Choose for Your Instrument

Transcription

1 Choose for Your Instrument GC Supplies - Instrument Quick Pick Guide Agilent Technologies Bruker/Scion (Varian) PerkinElmer Shimadzu Thermo Scientific

2 GC Supplies - Instrument Quick Pick Guide Choose for Your Instrument Your chromatography analysis does not end with the selection of the GC column. The combination of components selected for your instrument also make an important contribution to successful separations. Choose SGE to improve your chromatography. Sample Introduction Syringes The SGE Diamond Syringe Range offers significantly improved levels of durability, clarity and accuracy. SGE manual and autosampler syringes are designed for optimal sample introduction. Choose from a comprehensive range of syringe options including plunger protection, removable or fixed needles, a range of needle gauge and length options as well as needle-tip style alternatives. Sample Introduction Septa The role of septa for GC analysis is key as many chromatographic problems are caused by use of inappropriate septa material or inappropriate handling of the septa. Desired septa attributes: Reliably seal against the carrier gas pressure in the inlet. Capable of being pierced and resealed time after time. Capable of being pierced by the syringe needle without pieces being deposited in the GC inlet system. Must not contaminate or bleed material into the chromatographic system. Sample Introduction GC Inlet Liners The GC Inlet liner is where the sample is introduced and vaporized into the gaseous phase. The design of the liner is crucial, as is liner deactivation, to ensure reproducible and accurate chromatography. Sample Introduction GC Connections (ferrules and fittings) SGE GC Connections are designed to minimize time spent on installation, and are suitable for a wide range of applications. Poorly defined or selected connections can lead to an increase in dead volume, leaks and mismatched tubing sizes after temperature cycling.

3 Contents Agilent Technologies 4-7 Bruker/Scion (Varian) 8-11 PerkinElmer Shimadzu Thermo Scientific Expert Tips Choose SGE to improve your chromatography.

4 Agilent Technologies GC Supplies - Instrument Quick Pick Guide Autosampler Syringes All needles are 42 mm long with a cone tip. Agilent 7673, 7683, 7693A & 6850 ALS Volume Needle Gauge (OD mm) Fixed Dual Gauge Needle 23-26s 5 µl (0.63/0.47) 23-26s 10 µl (0.63/0.47) 23-26s 10 µl Gas Tight (0.63/0.47) Fixed Straight Needle Syringe Code Syringe Spare Needle Spare Plunger 5F-AG-0.63/0.47C F-AG-0.63/0.47C F-AG-GT-0.63/0.47C µl 26 (0.47) 5F-AG-0.47C µl (m) 23 (0.63) 5F-AG-0.63C µl 26 (0.47) 10F-AG-0.47C µl (m) 23 (0.63) 10F-AG-0.63C µl (m) Gas Tight 23 (0.63) 10F-AG-GT-0.63C Removable Dual Gauge Needle 23-26s 0.5 µl (0.63/0.47) 23-26s 10 µl Gas Tight (0.63/0.47) Removable Straight Needle 0.5BR-AG-0.63/0.47C * 10R-AG-GT-0.63/0.47C µl 26 (0.47) 0.5BR-AG-0.47C * 0.5 µl (m) 23 (0.63) 0.5BR-AG-0.63C * 1 µl 23 (0.63) 1BR-AG-0.63C * 10 µl 26 (0.47) 10R-AG-0.47C µl (m) 23 (0.63) 10R-AG-0.63C (m) Suitable for use with the Merlin Microseal Injector. * Denotes Spare Needle and Plunger kit. 4

5 Septa Choose from a number of different septa types: GP = For non-demanding routine applications. EC = Combines significantly longer injection life, low bleed and low injection port adhesion. MN = Premium septa for autosamplers, up to 400 injections per septum. HT = Bleed and temperature optimized, combined with outstanding mechanical properties. Type Material Durability Resealing Solvent Resistance Tear Resistance Maximum Temperature GP Silicone Good Good Excellent Good 200 C EC High Temperature Silicone Excellent Excellent Excellent Excellent 400 C MN High Temperature Silicone Excellent Excellent Excellent Excellent 400 C HT BTO Silicone Excellent Excellent Excellent Excellent 400 C Diameter Type For Agilent 7620, 5790, 5880, GP MN For Agilent 5700, 5800, GP EC HT For Agilent 7890, 6890,5890, 5880, 4890, GP EC MN HT For Agilent 5750, 710, 720, 810, GP HT EC

