether 5. Chloroprene 6.,-Dichloroethane 7. Acrylonitrile 8. Vinyl Acetate** 9. Ethyl-tert-Butyl Ether** 0. cis-, -Dichloroethene., -Dichloropropane. Bromochloromethane. Chloroform. Carbon Tetrachloride 5. Ethyl Acetate 6. Methyl Acrylate 7. Dibromofluoromethane 8. Tetrahydrofuran 9.,,-Trichloroethane 0. -Butanone.,-Dichloropropene. Benzene. Propionitrile. Methacrylonitrile 5. Pentafluorobenzene 6. tert-amyl-methyl Ether 7., -Dichloroethane 8. Isobutyl Alcohol 9. Isopropyl Acetate 50. Trichloroethene 5., -Difluorobenzene 5. Dibromomethane 5., -Dichloropropane 5. Bromodichloromethane 55. Methyl Methacrylate 56. n-propyl Acetate 57. -Chloroethyl Vinyl Ether 58. cis-, -Dichloropropene 59. Toluene-d8 60. Toluene 6. -Nitropropane 6. Tetrachloroethene 6. -Methyl--Pentanone 6. trans-, -Dichloropropene 65. -Bromo--Chloropropane 66.,, -Trichloroethane * -Chloroethanol in 860B mix requires lower scan range for identification;, -Dioxane requires fortification or identification using single-point high-calibration standard. ** Peaks 8 & 9 share ion () , , , 5 8, , , Transfer Line: Silcosteel transfer line Mount Temperature: 0 C Split Ratio: :0 split Injector: 50 C Carrier Gas:. ml/min. Helium, constant flow Linear Velocity: 0 C Oven: 5 C (hold min.) to 60 C/min. (hold 0 min.) to 5 0 C/min. (hold 5 min.) Source Temperature: 80 C Scan Range: 5 60 amu Ionization: EI , Ethyl Methacrylate 68. Dibromochloromethane 69., -Dichloropropane 70., -Dibromoethane 7. n-butyl Acetate 7. -Hexanone 7. Chlorobenzene-d5 7. Chlorobenzene 75. Ethylbenzene 76.,,, -Tetrachloroethane 77. m-xylene 78. p-xylene 79. o-xylene 80. Styrene 8. Bromoform 8. Isopropylbenzene 8. n-amyl Acetate 8. -Bromo--Fluorobenzene (ss) 85. cis-,-dichloro--butene 86. n-propylbenzene 87. Bromobenzene 88., -Dichlorobutane 08 06, ,,, -Tetrachloroethane 90. -Chlorotoluene 9.,, 5-Trimethylbenzene 9.,, -Trichloropropane 9. trans-, -Dichloro--Butene 9. -Chlorotoluene 95. tert-butylbenzene 96. Pentachloroethane 97.,, -Trimethylbenzene 98. sec-butylbenzene 99. p-isopropyltoluene 00., -Dichlorobenzene 0., -Dichlorobenzene-d 0., -Dichlorobenzene 0. n-butylbenzene 0., -Dichlorobenzene 05., -Dibromo--Chloropropane 06. Nitrobenzene 07. Hexachlorobutadiene 08.,, -Trichlorobenzene 09. Naphthalene 0.,, -Trichlorobenzene Capillary Column Applications Gas Chromatography See page for ordering information. For the most current product listing, visit 05

22 Capillary Column Applications Environmental Gas Chromatography Capillary Column Applications U.S. EPA Method 860B Volatile Organics Column: Elite-Volatiles Dimensions: 0 m, 0.5 mm i.d.,.0 μm Conc.: TurboMatrix 0 Headspace Trap Trap: Air Monitoring Thermostating Time: 80 C Needle Temperature: 90 C Dry Purge: 5 min. Desorb Temperature: 80 C Desorb Time: 0.5 min. Oven Temperature: 0 C (hold min.) to 00 0 C/min. (hold 0 min.) to 0 0 C/min. (hold 5 min.) Carrier Gas: Helium at ml/min. Detector: MS Scan Time: 0.0 sec. Transfer Line Temperature: 00 C Source Temperature: 00 C Trap Emission: 75 μa N9688. Dichlorodifluoromethane. Chloromethane. Vinyl Chloride. Bromomethane 5. Chloroethane 6. Trichlorofluoromethane 7. Ethanol (500 ppb) 8.,-Dichloroethene 9. Carbon Disulfide (0 ppb) 0. Allyl Chloride. Methylene Chloride. Acetone. trans-, -Dichloroethene. Methyl tert-butyl Ether 5. tert-butyl Alcohol (00 ppb) 6. Disopropyl Ether 7.,-Dichloroethane 8. Acrylonitrile 9. Vinyl Acetate 0. Allyl Alcohol (50 ppb). Ethyl-tert-Buyl Ether. cis-, -Dichloroethene., -Dichloropropane. Bromochloromethane 5. Chloroform 6. Ethyl Acetate 7. Carbon Tetrachloride 8. Methyl Acrylate 9. Propargyl Alcohol (500 ppb) 0. Dibromofluoromethane (SMC). Tetrahydrofuran.,,-Trichloroethane. -Butanone.,-Dichloropropene 5. Benzene 6. Pentafluorobenzene (IS) 7. tert-amyl-methyl Ether 8., -Dichloroethane 9. Isobutyl Alcohol (500 ppb) 0. Isopropyl Acetate. Trichloroethene., -Difluorobenzene (SMC). Dibromomethane., -Dichloropropane 5. Bromodichloromethane 6. Methyl Methacrylate 7. n-propyl Acetate 8. -Chloroethanol (500 ppb) 9. cis-, -Dichloropropene 50. Toluene-d8 (SMC) TIME (MIN.) 5. Toluene 5. Pyridine (50 ppb) 5. Tetrachloroethene 5. -Methyl--Pentanone 55. trans-, -Dichloropropene 56.,, -Trichloroethane 57. Ethyl Methacrylate 58. Dibromochloromethane 59., -Dichloropropane 60., -Dibromoethane 6. n-butyl Acetate 6. -Hexanone 6. -Picoline (50 ppb) 6. Chlorobenzene-D5 (IS) 65. Chlorobenzene 66. Ethylbenzene 67.,,, -Tetrachloroethane 68. m-xylene 69. p-xylene 70. o-xylene 7. Stryrene 7. Bromoform 7. Isopropylbenzene 7. -Bromo--Fluorobenzene (SMC) 75. Bromobenzene 76. n-propylbenzene 77.,,, -Tetrachloroethane 78. -Chlorotoluene 79.,, 5-Trimethylbenzene 80.,, -Trichloropropane 8. -Chlorotoluene 8. tert-butylbenzene 8. Pentachloroethane 8.,, -Trimethylbenzene 85. sec-butylbenzene 86. p-isopropyltoluene 87., -Dichlorobenzene 88., -Dichlorobenzene-d (IS) 89., -Dichlorobenzene 90. n-butylbenzene 9., -Dichlorobenzene 9., -Dibromo--Chloropropane 9. Nitrobenzene (50 ppb) 9. Hexachlorobutadiene 95.,, -Trichlorobenzene 96. Naphthalene 97.,, -Trichlorobenzene 06

23 Capillary Column Applications Environmental U.S. EPA Method 870 Semi-Volatile Organics 6,7, 8 0,. n-nitrosodimethylamine. Pyridine. Methyl Methanesulfonate. -Fluorophenol 5. Ethyl Methanesulfonate 6. Phenol-d6 7. Phenol 8. Aniline 9. Bis(-chloroethyl)ether 0. -Chlorophenol-d. -Chlorophenol., -Dichlorobenzene., -Dichlorobenzene-d., -Dichlorobenzene 5. Benzyl Alcohol 6., -Dichlorobenzene-d 7., -Dichlorobenzene 8. -Methylphenol 9, 5 6, ,7 0 0, 5 6 7,8 9, Bis(-chloroisopropyl)ether 0. -Methylphenol/ -Methylphenol. n-nitroso-di-n-propylamine. Acetophenone. Hexachloroethane. Nitrobenzene-d5 5. Nitrobenzene 6. Isophorone 7., -Dimethylphenol 8. -Nitrophenol 9. Benzoic Acid 0. Bis (-Chloroethoxy) Methane., -Dichlorophenol.,, -Trichlorobenzene. Naphthalene-d8. Naphthalene 5., 6-Dichlorophenol , , Chloroaniline 7. Hexachloropropene 8. Hexachlorobutadiene 9. -Chloro--Methylphenol 0. Isosafrole. -Methylnaphthalene. -Methylnaphthalene. Hexachlorocyclopentadiene.,,, 5-Tetrachlorobenzene 5.,, 6-Trichlorophenol 6.,, 5-Trichlorophenol 7. -Fluorobiphenyl 8. Safrole 9. -Chloronaphthalene 50. -Nitroaniline 5., -Naphthoquinone 5. Dimethylphthalate 5., -Dinitrobenzene , , 6-Dinitrotoluene 55. Acenaphthylene 56. -Nitroaniline 57. Acenaphthene-d0 58. Acenaphthene 59., -Dinitrophenol 60. -Nitrophenol 6. Pentachlorobenzene 6.,-Dinitrotoluene 6. Dibenzofuran 6.,,, 6-Tetrachlorophenol 65. Diethyl Phthalate 66. -Chlorophenyl Phenyl Ether 67. Fluorene 68. -Nitroaniline 69.,6-Dinitro--Methylphenol 70. Diphenylamine 7. Azobenzene , , ,, 6-Tribromophenol 7. Phenacetin 7. -Bromophenyl-Phenyl ether 75. Hexachlorobenzene 76. Pentachlorophenol 77. Pentachloronitrobenzene 78. Dinoseb 79. Phenanthrene-d0 80. Phenanthrene 8. Anthracene 8. Di-n-Butylphthalate 8. -Nitroquinoline--Oxide 8. Isodrin 85. Fluoranthene 86. Benzidine 87. Pyrene 88. Aromite 89. p-terphenyl-d 0, TIME (MIN.) Column: Elite-5 ms Dimensions: 0 m, 0.5 mm i.d., 0.5 μm Sample: 80 ng splitless injection of CLP standard Oven: 0 C (hold min.) to 90 C at 0 C/min. (hold 0 min.) to 0 C at C/min. (hold 0 min.) to 0 C at 6 C/min. (hold min.) Injector: 00 C Detector: MS, 80 C, scan range AMU Carrier: Helium at.0 ml/min. N Chlorbenzilate 9. Butyl Benzyl Phthalate 9. Kepone 9. Bis(-ethylhexyl)phthalate 9., '-Dichlorobenzidine 95. Benzo (a) Anthracene 96. Chrysene-d 97. Chrysene 98. Di-n-Octyl Phthalate 99. Benzo (k) Fluoranthene 00. Benzo (b) Fluoranthene 0. Benzo (a) Pyrene 0. Perylene-d 0. -Methylcholanthrene 0. Indeno (,, -cd) Pyrene 05. Dibenzo (a, h) Snthracene 06. Benzo (g, h,i) Perylene Capillary Column Applications Gas Chromatography See page for ordering information. For the most current product listing, visit 07

24 Capillary Column Applications Environmental Gas Chromatography Capillary Column Applications Essential Oils Citronella Java Oil. Limonene. Citronellal. Linalool. Borneol 5. γ-elemene 6. β-caryophyllene 7. Neryl Acetate 8. α-terpineol 9. Germancrene-Δ 0. β-citronellol. Geranyl Acetate. δ-cadenene. Nerol. Geraniol 5. Eugenol 6. α-bergamotene TIME (MIN.) 6 Column: Elite- Dimensions: 60 m, 0.5 mm i.d., 0.5 μm Sample:.0 μl split injection of Citronella Java Oil Oven: 00 C to 60 C at C/min. (hold min.) Injector: 50 C Detector: MS, 80 C Carrier: Helium at 0 cm/sec. Split Vent: 00 cc/min. 9 6 N Nitrogen Containing Herbicides. Eptam. Sutan. Vernam. Tillam 5. Ordram 6. Propachlor 7. Ro-Neet 8. Treflan 9. Balan 0. Simazine. Atrazine. Propazine. Tolban. Terbacil 5. Sencor 6. Bromacil 7. Dual 8. Paarlan 9. Prowl 0. Oxadiazon. GOAL. Hexazinone TIME (MIN.) Column: Elite-5 Dimensions: 0 m, 0.5 mm i.d., 5.0 μm Sample: 0. μl direct injection of nitrogen containing herbicides. Concentration approximately 0 ng per component. Oven Temperature: 60 C (hold min.) to 90 5 C/min. (hold 5 min.) Injector: 90 C Detector: FID, 90 C Carrier Gas: 0 cm/sec. 0 N960 08

25 Capillary Column Applications Environmental Pesticides. Tetrachloro-m-xylene. a-bhc. g-bhc. Heptachlor 5. Aldrin 6. b-bhc 7. d-bhc 8. Heptachlor Epoxide Synthetic Essential Oil Mixture, 6,7 5 8, ,, Endosulfan I 0. g-chlordane. a-chlordane. P, P'-DDE. Dieldrin. Endrin 5. P, P'-DDD 6. Endosulfan II Column: Elite-5 Dimensions: 0 m, 0.5 mm i.d., 5.0 μm Sample:.0 μl direct injection of a pesticide mix. Concentration: ppb (ng/ml) Oven Temperature: 50 C (hold 5 min.) to 75 C/min. (hold 5 min.) Injector: 00 C Detector: ECD, 75 C Carrier Gas: 0 cm/sec. N , TIME (MIN.) P, P'-DDT 8. Endrin Aldehyde 9. Endosulfan Sulfate 0. Methoxychlor. Endrin Ketone. Decachlorobiphenyl TIME (MIN.) Ethyl Butyrate. trans--hexenol. α-pinene. Benzaldehyde 5. Camphene 6. Octanol 7. β-myrcene 8. β-pinene 9. α-phellandrene 0. p-cymene. l-limonene. Camphor. trans-sabinene Hydrate. Linalool 5. Citronellal 6. l-menthone 7. Menthofuran 8. l-menthol 9. α-terpineol 0. Linalyl Acetate. β-citronellol. Nerol. Carveol. Anisaldehyde 5. Carvone 6. Geraniol 7. Anethole 8. Cinnamic Alcohol 9. Eugenol 0. Neryl Acetate. Geranyl Acetate. Vanillin. Coumarin. α-ionone 5. Ethyl Vanillin 6. β-caryophyllene 7. α-caryophyllene 8. β-ionone 9. Valencene 0. Ethyl Laurate. Amyl Cinnamic Aldehyde. Nootketone Column: Elite- Dimensions: 60 m, 0.5 mm i.d., 0.5 μm Sample:.0 μl split injection of flavor components Oven: 00 C to 60 C at C/min. (hold min.) Injector: 50 C Detector: 80 C Carrier: Helium at 0 cm/sec. Split Vent: 00 cc/min. N960 0 Capillary Column Applications Gas Chromatography See page for ordering information. For the most current product listing, visit 09

26 Capillary Column Applications Food and Flavors Gas Chromatography Capillary Column Applications Brewing Beer. Chloroform., -Butanedione (Diacetyl)., -Pentanedione TIME (MIN.) Essential Oils Lemon Oil 5 6 7, TIME (MIN.) Column: Elite BAC- Dimensions: 0 m x 0. mm x.8 μm Instrument: Headspace TurboMatrix 0 Table : HS Conditions Sample Temperature: 60 C Needle Temperature: 80 C Transfer Line Temperature: 00 C Equilibration Time: 5 min. Pressurization Time:.0 min. Injection Time: 0. min. Withdrawal Time: 0.0 min. Carrier Pressure: 5 psi Table : GC with ECD Conditions Initial Temperature: 5 C Time :. min. Rate : 0 C/min. Final Temperature: 50 C Hold: 0.6 min Injector Temperature: 00 C Liner: Zero Dilution Split: 5 ml/min. ECD: 50 C ECD Attenuation: Makeup Gas (Argon/Methane) 0 ml/min , Heptanol. α-thujene. α-pinene. Camphene 5. Sabinene 6. β-pinene 7. 6-Methyl-5-Hepten--One 8. Myrcene 9. Octanal 0. α-phellandrene. -Carene. α-terpinene. π-cymene. Limonene 5. γ-terpinene 6. Octanol 9 7. Terpinolene 8. Linalool 9. Nonanal 0. Citronellal. Terpinen--ol. α-terpineol. Decanol. Octyl Acetate Nerol 6. Neral 7. Carvone 8. Geraniol 9. Geranial 0. Nonyl Acetate. Citronellyl Acetate. Neryl Acetate N96579 Column: Elite-5 Dimensions: 0 m, 0. mm i.d., 0.5 μm Sample: Wet needle split injection of a neat lemon oil Oven: 75 C (hold 8 min.) to 50 C at C/min. Injector: 50 C Detector: FID, 50 C Carrier: Hydrogen at 0 cm/sec. Split Ratio: 00: N Geranyl Acetate. Dodecanal 5. β-caryophyllene 6. trans-α-bergamotene 7. α-humulene 8. β-bisabolene 0

27 Capillary Column Applications Food and Flavors 67 5 Column: Elite-WAX ETR Dimensions: 60 m, 0.5 mm i.d., 0.5 μm Sample: 0. μl split injection of a neat spearmint oil Oven: 75 C (hold min.) to 00 C at C/min. (hold 0 min.) Injector: 50 C Detector: FID, 50 C Carrier: Hydrogen at 0 cm/sec. Split Ratio: 00: N Capillary Column Applications Essential Oils Native Spearmint Oil α-pinene β-pinene Sabinene Myrcene α-terpinene L-Limonene TIME (MIN.) , 8-Cineole cis-ocimene γ-terpinene p-cymene Terpinolene -Octyl Acetate Octanol L-Menthone trans-sabinenehydrate β-bourbonene Linalool Terpinene--ol 8 0 β-caryophyllene Dihydrocarvone trans-dihydrocarvyl Acetate trans-β-farnesene α-terpineol Germacrene-Δ Carvone cis-carvyl Acetate trans-carveol cis-carveol cis-jasmone Viridiflorol Essential Oils Synthetic Mushroom Aroma Acetone Ethyl Acetate Methylene Chloride Hexanal Amyl Acetate -Butanol -Methyl--Butanol -Pentanol -Octanone -Octanol Nonanal -Octen--ol Furfural Benzaldehyde Octyl Alcohol Phenylacetaldehyde α-terpineol, -Nonadienal, -Decadienal Benzyl Alcohol TIME (MIN.) Gas Chromatography Column: Elite-WAX ETR Dimensions: 0 m, 0. mm i.d.,.0 μm Sample:.0 μl split injection of a synthetic mushroom aroma, concentration 0 ng per component Oven: 0 C to 0 C at 6 C/min. Injector: 60 C Detector: FID, 60 C Carrier: Hydrogen at 0 cm/sec. Split Ratio: 00: N96557 See page for ordering information. For the most current product listing, visit

28 Capillary Column Applications Food and Flavors Gas Chromatography Capillary Column Applications Sugars As Alditol Acetates TCA in Wine TCA 7 00 % 0 TIME (MIN.) Natural Wine Separation Products. TCA SIR of Channels El+ TIC 566. Rhamnitol. Fucitol. Ribitol. Arabinitol 5. Mannitol 6. Galactitol 7. Glucitol 8. Inositol Column: Elite-5 Dimensions: 5 m, 0.5 mm i.d., 0.5 μm Sample: 0.5 μl split injection of alditol acetate derivatives Oven: 90 C (hold 5 min.) to 50 C at 8 C/min. (hold 5 min.) Injector: 60 C Detector: 60 C Carrier: Helium at cm/sec. Split Ratio: 50: N9675 Column: Elite-5ms Dimensions: 0 m x 0.5 mm x 0.5 μm Instrument: Clarus 500 GC/MS Oven: 50 C (hold min.) to 0 C at 0 C/min. (hold 5 min.) Injector: 50 C Carrier: Helium (99.999%) Instrument: TurboMatrix Headspace HS-0 Trap Needle Temperature: 75 C Transfer Line Temperature: 75 C Oven Temperature: 75 C Trap Low Temperature: 0 C Trap High Temperature: 80 C Dry Purge Time: 5 min. Trap Hold Time: 5 min. Desorb Pressure Time: 0 min. Thermostatting Time: 0 min. Pressurization: min., cycles Decay Time:. min. Vial Pressure: 0 psi Column Pressure: 5 psi Trap Sorbent: CarboPack Y TIME (MIN.) N968