6 Agilent Technologies GC Supplies - Instrument Quick Pick Guide Inlet Liners Description and Geometry For Agilent 5890, 6850, 6890, 7890 and HP4890 Split / Splitless FocusLiner Split / Splitless Taper FocusLiner Split / Splitless FAST FocusLiner Split / Splitless Tapered FAST FocusLiner OD ID Length ConnecTite Liner Standard ConnecTite Liner Top Hole ConnecTite Liner Bottom Hole Split, Straight-through Liner Split, with Quartz Wool Split / Splitless with Single Taper Split / Splitless with Single Taper (Quartz Wool) Split / Splitless with Double Taper Direct, Straight-through Liner Split / Splitless Quartz, Straight-through Liner Splitless with Recessed Gooseneck Split / Splitless Recessed Gooseneck (Quartz Wool) Taper / Gooseneck FocusLiner Taper FocusLiner ConnecTite Straight Double Taper PTV/LVI O-rings and Sealing Rings Description Usage Viton O-ring Temperatures up to 300 C. Suitable for liners with OD of 6.3 mm Graphite Sealing Ring Temperatures up to 450 C. Suitable for all inlet liners above except and Graphite Sealing Ring Temperatures up to 450 C. Suitable for use with liners and

7 SilTite FingerTite Ferrules Description Column ID Ferrule ID SilTite Fingertite Agilent INJ / FID Kit mm 0.4 mm * SilTite FingerTite Agilent Capillary / FID Kit mm 0.4 mm * SilTite FingerTite Agilent INJ / MS Kit mm 0.4 mm * SilTite FingerTite Agilent INJ / FID Kit 0.53 mm 0.7 mm * SilTite FingerTite Agilent Injector Kit 0.53 mm 0.7 mm * SilTite FingerTite Agilent Capillary / FID Kit 0.53 mm 0.7 mm * SilTite FingerTite Agilent Capillary Injector Kit 0.53 mm 0.7 mm * Replacement Parts SilTite FingerTite Ferrule 0.4 mm mm 0.4 mm SilTite FingerTite Ferrule 0.5 mm 0.32 mm 0.5 mm SilTite FingerTite Ferrule 0.7 mm 0.53 mm 0.7 mm SilTite FingerTite Blanking Ferrule SilTite FingerTite Female Nut SilTite FingerTite INJ Base Seal mm SilTite FingerTite INJ Base Seal 0.53 mm SilTite FingerTite Capillary Adaptor SilTite FingerTite MS Adaptor SilTite FingerTite FID Detector SilTite FingerTite Injector mm * Each starter kit includes all the parts necessary to convert one GC system (one injector and one detector) to the SilTite FingerTite system. In addition there are five SilTite FingerTite nuts, ten SilTite FingerTite ferrules, and a ferrule install tool which allows you to seat the ferrule in the correct position on the capillary column. Ferrules Instrument Column ID Ferrule ID 15% Graphite / 85% Vespel Ferrules Injectors & Detectors at atmospheric pressure e.g. FID GC-MS Interface Connection 100% Graphite Ferrules Injectors & Detectors at atmospheric pressure e.g. FID (Not for GC-MS) mm 0.4 mm mm 0.5 mm mm 0.8 mm for 1/8" OD ed Columns 1/8" for 1/4" OD ed Columns 1/4" mm 0.4 mm mm 0.5 mm mm 0.8 mm mm 0.5 mm mm 0.8 mm for 1/8" OD ed Columns 1/8" for 1/4" OD ed Columns 1/4" SilTite Metal Ferrules mm 0.4 mm 10* GC-MS Interface Connection (Starter Kit) 0.32 mm 0.5 mm 10* mm 0.8 mm 10* mm 0.4 mm 10 # Split / Splitless Injectors (Starter Kit) 0.32 mm 0.5 mm 10 # mm 0.8 mm 10 # /32" 0.81 mm 10 # Replacement SilTite Metal Ferrules mm 0.4 mm All Connections 0.32 mm 0.5 mm mm 0.8 mm /32" 0.81 mm Replacement SilTite Nuts GC-MS Interface Connection Split / Splitless Injector Replacement SilTite Base Seals Split / Splitless Injector * Includes ten ferrules, two SilTite nuts. # Includes ten ferrules, two SilTite nuts and two SilTite Inlet Base Seals. 7

8 Bruker/Scion (Varian) GC Supplies - Instrument Quick Pick Guide Autosampler Syringes Volume Length Needle Gauge (OD mm) Tip Style Syringe Code Syringe Needle Plunger Bruker/Scion (Varian) 8035, 8100 and 8200 Removable Needle 1 µl* (0.47) Cone 1BR-VA8X ** 10 µl Gas Tight (0.5) S/Hole 10R-GT-VA8X-II Needle Alternatives for P/N (0.5) Bevel N10-VA8035-II (0.63) S/Hole N10-VA8X00H-0.63-II (0.5) S/Hole N10-VA800H-II(0.2) Bruker/Scion (Varian) CP-8400/8410, CP-9010/9050 Fixed Needle 10 µl (0.47) Bevel 10F-VA8400-5/ µl (0.63) Cone 10F-VA8400/BT-5/0.63C Removable Needle 10 µl Gas Tight (0.47) Cone 10R-BT-GT-0.47C *Not suitable for 8200 autosampler. **Denotes Plunger and Needle Kit. Septa Choose from a number of different septa types: GP = For non-demanding routine applications. EC = Combines significantly longer injection life, low bleed and low injection port adhesion. MN = Premium septa for autosamplers, up to 400 injections per septum. HT = Bleed and temperature optimized, combined with outstanding mechanical properties. Type Material Durability Resealing Solvent Resistance Tear Resistance Maximum Temperature GP Silicone Good Good Excellent Good 200 C EC High Temperature Silicone Excellent Excellent Excellent Excellent 400 C MN High Temperature Silicone Excellent Excellent Excellent Excellent 400 C HT BTO Silicone Excellent Excellent Excellent Excellent 400 C Diameter Type For Varian / Bruker 1177 Injector 9 GP EC MN HT For Varian / Bruker 1040, 1041, 1060, 1061 injector 9.5 GP EC HT For Varian / Bruker 1040, 1041, 1060, 1061 injector 11 GP EC MN HT

9 Inlet Liners Description and Geometry For 1177 Injector Split / Splitless FocusLiner Split / Splitless Taper FocusLiner Split / Splitless FAST FocusLiner Split / Splitless Tapered FAST FocusLiner Split, straight-through liner Split, with quartz wool Split / Splitless with single taper Split / Splitless with single taper (quartz wool) Split / Splitless with double taper Direct, straight-through liner OD ID Length Splitless with Recessed Gooseneck Split / Splitless Recessed Gooseneck (quartz wool) For 1075/1077 Injector Split, FAST FocusLiner Split with Quartz Wool Split FocusLiner with Top-end Restriction Splitless FocusLiner with Top-end Restriction Split, Taper FocusLiner Splitless, Slots at Both Ends Split FocusLiner Taper / Gooseneck FocusLiner Taper FocusLiner ConnecTite Straight Double Taper PTV/LVI 9

10 Bruker/Scion (Varian) GC Supplies - Instrument Quick Pick Guide Inlet Liners Continued Description and Geometry For 1078/1079 Injector Sintered Glass, Large Volume Injection (LVI) Liner OD ID Length 5 1.8/ Straight-through Liner SPME liner Splitless with Single Taper Split / Splitless with Single Taper Split / Splitless FocusLiner Split / Splitless Taper FocusLiner For 1093/1094 Injector ConnecTite SPI Liner, (Restriction = 0.25 mm) ConnecTite SPI Liner, (Restriction = 0.5 mm) for 0.53 mm ID On-column ConnecTite SPI Liner, (Restriction = 0.25 mm) Taper / Gooseneck FocusLiner Taper FocusLiner ConnecTite Straight Double Taper PTV/LVI O-rings and Sealing Rings Description Usage Viton O-ring for 1177 Injector Temperatures up to 300 C Graphite Sealing Ring for 1075 & 1077 Injectors Temperatures up to 450 C Graphite Sealing Ring for 1078 & 1079 Injectors Temperatures up to 450 C