29 Capillary Column Applications Forensics/Clinical Toxicology Anabolic Steroids Underivatized Cannabinoids TMS Derivatives 0, TIME (MIN.) Column: Elite-5 Dimensions: 5 m, 0.5 mm i.d., 0.5 μm Sample:.0 μl splitless injection of cannabinoids, concentration 00 μg/ml Oven: 50 C (hold 0.5 min.) to 5 C at 0 C/min., to 5 C at 0 C/min. Injector: 5 C Detector: MS, 0 C Carrier: Helium at 0 cm/sec. Splitless Hold Time: 0.75 min. Scan Range: AMU N9607. Cannabidiol. Δ 8 -Tetrahydrocannabinol. Δ 9 -Tetrahydrocannabinol. Cannibinol 5. -Hydroxy-Δ 9 -Tetrahydrocannabinol 6. -Nor-Δ 9 -Tetrahydrocannabinol Carboxylic Acid 7. -Nor-Δ 8 -Tetrahydrocannabinol Carboxylic Acid Column: Elite-5 Dimensions: 0 m, 0.5 mm i.d., 0.0 μm Sample: 0.5 μl split injection of anabolic steroids Concentration 000 ng/μl Oven: 80 C to 0 C at 0 C/min. (hold min.) Injector: 80 C Detector: FID, 0 C Carrier: Helium at 5 cm/sec. Split Ratio: 50: TIME (MIN.) 9 N Androstene-β,7β-diol. 7α-Methyl-5-Androstene-β,7β-Diol. 5α-Androstan-7β-ol--One. 9-Nortestosterone 5. 7α-Methylandrostan-7β-ol--One 6. Mesterolone 7. Testosterone 8. 7α-Methyltestosterone 9. -Dehydrotestosterone 0. -Dehydro-7α-Methyltestosterone. Bolasterone. Oxymethalone. 9-Nortestosterone-7-Propionate. Testosterone Propionate 5. Fluoxymesterone 6. -Chlorotestosterone-7-Acetate 7. Testosterone-7β-Cypionate 8. -Dehydrotestosterone Benzoate 9. -Dehydrotestosterone Undecylenate Capillary Column Applications Gas Chromatography See page for ordering information. For the most current product listing, visit

30 Capillary Column Applications Forensics/Clinical Toxicology Gas Chromatography Capillary Column Applications Blood Alcohol Blood Alcohol TIME (MIN.) TIME (MIN.) 6 Column: Elite-BAC- Dimensions: 0 m x 0. mm x.8 μm Sample:.0 ml Blood Alcohol Mix Oven: 0 C Isothermal Injector: 00 C Carrier: Helium Sample Equilibration Temperature: 70 C Sample Equilibration Time: 5 min. Vial Pressure: 0 psi Vial Pressurization Time: 0.5 min. Vial Sampling Time: 0.0 min. Transfer Line: 0. mm i.d. FS Hydroguard TM Tubing (N9057) Transfer Line Temperature: 00 C Injection Port Sleeve: mm i.d. Split Flow: 0 ml per min. N96579 Conc. w/v. Methanol 0.%. Acetaldehyde 0.%. Ethanol 0.%. Isopropanol 0.% 5. Acetone 0.0% 6. n-propanol 0.% Column: Elite-BAC- Dimensions: 0 m x 0. mm x. μm Sample:.0 ml Blood Alcohol Mix Oven: 0 C Isothermal Injector: 00 C Carrier: Helium Sample Equilibration Temperature: 70 C Sample Equilibration Time: 5 min. Vial Pressure: 0 psi Vial Pressurization Time: 0.5 min. Vial Sampling Time: 0.0 min. Transfer Line: 0. mm i.d. FS Hydroguard Tubing (N9057) Transfer Line Temperature: 00 C Injection Port Sleeve: mm i.d. Split Flow: 0 ml per min. N96577 Conc. w/v. Methanol 0.%. Acetaldehyde 0.%. Ethanol 0.%. Isopropanol 0.% 5. Acetone 0.0% 6. n-propanol 0.%

31 Capillary Column Applications Forensics/Clinical Toxicology Cocaine and Metabolites TIME (MIN.) Sympathomimetic Amines HFBA Derivatives. Amphetamine - HFBA. Phentermine - HFBA. Phenylpropanolamine - HFBA. Ephedrine - HFBA 5. Methamphetamine - HFBA 6. Fenfluramine - HFBA 7. Pseudoephedrine - HFBA 8. Methylenedioxyamphetamine - HFBA 9. Methylenedioxymethamphetamine - HFBA 0. Methylphenidate - HFBA Ecgonine Methyl Ester (TMS). Ecgonine (TMS). Cocaine. Coca Ethylene 5. Benzoylecgonine (TMS) Column: Elite-5 Dimensions: 0 m, 0.5 mm i.d., 0.5 μm Sample:.0 μl split injection of cocaine and cocaine metabolites Oven: 50 C to 0 C at 0 C/min. Injector: 50 C Detector: FID, 00 C Carrier: Helium at 0 cm/sec. Split Ratio: 0: Column: Elite-5 Dimensions: 0 m, 0.5 mm i.d., 0.5 μm Sample:.0 μl splitless injection of sympathomimetic amines Concentration approximately.5 ng/μl Oven: 0 C (hold min.) to 50 C at 0 C/min., to 00 C at 5 C/min. Injector: 5 C Detector: MS, 75 C Carrier: Helium at 0 cm/sec. Splitless Hold Time: min TIME (MIN.) 9 N N96076 Capillary Column Applications Gas Chromatography See page for ordering information. For the most current product listing, visit 5

32 Capillary Column Applications Industrial Chemicals Gas Chromatography Capillary Column Applications Alcohols and Aldehydes Column: Elite-WAX ETR Dimensions: 60 m, 0.5 mm i.d.,.0 μm Sample:.0 μl split injection of alcohols and aldehydes Oven: 5 C (hold 0 min.) to 50 C at C/min. (hold 0 min.) Injector: 50 C Detector: MS, 85 C Carrier: Helium at 50 cm/sec. Split Ratio: 7: Alcohol Mixtures Column: Elite-WAX ETR Dimensions: 60 m, 0.5 mm i.d.,.0 μm Sample:.0 μl split injection of alcohols Oven: 5 C (hold 0 min.) to 50 C at C/min. (hold 0 min.) Injector: 50 C Detector: MS (EI), 50 C Carrier: Helium at 5 cm/sec. Split Ratio: 8:. Pentane. Hexane. Heptane. Ethanol 5. Decane 6. -Propanol N9657 N TIME (MIN.) Butanol 8. Dodecane 9. -Pentanol 0. -Hexanol. Tetradecane. -Heptanol 9 0. Pentane. Heptane. Acetaldehyde. Dimethoxy Methane 5. Butyraldehyde 6. -Pentanol 7. -Penten--ol 8. -Octanol 9. Cyclohexanol 0. Furfural. Pentadecane. Benzaldehyde. Ethylene Glycol and -Methyl-, -Pentanediol. Furfuryl Alcohol 5. Nonadecane 6., -Butanediol 7. Diethylene Glycol TIME (MIN.). -Octanol. Hexadecane 5. -Nonanol 6. -Decanol 7. -Undecanol 8. -Dodecanol 6. Pentane. Methanol. -Methyl--Propanol (tert-butylalcohol). -Methyl--Buten--ol 5. -Buten--ol 6. Undecane 7., -Dimethyl--Propanol (Neopentanol) 8. -Penten--ol 9. -Methoxyethanol 0.,, -Trifluoroethanol , Ethoxyethanol. -Pentanol. -Methyl--Pentanol., -Dimethyl--Pentanol 5. Tetradecane 6. trans--hexen--ol 7. -Octanol 8. Ethylene Glycol 9. -Undecanol 0., -Butanediol TIME (MIN.)

33 Capillary Column Applications Industrial Chemicals Aldehydes Amines and Phenols TIME (MIN.) TIME (MIN.) Ethanal. Propanal. Butenal. Pentanal 5. Hexanal 6. Heptanal 7. Octanal 8. Nonanal 9. Decanal 0. Undecanal Column: Elite-WAX Dimensions: 0 m, 0.5 mm i.d., 0.50 μm Sample: Split injection of C-C aldehydes mixture, on-column concentration: 50 ng Oven: 0 C (hold 5 min.) to 00 C at 0 C/min. Injector: 00 C Detector: 00 C Carrier: Hydrogen at 5 cm/sec. Split Ratio: 00: N960. Diethylamine. Pyridine. Morpholine. Phenol 5. Aniline 6. -Chlorophenol 7. Diethylenetriamine 8. Octylamine 9. -Methyl--Pyrrolidinone 0. -Nitrophenol., 6-Dimethylaniline. Nicotine. -Nitroaniline Column: Elite-5Amine Dimensions: 0 m, 0. mm i.d.,.0 μm Sample:.0 μl split injection of miscellaneous amines and phenols in water On-Column Conc.: ng Oven: 0 to 0 0 C/min. Injector: 05 C Linear Velocity: 8 cm/sec. 0 C FID Sensitivity: 6. x 0- AFS Split Ratio: 5: N96677 Capillary Column Applications Gas Chromatography See page for ordering information. For the most current product listing, visit 7

34 Capillary Column Applications Industrial Chemicals Gas Chromatography Capillary Column Applications Aromatics Column: Elite-WAX ETR Dimensions: 60 m, 0.5 mm i.d.,.0 μm Sample:.0 μl split injection of an aromatics mixture Oven: 0 C (hold 0 min.) to 5 C at C/min. (hold 0 min.) Injector: 50 C Detector: MS, 80 C Carrier: Helium at 50 cm/sec. Split Ratio: 7: N9657 Industrial Solvents. Pentane. Hexane. Methyl Formate. Acetone 5. Tetrahydrofuran 6.,, -Trichloroethane 7. Ethyl Acetate 8. Methanol 9. Methylethyl Ketone 0. Methylene Chloride. Chloroform. Benzene. n-propyl Alcohol. sec-butyl Alcohol 5. Toluene 6. n-butyl Acetate 7. Isobutyl Alcohol 8. n-butyl Alcohol 9. o-xylene 0. Ethoxyethane. trans-decahydronaphthalene., -Xylene. cis-decahydronaphthalene.,, 5-Trimethylbenzene 5. p-cymene or p-isopropyltoluene 6.,, -Trimethylbenzene 7. α-methyl Benzene 8.,, -Trimethylbenzene TIME (MIN.) 9. Diisopropylbenzene 0. Triethylbenzene. Pentadecane. Nitrobenzene. Nonadecane. o-cresol 5. Bibenzyl ,9 5 6,7 0, 5 Column: Elite-MWAX Dimensions: 0 m, 0.5 mm i.d.,.0 μm Sample: Wet needle injection of neat solvents Oven: 50 C to 0 C at 0 C/min. Injector: 50 C Detector: FID, 50 C Carrier: Helium at 0 cm/sec TIME (MIN.) Industrial Solvents. Pentane. Hexane. Methyl Formate. Acetone 5. Tetrahydrofuran 6.,, -Trichloroethane 7. Ethyl Acetate 8. Methanol 9. Methylethyl Ketone 0. Methylene Chloride. Chloroform. Benzene. n-propyl Alcohol. sec-butyl Alcohol 5. Toluene 6. n-butyl Acetate 7. Isobutyl Alcohol 8. n-butyl Alcohol 9. o-xylene 0. Ethoxyethane 8,9 6,7 Column: Elite-WAX ETR Dimensions: 0 m, 0.5 mm i.d.,.0 μm Sample: Wet needle injection of neat solvents Oven: 50 C to 0 C at 0 C/min. Injector: 50 C Detector: 50 C Carrier: Helium at 0 cm/sec. 5 0, TIME (MIN.) N9678 N

35 Capillary Column Applications Petroleum Prudhoe Bay Crude Oil. Benzene. Heptane. Toluene. Octane 5. m-xylene and p-xylene 6. o-xylene 7. Nonane 8. Decane 9. Undecane 0. Dodecane Volatile Hydrocarbons Tridecane. Tetradecane. Pentadecane. Hexadecane 5. Heptadecane 6. Pristane 7. Octadecane 8. Phytane 9. Nonadecane 0. Eicosane Heneicosane. Docosane. Tricosane. Tetracosane 5. Pentacosane 6. Hexacosane 7. Heptacosane 8. Octacosane Column: Elite- Dimensions: 0 m, 0.5 mm i.d.,.0 μm Sample: 0. μl split injection of Prudhoe Bay crude oil Oven: 0 C to 85 C at 5 C/min. (hold 0 min.) Injector: 85 C Detector: 85 C Carrier: Hydrogen at 0 cm/sec. Split Ratio: 50: TIME (MIN.), , TIME (MIN.) N Methane. Ethylene. Acetylene. Ethane 5. Propylene 6. Propane 7. Cyclopropane 8. Propadiene 9. Propyne 8 0. Isobutane., -Butadiene. -Butene. n-butane. cis--butene 5. trans--butene 6. Isopentane 7. n-pentane Column: Elite-Q PLOT Dimensions: 0 m, 0. mm i.d. Sample: 00 μl split injection (0:), 000 ppm Oven: 50 C ( min.) to 0 C at 5 C/min. Injector: 50 C Detector: FID, 50 C Carrier: Helium at cm/sec. Split Flow: 0 ml/min. N9659 Capillary Column Applications Gas Chromatography See page for ordering information. For the most current product listing, visit 9

36 Capillary Columns Phase Cross-Reference Gas Chromatography Capillary Columns Phase Phase Description Equivalent Phase Elite-, Elite-ht 00% Dimethyl Packed: OV-, OV-0, SP-00, DC-00, UC-W98, S 96, CP-Sil 5, SE-0 Capillary: DB-, DB-ht, HP-, HP-0, Ultra-, SPB-, CP-Sil 5CB, Cl-Sil5CBMS, RSL-50, RSL-60, Rtx-, BP-, CB-, OV-, 007-(MS), SP-00, SE-0 Elite-5, Elite-5ht, 5% Diphenyl 95% Dimethyl Packed: OV-, OV-7, Dexsil 00, Fluorolube, CP-Sil 8 Elite-5ms Capillary: DB-5, DB-5ms, DB-5ht, HP-5, Ultra-, SPB-5, CP-Sil 8CB, RSL-00, Rtx-5, BP-5, CB-5, OV-5, 007-(MPS-5), SE-5, SE-5, XTI-5, Rtx-5 ms, PTE-5, HP-5MS Elite-5Amine 5% Diphenyl 95% Dimethyl Polysiloxane Rtx-5Amine; PTA-5 Elite-7, Elite-7ht, 50% Phenyl 50% Methyl Packed: OV-7, OV-, OV-, SP-50, DC-70 Elite-7ms Capillary: DB-7, DB-7ht, HP-7, RSL-00, Rtx-50, 007-7(MPS-50), SP-50, HP-50+ Elite-5, Elite-5ms 5% Phenyl 65% Methyl Capillary: DB-5, DB-5ms, Rtx-5, SPB-5, AT-5, Sup-Herb Elite-00 Trifluoropropylmethyl Polysiloxane DB-0; AT-0; VF-00MS; 007-0; Rtx-00 Elite-5 50% Cyanopropylmethyl Packed: OV-5, Silar 5 CP 50% Phenylmethyl Capillary: DB-5, HP-5, SP-0, CP-Sil CB, RSL-500, Rtx-5, BP-5, CB-5, OV-5, Elite-608 Specialty phase for semivolatile pesticides (U.S. EPA 608) Capillary: SPB-608, NON-PAKD Pesticide, DB-608, , HP-608 Elite-6, Specialty phase for volatiles Capillary: DB-6, DB-VRX, VOCOL, NONPAKD AT-6, Rtx-Volatiles, Elite-Volatiles (U.S. EPA 6 and 50.) Rtx-50., 007-6, , HP-6, CP-6, Rtx-6 Elite-0 6% Cyanopropylphenyl 9% Methyl Capillary: DB-0, Rtx-0, CP-6 Elite-70 % Cyanopropylphenyl 86% Dimethyl Packed: OV-70 Capillary: DB-70, SPB-7, CP-Sil 9CB, Rtx-70, BP-0, CB-70, OV-70, Elite-Alumina PLOT phase for analysis Packed: Alumina of light hydrocarbons Capillary: GS-Alumina, Al O /KC, Al O /Na SO, RT-Alumina Elite-Betacydex Betacyclodextrin for chiral separations Capillary: Cyclodex-B, LIPODEX C, Chirasil-D/L-Val, Rt-bDEXm Elite-CLPesticides Specialty phase for chlorinated pesticides Rtx-CLPesticides Elite-CLPesticides Specialty phase for chlorinated pesticides Rtx-CLPesticides Elite-FFAP Polyethylene Glycol Acid Modified Packed: OV-5, FFAP, Carbowax 0M-Terephthalic acid Capillary: DB-WAX, HP-FFAP, Nukol, SUPEROX FA, STABILWAX-DA, 007-FFAP, OV-5, DB-FFAP Elite-Molesieve PLOT phase for analysis Packed: Molesieve 5A of permanent gases Capillary: GS-Molesieve, Molesieve 5A, #PLT-5A, Rt-Molesieve 5A Elite-PONA Dimethylpolysiloxane processed for detailed analysis of petroleum naphtha Capillary: DB-Petro00, Petrocol DH, HP-PONA, SPB-, 007-, Rtx- PONA Elite-Q PLOT phase for analysis Packed: Chomosorb 0, HayeSep Q, Porapak Q of light gases and hydrocarbons Capillary: GS-Q, PoraPLOT Q, Rt-QPLOT Elite-VMS Specialty phase for U.S. EPA Volatile Organics Rtx-VMS Elite-WAX Polyethylene Glycol Packed: Carbowax 0M, SUPEROX, SUPELCOWAX 0, PEG Capillary: DB-FFAP, HP-0M, SUPELCOWAX 0, CP-WAX 5CB, SUPEROX II, CB-WAX, STABILWAX, BP-0, Elite-CW, 007-CW, Carbowax, HP-Innowax 0

37 Capillary Columns PerkinElmer Elite Series Capillary Columns Elite- Dimethylpolysiloxane 00% Dimethyl Polysiloxane phase: The 00% Dimethyl Polysiloxane is a highly versatile phase that is extremely rugged, exhibiting long column lifetime, low bleed, and high maximum operating temperatures. Primary applications: Elite columns are ideal for the analysis of non-polar petrochemical samples, such as detailed hydrocarbon analysis, hydrocarbon gases, petroleum oxygenates, petroleum aromatics, fuels, waxes, oils, sulfur compounds, mercaptans, and carbon disulfide. It also is an excellent phase for solvents, chemicals, flavors, fragrances, essential oils, air toxins, chlorofluorocarbons, arson analysis, and high-temperature applications. Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 0/50 N to 0/50 N to 0/50 N to 0/0 N to 0/50 N to 0/0 N to 0/50 N to 0/0 N to 0/0 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/0 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/0 N to 00/0 N to 0/50 N to 0/50 N to 0/0 N to 80/00 N to 60/80 N to 0/50 N to 0/50 N to 0/50 N to 0/0 N to 80/00 N to 60/80 N to 0/50 N to 0/50 N to 0/0 N to 80/00 N to 60/80 N * to 60/80 N * to 0/60 N * to 0/0 N * to 0/0 N * to 70/90 N * to 60/80 N * to 0/0 N * to 0/0 N * to 70/90 N Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) 0.5* to 60/80 N * to 0/0 N * to 70/90 N to 70/90 N to 0/0 N to 0/0 N to 0/0 N to 70/90 N to 70/90 N to 0/0 N to 0/0 N to 70/90 N to 70/90 N to 0/0 N * Ferrule size same as 0.5. Elite-ht (High-Temp) Dimethylpolysiloxane Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 80 N to 80 N to 80 N to 80 N Capillary Columns Gas Chromatography See page for ordering information. For the most current product listing, visit