11 SilTite FingerTite Ferrules Description Column ID Ferrule ID SilTite FingerTite Bruker/Scion (Varian) Injector/GC-MS Kit mm 0.4 mm * SilTite FingerTite Bruker/Scion (Varian) Injector/FID Kit mm 0.4 mm * SilTite FingerTite Bruker/Scion (Varian) Injector/FID Kit 0.53 mm 0.7 mm * SilTite FingerTite Bruker/Scion (Varian) Injector Kit 0.53 mm 0.7 mm * Replacement Parts SilTite FingerTite Ferrule 0.4 mm mm 0.4 mm SilTite FingerTite Ferrule 0.5 mm 0.32 mm 0.5 mm SilTite FingerTite Ferrule 0.7 mm 0.53 mm 0.7 mm SilTite FingerTite Ferrule Blanking SilTite FingerTite Female Nut * Each starter kit includes all the parts necessary to convert one GC system (one injector and one detector) to the SilTite FingerTite system. In addition there are five SilTite FingerTite nuts, ten SilTite FingerTite ferrules, and a ferrule install tool which allows you to seat the ferrule in the correct position on the capillary column. Ferrules Instrument Column ID Ferrule ID 15% Graphite / 85% Vespel Ferrules mm 0.4 mm GC-MS & Detectors at atmospheric pressure e.g. FID 0.32 mm 0.5 mm mm 0.8 mm ed Columns 1/8" OD ed Columns 1/8" /4" OD ed Columns 1/4" % Graphite Ferrules mm 0.5 mm mm 0.8 mm Injectors & Detectors at atmospheric pressure e.g. FID 1/8" OD ed Columns 1/8" /4" OD ed Columns 1/4" SilTite Metal Ferrules mm 0.4 mm 10* GC-MS Interface Connections (Starter Kit) 0.32 mm 0.5 mm 10* mm 0.8 mm 10* Nuts for Varian Injector Replacement SilTite Ferrules mm 0.4 mm GC-MS Interface Connections 0.32 mm 0.5 mm mm 0.8 mm /32" 0.81 mm Replacement SilTite Nuts SilTite Metal Nuts *Includes ten ferrules, two SilTite nuts. 11

12 PerkinElmer GC Supplies - Instrument Quick Pick Guide Autosampler Syringes All needles are 70 mm long with a cone tip style. PerkinElmer AutoSystem Volume Needle Gauge (OD mm) Syringe Code Syringe Spare Needle Spare Plunger Fixed Needle 5 µl 26 (0.47) 5F-PE-0.47C µl 23 (0.63) 5F-PE-0.63C µl Gas Tight 26 (0.47) 5F-PE-GT-0.47C µl Gas Tight 23 (0.63) 5F-PE-GT-0.63C µl 23 (0.63) 50F-PE-0.63C Removable Needle 0.5 µl 26 (0.47) 0.5BR-PE-0.47C * 0.5 µl 23 (0.63) 0.5BR-PE-0.63C * *Denotes spare Needle and Plunger kit. Septa Choose from a number of different septa types: GP = For non-demanding routine applications. EC = Combines significantly longer injection life, low bleed and low injection port adhesion. MN = Premium septa for autosamplers, up to 400 injections per septum. HT = Bleed and temperature optimized, combined with outstanding mechanical properties. Type Material Durability Resealing Solvent Resistance Tear Resistance Maximum Temperature GP Silicone Good Good Excellent Good 200 C EC High Temperature Silicone Excellent Excellent Excellent Excellent 400 C MN High Temperature Silicone Excellent Excellent Excellent Excellent 400 C HT BTO Silicone Excellent Excellent Excellent Excellent 400 C Diameter Type For PerkinElmer Sigma, 900, 990, 8000 Series, AutoSystem and Clarus 11 GP EC MN HT

13 Inlet Liners Description and Geometry For AutoSystem & Clarus 500, 600 Split / Splitless Single Taper liner Split / Splitless FocusLiner Split / Splitless Taper FocusLiner Split, straight-through liner OD ID Length Splitless, straight-through liner Split / Splitless for PSS injector Split / Splitless FocusLiner for PSS injector Large Volume Injection (LVI) liner for PSS injector, sintered glass ed Column liner For 8000 and Sigma series Split / Splitless Splitless with single taper PTV Liner PTV liner with 0.25 mm ID restriction (recessed gooseneck) For AutoSystem Injectors ConnecTite Liner Standard ConnecTite Liner Top Hole ConnecTite Liner Bottom Hole Taper / Gooseneck FocusLiner Taper FocusLiner ConnecTite Straight Double Taper PTV/LVI O-rings and Sealing Rings Description Usage Viton O-ring Temperatures up to 300 C. For use with 6.2 mm OD liners Graphite Vespel Sealing Ring for PSS system Temperatures up to 325 C. For use with 4 mm OD liners