38 Capillary Columns PerkinElmer Elite Series Capillary Columns Gas Chromatography Capillary Columns Elite-5 (5% Diphenyl) Dimethylpolysiloxane Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 5/50 N to 5/50 N to 0/50 N to 0/0 N to 5/0 N to 5/0 N to 5/0 N to 5/0 N to 5/0 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/0 N to 0/50 N to 0/50 N to 0/0 N to 0/50 N to 0/0 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N * to 0/0 N * to 0/0 N * to 0/0 N * to 0/0 N * to 70/90 N * to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 70/90 N to 0/0 N * Ferrule size same as 0.5. Elite-5Amine Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 00/5 N to 00/5 N to 00/5 N to 00/5 N to 00/5 N to 90/05 N to 90/05 N to 90/05 N to 80/05 N to 80/05 N to 00/5 N Elite-5ht (High-Temp) (5% Diphenyl) Dimethylpolysiloxane Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 00 N to 00 N to 00 N to 00 N Elite-5ms (5% Diphenyl) Dimethylpolysiloxane Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 5/0 N to 5/0 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 5/50 N to 0/50 N to 0/50 N to 5/50 N to 0/50 N to 0/50 N to 0/50 N to 5/50 N to 0/50 N to 0/50 N to 5/50 N to 0/50 N to 0/50 N to 0/50 N to 5/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/0 N to 0/0 N

39 Capillary Columns PerkinElmer Elite Series Capillary Columns Elite-7 (50% Phenyl) Methylpolysiloxane Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 80/00 N to 80/00 N to 80/00 N to 80/00 N to 80/00 N to 80/00 N to 0/00 N to 00/0 N to 0/0 N to 00/0 N to 00/0 N to 00/0 N to 90/0 N to 00/0 N to 00/0 N to 90/0 N to 90/0 N to 00/0 N to 00/0 N to 90/0 N to 00/0 N to 00/0 N to 90/0 N * to 60/80 N * to 70/90 N * to 70/90 N * to 60/80 N to 50/70 N to 60/80 N to 60/80 N to 60/80 N967 8 * Ferrule size same as 0.5 Elite-7ht (High-Temp) (50% Phenyl) Methylpolysiloxane Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) Each to 00/0 N to 00/0 N to 00/0 N to 00/0 N to 00/0 N ( ) Elite-7ms (Low Bleed) (50% Phenyl) Methylpolysiloxane Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 0/0 N to 00/0 N to 00/0 N to 00/0 N to 00/0 N to 00/0 N to 00/0 N to 00/0 N to 00/0 N Elite-5 (5% Diphenyl) Dimethylpolysiloxane Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 00/0 N to 00/0 N to 00/0 N to 90/0 N * to 80/00 N * to 90/0 N * to 80/00 N to 60/80 N to 60/80 N to 60/80 N965 7 Elite-5ms (5% Phenyl) Methylpolysiloxane Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 90/0 N to 90/0 N to 00/0 N Capillary Columns Gas Chromatography See page for ordering information. For the most current product listing, visit

40 Capillary Columns PerkinElmer Elite Series Capillary Columns Gas Chromatography Capillary Columns Elite-00 Trifluoropropylmethyl Polysiloxane Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 90/0 N to 90/0 N to 90/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 90/0 N to 90/0 N to 90/0 N to 80/00 N to 80/00 N to 80/00 N to 0/0 N to 0/0 N to 0/0 N to 00/0 N to 00/0 N to 00/0 N to 90/0 N to 90/0 N to 90/0 N to 80/00 N to 80/00 N to 80/00 N to 60/80 N to 60/80 N to 60/80 N Elite-5 (50% Cyanopropylmethyl) Phenylmethylpolysiloxane Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) Each to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N to 0/0 N * to 00/0 N * to 00/0 N to 00/0 N to 00/0 N Elite-50. Specialty Phase for Analysis of Volatiles (U.S. EPA 50.) Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) Each to 50/70 N * to 50/70 N * to 50/70 N to 50/70 N Elite-608 Specialty Phase for Semivolatile Pesticides (U.S. EPA 608) Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 90/0 N * to 70/90 N * to 60/80 N * to 70/90 N * to 60/80 N to 70/90 N to 60/80 N to 70/90 N to 60/80 N * Ferrule size same as 0.5 ( ) ( )

41 Capillary Columns PerkinElmer Elite Series Capillary Columns Elite-6 Specialty Phase for Analysis of Volatiles (U.S. EPA 6) Length (m) Film Thickness (μm) Temperature Limits ( C) * 0.5* to 0-0 to 0-0 to 0-0 to 0-0 to 0-0 to 0-0 to 0-0 to 0-0 to 0-0 to 0 N9600 N9609 N960 N960 N960 N960 N9605 N9606 N9607 N * Ferrule size same as 0.5 Elite-0 (6% Cyanopropylphenyl) Methylpolysiloxane Inner Diameter (mm i.d.) * 0.5* Length (m) Film Thickness (μm) Temperature Limits ( C) to 80-0 to 80-0 to 80-0 to 60/80-0 to 80-0 to 60/80-0 to 80-0 to 60/80-0 to 80-0 to 80-0 to 80-0 to 60/80-0 to 60/80-0 to 60/80-0 to 60/80-0 to 60/80-0 to 60/80-0 to 60/80 N960 N96 N96 N96 N96 N965 N966 N967 N968 N960 N96 N969 N96 N96 N96 N965 N966 N Film Thickness (μm) Temperature Limits ( C) to 80-0 to 80-0 to 80-0 to 70/80-0 to 70/80-0 to 70/80-0 to 80-0 to 80-0 to 60/80-0 to 60/80-0 to 60/80-0 to 80-0 to 80 Temperature Limits ( C) * 0.5* 0.5* 0.5* to 60/80-0 to 80-0 to 80-0 to 60/80-0 to 80-0 to 80-0 to 60/80-0 to 60/80-0 to 80-0 to 80-0 to 60/80-0 to 60/70-0 to 50/70-0 to 60/70-0 to 50/70-0 to 50/70-0 to 60/70-0 to 60/70-0 to 50/70 N968 N969 N960 N96 N96 N96 N96 N965 N966 N967 N968 N9650 N969 N965 N965 N965 N965 N9656 N Elite-BAC Blood Alcohol Analysis Columns for GC and High-Speed Headspace Gas Chromatography Now using the PerkinElmer Blood Alcohol columns, standard separations and automated separations of less than.5 minutes can be accomplished. Sample concentrations range from 0.0 to 0.05% with quantitative precision of <% RSD. A full range of analytes with a choice of internal standards can be used with excellent quantitative performance. Two columns may be used in parallel for confirmation of peak identity. Description Inner Diameter (mm i.d.) Length (m) Film Thickness (μm) Elite BAC- Elite BAC- Elite BAC N9657 N9657 N N9657 N9658 N9659 N9660 N968 N969 N960 N96 N96 N96 N965 N966 N Description Inner Diameter (mm i.d.) Length (m) Film Thickness (μm) Elite BAC- Elite BAC- Elite BAC- Elite BAC N96579 N96578 N96577 N Gas Chromatography Length (m) Film Thickness (μm) Standard Blood Alcohol GC Columns Elite-70 (% Cyanopropylphenyl) Methylpolysiloxane Inner Diameter (mm i.d.) Length (m) Capillary Columns Inner Diameter (mm i.d.) Inner Diameter (mm i.d.) Elite-Betacydex Betacyclodextrin for Chiral Separations Inner Diameter (mm i.d.) Length (m) Film Thickness (μm) Temperature Limits ( C) to 0 N See page for ordering information. For the most current product listing, visit 5

42 Capillary Columns PerkinElmer Elite Series Capillary Columns Elite-CLPesticides Elite-CLPesticides is specially designed to overcome the coelutions and analyte breakdown typically encountered in chlorinated pesticide analyses for U.S. EPA methods 808, 608, and CLP. Column bleed measured by ECD is extremely low at temperatures greater than 00 C, which is critical for baking out the column to remove high-boiling compounds commonly found in pesticide/pcb extracts. Gas Chromatography Capillary Columns Primary Applications Chlorinated Pesticides and Herbicides. U.S. EPA Methods 50, 608, 69, 808, 85, and CLP. Features and Benefits: Thermally stable to 0 C Low column bleed ideal for ECD or GC/MS analysis Exceeds performance criteria for U.S. EPA Methods 808, 608, CLP Baseline separation in less than 5 minutes Inner Film Diameter Length Thickness (mm i.d.) (m) (μm) N N N N N N Elite-CLPesticides Inner Film Diameter Length Thickness (mm i.d.) (m) (μm) N N N N N N

43 Capillary Columns PerkinElmer Elite Series Capillary Columns Elite-FFAP Nitroterephthalic Acid Modified Polyethylene Glycol (Bonded) Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) Elite-SimDist Dimethylpolysiloxane Processed for Simulated Distillation Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 50 N to 50 N to 50 N to 50 N * to 0/50 N * to 0/50 N to 0/50 N to 0/50 N Elite-HT SimDist for High-Temperature Simulated Distillation Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 00 N Elite-MTBE Low Polarity Stationary Phase Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 50 N to 50 N Elite-PONA Dimethylpolysiloxane Processed for Detailed Analysis of Petroleum Naphtha Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 00/0 N to 00/0 N Elite-RX for Analysis of Drugs of Abuse Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) Phase: Elite--RX to 0/50 N to 0/50 N966 5 Phase: Elite-5ms-RX to 0/50 N to 0/50 N Phase: Elite-7-RX to 0/0 N to 0/0 N * to 60 N to 60 N966 5 Elite-TPH Specialty Phase for Analysis of Total Petroleum Hydrocarbons Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 0 N * to 90 N Elite-VMS Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N Elite-Volatiles Specialty Phase for Analysis of Volatile Organic Compounds Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 0 N to 0 N to 0 N to 0 N * to 0 N * to 0 N969 7 * Ferrule size same as 0.5 Capillary Columns Gas Chromatography See page for ordering information. For the most current product listing, visit 7

44 Capillary Columns PerkinElmer Elite Series Capillary Columns Gas Chromatography Capillary Columns Elite-MWAX Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 0/50 N Elite-WAX Polyethylene Glycol Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 0/50 N to 50/60 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N * to 0 N * to 50 N * to 0/50 N * to 50 N * to 0/50 N * to 0/50 N to 50 N to 0/50 N to 50 N to 0/50 N to 0/50 N Elite-WAX ETR (Extended Temperature Range) Polyethylene Glycol Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 50 N to 0/50 N to 60 N to 50 N to 0/50 N to 0/50 N to 50 N to 50 N to 0/50 N to 0/50 N to 0 N to 0 N to 0 N to 0/0 N to 0/50 N to 0/0 N to 0/50 N to 0/0 N to 0/50 N * Ferrule size same as 0.5 Elite-XLB Specialty Phase for GC/MS with Exceptionally Low Bleed Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/60 N to 0/0 N to 0/0 N

45 Capillary Columns PerkinElmer Elite Series Guard and PLOT Columns Elite Guard Columns Elite-Alumina/KCI* PLOT Guard Columns Maintain the integrity of your capillary column with a fused silica Guard Column. Using the Elite-Guard or Elite-Siltek Guard Column lengthens the life of the capillary column and improves the analyte focusing. The 5 m length of deactivated uncoated fused silica is connected to the inlet end of the capillary column and traps nonvolatile residues, preventing them from collecting at the head of the analytical column. This length of fused silica contains no stationary phase, adding only a minimal amount of time to the analysis. PerkinElmer offers both the Intermediate-polarity deactivated guard column and the Siltek deactivated guard column as it is important to match the polarity of the solvent and the polarity of the surface deactivation. The Elite-Guard intermediate polarity deactivated column has an operating temperature up to 5 C. Siltek deactivation creates a highly inert surface for very active compounds such as chlorinated pesticides with a maximum temperature range up to 80 C. Features and Benefits: Increases the life of the capillary column Maintains retention time and resolution on capillary column Traps nonvolatile particles Improves column performance Elite-Guard temperature range to 5 C Elite-Siltek Guard temperature range to 80 C Elite-Guard Inner Diameter Length (mm i.d.) (m) N N N N N N Elite-Siltek Guard Inner Diameter Length (mm i.d.) (m) N N N Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) N/A up to 00 N * Lower Polarity than Elite Alumina. Elite-Alumina PLOT Phase for Analysis of Light Hydrocarbons Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) N/A -60 to 00 N N/A -60 to 00 N Note: -60 C is the lowest temperature used on this phase in our lab. Lower temperatures may be used depending on the sample. Elite-Cyclosil B PLOT for Chiral Separations Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) to 0 N to 0 N Elite-Molesieve PLOT Phase for Analysis of Permanent Gases Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) N/A -60 to 00 N966 6 Note: -60 C is the lowest temperature used on this phase in our lab. Lower temperatures may be used depending on the sample. Elite-Q PLOT Phase for Analysis of Light Gases and Hydrocarbons Inner Film Temperature Diameter Length Thickness Limits (mm i.d.) (m) (μm) ( C) 0. 0 N/A -60 to 50 N N/A -60 to 50 N Note: -60 C is the lowest temperature used on this phase in our lab. Lower temperatures may be used depending on the sample. Capillary Columns Gas Chromatography See page for ordering information. For the most current product listing, visit 9

46 Capillary Columns PerkinElmer Packed Columns Packed Columns Packed Packed Empty Empty Length o.d. mm i.d. mm i.d. mm i.d. mm i.d. Instrument Type Material Shape (ft.) (in.) Gas Chromatography Capillary Columns AutoSystem GC Stainless /8 N N Clarus Steel 6 /8 N N (not on-column) /8 N N900 0 / 6 / N N / N N9007 Glass / N N9008 N900 6 / N N N9009 N900 / N N900 5 AutoSystem GC/XL Glass / N (on-column) 6 / N N / N90508 N Note: Stainless steel columns are metal-fitted at both ends to contain the packing. For on-column applications, please request glass wool plugs instead of metal frits when ordering. Choose the appropriate part number from table above. Follow form at bottom of page to choose support material, % liquid phase, and mesh size. This information is required to place an order. 0

47 Detectors Electron Capture Detectors (ECD) Add-On Kit The ECD is a versatile, nondestructive detector which responds strongly to halogen-containing compounds as well as to certain other electron-capturing substances. The ECD s high sensitivity and selectivity make it an ideal choice for pesticide-residue analysis and for detection of halogen-derivatized compounds. The ECD has an independent temperature range of C. The detector contains thermal protection that prevents heating the Ni 6 source to temperatures beyond safe operating limits. Two ECDs can be installed and operated simultaneously on the AutoSystem Series and Clarus GCs. Nitrogen or argon/methane is the required detector operating gas. The base of the detector terminates in a /8 in. fitting. To Amplifier ECD Add-On Kit (Manual Pneumatics) Kit includes all parts necessary to install an ECD on the AutoSystem Series or Clarus GCs. Includes detector, heater, sensor, heater block, /6 in. makeup gas line, makeup gas needle valve, and vent tube assembly. Requires but does not include ECD amplifier (N600). Installation by PerkinElmer Service is recommended. Voltage 0 V AutoSystem N600 0 V AutoSystem N V Clarus N V Clarus N ECD Amplifier Required for use with ECD detector with add-on kit. Collector Anode ECD Add-On Kit (PPC Pneumatics) Kit includes detector, heater, sensor, heater block, and programmable pneumatic control for makeup gas. Requires, but does not include, ECD amplifier (N600). The AutoSystem XL or Clarus GCs must be PPC ready. If not, a PPC upgrade kit (N606) is required. (See page 66 for more information.) Installation by PerkinElmer Service is required, but not included. Voltage 0 V N60 0 V N60 07 Vent Tube Assembly Flexible tube to safely vent toxic sample effluent. Column Adapters Capillary Column Adapter/Receiver Ni 6 Foil (Source) Adapter converts /8 in. fitting to /6 in. for use with capillary columns. Note: Glass-lined tubing reduces background from polyimide coating in high-temperature applications. N Makeup Gas In Column Connection N600 7 PID/ECD Series Operation Kit Kit for directing effluent from PID to ECD. / in. Packed Column Adapter For use with / in. packed columns. /8 to / in. adapters fit both injector and detector ends. (Pkg. ) ECD Wipe Test Kit N N U.S. Federal law requires that all ECDs be wipe-tested periodically as described in the instrument operator s manual. In the U.S., possession and use of ECD is regulated by N.R.C. and/or state regulatory agencies. Licensing by regulatory agencies is required. Outside of the U.S., check with governing bodies for licensing and regulations covering possession and use. This kit contains everything necessary to do a complete wipe test. For use on any model GC ECD Detectors Gas Chromatography See page for ordering information. For the most current product listing, visit

48 Detectors Flame Ionization Detector (FID) Auto-Ignite Gas Chromatography Detectors Add-On Kits Auto-Ignite FID with PPC Add-On Kit Kit includes detector assembly with heater and sensor, heater block, igniter, programmable pneumatics, and controls for detector combustion gases. Requires but does not include amplifier (N606) and AutoSystem XL firmware revision. or higher. The AutoSystem XL must be PPC ready. If not, a PPC upgrade kit (N606) is required. Note: AutoSystem XL GCs shipped prior to January 997 require a new detector cover. Installation by PerkinElmer Service is required, but not included. Voltage 0 V N V N Auto-Ignite FID Add-On Kit (Manual Pneumatics) Kit includes detector assembly with heater and sensor, heater block, igniter, hydrogen pressure regulator, and needle valve. Requires, but does not include, amplifier (N606). Requires AutoSystem XL to have firmware revision. or higher. Note: AutoSystem XL GCs shipped prior to January 997 require a new detector cover (N605). Voltage 0 V AutoSystem N V AutoSystem N V Clarus N V Clarus N FID Amplifier Required for use with FID Detector Add-On Kit. Auto-Ignite FID Replacement Parts N Description Collector Head Assembly N Silicone Rubber O-Ring* (not shown) 0990 Polarizer Nozzle N Spring Washer Nozzle Insulator N Nozzle Collector N FID Jet Contact/Spring N Jet Assembly N FID Body N Nozzle Assembly N Detector Series Operation Kit TCD/FID Series Operation Kit Used to direct sample effluent from the TCD to the FID. PID/FID Series Operation Kit Used to direct sample effluent from the PID to the FID. FID Miscellaneous Accessories Description Auto-Ignite Nozzle Replacement Tool N For removing nozzle from auto-ignite FID body Auto-Ignite FID Catalytic Reactor Accessory N606 6 Capillary Column Adapter N For capillary column use with the FID /8 to /6 in. detector adapter Ceramic Column Cutter N Cotton Applicators N907 Detector Cover (Brown Color) N605 Detector Cover (White Color) N605 Eraser Brush-Pencil Jet Assembly N Jet Replacement Tool N / in. nut driver for removing jet from auto-ignite FID body Quartz Wool N605 6 Replacement Stainless Steel Glow Plug N for Auto-ignite FID Septa, low bleed (pkg. 50)** N / in. Packed Column Adapter For use with / in. packed columns. /8 to / in. adapter fits both injector and detector ends ** For more Septa see page 59. * N N

49 Detectors Flame Ionization Detector (FID) External Igniter Add-On Kits External Igniter FID with PPC Add-On Kit Kit includes detector, heater and sensor, heater block, igniter, programmable pneumatics, and controls for detector combustion gases. Requires but does not include FID amplifier (N606). The AutoSystem XL must be PPC ready. If not, PPC upgrade kit (N606) is required. (See page 66 for more information.) Installation by PerkinElmer Service is required, but not included. * Voltage 0 V N600 0 V N60 89 External Igniter FID Add-On Kit (Manual Pneumatics) Kit includes detector assembly with heater and sensor, heater block, igniter, hydrogen pressure regulator, and air needle valve. Requires, but does not include, FID amplifier board (N606). Voltage 0 V N V N FID Amplifier Required for use with FID Detector Add-On Kit. Replacement Parts N Description Collector Head Assembly N *Collector Assembly O-Ring (not shown) 0990 Collector Cap N Nozzle Insulator N Nozzle Ring 099 FID Nozzle N FID Jet Contact N Jet Assembly N Polarizer Replacement Kit N FID Body N Collector Adapter, Teflon ** (not shown) N6057 ** Note: If instrument was purchased prior to March 99, the following items must also be ordered: one each of N6056 and Detectors Gas Chromatography See page for ordering information. For the most current product listing, visit