14 PerkinElmer GC Supplies - Instrument Quick Pick Guide SilTite FingerTite Ferrules Description Column ID Ferrule ID SilTite FingerTite PerkinElmer Injector/GC-MS Starter Kit mm 0.4 mm * SilTite FingerTite PerkinElmer Injector/FID Starter Kit mm 0.4 mm * SilTite FingerTite PerkinElmer Injector/FID Starter Kit 0.53 mm 0.7 mm * SilTite FingerTite PerkinElmer Injector Starter Kit 0.53 mm 0.7 mm * Replacement Parts SilTite FingerTite Ferrule 0.4 mm mm 0.4 mm SilTite FingerTite Ferrule 0.5 mm 0.32 mm 0.5 mm SilTite FingerTite Ferrule 0.7 mm 0.53 mm 0.7 mm SilTite FingerTite Ferrule Blanking SilTite FingerTite Female Nut * Each starter kit includes all the parts necessary to convert one GC system (one injector and one detector) to the SilTite FingerTite system. In addition there are five SilTite FingerTite nuts, ten SilTite FingerTite ferrules, and a ferrule install tool which allows you to seat the ferrule in the correct position on the capillary column. Ferrules Instrument Column ID of Nut Ferrule ID 15% Graphite / 85% Vespel Ferrules mm 1/16" 0.4 mm mm 1/8" 0.4 mm mm 1/16" 0.5 mm For Injectors & Detectors at 0.32 mm 1/8" 0.5 mm atmospheric pressure e.g. FID mm 1/16" 0.8 mm mm 1/8" 0.8 mm /8" OD ed Columns 1/8" 1/8" /4" OD ed Columns 1/4" 1/4" % Graphite Ferrules mm 1/16" 0.5 mm mm 1/8" 0.5 mm For Injectors & Detectors at mm 1/16" 0.8 mm atmospheric pressure e.g. FID (Not for GC-MS) mm 1/8" 0.8 mm /8" OD ed Columns 1/8" 1/8" /4" OD ed Columns 1/4" 1/4" SilTite Metal Ferrules mm 0.4 mm 10* For GC-MS Interface Connection (Starter Kit) 0.32 mm 0.5 mm 10* mm 0.8 mm 10* Replacement SilTite Ferrules mm 0.4 mm For GC-MS Interface Connection 0.32 mm 0.5 mm mm 0.8 mm /32" 0.81 mm Replacement SilTite Nuts Replacement SilTite Nuts *Includes ten ferrules, two SilTite nuts. 14

15 Shimadzu GC Supplies - Instrument Quick Pick Guide Autosampler Syringes All needles are 42 mm long with a cone tip style. Shimadzu AOC14, AOC17 and AOC20 Volume Needle Gauge (OD mm) Syringe Code Syringe Spare Needle Spare Plunger Fixed Needle 5 µl 23 (0.63) 5F-S-0.63C Removable Needle 0.5 µl 26 (0.47) 0.5BR-S-0.47C * 0.5 µl 23 (0.63) 0.5BR-S-0.63C * 10 µl 26 (0.47) 10R-S-0.47C µl 23 (0.63) 10R-S-0.63C µl Gas Tight 23 (0.63) 10R-S-GT-0.63C *Denotes spare Needle and Plunger kit. Septa Choose from a number of different septa types: Enduro Blue = For non-demanding routine applications. EC = Combines significantly longer injection life, low bleed and low injection port adhesion. HT = Bleed and temperature optimized, combined with outstanding mechanical properties. Type Material Durability Resealing Solvent Resistance Enduro Blue Tear Resistance Maximum Temperature High Temperature Silicone Excellent Excellent Excellent Excellent 350 C EC High Temperature Silicone Excellent Excellent Excellent Excellent 400 C HT BTO Silicone Excellent Excellent Excellent Excellent 400 C Type Shimadzu 9A, 14, 15A, 16, 17A, 2010 & 2014 Enduro Blue EC HT

16 Shimadzu GC Supplies - Instrument Quick Pick Guide Inlet Liners Description and Geometry OD ID Length For GC-2010 (SPL-2010 Injector), GC-2014 (SPL-2014 Injector) and GC-17A (SPL-17 Injector) Split / Splitless FocusLiner * Split / Splitless Taper FocusLiner * Split / Splitless FocusLiner Split / Splitless Taper FocusLiner ConnecTite Liner Standard ConnecTite Liner Top Hole ConnecTite Liner Bottom Hole Split, straight-through liner Splitless straight-through liner Split / Splitless with Single Taper Split / Splitless with middle gooseneck Split / Splitless with recessed gooseneck and quartz wool Split / Splitless with middle gooseneck ConnecTite (0.53 mm ID columns) SPME Liner For GC-14(SPL-14 Injector) Split / Splitless FocusLiner Split / Splitless Taper FocusLiner Split / Splitless with 2.0 mm middle gooseneck Split / Splitless with single taper Taper / Gooseneck FocusLiner Taper FocusLiner ConnecTite Straight Double Taper PTV/LVI Splitless, Direct, wide bore liner for Shimadzu 9A/16A GC * When using a standard 42 mm needle for autosamplers, the sample will be injected on top of the wool for this liner. O-rings and Sealing Rings Description Usage Viton O-ring 16 Temperatures up to 300 C. For 2010 & 2014 (SPL-2010 Injector & SPL-2014 Injector) Graphite Sealing Ring Temperatures up to 450 C. For 14, 15A & 16 (SPL-14 injector) Graphite Sealing Ring Temperatures up to 450 C. For 17A (SPL-17 injector)

17 SilTite FingerTite Ferrules Description Column ID Ferrule ID SilTite FingerTite Shimadzu 2010 INJ / FID Starter Kit mm 0.4 mm * SilTite FingerTite Shimadzu 2010 INJ / MS Starter Kit mm 0.4 mm * SilTite FingerTite Shimadzu 2010 INJ / FID Starter Kit 0.53 mm 0.7 mm * SilTite FingerTite Shimadzu 2010 Injector Starter Kit 0.53 mm 0.7 mm * SilTite FingerTite Shimadzu 17A INJ / FID Starter Kit 0.53 mm 0.7 mm * SilTite FingerTite Shimadzu 17A Injector Starter Kit 0.53 mm 0.7 mm * Replacement Parts SilTite FingerTite Ferrule 0.4 mm mm 0.4 mm SilTite FingerTite Ferrule 0.5 mm 0.32 mm 0.5 mm SilTite FingerTite Ferrule 0.7 mm 0.53 mm 0.7 mm SilTite FingerTite Ferrule Blanking SilTite FingerTite Female Nut * Each starter kit includes all the parts necessary to convert one GC system (one injector and one detector) to the SilTite FingerTite system. In addition there are five SilTite FingerTite nuts, ten SilTite FingerTite ferrules, and a ferrule install tool which allows you to seat the ferrule in the correct position on the capillary column. Ferrules Column ID Description GC14A, GC17A, GC2010 and GC2014 Detector / Injectors (Not for MS interfaces or QP2010 Injector) mm ID columns 100% Graphite mm ID columns 100% Graphite mm OD packed columns 100% Graphite mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules n/a SilTite Metal Nuts - Slotted QP5000/5050 Standard MS Interface QP5000-I mm ID columns 15% Graphite/ 85% Vespel Ferrules QP5000-I 0.32 mm ID columns 15% Graphite/ 85% Vespel Ferrules QP5000-II & QP mm ID columns 15% Graphite/ 85% Vespel Ferrules QP5000-II & QP mm ID columns 15% Graphite/ 85% Vespel Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Ferrules n/a SilTite Metal Nuts-QP5000/5050 Standard MS interface QP5000/5050 Wide Bore MS Interface, QP2010 Injector and QP2010 Standard MS Interface mm ID columns 15% Graphite/ 85% Vespel Ferrules mm ID columns 15% Graphite/ 85% Vespel Ferrules mm ID columns 15% Graphite/ 85% Vespel Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules mm ID columns SilTite Metal - Initial Installation 10* mm ID columns SilTite Ferrules n/a SilTite Metal Nuts Replacement SilTite Nuts 2010 GC-MS System GC-MS System with QP5000 series MS /2014 GC Injectors and atmospheric detectors QP5000 Jet Separator MS Interface QP5000 Direct MS Interface All Injectors Jet Separator (Starter Kit), except 2010/ * Includes ten ferrules, two SilTite nuts. 17