50 Detectors Flame Ionization Detector (FID) Replacement Parts Gas Chromatography Detectors Catalytic Reactor Accessory The catalytic reactor converts CO and CO to methane conveniently and efficiently. The lower detection limit is extended to well below 0. ppm. The catalytic reactor consists of a special catalytic reactor base which replaces the FID base. The reactor body contains a quantity of catalyst held in place by a quartz wool plug. Kits include base assembly, reactor tube, and instructions. External Igniter FID Catalytic Reactor Accessory Auto-Ignite FID Catalytic Reactor Accessory Catalytic Reactor Replacement Parts Description Catalyst N Jet Assembly N Quartz Wool N605 6 Catalyst N FID Base N606 6 Miscellaneous Accessories External Ignite Nozzle Replacement Tool For removing nozzle from External Ignite FID body. Hydrogen Regulator Replacement Kit Hydrogen/Air Replacement Needle Valve Igniter Assembly Complete replacement igniter assembly with glow plug. Replacement Glow Plug for External Ignite FID FID Flow Measurement Adapter N N N60 96 N N605 9

51 Detectors Flame Photometric Detector (FPD) Add-On Kits The FPD is a highly sensitive and selective detector for both sulfur and phosphorus compounds. It is especially suitable for environmental monitoring of H S and sulfur gases in general and for organophosphorus compounds present at trace levels in pesticide analysis. Alkyl tin compounds can also be analyzed by changing the filter assembly. The sulfur filter is shipped standard. The FPD mounts in either the front or rear detector position. This allows many detector combinations, such as FPD/FPD, FPD/TCD, and FPD/ELCD. The AutoSystem also includes a linearizer function for the sulfur mode and convenient control of the photomultiplier tube from the keyboard. The FPD is capillary-column compatible. The detector will accept columns of 0.50 mm i.d. or less. The standard jet shipped with the FPD does not have a glass-lined tail pipe. If an all-glass system is required and glass packed columns will be used, then a glass-lined tail pipe should be ordered (N6006). As a reminder, use of packed / in. columns requires a /8 to / in. adapter. Filters 8 Description Phosphorus Lens (Yellow) N Sulfur Lens* (Blue) N Tin Lens (Orange) L57 7 * Shipped standard. Filter Assembly 5 7 Air 6 Hydrogen FPD Add-On Kit (Manual Pneumatics) Kit includes detector, heater, sensor, heater block, hydrogen needle valve, air pressure regulator, and sulfur photomultiplier filter. Requires but does not include FPD amplifier (N60095). Firmware revision.6 or greater required. Firmware must be PerkinElmer Service installed. AutoSystem operator s manual ( ) revision E or higher required. Voltage 0 V AutoSystem N V AutoSystem N V Clarus N V Clarus N FPD Amplifier Firmware revision.6 or greater required. Firmware must be PerkinElmer Service installed. AutoSystem operator s manual ( ) revision E or higher required. FPD Replacement Parts for AutoSystem Series GCs Description O-Ring Seal Assembly and Window N (heat shield) Liner (window) N FPD Body (upper) N Window Holder N FPD Jet, N Glass-lined Jet Tailpipe N (for all-glass system) FPD Body (lower) N600 6 Photomultiplier Tube FPD with PPC Add-On Kit Kit includes detector, heater, sensor, heater block, programmable pneumatic control for detector combustion gases, and sulfur photomultiplier filter. Requires but does not include FPD amplifier (N60095). AutoSystem XL GC must be PPC ready. If not, a PPC upgrade kit (N606) is required. (See page 66 for more information.) Installation by PerkinElmer Service is required, but not included. Voltage 0 V N608 0 V N Packed Column Adapter /8 to / in. adapter for use with / in. packed columns. (Set of ) N Detectors Gas Chromatography See page for ordering information. For the most current product listing, visit 5

52 Detectors Mass Spectrometer Detector The Clarus Mass Spectrometer The Clarus mass spectrometer is the fastest sampling and widest-mass-range quadrupole mass spectrometer available for GC/MS. State-of-the-art Pentium electronics process more scans across each peak, resulting in unmatched accuracy and precision, and better overall spectral fidelity. This, coupled with unique productivity tools, provides the functionality necessary to achieve optimum performance, completing work quickly, easily, and efficiently. The wide mass range and flexible data acquisition modes help tackle the most complex applications while rugged instrument design delivers maximum uptime, easy maintenance, and lower operating cost. Clarus Mass Spectrometer Combine the Clarus mass spectrometer with the Clarus gas chromatograph, market-leading TurboMatrix sample handling accessories, flexible user-friendly TotalChrom software, and worldclass service and support for an integrated, complete analytical solution from one familiar name PerkinElmer. Whatever your application Environmental, Chemical, Petrochemical, Flavor and Fragrance, Food, Beverage, Forensic, Pharmaceutical PerkinElmer delivers the accuracy and precision you need. Flexible Column Choices Because the Clarus mass spectrometer allows a carrier gas flow of up to 5 ml per minute in EI, you have more column choices than with other GC/MS systems. Narrow-, medium-, and wide-bore columns can be used, with almost unlimited choice of stationary phase, diameter, and analytical method with Clarus mass spectrometer. Column Internal Diameter Typical Flows Clarus Mass Spectrometer Others Narrow-bore 0.0 to 0.8 mm i.d. 0. to 0.8 ml/min. X X Medium-bore 0.5 mm i.d to.5 ml/min. X X Wide-bore* 0. to 0.5 mm i.d. to 5 ml/min. X * Columns with low pneumatic impedance may require attachment of additional length of deactivated fused-silica capillary tubing to provide proper pressure drop from injector to mass spectrometer (Part Nos. N905, N909, and N90). Clarus Mass Spectrometer Benefits: Fastest Scan Rates unprecedented speed with better chromatographic peak definition ensuring better quality results. Opens the use of quadrupole technology to fast GC applications. Widest Mass Range uncompromised performance over a wide mass range. SIFI Scanning Mode selected Ion Monitoring (SIM) and full scan in the same run resulting in the most complete characterization of the sample. No need to run the sample twice. Gold Component Technology improved stability and reduced maintenance. Easy Access Ion Source less than 5-minute changeover. Sealed, Long-Life Photomultiplier eliminates expensive replacement costs of electron multipliers. Better reliability. 6

53 Detectors Mass Spectrometer Detector Cables Description Cable, RS, 7 ft. Length (85 cm) S Personal Computer to AutoSystem XL Integral LINK (included with TurboMass Gold) Cable, RS, 5 ft. Length (660 cm) S Personal Computer to AutoSystem XL Integral LINK Computer to MS Cable E For use with TurboMass Mass Spectrometers only Ethernet Cable For TurboMass Gold Mass and Clarus 500 Spectrometers only GC Start/Ready Cable E GC to MS Interface Cable E600 0 Inner Source Replacement Parts Description CI Ion Exit Plate E60 5 Extra EI Electron Trap E600 7 Extra CI Ion Volume E Extra EI Ion Volume E Extra EI Repeller E609 Ion Exit Plate E60 66 Filament Assembly and Standard Tungsten Filament E For use with TurboMass Spectrometers only Inner Source Heater Assembly E Inner Source O-Ring Seal E577 Inner Source Thumbscrew E Standard Rhenium Filament N Trap Contact E Ionizer Replacement Parts Description Clarus 500 and TurboMass Extra EI Inner source N Assembly (Tungsten) Clarus 500 and TurboMass Gold Extra EI Inner Ion E Source Assembly (Rhenium) Clarus 500 and TurboMass Gold Extra PCI/NCI E Inner Ion Source Assembly (Rhenium) Requires PCI or PCI/NCI configuration option Extra Outer Ion Source and Optics Assembly E Manuals Description Clarus 500 MS Manual Set TurboMass Gold Manual Kit Includes: User s Guide-EPCAS software, User s Guide-EPCAS hardware, and TurboMass Gold Tutorial TurboMass Software User s Manual S TurboMass Hardware User s Manual Miscellaneous Accessories BTO TM (Bleed Temperature Optimized) Injector Septa Maximum recommended operating temperature 00 C. Low bleed, high temperature. mm diameter. GC/MS Sensitivity Test Mix Includes standard solutions of benzophenone, hexachlorobenzene, and octafluoronaphthalene for testing instrument sensitivity. GC/MS Test Mix Triazine High molecular weight test standard. 00 mg. Forepump Vacuum Filter Kits Includes: Foreline Adsorption Trap (0999), Nipple NW5 Extension Tube (099086), NW5 Clamp Ring (0999), NW5 Centering Ring (09990), Installation Instructions (0996), and Activated Alumina Reagentreplacement (09950). E600 9 Outlet Mist Filter Replacement Parts Description Centering Ring Clamp 0999 Copper Tubing, Precleaned (50 ft.) N FC- Tuning Compound N607 5 Filament Allen Wrench Forepump Oil Gas Purifier for GC/MS N Glass Bulb for Reference Gas E608 6 Penning Gauge Spares Kit N Vacuum line (7 ft.) E Eraser Brush-Pencil Ceramic Column Cutter N Cotton Applicators N907 Septa, low bleed (pkg. 50)* N * For more septa see page 59. Vent Kit N E N The Mass Spectrometer Vent Kit eliminates the introduction of oxygen, water vapor, and other airborne contaminants which can degrade sensitivity and performance of the mass spectrometer. The Clarus GCs should be vented with UHP nitrogen ( %). Helium should not be used as Helium molecules penetrate the glass sleeve on the photomultiplier tube, compromising the vacuum and lowering sensitivity. N Detectors Gas Chromatography See page for ordering information. For the most current product listing, visit 7

54 Detectors Mass Spectrometer Detector Clarus MS TurboMass Single Additional Workstation License Allows TurboMass software to be run on one additional computer. Does not include manuals. Note: Network setup is the responsibility of the customer. S Wiley Mass Spectral Library Does not include the NIST library. E Gas Chromatography Detectors MSVent Add-On Kit for the Clarus GC/MS Includes: all the necessary parts to add an MSVent accessory to a Clarus GC/MS. Requires a PreVent option (N60) to be already installed in the Clarus gas chromatograph. Software TurboMass 5. Software Kit Includes: the TurboMass 5. software CD, TurboMass User s Manual CD, and Utilities CD. Description NIST Mass Spectral Library (00) N NIST98 to 00 Upgrade Kit N Pfleger/Maurer/Weber Drug and Pesticide Spectral Library TotalChrom Workstation Reprocess-Only Kit for TurboMass Mass Spectrometers Only N N Allows data collected from a conventional detector via TurboMass software to be analyzed with TotalChrom Workstation Chromatography Data System software. Includes: CD and.5 in. diskette media, user manuals, mouse pad, and installation instructions. S706 8 Transfer Line Description Transfer Line Carrier Tube E Transfer Line O-Ring E5769 Transfer Lines /8 in. Nut E Upgrade Kits EI to PCI/NCI Upgrade Includes: Cl ion source, reagent gas tubing, flow regulators, valves and solenoids, and dual-polarity electronic options. Installation by PerkinElmer Service is required, but not included. TurboMass Gold Computer Upgrade Upgrade kit includes: Dell GX70 computer plus 7" flat panel monitor and Windows XP SP. TurboMass 5. software is included free. Service installation is not required. N TurboMass Upgrade Kit E Upgrade kit includes: Dell GX70 computer with Windows XP SP, 7" flat panel monitor, TurboMass 5. software and manual plus all necessary electronic and hardware components. Installation by a PerkinElmer Service professional is required, but not included. N

55 Detectors Nitrogen Phosphorus Detector (NPD) Add-On Kits Replacement Parts NPD Add-On Kit (Manual Pneumatics) Description The NPD can be used for the analysis of organic compounds containing nitrogen or phosphorus down to the picogram level. The NPD has become the detector of choice for low-level drug and pesticide applications because of its sensitivity and selectivity. Kit includes detector, heater, sensor, heater block, air needle valve, and hydrogen pressure regulator with snubber and two beads. Requires but does not include amplifier. For AutoSystem GC Firmware revision. or greater is required. Firmware must be PerkinElmer Service installed. Voltage 0 V AutoSystem N V AutoSystem N V Clarus N V Clarus N NPD Amplifier Required for use with NPD Add-On Kit. NPD with PPC Add-On Kit Kit includes detector, heater, sensor, heater block, and programmable pneumatic control for detector combustion gases and two beads. Requires but does not include amplifier (N6009). The AutoSystem XL or Clarus GC must be PPC ready. If not, the PPC upgrade kit (N606) is required. (See page 66 for more information.) Installation by PerkinElmer Service is required, but not included. Voltage 0 V N606 0 V N Column Adapter / in. Packed Column Adapter /8 to / in. detector receiver adapter for use with / in. packed columns. Two included (injector/detector). N Collector Head N Bead Assembly (pkg. 5) N Single pkg. N Jet Assembly N NPD Body N Air in Hydrogen in Column Connection Detectors Gas Chromatography See page for ordering information. For the most current product listing, visit 9

56 Detectors Photoionization Detector (PID) Gas Chromatography Detectors Add-On Kits PID Add-On Kit (Manual Pneumatics) The PID utilizes a high-intensity ultraviolet light source to ionize the sample components eluting from the column in order to generate the chromatographic signal. The PID has a maximum recommended operating temperature of 50 C. The lamp can be replaced with a blanking disk to allow bake-out operation (up to 50 C). Kit includes detector, heater, sensor, makeup gas needle valve, and all necessary mounting hardware for installation on an AutoSystem GC. Requires but does not include amplifier (N6006) and lamp power supply (N6006). Firmware revision. or greater is required. Firmware must be PerkinElmer Service installed. AutoSystem operator s manual ( ) is required if not revision ƒ or higher. Voltage 0 V AutoSystem N V AutoSystem N V Clarus N V Clarus N PID Amplifier Required for use with PID Add-On Kit. PID Lamp Power Supply Required for use with PID Add-On Kit. PID with PPC Add-On Kit N N Kit includes detector, heater, sensor, heater block, and programmable pneumatic control for makeup gas. Requires but does not include amplifier (N6006) and power supply (N6006). The GC must be PPC ready. If not, a PPC upgrade kit (N606) is required. (See page 66 for more information.) Installation by PerkinElmer Service is required, but not included. Voltage 0 V N600 0 V N Detector Series Operation Kits Description PID/FID, PID/ECD N Series kit for directing effluent from a PID to an FID or an ECD Miscellaneous Accessories Description Bakeout Disk Lamp Cleaning Compound / in. Detector Receiver /8 in. Detector Receiver Replacement Lamps and Parts Description PID Lamp (0.eV), For most applications including aromatics, alkenes, and aliphatics higher than C. Shipped standard with PID PID Lamp (9.5eV), Improved selectivity for multiple ring aromatic, sulfur compounds PID Lamp Window Seal PID Lower Lamp Seal Shoulder Pin Cap Nut Base Assembly Spring 0097 Cap with Harness N

57 Detectors Thermal Conductivity Detector (TCD) Add-On Kits Lower Internal Volume and Smaller Overall Size No Makeup Gas Required with 0.5 mm and 0. mm i.d. Capillary Columns Series Connection Option Excellent Sensitivity Over a Wide Dynamic Range TCD Add-On Kit (Manual Pneumatics) Kit includes all necessary items to install the TCD into the instrument: detector, heater, sensor, heater block, /6 in. gas line, and flow controller pneumatics. Requires, but does not include, amplifier (N6005). The TCD can only be installed in the rear detector position. Voltage 0 V AutoSystem N600 0 V AutoSystem N V Clarus N V Clarus N TCD Amplifier TCD with PPC Add-On Kit Kit includes detector, heater, sensor, heater block, and programmable pneumatic control for reference gas. Requires but does not include amplifier (N6005). The TCD can only be installed in the rear detector position. The GC must be PPC ready. If not, a PPC upgrade kit (N606) is required. (See page 66 for more information.) Installation by PerkinElmer Service is required, but not included. Voltage 0 V N60 0 V N TCD with PPC Makeup Gas Kit Includes parts required to add PPC controlled makeup gas to an existing TCD. Includes tubing, tee-piece, PPC pneumatics module, and PPC frit # (N6055). Requires PPC capability in the GC. N6050 Column Adapters N Description /8 to / in Column adapter for use with / in. packed columns /8 to /6 in. N Column adapter for use with capillary columns Thermal Conductivity Detector TCD/FID Series Operation Kit TCD and FID series operation kit for directing effluent from a TCD to an FID. N TCD Detector Makeup Gas Kit (Manual Pneumatics) For use with TCD (at low flow rates). Required when using 0.5 mm i.d. and recommended when using 0. mm i.d. capillary columns. Kit includes m of /6 in. tubing to connect to gas supply, graphite/vespel ferrules, manual pneumatics, and installation instructions. N Detectors Gas Chromatography See page for ordering information. For the most current product listing, visit

58 Headspace Accessories and Supplies Headspace Instruments PerkinElmer TurboMatrix Headspace Samplers PerkinElmer TurboMatrix Headspace Samplers eliminate tedious and error-producing steps required in other GC sample preparation techniques, enabling you to analyze volatile compounds in less time. The intuitive touch-screen graphical user interface provides easy control of the sampler. TurboMatrix 6 TurboMatrix 0 TurboMatrix Headspace Trap The TurboMatrix Headspace (HS) system is fully self-contained and can be interfaced to almost any gas chromatograph, giving you access to PerkinElmer s proven headspace technology, regardless of the brand or model GC you have in your laboratory. The TurboMatrix system maximizes sample throughput. The system can simultaneously thermostat up to samples, ensuring that the next sample is always ready for analysis upon completion of the previous run. This adds up to a significant time saving since there is no need to wait for the next sample to heat. Volatile compounds in almost any sample matrix can be analyzed simply and quickly by headspace gas chromatography. Only PerkinElmer headspace samplers utilize a pneumaticpressure-balanced system, a proven technology that s been used in all PerkinElmer headspace samplers for more than 5 years. This unique, patented technique provides higher sensitivity and better performance than alternative techniques. The pressure-balanced sampling technique: Produces sharper peaks by rapidly transferring a narrow sample band to the GC column. Increases sensitivity since there is no carrier gas dilution of sample. Avoids fractionation due to pressure changes in the syringe. Eliminates multiport valves that are prone to adsorption and may introduce dead volumes. Provides exceptional reproducibility equal to that obtainable with liquid. The TurboMatrix system is available in your choice of entry-level, mid-range, or high-capacity systems. And, since upgradeability is built in, you can adapt your system to changing requirements by upgrading from one model to the next or adding accessories that provide more capabilities.

59 Headspce Add-On Kits Cryofocusing Add-On Kit, TurboMatrix HS Adds cryofocusing capability to a TurboMatrix 0 or TurboMatrix 0 headspace sampler. Includes water trap to remove the water from headspace samples taken from aqueous solutions. Note: Requires but does not include, LN Dewar (B05009). Also requires, but does not include, an options board to be installed in the TurboMatrix 0 headspace sampler. Installation by PerkinElmer Service is required, but not included. M HS 0XL Cryofocusing Accessory (White Color) Consists of cryofocusing module, firmware, required tubing unions, and water trap to be installed in AutoSystem GC. Requires liquid nitrogen storage tank. Installation by PerkinElmer Service is required, but not included. N Replacement Water Trap for Cryofocusing Accessory Options Board/BCD Output Board, TurboMatrix HS Required for installation of the following options on the TurboMatrix 0 headspace sampler Vial Shaker and Cryofocusing and when upgrading a TurboMatrix 6 or 0 headspace sampler to a TurboMatrix 0. Also provides output of BCD information regarding tube position numbers and six relays for timed control of external devices. Installation by PerkinElmer Service is required, but not included. (Fitted as standard on TurboMatrix 0 HS). HS 0 Options Board Allows up to six optional control ICs. Installation by PerkinElmer Service is required, but not included. TurboMatrix Headspace PPC Add-On Kit Includes parts to convert a headspace sampler from manual pneumatics to electronic Programmable Pneumatic Control (PPC). Installation by PerkinElmer Service is required, but not included. Headspace Accessories and Supplies B M B08 6 M058 8 Vial Shaker Add-On Kit, Headspace and Headspace Trap HS 0XL Shaker Accessory Add-On Kit Add-On Kits Adds a Frequency Scanning Shaker to a TurboMatrix 0 or TurboMatrix 0 headspace sampler. Note: Requires, but does not include, an options board to be installed in the TurboMatrix 0 headspace sampler. Installation by PerkinElmer Service is required, but not included. M059 Adds Frequency Scanning Shaker to vibrate all samples in thermostatting chamber. Installation by PerkinElmer Service is required, but not included. Color Blue N Red B Headspace Accessories and Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit

60 Gas Chromatography Headspace Accessories and Supplies Headspace Accessories and Supplies Headspace Accessories Miscellaneous Accessories TurboMatrix HS Standard Length Heated Transfer Line (960 mm) For operation up to 0 C. TurboMatrix HS/HS Trap Long Heated Transfer Line (650 mm) For operation up to 0 C. Fused Silica Capillary Transfer Line Tube i.d. (mm) Length (m) N N Siltek Deactivated Fused Silica Transfer Line Tube i.d. (mm) Length (m) N N Zero Dilution Inner Liner To be used with zero dilution outer liner. The powerful zero dilution liner combination allows you to achieve lower detection limits, sharpen peak shape, and increase throughput for many routine analyses. Installed in an AutoSystem Series or Clarus GC standard capillary or PSS injector, this optional special hourglass insert connects the fused-silica transfer line from the headspace sampler to the capillary column, permitting undiluted and efficient sample transfer. The insert provides the advantages of a direct connection, while maintaining the capability to perform split injections. N06 Zero Dilution Capillary Injector Outer Liner To be used with zero dilution inner liner. The powerful zero dilution liner combination allows you to achieve lower detection limits, sharpen peak shape, and increase throughput for many routine analyses. Installed in an AutoSystem Series or Clarus GC standard capillary injector, this optional special hourglass insert connects the fused-silica transfer line from the headspace sampler to the capillary column, permitting undiluted and efficient sample transfer. The insert provides the advantages of a direct connection, while maintaining the convenience of using a split injector as an interface. N05 7 Zero Dilution PSS Injector Outer Liner Gas Chromatography Theory and Practice, Static Headspace Book by L. Ettre and B. Kolb M06 M N07 90 N00 5 TurboMatrix HS Trap Cold Trap Tube (Carbotrap C) Standard cold trap (M0009) packed with Carbopack C. O-Ring 7 mm TurboMatrix Headspace Sampler User s Manual Cool Platen For storage of vials below ambient down to +5 C. Contains cool platen and tubing. Requires a thermostatted external cooling circulation water bath. Installation by PerkinElmer Service is required, but not included. Note: Requires, but does not include, Cryostat Liquid Immersion Cooler. B Extended Transfer Line (650 mm HS 0/0XL) Extra-long transfer line to allow installation of HS 0XL on the right side of the AutoSystem Series/Clarus GC or to any gas chromatograph where the HS 0XL is situated at an extended distance. High Pressure Sampling Accessory Used for operation with capillary columns requiring a low head pressure. Also used for carrier gas flow control. Accessory includes high-pressure sampling module with pressure regulator, gauge, firmware, tubing, and unions. Installation by PerkinElmer Service is required, but not included. Note: Requires, but does not include, Options Board. HS 0XL to AutoSystem Series Left Side Mounting Kit (White Color) For connecting the HS 0XL transfer line through the left side of the AutoSystem XL GC directly to the column in the oven instead of via the injection port. Includes a new GC side panel and parts for attaching the transfer line to the GC. Requires, but does not include, some type of zero dead volume connector to connect to the column (for example, a universal capillary column connector, N909). Installation by PerkinElmer Service is recommended. N HS 0XL Instruction Manual N M00 9 B B

61 Internal Carrier Gas Pressure Control For carrier gas control. Includes regulator, gauge, tubing, and unions. Installation by PerkinElmer Service is required, but not included. Recycle Mode Accessory Continuously repeats sequence with setup method. Installation by PerkinElmer Service is required, but not included. Note: Requires, but does not include, Options Board. Remote Control Software (RCS) HS 0XL Control Software Windows -based, flexible, easy-to-use external control software for the HS 0 and HS 0XL. The user can develop and store methods and sequences. Run reports can be obtained, stored, and printed. On-screen, context sensitive help available. Can be operated in combination with PerkinElmer TotalChrom TM Software. Requires RS- Interface for the HS 0XL. TurboMatrix HS PC (RCS) v. for WIN NT NOTE: This software version is only supported under Windows NT.0 Service Pack 6a. Windows 000 users should order Version. (see Part Number N60000 below). This software requires the HS unit to have firmware version.87 or earlier. Provides full external control of a TurboMatrix headspace sampler from a personal computer running under Windows 95, 98 or NT. Methods and sequences can be generated, stored, edited, printed and executed. Functions include setup, diagnostics, user defined access levels and run reports. On-screen interactive help function is available. Cable included. M08 8 TurboMatrix HS PC (RCS) v. for WIN 000 NOTE: This software requires the HS unit to have firmware version.87 or earlier. Provides full external control of a TurboMatrix headspace sampler from a personal computer running under Windows 000 SP. Methods and sequences can be generated, stored, edited, printed and executed. Functions include setup, diagnostics, user defined access levels and run reports. On-screen interactive help function is available. Cable included. N Headspace Accessories and Supplies B B B TurboMatrix HS Trap PC (RCS) v.0 Headspace Accessories NOTE: This software requires the HS unit to have firmware version.00. Provides full external control of a TurboMatrix headspace sampler from a personal computer running under Windows XP SP or Windows 000 SP. Methods and sequences can be generated, stored, edited, printed and executed. Functions include setup, diagnostics, user defined access levels and run reports. Includes control of the TurboMatrix Trap if present on the HS unit. Onscreen interactive help function is available. Cable included. RCS version.0 is available for those who do not wish to update from TotalChrom (TC) 6.. and/or for those who need to use a TurboMatrix HS unit with revision.0 or lower firmware. Sample Trays TurboMatrix 0 Mid-Range Sample Tray 0-position sample tray for use on the mid-range headspace sampler. TurboMatrix 0 High-Capacity Sample Tray 0-position sample tray for use on the high-capacity headspace sampler. Tools O-Ring Removal Tool For replacing O-Rings in upper and lower seal assemblies. Headspace Vial Gauge Used to check 0 ml headspace vials for correct dimensions. Adapter Sleeve Torsion Bar For loosening upper seal. Thumbscrew Removal Tool For removing lower seal assembly. Spigot Key For loosening lower seal. Open End Wrench, / - 5/6 in. For use in mounting the Transfer Line. N B079 0 B B B00 0 B M059 M Headspace Accessories and Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit 5

62 Gas Chromatography Headspace Accessories and Supplies Headspace Accessories and Supplies Headspace Accessories Open End Wrench, Sw-7 Transfer Line End Cap PE Injector Transfer Line Adapter TurboMatrix and HS 0XL Adapter Kits for Non-PerkinElmer Gas Chromatographs All kits include a Modified Septum Nut Adapter and the instructions for physical installation and interfacing of the two instruments. Use the standard PerkinElmer cables (N006, needed) for ready/run connections. Headspace Adapter Kit for Carlo Erba For connecting a TurboMatrix or HS 0 (XL) headspace sampler to a Carlo Erba Mega or Vega gas chromatograph. Headspace Adapter Kit for Fisons Series 8000 For connecting a TurboMatrix or HS 0 (XL) headspace sampler to a Fisons Series 8000 gas chromatograph. Headspace Adapter Kit for Gerstel CIS Injector For connecting a TurboMatrix or HS 0 (XL) headspace sampler to a Gerstel Cooled Injector System Inlet. As the Gerstel injector can be installed on several GC models, customer should contact the GC manufacturer for the appropriate Remote Start/Stop Cable. B Headspace Adapter Kit for HP 6890, HP 6850, or HP 5890 On-Column B B B B B For connecting a TurboMatrix or HS 0 (XL) headspace sampler to an on-column injector of an HP 6890, HP 6850, HP 5890, or HP 5890 Series gas chromatograph. Note: Installation on HP 6890 and HP 6850 requires a TurboMatrix/HS 0 (XL) to HP 6890/6850 GC Ready/Start Cable (N60-00). For installation on HP 5890, customer should contact Hewlett-Packard for the appropriate Remote Start/Stop Cable. B Headspace Adapter Kit for Shimadzu For connecting a TurboMatrix or HS 0 (XL) headspace sampler to the following Shimadzu gas chromatographs: GC 9a for capillary columns, A packed columns, B packed columns, 7A packed, and capillary columns. B Headspace Adapter Kit for Shimadzu GCA/B For connecting a TurboMatrix or HS 0 (XL) headspace sampler to a Shimadzu GC A/B gas chromatograph with capillary columns. Headspace Adapter Kit for Shimadzu GC6 For connecting a TurboMatrix or HS 0 (XL) headspace sampler to a Shimadzu GC 6 gas chromatograph. Headspace Adapter Kit for Thermo Trace GC For connecting a TurboMatrix or HS 0(XL) headspace sampler to a Thermo Trace gas chromatograph. Headspace Adapter Kit for Varian Capillary Column Injector For connecting a TurboMatrix or HS 0(XL) headspace sampler to a Varian 00 or 800 gas chromatograph capillary column injector. Customer should contact Varian for the appropriate Remote Start/Stop Cable. N Headspace Adapter Kit for Varian Packed Column Injector For connecting a TurboMatrix or HS 0(XL) headspace sampler to a Varian 00 or 800 gas chromatograph packed column injector. Customer should contact Varian for the appropriate Remote Start/Stop Cable. B Headspace Adapter Kit for Varian/Finnigan ITS0 For connecting a TurboMatrix or HS 0(XL) headspace sampler to a Varian/Finnigan ITS0 GC/MS System. Installation Instructions: Headspace to Non-PerkinElmer Gas Chromatographs B B N6000 B Instructions for physical installation and interfacing of the TurboMatrix or HS 0(XL) headspace sampler to non-perkinelmer GCs. Note: This kit is intended for GC s not listed above. B

63 TurboMatrix Headspace to HP 6890 GC Ready Start Cable Connects a TurboMatrix Headspace Sampler to an HP 6890 or HP 6850 GC. Note: Customer should contact gas chromatograph manufacturer for the appropriate Remote Start/Stop Cable. Start/Ready Cables Description HS 0XL to Agilent 6890 GC N For all PerkinElmer GCs and HP 5890 ( needed) N006 5 TurboMatrix Headspace/HS 0/ HS 0XL Replacement Parts and Needle Identification Needle Identification The number of rings engraved into the needle top in various types of needles. Number of Rings Number of Rings Needle Type for Stainless Steel for Platinum Iridium Wide-Bore none Small-Bore none Jet Replacement Parts Headspace Accessories and Supplies N Description Platinum/Iridium Needle, Wide-Bore B069 7 Platinum/Iridium Needle, Small-Bore B Platinum/Iridium Needle, Jet B Silcosteel Needle, for Headspace Trap Only N Stainless Steel Needle, Wide-Bore B Stainless Steel Needle, Small-Bore B Stainless Steel Needle, Jet (ships with instrument) B Needle Seal Assembly (without O-Rings) B O-Ring for Needle Seal Assembly (pkg. 0) B0980 Vespel Ferrule 6 in. (pkg. 0) Male Nut 6 in. N908 5 GLT Adapter Tube B GLT Adapter Tube, Silcosteel N Graphite/Vespel Ferrule 6 in. x 0. mm (for use with 0.5 mm i.d. transfer line, pkg. 0) Graphite/Vespel Ferrule 6 in. x 0.5 mm (for use with 0. mm i.d. transfer line, pkg. 0) Nut 6 in. Swagelok N Fused-Silica Capillary Transfer Line: 0.5 mm i.d. x 5 m length N mm i.d. x 5 m length N TurboMatrix Upgrade Kits Headspace Accessories TurboMatrix 6 to 0 Upgrade Kit (Headspace Only) Includes parts to upgrade an entry-level headspace sampler to a mid-range headspace sampler that can perform automated analysis of up to 0 vials with overlapping themostatting of up to vials. Installation by PerkinElmer Service is required, but not included. M TurboMatrix 6 to 0 Upgrade Kit (Headspace Only) Includes parts to upgrade an entry-level headspace sampler to a high-capacity headspace sampler that can perform automated analysis of up to 0 vials with overlapping themostatting of up to vials. Installation by PerkinElmer Service is required, but not included. M TurboMatrix 0 to 0 Upgrade Kit (Headspace and Headspace Trap) Includes parts to upgrade a mid-range headspace sampler to a high-capacity headspace sampler that can perform automated analysis of up to 00 vials with overlapping themostatting of up to vials. Installation by PerkinElmer Service is required, but not included. M Note: Requires, but does not include, an options board (M055) to be installed in the headspace sampler. Installation by PerkinElmer Service is required, but not included Headspace Accessories and Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit 7

64 Gas Chromatography Headspace Accessories and Supplies Headspace Accessories and Supplies Headspace Vials, Caps, and Septa Headspace Caps and Septa Patented safety springs and caps designed to release at vial headspace pressures above 7 psi. Aluminum-Coated Silicone Rubber Headspace Septa Includes caps and starsprings (9 mm diameter). Maximum temp. 0 C. Description pkg. 00 B00 0 pkg. 000 B pkg. 000 (preassembled) B Butyl Rubber Headspace Septa Includes caps and starsprings (9 mm diameter). Maximum temp. 00 C. Description pkg. 00 B pkg. 000 B pkg. 000 (preassembled) N PTFE-Coated Butyl Rubber Headspace Septa Includes caps and starsprings (9 mm diameter). Maximum temp. 00 C. Description pkg. 00 B pkg. 000 B000 6 pkg. 000 (preassembled) B PTFE-Coated Silicone Rubber Headspace Septa Includes caps and starsprings (9 mm diameter). Maximum temp. 0 C. Description pkg. 00 B00 86 pkg. 000 B00 77 pkg. 000 (preassembled) B Headspace Septa Recommended Temperature Chart Upper Temperature Material Limit at Vial Inertness Butyl Rubber 00 C Poor PTFE-Coated Butyl Rubber 00 C Good Aluminum-Coated Silicone 0 to 0 C Good PTFE-Coated Silicone 0 C Good Headspace Vials Headspace Starter Kit Consisting of 000 vials (B006), two sets of septa, each with aluminum caps and starsprings: 00 PTFE-coated butyl rubber septa (B009), 00 PTFE-coated silicon rubber septa (B00). Also included are: hand crimper (N90785), pressure gauge with needle for vials (B05077), two needle seal assemblies (B05008), 0 O-Rings (B0980), and a book by B. Kolb and L.S. Ettre, Static Headspace Gas Chromatography Theory and Practice (N00). Headspace Safety Sample Vials B Description pkg. 000 B

65 Vial Crimping Tools Benchtop Crimper The PerkinElmer Benchtop Crimper with interchangeable jaws provides a fast and consistent crimp on each vial, every time. Once crimping pressure is set, the lever action will repeatedly afford the user a perfectly crimped vial, with little effort. Jaws and decrimping jaws are available for mm and 0 mm crimp caps. Description Benchtop Crimper with 0 mm Jaw N Benchtop Crimper without Jaws N Jaws for Benchtop Crimper, mm N Jaws for Benchtop Crimper, 0 mm N66009 Headspace Accessories and Supplies Headspace Vials, Caps, and Septa Electronic Crimpers New from PerkinElmer, the 0 mm electronic crimpers and decappers are easy to use and fully rechargeable. Ergonomically designed to alleviate the potential for Carpal Tunnel Syndrome and provide a consistent crimp pressure numerous times. The electronic crimper is provided with a standard Black and Decker VeraPak Gold battery and charging unit. This hand-held device will crimp several hundred vials from one charge. Crimping pressure is fully adjustable for precision control. Also available in mm. See page 90. Features and Benefits: Precision control crimping Ergonomically designed grip Numerous reproducible crimps from a single charge Includes standard Black and Decker VersaPak Gold battery and charger Description 0 mm Electronic Hand Crimper, 0 V N mm Electronic Hand Crimper, 00 V N mm Electronic Hand Crimper, 0 V N mm Electronic Hand Crimper, 0 V N mm Electronic Hand Decapper, 0 V N mm Electronic Hand Decapper, 00 V N mm Electronic Hand Decapper, 0 V N mm Electronic Hand Decapper, 0 V N Electronic Crimper Battery N9058 Hand Crimpers Hand Crimper N9057 Description Hand Held Crimper, 0 mm N Hand Held Decapper, 0 mm N Headspace Accessories and Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit 9

66 Injectors Capillary Injectors Injector Replacement Parts Components Gas Chromatography Injectors 8 Manual Gas Control Injector Cover N608 Septum Cap N Thermogreen TM Septum (pkg. 50)* N Injector Top Nut N Injector Head N60058 O-Ring, Silicone for Glass Liner (pkg. 0) N607 9 Maximum injector temperature 50 C, O-Ring, Graphite for Glass Liner (pkg. 5) N6078 Maximum injector temperature 50 C. O-Ring, KALREZ for Glass Liner (pkg. ) N Maximum injector temperature 50 C. O-Ring, Viton for Glass liner (pkg. ) N9078 Maximum injector temperature 50 C, recommended for use with Mass Spec. ships with instrument Quartz Liner ( mm) for Splitless Operation N600 Quartz Liner ( mm) for Split Operation N600 or Large Volume Splitless Injection Glass Liner ( mm) for Splitless Operation N607 Glass Liner ( mm) for Split Operation N Deactivated Liner for Splitless Operation N60 09 mm, packed with wool. (pkg. 5) Deactivated Liner for Split Operation N600 6 mm, packed with wool. (pkg. 5) Deactivated Uniliner N60 mm, packed with wool. (pkg. 5) Injector Body N /8 in. Swagelok TM Nut Brass (pkg. 5) N Restrictor N /8 in. Graphite/Vespel Ferrule (pkg. 0) / in. Graphite Ferrule (pkg. 0) / in. Swagelok Nut, Stainless Steel (pkg. 5) N Injector Adapter N Charcoal Trap N60075 Charcoal Trap for PPC Version** N Split Vent Tube N60059 Column Nut /6 in. Long length for reversed ferrule (pkg. 5) * For more septa, see page 59. ** Not shown. Miscellaneous Accessories Description oz. Replacement Charcoal (0/60 mesh) g. Quartz Wool (Untreated) N605 6 Column Ferrule Graphite/Vespel Liner Removal Tool N Merlin Microseal Adapter Kit N90 Includes: Merlin Microseal septa, nut, and injection port adapter Merlin Microseal Septa N905 8 Zero Dilution Liner (Inner) N06 Zero Dilution Liner (Outer) N

67 Injectors Capillary Injectors Split/Splitless Injector Add-On Kits Capillary Injector with PPC Kit includes split/splitless injector with programmable pneumatic control for carrier gas, split vent, heater, sensor, and heater block. The AutoSystem XL must be PPC ready. If not, a PPC upgrade kit (N606) is required. (See page 66 for more information.) Installation by PerkinElmer Service is required, but not included. Voltage 0 V N608 0 V N609 8 Complete Capillary Injector Add-On Kits Kit includes split/splitless injector in module with heater and sensor, 0-60 psig pressure regulator, and transducer for pressure readout. For manual gas control. Voltage 0 V AutoSystem N V AutoSystem N V Clarus N V Clarus N Dual Capillary Column Adapter Kit Kit includes all necessary hardware to install two capillary columns to a capillary injector. Note: Kit does not include appropriate /8 in. -hole ferrule. (See page 9) For manual gas control. Voltage 0 V N60050 Split/Splitless Injector Starter Kit for Manual Gas Control Includes: mm i.d. quartz liner, mm i.d. quartz liner, silicone O-Rings (0), Thermogreen septa (50), 0.5 mm graphite ferrules (0), 0.8 mm graphite ferrules (0), /6 in. stainless steel nuts (5), untreated quartz wool, packing rod, and wafer scribes (0). N Injectors Gas Chromatography See page for ordering information. For the most current product listing, visit 5

68 Injectors Packed Column Injector Add-On Kits Injector Replacement Parts Gas Chromatography Injectors Packed Column Injector Kit with Manual Pneumatics Includes: complete injector assembly with heater and sensor, 0-00 ml flow controller, and column head pressure gauge for installation into the AutoSystem. Voltage 0 V* N V* N600 5 Packed Column Injector Kit with PPC The kit includes complete injector assembly with programmable pneumatic control, heater, sensor, and heater block. The GC must be PPC ready. If not, a PPC upgrade kit (N606) is required. (See page 66 for more information.) Voltage 0 V* N606 0 V* N Packed Column Injector Kit with Screen Readout and Manual Pneumatics Includes: complete injector assembly with heater and sensor, 0-00 ml flow controller and column head pressure gauge, and transducer for screen readout of column carrier flow. Voltage 0 V* AutoSystem N V* AutoSystem N V* Clarus N V* Clarus N Packed Column Injector Kit AutoSystem XL and Clarus The kit includes complete injector, heater, sensor, and heater block. (Does not include pneumatics.) Voltage 0 V* N V* N Packed Column Injector Starter Kit Includes glass liner, needle guide, Thermogreen septa (50), untreated quartz wool, and packing rod. Packed On-Column Injector for / in. (Long-Legged) Glass Columns N For use with / in. (long-legged) on-column glass column. Includes: complete injector, heater, and sensor and heater block. Does NOT include pneumatics. Voltage 0 V* N V* N * Service installation required. 5 Description Septum Cap N Septa Thermogreen (pkg. 50)** N Needle Guide N Glass Liner N Quartz Liner N6000 Packed Injector Assembly N ** For more septa see page