18 Thermo Scientific GC Supplies - Instrument Quick Pick Guide Autosampler Syringes Thermo Scientific / CE Instruments / Fisons All needles have a cone tip style. Autosampler Syringe Specifications TriPlus AS3000 AS2000 AS200/ Volume Length Gauge Syringe Code 800 (OD mm) Septa Plunger Stop Syringe Needle Fixed Needle 10 µl (0.63) 10F-C/T-GT-5/0.63C ü µl (0.63) 10F-BT-GT-5/0.63C µl (0.63) 10F-BT-8/0.63C µl (0.47) 10F-C/T-8/0.47C ü µl (0.47) 10F-BT-8/0.47C µl (0.63) 10F-C/T-5/0.63C ü µl (0.63) 10F-VA8400/BT-5/0.63C µl (0.47) 10F-C/T-5/0.47C ü µl (0.47) 10F-BT-5/0.47C Removable Needle 10 µl (0.47) 10R-C/T-5/0.47C ü µl (0.47) 10R-BT-GT-0.47C µl (0.63) 10R-C/T-5/0.63C ü µl (0.63) 10R-BT-0.63C µl (0.47) 10R-C/T-8/0.47C ü µl (0.47) 10R-BT-8/0.47C Choose from a number of different septa types: GP = For non-demanding routine applications. EC = Combines significantly longer injection life, low bleed and low injection port adhesion. MN = Premium septa for autosamplers, up to 400 injections per septum. HT = Bleed and temperature optimized, combined with outstanding mechanical properties. Type Material Durability Resealing Solvent Resistance Tear Resistance Maximum Temperature GP Silicone Good Good Excellent Good 200 C EC High Temperature Silicone Excellent Excellent Excellent Excellent 400 C MN High Temperature Silicone Excellent Excellent Excellent Excellent 400 C HT BTO Silicone Excellent Excellent Excellent Excellent 400 C Diameter Type For TRACE GP EC MN HT For TRACE 1300 and Focus 17* EC * MN * HT * Maximum temperature for the Thermo septa diameter 17 mm is 330 C. Inlet Liners Description and Geometry For TRACE and Focus OD ID Length Splitless FocusLiner (for use with 70 mm Needle) Splitless FocusLiner with Top-end Restriction (for use with 70 mm Needle)

19 Inlet Liners Continued Description and Geometry OD ID Length Split FocusLiner (for use with 50 mm Needle) Splitless FocusLiner (for use with 50 mm Needle) Splitless with Single Taper Splitless with Single Taper Splitless, Straight-through Liner SPME Liner Split, Straight-through Liner TRACE 2000 PTV Liner Sintered Glass, Large Volume Injection (LVI) Liner ConnecTite Liner Standard ConnecTite Liner Top Hole ConnecTite Liner Bottom Hole For TRACE 1300 Split / Splitless FocusLiner Split / Splitless Taper FocusLiner Split / Splitless FAST FocusLiner Split / Splitless Tapered FAST FocusLiner ConnecTite Liner Standard ConnecTite Liner Top Hole ConnecTite Liner Bottom Hole Split, Straight-through Liner Split, with Quartz Wool Split / Splitless with Single Taper Split / Splitless with Single Taper (Quartz Wool) Split / Splitless with Double Taper Direct, Straight-through Liner Split / Splitless Quartz, Straight-through Liner / Taper / Gooseneck FocusLiner Taper FocusLiner ConnecTite Straight Double Taper PTV/LVI Splitless with Recessed Gooseneck Split / Splitless Recessed Gooseneck (Quartz Wool)