69 Injectors Packed Column Injector Miscellaneous Accessories Injector/Detector Adapter / in. Adapter fits on injector and detector outlet (inside oven) for use with / in. columns. Liner Removal Tool Allows easy removal of glass liners from injector port N Quartz Wool Quartz wool (untreated) for packing glass liners. (5 g.) Silanized Glass Wool Packing for wide-bore glass liners. ( oz.) Wide-Bore Adapter Kit 0.5 Capillary Column Adapter Kit N Silanized Glass Wool The AutoSystem Wide-Bore Adapter Kit allows conversion of the packed inlet for 0.5 mm capillary column operation. The kit includes 0-0 ml flow control element, wide-bore adapter with /6 in. fitting, wide-bore glass liner, and column support hanger. Can be used in both on-column and off-column modes of operation. N Injectors Gas Chromatography See page for ordering information. For the most current product listing, visit 5

70 Injectors POC Injector POC Replacement Parts 5 Components Septum Cap N Septa (pkg. 50)** N Needle Guide N Liner/Hour Glass N Body Assembly N ** For more septa see page 59. Programmed-Temperature On-Column Injector System The Programmed-Temperature On-Column (POC) Inlet is designed to be used with fused-silica capillary columns. The sample is injected onto the column while the inlet is cool.after the injection, the inlet begins to heat. This delay in heating avoids the flash vaporization associated with a normal injection. This explosive vaporization can cause thermal breakdown and/or discrimination of certain analytes, which can be avoided by using the POC. Gas Chromatography Injectors 5 The POC Injector is best used to achieve recovery of compounds of greater than C 60 (e.g., polywaxes). The POC utilizes flow control, producing the best recovery out to C 00 or greater. POC Injector with Manual Flow Controller and Head Pressure Gauge Kit includes all necessary hardware to install injector into AutoSystem Series or Clarus Series. Voltage 0 V* N V* N POC Injector with Manual Flow Controller and Head Pressure Gauge with Flow Readout on Screen Kit includes all necessary hardware to install injector into AutoSystem Series or Clarus Series. Voltage 0 V* N V* N POC Injector with PPC Add-On Kit Kit includes injector with programmable pneumatic control, heater, sensor, and heater block. The AutoSystem XL or Clarus GC must be PPC TM ready. If not, a PPC upgrade kit (N606) is required. (See page 66 for more information.) Installation by PerkinElmer Service is required, but not included. Voltage 0 V* N60 0 V* N60 9 POC Injector Starter Kit Includes: needle guides (5), universal connectors (5), 0.5 mm i.d. deactivated fused silica (5 m), /6 in. stainless steel nuts (5), 0.8 mm graphite ferrules (0), Thermogreen septa (50), and wafer scribes (0). * Service installation suggested. AutoSystem firmware revision.7 or higher. Operator s manual ( ) revision F or greater. N

71 Injectors PSS Injector Programmed-Temperature Split/Splitless Injector System PSS Injector Add-On Kits with Manual Pneumatics The programmed-temperature split/splitless (PSS) inlet allows accurate sample delivery to a capillary column. The PSS allows the analysis of thermally labile compounds, while eliminating the discrimination of high-boiling compounds. One of the major advantages of the PSS is that any nonvolatile material will remain in the inlet liner and not on the front of the column. PSS with pneumatics and pressure readout on screen. Kit includes all necessary hardware to install injector into GC. Voltage 0 V* AutoSystem N V* AutoSystem N V* Clarus N V* Clarus N PSS Injector with PPC Kit includes injector with programmable pneumatic control, heater, sensor, and heater block. The GC must be PPC ready. If not, a PPC upgrade kit (N606) is required. (See page 66 for more information.) Voltage 0 V* N600 0 V* N60 6 PSS Injector Starter Kit Includes: universal connectors (5), 0.5 mm i.d. deactivated fused-silica (5 m), mm i.d. quartz liner, mm i.d. quartz liner, glass hourglass liner, /6 in. stainless steel nuts (5), 0.5 mm i.d. graphite ferrules (0), 0.8 mm i.d. graphite ferrules (0), Viton O-Rings (6), graphite O-Rings (5), untreated quartz wool, wafer scribes (0), and Thermogreen septa (50). Zero Dilution Liners Used together as set. N Description Inner Liner N06 Outer Liner N07 90 * Service installation suggested. PSS Replacement Parts Description Septum Cap N Injector Cover N608 Septa** (pkg. 50) N Trap, Charcoal non PPC version N60075 PPC version (not shown) N Nut N Septum Purge N O-Ring Viton (pkg. 0) max. temp N C, recommended for use with mass spec. Shipped with instrument. O-Ring KALREZ (pkg. ) max. temp. 50 C O-Ring Graphite (pkg. 5) N6075 max. temp. 50 C Quartz Liner, mm Split Mode N600 7 Shipped with instrument. Quartz Liner, mm Splitless Mode N On-column liner N Body Assembly N Ferrule /8 in. x /6 in. (pkg. 0) Nut /8 in Split Vent Line N60059 Purge Restrictor N Nut ** For more septa see page Manual Pneumatic Control (non-ppc) Injectors Gas Chromatography See page for ordering information. For the most current product listing, visit 55

72 Injectors PreVent Gas Chromatography Injectors Enhanced Large Volume Injection Allows the use of chlorinated solvents with an electron capture detector. PreVent Time-Saver Mode Conventional C5 00 C C6 0 Analyze Cleanup Equilibrate PreVent 00 Analyze Cleanup Equilibrate μl of 0 pg/μl Pesticide Solution in n-hexane 50 μl of 0 pg/μl Solution in Methylene Chloride Three Successive Injections of Diesel Oil Normal Injection Septum changed and liner inspected during run Normal Injection PreVent Isolation Mode Eliminates downtime during routine injector maintenance. Can provide approximately 00 extra analytical hours of productivity per system per year. ELVI Mode Facilitates manual injection volumes up to 50 μl and automatic injection volumes up to 50 μl without solvent reaching the column or detector. Time-Saver Mode Prevents unwanted, high molecular weight material from reaching the detector. Shortens analysis time, facilitates isothermal chromatography and protects the detector from contamination. ProTect Mode Eliminates contamination by preventing heavy components in the sample from reaching the expensive and retentive chromatographic column. Allows backflushing during chromatographic run. PreVent Add-On Kit Kit includes all necessary hardware to add PreVent capability to an existing PSS injector with PPC or to a capillary injector with PPC. Includes restrictor and mid-point PPC module. PreVent Hourglass Guide PreVent Restrictor Description 0.06 mm i.d., 08 mm Length N to 0.5 mm i.d., 0 mm Length N600 7 PreVent Spacer ProTect Add-On Kit Includes all the necessary parts to add a ProTect accessory to a Clarus GC. Includes one ProTect column. ProTect Replacement Column MSVent Add-On Kit for the Clarus 500 GC/MS Includes all the necessary parts to add an MSVent accessory to a Clarus GC/MS.* * Requires a PreVent option (N60) to be already installed in the Clarus 500 GC gas chromatograph. N60 09 N N N N N

73 Injector Supplies Injector Liners Glass Inlet Liners Inlet liners for split injection have mixing chambers with tortuous flow paths to allow full vaporization of the sample. Deactivating the surface of these liners prevents active compounds from degrading. Packing the liner with wool will trap non-volatile residue and prevent column contamination when analyzing dirty samples. Inlet liners for splitless injection are generally designed as straight tubes, although new designs such as the gooseneck will help contain the sample in the injector. Packing these liners with wool will also help trap non-volatile residue and prevent column contamination. Capillary Split/Splitless Injector Liners ID OD Length Pk Description mm mm mm Size NEW! PSS Splitless Glass Liner Siltek Deactivated Surface Liner (with wool) N General purpose use, ideal for chlorinated pesticides analyses Split Glass Liner Siltek Deactivated Surface Liner (with wool) Universal liner for general N600 6 purpose analyses. Surface provides inertness over a wide sample ph range. Wool can be adsorptive if fibers are broken NEW! Split Glass Liner (with wool) N Universal liner for general purpose analyses NEW! Split Siltek Deactivated Glass Liner (with wool) Universal liner for general purpose N analyses. Deactivated surface provides minimal bleed and inertness over a wide sample ph range NEW! Clarus Cup Split Glass Liner Good for both high and low molecular weight N compounds. Sample vaporization is aided by tortuous flow path and minimizes molecular weight discrimination. Difficult to clean NEW! Clarus Cyclosplitter Glass Liner Patented cylindrical design for dirty samples, N easy to clean and allows many injections before cleaning is required. Not recommended for large volume injections Uniliner Deactivated Glass Liner (with wool) N60 Universal liner for general purpose analyses NEW! Clarus Splitless Glass Liner Low volume sample analyses, beneficial with N headspace and purge/trap Quartz Liner for Splitless Operation (ships with instrument) N600 Standard injector liner Glass Liner for Splitless Operation N607 Universal liner for general purpose analyses Deactivated Glass Liner for Splitless Operation (with wool) N60 09 Good for analyses of trace samples NEW! Siltek Deactivated Liner (with wool) for Splitless Operation Optimum sample N dispertion for active samples. Surface provides inertness over a wide sample ph range. Wool can be adsorptive if fibers are broken Quartz Liner for Split Operation N600 Good for large volume injection samples Glass Liner for Split Operation N Universal liner for general purpose analyses NEW! Siltek Deactivated Double Gooseneck Glass Liner (with wool) Optimum sample N65000 dispertion for active samples. Decreases breakdown of active compounds such as endrin and DDT. Chamber contains sample vaporization cloud. Not suitable for PPC systems NEW! Cyclo Double Gooseneck Liner for Split Operation Cylindrical design for large N volume and trace dirty samples. Decreases injection port discrimination. Cannot be packed with wool and more difficult to clean Zero Dilution Glass Outer Liner Ideal for trace HS work N05 7 Use in conjunction with N06 Zero Dilution Glass Inner Liner Ideal for trace HS work N06 Use in conjunction with N05 Column installs at left side of image. Injector Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit 57

74 Injector Supplies Injector Liners Programmed Temperature Split/Splitless (PSS) Injector Liners Column installs at left side of image. ID OD Length Pk Description mm mm mm Size Gas Chromatography Injector Supplies Packed Column Injector Liners Column installs at left side of image. Quartz Liner for Splitless operation (ships with instrument) 86. N Excellent liner for low volume analyses NEW! Siltek Deactivated Glass PSS Liner N Used for low volume trace sample analyses Quartz Liner for Split operation (ships with instrument) 86. N600 7 Approved PerkinElmer standard injector liner NEW! Siltek Deactivated Glass Liner for Split operation N (with wool) Maximum inertness and packed with wool gives optimum sample dispersion. Surface provides inertness over wide sample ph range. Wool can be adsorptive if fibers are broken NEW! Siltek Deactivated Glass Liner for Split operation Max N inertness gives optimum sample dispersion. Deactivated surface provides minimal bleed and inertness over a wide sample ph range Zero Dilution Outer Liner.8 8 N07 90 Use in conjunction with N06 Zero Dilution Inner Liner 7 N06 Use in conjunction with N07 On-column Glass Liner. 86. N Liner/Hour Glass for POC Injector N ID OD Length Pk Description mm mm mm Size Drilled Uniliner (hole on top) Excellent liner for high sample N60 recovery and linearity, recommended for aqueous injections. Good for PPC equipped GCs NEW! Drilled Uniliner (hole on bottom) Recommended for analysis N in which compounds of interest could be affected by a tailing solvent peak. Good for PPC equipped GCs NEW! Gooseneck Drilled Uniliner (hole on top) Use for trace, active N samples, high recovery and linearity NEW! Gooseneck Drilled Uniliner (hole on bottom) Use for trace, N active samples, high recovery and linearity NEW! Open Top Uniliner (with wool) Packed with fused silica wool, N65006 highly recommended for high molecular weight active samples. The fused silica wool traps dirt and sample residue NEW! Cyclo Uniliner Cylindrical design for high molecular weight N samples provides an excellent vaporization surface. Spiral traps dirt reducing further residue sample interaction Wide-Bore Column Glass Liner 6 9. N Wide-Bore Column On/Off Quartz Liner 6 9. N600 58

75 Injector Supplies Injector Septa Merlin MicroSeal Merlin MicroSeal Adapter Kit Increase lifetime with over 000 injections Step sealing system Temperature ranges up to 5 C Pressure ranges 0 to 00 psi Low bleed, long life alternative for injector port septa Quick and easy installation The Merlin MicroSeal Septa is a unique replacement septa employing a two-step sealing system and an advanced elastomer material. Because the syringe needle does not pierce the septa, there is no debris and ghost peaks are greatly reduced. The MicroSeal Septa also reduces the incidence of bent syringe needles and liner contamination. Usable in either manual or autosampler applications, this septa can improve your productivity and run reliability. Designed to be used with gauge straight needle syringes. Pressure ranges from to 00 psi and injection port temperatures up to 5 C. Easy installation on most PerkinElmer chromatographs. Merlin MicroSeal Nut Merlin MicroSeal Adaptor High Pressure Merlin MicroSeal Kit: Includes: Merlin MicroSeal septa, nut, and injection port adapter. Merlin MicroSeal Septum Merlin MicroSeal Septa. (pkg ) Septa for Use with All Injectors PTFE-Silicone Injector Septa Merlin MicroSeal Septum Maximum recommended operating temperature 00 C. mm diameter. N90 N905 8 Description Package of Package of Merlin MicroSeal Septum Cut-Away View Syringe needle Syringe needle wiper O-rings seal needle during injection Microseal septum Duckbill opens easily, seals reliably BTO TM (Bleed Temperature Optimized) Injector Septa Maximum recommended operating temperature 00 C. Low bleed, high temperature. mm diameter. Description Package of 50 N Thermogreen Injector Septa Maximum recommended operating temperature 50 C. Low bleed, high temperature. mm diameter. Description Package of 50 N Low Bleed Injector Septa Maximum recommended operating temperature 0 C. mm diameter. Description Package of 50 N90 8 Silicone Injector Septa Septum nut aligns needle Septum cup Spring Maximum recommended operating temperature 50 C. mm diameter. Description Package of Injector Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit 59

76 Injector Supplies Subambient Accessories Gas Chromatography Injector Supplies PerkinElmer offers subambient systems which are microprocessor controlled. This control allows precise injection of coolant for the greatest accuracy. Our design assures you of minimum thermal gradients, thereby eliminating the peak splitting often found in other systems. NOTE: All of the subambient systems require, but do not include, PerkinElmer Service installation. Pressure Ratings LN 0 0 psi CO psi AutoSystem Subambient Accessories Liquid Carbon Dioxide (CO ) Subambient Accessory Contains all of the necessary hardware to add subambient capability. Capable of operating down to -50 C. Installation by PerkinElmer Service is required, but not included. Liquid Nitrogen (LN ) Subambient Accessory Contains all of the necessary hardware to add subambient capability. Capable of operating down to -99 C. Installation by PerkinElmer Service is required, but not included. Liquid Nitrogen (LN ) Subambient Accessory for Temperature Programmable Injectors N N Contains all of the necessary hardware to add subambient capability to two temperature programmable injectors (PSS/Program Split Splitless, POC/Program On-Column) on one Gas Chromatograph. Capable of operation down to -99 C. Requires but does not include oven LN subambient. Installation by PerkinElmer Service is required, but not included. N Subambient Accessories Liquid Carbon Dioxide (CO ) Subambient Accessory Contains all the necessary hardware to add subambient capability to AutoSystem XL or Clarus GC. Operating temperature range down to -50 C. Installation by PerkinElmer Service is required, but not included. N6059 Liquid Nitrogen (LN ) Subambient Accessory Contains all the necessary hardware to add subambient capability to AutoSystem XL or Clarus GC. Operating temperature range down to -99 C. Installation by PerkinElmer Service is required, but not included. N

77 Injector Supplies Syringes Autosampler Syringes Replacement Syringe Needle Description Volume/o.d. Low injection volume analysis. 0.5 μl/0.6 N605 0 N Plunger type: metal plunger in needle. Routine analysis. Shipped with instrument. 5 μl/0.6 N Plunger metal plunger in barrel with Teflon -tipped seal. 0.5 capillary column on-column injection. 5 μl/0.7 N6080 Plunger type: metal plunger in barrel. Low injection volume. 0.5 capillary on-column injection. 5 μl/0.7 N605 0 N Plunger type: metal plunger in needle. Routine analysis, plunger type: metal plunger in barrel. 5 μl/0.6 N605 0 Metal plunger in barrel type 50 μl/0.7 N μl/0.6 N Needle Syringes Why a 7 cm Needle? All PerkinElmer injectors have been tested and optimized for use with a 7 cm needle. A 7 cm needle is critical to be sure your sample is deposited in the optimal zone. Point Style General-purpose point style designed for septum penetration in all chromatographic techniques. The needle has a bevel with the tip slightly bent to minimize coring and needle plugging. Point Style Needle has a 90 bevel. Point style is recommended when the syringe is used for accurate pipetting of liquids. Excellent for mixing standards of very small volume. Fixed Needle Syringes Syringe P.S. # P.S. # Capacity 0 μl μl* μl N μl N μl N Fixed Needle Syringe Six Pack Contains six syringes (0 μl, fixed needle, point style #, 0005). Fitted with 7 cm needle. Removable Needle Syringes (RN) N900 6 Syringe P.S. # Capacity 0 μl* N μl N μl N μl N μl N μl N905 * Standard syringe but fitted with 7 cm needle for PerkinElmer injectors. Injector Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit 6

78 Injector Supplies Syringes Gas Chromatography Injector Supplies Replacement Needles for Removable Needle Syringes (RN) Syringe P.S. # Capacity Gauge Length Qty. 0 μl** 6S 7 cm pkg. N μl 6S in. pkg. N μl S in. pkg. N μl S in. pkg. N μl S in. pkg. N906 5 Replacement Needles for RN Syringes Needle Gauge Volume 6S 0 μl N90 5 S 5, 50, 00 μl N90 5 S 50 μl N906 5 P.S. = Point Style ** Recommended for PerkinElmer injectors. Syringes Gas Tight Fixed Removable Syringe Needle (N) Needle (RN) Capacity 0 μl N900 6 N μl N90 59 N μl N90 7 N μl N μl N N μl N N ml N N ml N ml N ml N N ml Gas Tight Syringe N9066 Ultramicro Volume Syringes Recommended for liquid sample injections of less than 5 μl for gas chromatography. Syringes come standard with needle length of 7 cm optimum for PerkinElmer injectors. Syringe Needle Syringe Capacity Gauge 0.5 μl 5 N90.0 μl 6* μl μl 5 N905.0 μl N μl * Recommended for PerkinElmer Wide-Bore Capillary Adapter. 6

79 Laboratory Supplies Gas Sampling Supplies Filters and Traps Carrier Gas Filter for GC/MS in. long with /8 in. fitting. Gas In-line Filter This in-line filter removes moisture, oil, and particulate from gas supplies. Large capacity filter requires fewer filter changes, and improves baseline stability and chromatographic results. Free-standing model also available. Maximum pressure 00 psig. Trap packing can be refilled. Approximate dimensions: / x 7 in. with /8 in. fittings. Description Base-Mount Filter N In-line Gas Filter N Packing Refill Kit (sufficient for two refills) N Hydrocarbon Trap Use our activated charcoal in-line trap to remove gaseous hydrocarbons from carrier gas supply. This trap will remove all hydrocarbons at room temperature except methane. Essential for purge- and-trap systems, or high-sensitivity FID operation when contamination is a problem. Maximum pressure 000 psig. Frits at the end prevent any particles from entering the gas stream. Trap is purged with nitrogen and should be purged with the gas you plan to use. Approximate dimensions: x in. with /8 in. fittings. Indicating Oxygen Trap Indicating trap has a capacity of 0 cc of pure oxygen. The trap has a maximum pressure of 00 psig. The trap is shipped in the active state purged with hydrogen. It is recommended that you purge the trap with the gas you will be using. Approximate dimensions: /8 x 0 / in. Includes /8 in. fittings. It is recommended that the indicating trap be used downstream of the high-capacity oxygen trap. N Gas Flow High-Capacity Oxygen Filter Indicating Oxygen Filter Indicating Packing N N909 7 Gas Flow Oxygen Trap High efficiency oxygen trap has a capacity of.5 liters at room temperature. It is also effective for removing sulfur compounds such as hydrogen sulfide and mercaptans. This oxygen trap is for use with nonoxidizing gases such as; He, Ar, N, and CH. Oxygen removal to below 70 ppb using normal GC flow rates. The catalyst is a copper-based material that forms copper oxide in the presence of oxygen; no gas is produced from this reaction. This trap is intended for use with gases containing less than % oxygen. The trap is delivered active purged with nitrogen. (Purging with the gas you will be using is recommended.) Maximum pressure 000 psig. Approximate dimensions: x in. including fitting end; fittings are /8 in. Safe Glass Moisture Trap N In-line moisture trap. Drierite indicating agent and Molecular Sieve 5A are packed in glass which is enclosed in a safety plastic tube in the event the glass breaks. Unique loading design allows operation in any orientation without channeling. For use with pressures up to 00 psig. Designed for use with GC detectors that require high-purity gases. Recommended for ELCD and ECD systems in which moisture and contamination are a problem. Trap is shipped active and purged with nitrogen. It is recommended that you purge the trap with the gas you plan to use. Approximate dimensions: /8 x 0 / in. with /8 in. end fittings. Recommended Filters N Detector Carrier Gas H Air ECD Moisture Trap and Oxygen Trap ELCD Hydrocarbon Trap* Hydrocarbon Trap FID Hydrocarbon Trap* Moisture Trap Moisture Trap FPD Hydrocarbon Trap* Moisture Trap Moisture Trap MS Indicating Oxygen Trap NPD Hydrocarbon Trap* Moisture Trap Moisture Trap PID Hydrocarbon Trap* TCD Hydrocarbon Trap* * Oxygen Trap if capillary columns are used. Note: All gases MUST have a minimum purity of %. Gases for either ELCD or mass spectrometer MUST have a minimum purity of %. Laboratory Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit 6

80 Laboratory Supplies Gas Sampling Supplies Gas Purification Systems Gas Chromatography Laboratory Supplies All-In-One Gas Purification System The trace contaminant removal available from the three-cartridge Gas Purification System is now available in a single-cartridge system. The purifier consists of a manifold head and an all-welded steel cartridge with a multiple-layer adsorbent bed to sequentially remove water, oxygen, sulfur compounds, and hydrocarbons. The All-In-One Gas Purification System has a capacity for oxygen of at least 50 cc, enough to purify eight 9 cu. ft. tanks of % pure helium. Water capacity is at least.7 g, while capacity for hydrocarbons (as n-butane) is 5. g. The system comes ready to wall mount, but may be bench-mounted by removing from the bracket and attaching to a bench-mount base (included). It is shipped fully activated and filled with high-purity helium. Product Gas Purification System with Trap,.8 in. Fittings N Replacement Cartridge N Gas Supply Installation Kit Including hardware to hook up three gas supplies to gas chromatograph. Kit includes: () safety gas flow restrictor for hydrogen ( ), () restrictor warning tag (00096), () restrictor tag (000960), (50 ft.) /8 in. refrigeration grade copper tubing (N900077), (6) /8 in. Swagelok nut (09908), (6) /8 in. brass front ferrules (09909), (6) /8 in. brass rear ferrules (09900), () /8 in. Swagelok brass -way tee (099070), () / in. NPT x /8 in. Swagelok adapter ( ), and () / in. NPT x /8 in. NPT reducer female (0990). N6500 Three-Cartridge Gas Purification System This system will provide in-line contaminant removal for your GC gases. This system has convenient replaceable cartridges with a visual indicator. The PerkinElmer Gas system consists of three cartridges in series to reduce column damaging impurities. The first cartridge in the system will remove residual hydrocarbons and water from the carrier gas stream. The second cartridge provides high-capacity oxygen removal (capacity is at least 000 cc of pure oxygen); the third cartridge contains an inorganic indicator that changes from light green to gray to provide warning when the high-capacity oxygen trap is depleted. All systems are helium leak tested after assembly. Approximate dimensions: cm W x cm H x 8 cm D; weight kg. Cartridges are easy to replace High capacity Wall bracket gets the system up and out of the way Product Gas Purification System, /8 in. fittings N complete system (includes all three traps) Hydrocarbon Moisture Replacement Cartridge N High Capacity Oxygen Replacement Cartridge N Indicating Oxygen Replacement Cartridge N Replacement Cartridge Set, one each N hydrocarbon/moisture, high-capacity oxygen and indicating oxygen Bypass Accessory, allows operation of system N when installed in place of cartridge Bench Mount Adapter N

81 Laboratory Supplies Gas Sampling Supplies High Purity Brass Regulators PerkinElmer regulators are constructed of high-purity brass barstock and have stainless steel diaphragms and metal-to-metal seals. They are suitable for use with high-purity (>99.995% pure) non-corrosive gases. Regulators terminate in a / in. NPT Swagelok fitting. Barstock body construction Stainless steel diaphragms Metal-to-metal seals Use with high-purity carrier gas High-purity Brass Regulators (Dual Stage) Delivery Cylinder CGA Delivery Pressure Pressure Gauge Fitting Pressure Use Range (psig) Gauge (psig) (psig) CGA-50 H and Ar/CH mixes CGA-580 He, Ar High-purity Brass Regulators (Single Stage) Delivery Cylinder CGA Delivery Pressure Pressure Gauge Fitting Pressure Use Range (psig) Gauge (psig) (psig) CGA-50 H and Ar/CH mixes CGA-580 He, Ar CGA-590* Air * Supplied with Adapter. PG-H Pure Gas Hydrogen Generators The PG-H series Hydrogen Generators employ the newest membrane technology available for the safe production of pure hydrogen gas. The patented DBS PG-H series of Hydrogen Pure Gas Generators is ideal for operation with gas analyzers, as fuel gas for flame tools, or as a source of pure hydrogen. Electrolytic membrane technology is preferred over alternative hydrogen generating techniques because it is clean, requires less maintenance, and there is no need to store chemicals to maintain operation. Only pure water, either distilled or deionized, is required to provide trouble-free, long-term operation. Features and Benefits: LCD display shows set points, operating conditions and status Continuous or intermittent operation Visual operating status lights Alarm conditions Flow indicator informs the operator at a glance that hydrogen gas is flowing at the specified rate Bi-directional RS interface Selectable auto start Remote control (optional) Cascading of or more units (optional) PC-Control capability PG-H Series Hydrogen Generator High-Purity Brass Regulator Safety Straps Nylon adjustable cylinder safety straps hold tanks securely to bench top or wall. Model/Component Wall Mount N Bench Mount N Model/Component Deionizer Bag N Desiccant Cartridge, Fitting, and Refill Kit N Desiccant Refill (pkg. ) N PG-H 00 Hydrogen Generator 00 ml/min. N PG-H 60 Hydrogen Generator 60 ml/min. N PG-H 50 Hydrogen Generator 50 ml/min. N PG-H 500 Hydrogen Generator 500 ml/min. N Laboratory Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit 65

82 Laboratory Supplies Instrument Pneumatics Accessories Gas Chromatography Laboratory Supplies Manual Pneumatics 0-0 ml/min. Flow Accessory For use when converting a flow controller for low flow applications. Auxiliary Gas Pneumatics Box For use with carrier or combustion gas psig gauge. This compact unit comes in either wall or bench mount, with or without toggle valve for quick shutoff. Design allows several units to be installed together. /8 in. Swagelok fittings for gas inlet/outlet. Mounting screws included. Dimensions: 5 x x 7 in. (D x W x H). Description With Toggle Valve N Without Toggle Valve N Flow Controller and Gauge with Screen Readout Includes: flow controller, gauge, and transducer for mounting into an empty instrument pneumatic panel. PPC Detector Control Pneumatics Add-On Kit Kit includes parts to add one channel of PPC control for detector gas to an existing detector. For use with hydrogen or air on FID, NPD, and FPD; makeup on ECD and PID. The GC must be PPC ready. If not, a PPC upgrade kit (N606) is required. Requires, but does not include, appropriate PPC frit (see table). Note: Do not use for ELCD or TCD makeup. These require special kits with tees. The AutoSystem XL must be PPC ready. If not, a PPC upgrade kit (N606) is required. Installation by PerkinElmer Service is required, but not included. PPC Flow Control Pneumatics Add-On Kit for Packed or POC Injector N N N608 9 Kit includes parts to add PPC flow control for carrier gas to an existing packed or POC injector. Requires but does not include appropriate PPC frit (see table). The GC must be PPC ready. If not, a PPC upgrade kit (N606) is required. Installation by PerkinElmer Service is required, but not included. N609 0 PPC Upgrade Kit Kit includes the main control board and hardware to add PPC capability to an existing AutoSystem XL or Clarus Gas Chromatograph. Installation by PerkinElmer Service is required, but not included. Preset Pressure Regulator Consists of a preset (0 psig) nonadjustable pressure regulator for use with manual detector gas controls. Recommended for use on hydrogen and air for FID. Pressure Regulator with Screen Readout Includes pressure regulator (0-60 psig) and transducer for mounting into an empty instrument panel. PPC Frits N606 5 N607 9 N60005 Injector/ Detector Gas Frit No. Color ECD Argon/ Black N Methane or Nitrogen FID Air 6 Blue N FID Hydrogen Black N FPD Air 5 Green N FPD Hydrogen Black N NPD Air 5 Green N NPD Hydrogen Silver N605 8 Packed Carrier Black N POC Carrier Yellow N605 8 POC Carrier Use Red N605 8 for Low Flows (i.e., < ml/min.) Split/Splitless Carrier 6 Blue N or PSS TCD Helium Black N TCD Hydrogen Yellow N

83 Laboratory Supplies Maintenance Supplies Flow Meters Tools Digital Flow Meter The PerkinElmer Model 570 meets ISO 9000 and Good Laboratory Practice (GLP) requirements. The flow meter comes with a Certificate of Calibration that states all of the traceability information needed for ISO-9000 compliance. The Model 570 is uniquely indentified by serial number, internal instrument number, and date(s) of calibration. It is also capable of periodic recalibration. Product Digital Flow Meter N Replacement Glass for Digital Flow Meter N PerkinElmer Electronic Flowmeter 000 Flow range ml/min. Operating Temperature 0 to 5 C Traceable to NIST Primary Standard Split Ratio Mode Accuracy +/- -% LCD Alphanumeric Display The PerkinElmer Flowmeter 000 allows for rapid real-time flow measurements. Flow rates measured in ml/min. (volumetric flow). The PerkinElmer Flowmeter 000 can quickly calculate split ratios. Ratios are displayed in real time. Flowmeter not compatible with corrosive or flammable gases. Portable operation. (9 V battery included). Soap Bubble Flow Meters N The glass soap bubble flow meters are calibrated in and 0 ml two-stage or, 0, and 00 ml three-stage for easy flow reading. Bubble meters come complete with liquid soap, rubber squeeze bulb, miscellaneous-sized plastic tube pieces to adapt to various fittings, and instructions (stand required, but not included N90). Product Two-stage Three-stage N Stand N90 7 Adjustable Wrench Adjustable in. steel wrench for cylinder pressure regulators. Wrench opens out to / in. Fits all regulators listed in this catalog. Basic Tool Kit Tools come in tool box for easy storage and use. Kit includes: open-end wrench set (6 pc.), screwdriver set (6 pc.), adjustable wrench (6 in.), chain nose pliers (narrow), wire cutters, and wire strippers. Deluxe Tool Kit Great for use on all lab instruments! Kit includes the following tools: openend wrench set (6 pc.), screwdriver set (6 pc.), adjustable wrench (6 in.), chain nose pliers (narrow), wire cutters, wire strippers, slip-joint pliers (6 in.), long nose No. 5 stainless steel tweezers ( /8 in.), needle file set (6 pc.), Allen key set ( pc. imperial sizes), and Allen key set (9 pc. metric sizes). Shipped in a plastic tool box for convenient storage. 6-Piece, Open-End Wrench Set Six sizes. Includes: / x 5/6 in. 5/6 x /8 in. /8 x /6 in. 7/6 x / in. / x 9/6 in. 9/6 x 5/8 in. Tubing N90 55 N907 N N Description Qty. Precleaned Copper Tubing 50 ft. N Teflon Tubing, /8 in. o.d. ft Teflon Tubing, /6 in. o.d. Hall Solvent Lines ft Tygon Tubing, / in. i.d., /8 in. o.d. for ft Water and Air (not for carrier gas) Laboratory Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit 67

84 Laboratory Supplies Valves Valves Gas Chromatography Laboratory Supplies There are two types of valves offered. Internal Volume sample size is determined by an etched rotor inside the valve. External Volume sample size is determined by a sample loop outside the valve. External valves are used primarily for sample injection and/or switching applications. A valve used for just switching requires another valve for sample injection. Valves include nuts and ferrules, but not loops. -Port Valve Requires 90 actuator and standoff for automatic operation. Replacement Max. Max. Valve Rotor Rotation Temp. Pressure Fitting (in.) Coating 90 0 C 00 psi /6 N Port Valve Requires 60 actuator and standoff for automatic operation C 00 psi /6 N C 00 psi /6 N C 00 psi /8 N Port Valve Requires 60 actuator and standoff for automatic operation C 00 psi /6 N N C 00 psi /6 N908 8 N C 00 psi /8 N N Port Valve Requires 5 actuator and standoff for automatic operation C 00 psi /6 N C 00 psi /6 N C 00 psi /8 N Port Valve Requires 6 actuator and standoff for automatic operation C 00 psi /6 N N C 00 psi /6 N N C 00 psi /8 N9080* 765 * Special /8 in. standoff included. 8-Port Valve N

85 Laboratory Supplies Valves/Loops -Port Internal Valve and Rotor for Liquid Sample Injection Replacement Valve Rotor Fixed Volume (μl) Fitting Size Port Diameter 0.06 /6 in N /6 in N N /6 in N N /8 in N Max. Temp. = 75 C, Max. Pressure = 500 psi, Fitting Size = /6 in. These valves require a 90 actuator and standoff for automatic operation. Sample Loops -Port Internal Valve and Rotor Sample Loops 6-Port 8-Port 0-Port Volume Size 00 μl /6 in. N N N μl /8 in. N N μl /6 in. N N N μl /8 in. N μl /6 in. N N μl /8 in. N N ml /6 in. N N N ml /8 in. N N ml /6 in. N N N ml /8 in. N N ml /6 in. N N ml /8 in. N N /8 in. fitting loop for valves with 0.00 in. standard port diameter. /6 in. fitting loop for valves with 0.06 in. standard port diameter. Laboratory Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit 69

86 Laboratory Supplies Valve Accessories Adapters Fused-Silica Adapters These adapters allow connection of fused-silica to unions, valve ports, and reducers. Gas Chromatography Laboratory Supplies Description i.d. Colum i.d. Fitting 0.5 mm 0.8 mm mm /6 in. N Fused-Silica Tubing Stainless Steel Nut Valve Body Air Actuators Rotor mm 0.5 mm /6 in. N Any /6 in. N mm 0.8 mm mm /6 in. N mm 0.5 mm /6 in. N Any /6 in. N Removable Polyimide Liner Polyimide Ferrule Slot Standard Port Diameter For Use With Degree Rotation - and -port valves 90 N port valves 60 N port valves 5 N port valves 6 N Actuator Knob N909 Actuator Knob Manual knob allows manual switching of valves. Can be used with any valve or standoff listed, except closemount assembly. Air Actuator Extension Kit Angle Bracket N Extension screw allows easy tightening of the air actuator to the standoff. Required on AutoSystem Series/Clarus GC. Closemount N90908 N909 8 N Angle Bracket General purpose bracket for mounting standoff and actuators. Closemount Assembly Allows close mounting of actuator and valve. Primarily used for mounting valve outside oven. (Not to be used with manual actuator knobs) Restrictor Rotor Removal Tool At ambient conditions, flows range from -00 ml/min. (inlet at 5 psi). Includes: stainless steel lines (8 in. long, /6 in. o.d., 0.00 in. i.d.) and inlet filter. Magnet end allows easy removal of rotor from valves. N N90908 N908 0 N

87 Laboratory Supplies Valve Accessories Special Standoff for 0-Port Valve This standoff will allow connection of a 0-port /8 in. valve to the AutoSystem Series/Clarus GC. N Starter Kit N908 7 Standoffs A standoff supports both the actuator and the valve. The standoff places the valve at the specific distance from the actuator. A /8 in. standoff is recommended for mounting valves in PerkinElmer GC ovens. Standoff and actuator sold separately. Length in. N / in. N /8 in. N in. N909 5 Kits Sample Loop Air Actuator Mounting Kit Solenoid Kit Fitting Solenoid Sample Valve Mounting Bracket Column Kit includes all necessary hardware to install valves on AutoSystem Series/Clarus GC. Each kit is capable of mounting up to two gas valves inside the oven. Includes detailed instructions that show how to use gas valves, set up timed events, and configure the AutoSystem GC software. N Kit is required for each air actuator. Solenoid Kit allows precise pulse of air needed to drive air actuator. Kit includes instructions. For use with AutoSystem Series/Clarus GC only. N Kit includes: Description Qty. u Screen Filter for use with 6 N90880 Replacement Filters for N90879 Filter Union /6 in. with Removable N90879 Screen for use with Gas Line Filter Reducer /8 in. Swagelok to /6 in. N9097 Valco for Packed Column Adapter Reducer /8 in. Swagelok Male Nut N908 to /6 in. Valco for Injector/Detector Adapter Stainless Steel Tubing, 50 cm, N909 /6 in. o.d. to 0.0 in. i.d. for Carrier to detector Stainless Steel Tubing, 5 cm, N /6 in. o.d. to 0.0 in. i.d. for Sample Input/Output Valco Ferrule /6 in. 0 N9085 Valco Nut /6 in.* 6 N908 * Cannot be used with fused-silica adapters (N9086 or N9087). Tubing Kits Particulate contamination is the leading cause of valve failure. This tubing has been washed and precleaned, with solvent and microfiltered steam from deionized water to remove organic and ionic particulate contamination. Each kit contains two pieces of /6 in. o.d. S/S tubing. 0.0 in. Length 0 cm N cm N cm N cm N Laboratory Supplies Gas Chromatography See page for ordering information. For the most current product listing, visit 7

88 Laboratory Supplies Valve Fittings Gas Sampling Valve Fittings Ferrules Description Qty. /6 in. stainless steel pkg. N /8 in. stainless steel pkg. N Gas Chromatography Laboratory Supplies Plugs and Caps Reducers /8 in. HEX / in. HEX Standard Nuts Unions / in. HEX / in. HEX 7/6 in. HEX 7/6 in. HEX Description Qty. /6 in. plug pkg. N /8 in. plug pkg. N /6 in. cap pkg. N /8 in. cap pkg. N909 0 Description Qty. /8 in. Swagelok TM to /6 in. Valco pkg. N9097 /6 in. adapter for /6 in. port pkg. N908 Description Qty. /6 in. pkg. N908 5 /8 in. pkg. N908 Description Qty. /6 in. to / in. reducing union pkg. N /6 in. union pkg. N /8 in. to /6 in. reducing union pkg. N /8 in. union pkg. N

89 TotalChrom Software TotalChrom Data Handling Systems Chromatography Data Systems A proven solution with leading edge productivity. Streamlining Your Laboratory Workflow The entire process, from setting up an analytical method to the final approval of reports, is a streamlined series of operations in TotalChrom. TotalChrom features TC Publisher, a powerful application that extends report capabilities beyond the standard templates by providing a sophisticated laboratory report generator using standardized tools. Unique features let you graphically format the exact report as needed without extensive training or special commands. It ensures that the stages of chromatographic analysis, report generation and distribution are quick, easy, and complete. low resolution image TotalChrom Navigator Screen PerkinElmer s TotalChrom Chromatography Data System is designed to provide laboratories with the total answer to chromatography data-handling needs. Acquiring, processing, reporting, reviewing, and approving data is a streamlined series of operations in PerkinElmer s TotalChrom Chromatography Data Systems (CDS), software designed to fit your laboratory workflow and maximize productivity. With its scalable architecture, CFR Part compliance features and proven algorithms, TotalChrom offers a computing strategy to manage your chromatography data quickly and securely in both regulated and non-regulated environments. When configured with a PerkinElmer Clarus 500 Gas Chromatograph or a PerkinElmer Series 00 Liquid Chromatograph, the TotalChrom Data System is the controller and data manager for the overall system. In addition, TotalChrom can also control selected instruments from other vendors and can acquire data from any chromatographic system through A/D interface. Report templates can perform calculations between different peaks in the same sample or even between samples, as well as automate statistical determination for replicate injections, with full control over the output format. Quickly and Easily Navigate, Review, and Approve Your Data In the paper world, reports need to be reviewed and signed. The TotalChrom Review & Approve (R&A) feature is a Graphical Reviewing environment that allows intuitive navigation into data and reports, and provides for the implementation of a data approval cycle. With TotalChrom R&A, chromatograms, raw data, results, and reports can be easily viewed and compared at a glance. Reviewing and approving reports can be done electronically, with multiple levels of authority and secure electronic signatures. High-throughput applications have dramatically increased the amount of information produced every day in a laboratory. This feature streamlines tedious data review by using one single environment to navigate into data, just like we, every day, navigate into . TCPublisher Replicate Injections Report TotalChrom Client/Server (TC C/S) Data System is the solution in multi-user environments. TC C/S systems can easily integrate all existing chromatographs into a single networked system supporting an unlimited number of users and an unlimited number of chromatographs. TCPublisher Single Injection Report TCPublisher Dual Channel Report 7

90 Software Intelligent Interfaces Software Gas Chromatography dotlink dotlink Interfacing with ease. All totalchrom systems utilize PerkinElmer Intelligent Interfaces to connect each chromatography system to the data system PC. Each interface contains buffered RAM memory to maintain data collection in the event that the PC or PC network becomes inoperative during data acquisition. Data from instruments is never lost and chromatograph productivity is preserved. Analog chromatographs connect to TotalChrom through NCI (Network Chromatograpy Interface) Series Intelligent Interfaces. The model NCI 90 is a single-channel device, while the model NCI 90 is a dual-channel device. Both interface models are capable of taking analog detector data (unipolar or bipolar) at sampling rates from 0. to 00 Hz. dotlink is a Windows CE-based interface that allows you to connect your Clarus GC, Agilent 00 GC, Agilent 6890 GC, and Series 00 HPLC directly to the network. Designed to face today s workload challenges and provide Ethernet connectivity, dotlink allows external buffering with a minimal need for validation. The dotlink box integral link has a small footprint, providing valuable space for your laboratory. dotlink supports the following GC and HPLC configurations: Maximum of PerkinElmer Clarus GCs Maximum of PerkinElmer Series 00 HPLC System Stack Maximum of Agilent 6890 GCs Maximum of Agilent 00 HPLC/UV System Stack dotlink Recommended Model Applications Memory dotlink - Clarus 500 GCs MB N Integral Link Integral Link for Clarus GC Provides a digital-to-digital connection between the Clarus GC and TotalChrom. Requires AutoSystem XL IPM for TotalChrom Workstation or Client/Server Software. Also requires appropriate cable for connection to TotalChrom system. N Integral LINK for Clarus GC and TotalChrom Workstation Software Provides digital-to-digital connection between the Clarus GC and TotalChrom Chromatography Workstation or the Clarus 500 Mass Spectrometer. Includes Integral LINK, TotalChrom Workstation Software, AutoSystem XL IPM, and serial cable. Analog Board with Integral LINK* Description Analog Board with Integral LINK N Analog Board with Integral LINK N and TotalChrom Workstation Software * For ARNEL Analyzers only. NCI Intelligent Interfaces NCI Series Intelligent Interfaces are bit, either single or dual-channel, buffered, A/D converters which have softwareselectable input voltage ranges of 0,,, and 0. V with 6 decade dynamic range, programmable sampling rates from 0. to 00 points per second selectable in TotalChrom software, less than microvolt noise (peak to peak), 0.% linearity, three sense input lines, and one-system READY relay for communication with Autosamplers. Includes: a board containing seven programmable relays and a Rack/Vial Port (TTL voltage levels) for reading Autosampler vial BCD information. Memory is segmentable for multiple chromatograms. Software selectable symmetric bipolar or unipolar mode operation. All Interfaces carry a -year return to Service Depot warranty. Model NCI 90 Intelligent Interface with RVP/Relay Board Single-channel A/D with 56KB RAM memory and RVP/ Relay board. Stores up to 0K data points. Unipolar/ bipolar operation modes. Requires but does not include one IEEE or RS interface cable. Includes power cord. Voltage 0 V S V S Model NCI 90 Intelligent Interface with RVP/Relay Board N Dual-channel A/D with 56KB RAM memory and RVP/ Relay board. Stores up to 0K data points. Unipolar/ bipolar operation modes. Requires but does not include one IEEE or RS interface cable. Includes power cord. Voltage 0 V S V S

91 Software Intelligent Interfaces Power Cords 0 V No charge when ordered with 0 V Interface. Country UK, Cyprus, Nigeria, Zimbabwe, Singapore, 0999 Malaysia, Zambia Australia, New Zealand Europe, Saudi Arabia, Egypt, South Africa, India, Thailand, China Denmark, Greenland Switzerland, Liechtenstein SoftLINK SoftLINK Entry-level solution for instrument connectivity. Designed for workstation environments, SoftLINK TM provides instrument connectivity at a glance. SoftLINK is able to control Series 00 HPLC/UV or up to Clarus GC. SoftLINK/TotalChrom Workstation Software Includes: appropriate cable for connection of SoftLINK to TotalChrom system, TotalChrom software, and Clarus 500 GC IPM.** SoftLINK Software Kit Includes: appropriate cable for connection to TotalChrom system, SoftLINK software CD, utilities CD, and the install sheet. USB to Serial Adapter for SoftLINK One serial port is required for each Clarus 500 GC. Additional ports can be added via this USB converter. ** SoftLINK is not available with PerkinElmer-ARNEL systems. N N Software Gas Chromatography See page for ordering information. For the most current product listing, visit 75

92 Software Interface Modules Interface Personality Modules (IPM) Interface Validation Modules (IVM) Gas Chromatography Software IPMs are instrument-specific software programs that interpret and translate instrument control and data acquisition parameters between TotalChrom TM and a specific digital instrument. IPMs are downloaded from the host PC (TotalChrom) by a configuration function to a specific port. (Serial or Ethernet) on a dotlink interface (internal or external). Downloaded IPMs are stored in nonvolatile memory in the dotlink interface. IPM for AutoSystem, AutoSystem XL, and Clarus GCs Provides control for the PerkinElmer AutoSystem Series and Clarus GCs and their associated liquid Autosampler, with simultaneous digital data acquisition from two inboard detectors. Utilizes one serial port on a dotlink interface and may be configured to any port or ports on any LINK interface or interfaces connected to a single TotalChrom acquisition system. For TotalChrom Professional users, v.0 or higher is required, but not included. N IPM for Agilent 5890 Series II and Agilent 5890A GCs Provides control for the Agilent Series 5890 GCs and their associated liquid Autosamplers, with simultaneous digital data acquisition from two inboard detectors. Utilizes one serial port on a Model 600 LINK Series interface and a second port for each associated Autosampler that is to be controlled. This IPM may be configured to any port or ports on any LINK interface or interfaces connected to a single TotalChrom acquisition system. Requires one serial cable for each connected Agilent GC and one serial cable for each connected Autosampler. For TotalChrom Professional users, v.0 or higher is required, but not included. Note: Each Agilent 5890 and 767 autosampler must have the appropriate Agilent serial external controller card(s) and remote start cable installed. N IPM for Agilent 6890/6890Plus Provides control for the Agilent Series 6890 GCs and their associated liquid Autosampler, with simultaneous digital data acquisition from two inboard detectors. Utilizes one serial port on a dotlink. This IPM may be configured to any port or ports on any LINK interface or interfaces connected to a single TotalChrom acquisition system. It is recommended that no more than two Agilent 6890 GCs be configured per workstation LINK interface. Requires one serial cable for each connected Agilent GC. Control of the Agilent 6890/ 6890Plus is not available for TC Pro. N Model 50 Interface Validation Module, 0 V The Model 50 IVM is a calibrated analog peak pattern generator for use in testing/validating analog to digital converters such as the NCI 90/90 and the Series 900/900A Intelligent Interfaces. The module generates eight possible analog patterns at selectable voltage ranges of 0-0., 0-, 0-, and 0-0 volts. Factory calibration is traceable to a NIST standard volt. Includes remote start/stop cable and analog signal cable for connection to PerkinElmer NCI/900/900A Series Intelligent Interfaces. Includes -year return to Service Depot warranty. Voltage 0 V S V S TotalChrom Workstation Model 50 IVM Software Allows user to test any NCI Series and M900A Series Intelligent Interfaces to validate interface operations (linearity, reproducibility, etc.). Contains special TotalChrom interface test methods and automated validation logs to maintain results of interface tests in software. Requires, but does not include, a Model 50 Interface Validation Module. N

93 Software Serial Cables IEEE Cables All TC Versions Serial Cables Cable Length m m m m External Communications Cable Shielded DB9 Male/Female 9-pin external RS- communications cable. For M9/M600 LINK Interfaces Cable Length 7 ft. S ft. S ft. S ft. S For M950/970 Interfaces Cable Length 7 ft. S ft. S ft. S ft. S For NCI Interfaces Cable Length 7 ft. S ft. S ft. S ft. S For dotlink Interfaces Cable Length 0 ft ft For M9A and M600/60 Link Interfaces Cable Length 7 ft. S ft. S ft. S ft. S For NCI Interfaces TotalChrom TM WS and C/S Serial Cables to Lantronix Terminal Server TotalChrom WS and C/S Serial Cables to PC Cable Length 7 ft. S ft. S ft. S ft. S Agilent 6890 HS0/ATD00 Ready/Run Cables N Description Cable Kit, HS0/ATD00 to Agilent 6890 N Cable Kit, M950/970 Series Interface to Agilent 6890 N Serial Cables* for Instrument Interface Description PerkinElmer Clarus GC to dotlink, 0 ft PerkinElmer Clarus GC to dotlink, 5 ft PerkinElmer Clarus GC to M600/M60 LINK, 0 ft. PerkinElmer Clarus GC to M600/M60 LINK, 5 ft. M900/960/970 Series Interface to M600/M60 S5000 LINK, 6 ft. (not for M9) NCI Series Interface to dotlink, 7 ft. S NCI Series Interface to M600/M60 LINK, 6 ft. S5000 Agilent 00 GC-Autosampler to dotlink, 0 ft (Required quantity: ) Agilent 5A Autosampler Controller S50005 (on 5890GC) to M600/M60 LINK, 0 ft. Agilent 5A Autosampler Controller S (on 5890GC) to M600/M60 LINK, 5 ft. Agilent 5890A/Series II GC to M600/M60 LINK, 0 ft. Agilent 6890 GC/-Agilent 6890Plus GC Autosampler to dotlink, 0 ft. Agilent 6890 GC/-Agilent 6890Plus GC Autosampler to dotlink, 5 ft. Agilent 6890 GC/-Agilent 6890Plus GC- S50005 Autosampler to M600/M60 LINK, 0 ft. Agilent 6890 GC/-Agilent 6890Plus GC- S Autosampler to M600/M60 LINK, 5 ft. Agilent 767A Autosampler Controller (on 5890GC) to M600/M60 LINK, 0 ft. Agilent 767A Autosampler Controller (on 5890GC) to M600/M60 LINK, 5 ft. * Special serial cards, instrument communication kits, and IPM software may be required to complete interfacing of a LINK interface to a digital chromatograph. Please contact your local PerkinElmer Sales Representative for details. M900 Series BCD Cables for Autosamplers Description PerkinElmer HS00, HS0, ATD50, AS000, AS Software Gas Chromatography See page for ordering information. For the most current product listing, visit 77

94 Software Software Kits Serial Communications Cards for TurboChrom TotalChrom Workstation SI/DI Upgrade Kits Gas Chromatography Software Agilent 5890A/Series II GC Description Serial Card S Agilent 767A Controller Description Remote Start Cable S Serial Card and Control Board S Serial Card and EPROM S TotalChrom Workstation Manuals Application Manager s Guide Application Manager s Guide covering installation and system management of TotalChrom Workstation software. Manual Set Complete manual set including User s Guide (volumes and ), Application Manager s Guide, and Tutorial. TotalChrom Tutorial Software tutorial that teaches basic data acquisition, method development, optimization techniques, sequence development, and calibration. User s Guide (Volumes and ) User s manual covering instrument configuration and basic operation of TotalChrom TM Workstation software. N N N N v6.x Workstation Migration to v6..x Workstation Migrates an existing TurboChrom TM Workstation v.x or v6.x acquisition system, and associated RPO systems, to TotalChrom Workstation v6..x software. Requires verification of ownership of TurboChrom v6.x software. Software supplied on CD-ROM media v.x or v6.x. N v6..x Workstation Migration to v6..x Workstation Migrates an existing TotalChrom Workstation v6..x acquisition system, and associated RPO systems, to TotalChrom Workstation v6..x software. Requires verification of ownership of TotalChrom v6..x software. Software supplied on CD-ROM media. TotalChrom Workstation Software N Description Multi-Instrument Software Kit N Reprocess-Only Software Kit N

95 Thermal Desorbers TurboMatrix Thermal Desorbers TurboMatrix Thermal Desorbers for GC... driving unrivaled Performance through Innovation. Thermal desorption is a technique that simplifies and speeds a wide range of gas chromatography (GC) applications, including indoor and outdoor air monitoring, analysis of outgassing from semiconductor materials, polymers, upholstery and furnishings, packaging, pharmaceuticals, and analysis of flavors and fragrances. As the undisputed market leader in GC sample handling, we took the next step to offer you even more benefits for your lab. PerkinElmer offers a family of five different TurboMatrix TM Thermal Desorber (TD) models in both single-tube and automated 50-tube configurations: TurboMatrix 00 TD single-tube and manual pneumatics TurboMatrix 50 ATD 50-tube autosampler and manual pneumatics TurboMatrix 00 TD single-tube and programmable pneumatic control TurboMatrix 50 ATD 50-tube autosampler and programmable pneumatic control TurboMatrix 650 ATD 50-tube autosampler, programmable pneumatic control and a variety of other accessories for a wide range of applications This broad offering allows you to match technology to your laboratory and applications needs. Confirmatory Analysis The TurboMatrix 650 ATD allows samplesplit re-collection on same or different tubes, delivering the ability to audit samples and perform confirmatory analysis and repeat analysis under a different set of conditions. Integrity Testing Sensors monitor all aspects of system operation to ensure that the instrument is working as it should and provide an early indication of possible problems with the analysis. Analytical techniques such as tube and trap impedance testing and the standard addition options help ensure sample integrity. All of these are designed to provide the user with the highest confidence in the final analytical results. Reduced Cost Per Sample The TurboMatrix Thermal Desorbers save money and minimize laboratory waste. After each use, all sample tubes can be reconditioned and conveniently reused. The system provides cryogenfree operation down to -0 C, reducing operating costs. Unlike other techniques, thermal desorption requires no solvents, thus reducing cost, risk of contamination, analyst exposure and the need for solvent disposal. Maximize Sample Throughput Since the thermal desorber unit can run simultaneously with the GC, you can start your next desorption run as the GC processes the previous run for maximum productivity. Improved chromatography and narrow peak widths as a result of 0 C per second trap heating rate Higher productivity with overlapping tube desorption and chromatography Wider boiling range analysis and improved water management using the backflush mode, where multiple adsorbents can be used in series Uncompromised narrow-bore capillary chromatography due to rapid desorption of the focusing trap (0 C per second) 79

96 Thermal Desorbers Ozone Precursor Accessories Gas Chromatography Thermal Desorbers Air Toxics Columns Methyl Silicone Column For use with Air Toxics TM (T0) Analyzer System with FID/ECD detectors. 00 m x 0. mm i.d. x 5 μm. Methyl Silicone Column The STS 5 is used for sequential sampling of air onto a series of up to ATD sample tubes. It is a portable unit and can be operated either by a V battery or 0/0 V. The sampler includes cables with jack plug connectors (for use with the monitoring pump) and a set of diffusion limiting caps. The STS 5 requires but does not include sample tubes and a monitoring pump. Also requires a V battery or an electrical adapter. L V Rechargeable Battery Waterproof, suitable for outdoor use. Air Monitoring Pump 0 V Cable For connecting the STS-5 to a generic V battery. N For use with the Air Toxics (T0) Analyzer System with Mass Spectrometer 60 m x 0. mm i.d. x 5 μm. Model STS 5 Sequential Tube Sampler Model STS 5 Accessories N L L L85007 Diffusion Limiting Caps (pkg. 5) Electrical Adapter Allows for direct connection to wall outlet. Also acts as a battery charger for V battery (0/0 V). Personal Monitoring Pump Description Size 5-00 ml/min. 0 V N ml/min. 0 V N STS 5 Maintenance Kit Description Includes: Rotor Tube Seals (pkg. 50), Filter N Disks (pkg. 5), Diffusion Limiting Caps (pkg. 5), and Rotor Seal (pkg. 0) Rotor Filter Disk L80 5 Viton O-Ring For use in diffusion limiting cap and tube seals. (pkg. 50) Ozone Precursor Accessories Alumina PLOT TM Column 50 m x 0. mm i.d. ATD 00 Air Monitoring Trap Low flow trap packed with carbonaceous sorbents suitable for ozone precursor and air toxics monitoring. (pkg. ) Methyl Silicone Column 50 m x 0. i.d. x.0 μm Nafion Dryer Particulate Filter Kit Includes disposable filter and fittings. For use in the ozone precursor analyzer. Restrictor Tubing 0.0 mm i.d. uncoated, deactivated, fused-silica restrictor tubing. For use in the ozone precursor analyzer. N L7508 N L L N L750 7 N

97 Thermal Desorbers Sample Tubes Caps for TurboMatrix Brass Long-Term Storage Caps Recommended for long-term storage. Two required per tube. Also requires Teflon ferrule (L0005). (pkg. ) Combined Teflon Ferrule For use with / in. Brass Long-term Storage Cap ( ). Two () required per tube. (pkg. ) Diffusion Caps Standard For passive air sampling to ensure correct diffusion path length. (pkg. 0) Diffusion Caps with Membrane Same as above but with a silicone membrane. (pkg. 0) Pen Clips For stainless steel ATD tubes. (pkg. 0) PFA Teflon Ferrules for TurboMatrix Storage End Caps (pkg. 0) TurboMatrix Analytical Caps Required for use on the TurboMatrix instrument during analysis PTFE Caps with O-Ring. (pkg. 0) Replacement Parts for ATD 00 Tube Seal and Tube L L L L0709 M065 8 N Description Qty. Packed Sample Tube(s)* Sample Tube(s)* Packing Retaining Gauzes 00 L070 Retaining Springs 50 L07 86 Chamfer Holder O-Ring Tube Seal O-Ring Grip Seal O-Ring Nozzle Filter Disk L759 * See Sample Tube product listing above Sample Tubes for TurboMatrix Packed Sample Tubes for TurboMatrix Pkg. Stainless Steel Glass Qty. Sorbent 0** Air Toxics Tube N N ** Carbopack B 60/80 N N ** Carbopack B 60/80 N N Carbopack C 60/80 Carbosieve SIII 60/80 0** Carbosieve SIII 60/80 N N ** Chromasorb 06 N N ** NIOSH 59 tube N N ** Tenax GR 60/80 N N ** Tenax TA 60/80 N N ** Shipped with brass long-term storage caps. Packed Sample Tubes for TurboMatrix Empty Sample Tubes with Caps Glass Lined Pkg. Stainless Steel Stainless Steel Glass Qty. 0* M M M * M * Shipped with Analytical End Caps (N6009). Empty Sample Tubes Without Caps Pkg. Stainless Steel Glass Qty. 0 L708 L L709 Thermal Desorbers Gas Chromatography See page for ordering information. For the most current product listing, visit 8