20 Thermo Scientific GC Supplies - Instrument Quick Pick Guide O-rings and Sealing Rings Description Usage For 8000 & TRACE GCs Graphite Sealing Ring For TRACE 1300 Viton O-Ring 8 mm ID. Temperatures up to 450 C. Suitable for use with liners and Temperatures up to 300 C. Suitable for liners with OD of 6.3 mm Graphite Sealing Ring Temperatures up to 450 C. Suitable for all inlet liners above except and Graphite Sealing Ring Temperatures up to 450 C. Suitable for use with liners and SilTite FingerTite Ferrules Description Column ID Ferrule ID SilTite FingerTite Thermo Injector/FID Starter Kit mm 0.4 mm * SilTite FingerTite Thermo Injector/GC-MS ISQ Starter Kit mm 0.4 mm * SilTite FingerTite Thermo Injector/GC-MS Starter Kit mm 0.4 mm * SilTite FingerTite Thermo Injector/FID Starter Kit 0.53 mm 0.7 mm * SilTite FingerTite Thermo Injector Starter Kit 0.53 mm 0.7 mm * For TRACE 1300 SilTite FingerTite INJ / FID Starter Kit mm 0.4 mm * SilTite FingerTite Capillary / FID Starter Kit mm 0.4 mm * SilTite FingerTite INJ / MS Starter Kit mm 0.4 mm * Replacement Parts SilTite FingerTite Ferrule 0.4 mm mm 0.4 mm SilTite FingerTite Ferrule 0.5 mm 0.32 mm 0.5 mm SilTite FingerTite Ferrule 0.7 mm 0.53 mm 0.7 mm SilTite FingerTite Ferrule Blanking SilTite FingerTite Female Nut SilTite FingerTite INJ Base Seal mm SilTite FingerTite MS Adaptor SilTite FingerTite Injector mm * Each starter kit includes all the parts necessary to convert one GC system (one injector and one detector) to the SilTite FingerTite system. In addition there are five SilTite FingerTite nuts, ten SilTite FingerTite ferrules, and a ferrule install tool which allows you to seat the ferrule in the correct position on the capillary column. Ferrules Description Column ID Ferrule ID SilTite Metal Ferrules mm 0.4 mm 10* For GC-MS Interface Connections (Starter Kit) 0.32 mm 0.5 mm 10* mm 0.8 mm 10* mm 0.4 mm 10 # For TRACE 1300 Split / Splitless Injectors (Starter Kit) 0.32 mm 0.5 mm 10 # mm 0.8 mm 10 # /32" 0.81 mm 10 #

21 Ferrules Continued Description Column ID Ferrule ID 15% Graphite / 85% Vespel Ferrules mm 0.4 mm mm 0.5 mm For All Injectors & Detectors (Not 0.53 mm 0.8 mm for 8000 Series, Focus, TRACE/ 1/8" OD ed Ultra GC) Columns 1/8" /4" OD ed Columns 1/4" For All Focus, Trace/Ultra mm 0.4 mm 10# Injectors & Detectors at atmospheric pressure e.g. FID 0.32 mm 0.5 mm 10# (Not for GC-MS) 0.53 mm 0.8 mm 10# Brass Nut for Focus, Trace/ Ultra GC Injectors & Non-MS Detectors mm 0.4 mm mm 0.5 mm For TRACE 1300 Injectors & Detectors at atmospheric pressure e.g. FID For TRACE 1300 GC-MS Interface Connection 100% Graphite Ferrules For Injectors & Detectors at atmospheric pressure e.g. FID (Not for GC-MS) For TRACE 1300 Injectors & Detectors at atmospheric pressure e.g. FID (Not for GC-MS) 0.53 mm 0.8 mm for 1/8" OD ed Columns 1/8" for 1/4" OD ed Columns 1/4" mm 0.4 mm mm 0.5 mm mm 0.8 mm mm 0.5 mm mm 0.8 mm /8" OD ed Columns 1/8" /4" OD ed Columns 1/4" mm 0.5 mm mm 0.8 mm for 1/8" OD ed Columns 1/8" for 1/4" OD ed Columns 1/4" Replacement SilTite Metal Ferrules mm 0.4 mm For All GC-MS Interface 0.32 mm 0.5 mm Connections 0.53 mm 0.8 mm /32" 0.81 mm mm 0.4 mm For TRACE 1300 Connections 0.32 mm 0.5 mm mm 0.8 mm /32" 0.81 mm Replacement SilTite Nuts SilTite Metal Nuts For TRACE 1300 GC-MS Interface Connection For TRACE 1300 Split / Splitless Injector Replacement SilTite Base Seals For TRACE 1300 Split / Splitless Injector * Includes 10 ferrules, 2 SilTite nuts. # To be used in combination with brass nut ( ) 21

22 Expert Tips GC Supplies - Instrument Quick Pick Guide Problem Resolution No Column Flow Check carrier gas flow and adjust. Replace septum/injector seal with EC septum. Visually check column integrity i.e. is it broken? Remove section if small enough or replace column. High Column Bleed Retention Time Shifts Poor Resolution or Loss of Resolution Phase Breakdown Poor or No Detector Response For All Peaks Check published maximum temperature. Check carrier flow rates / velocity, correct for column/length adjust if necessary. Check column has not moved in detector. Check for leaks produced during initial heating. Check oxygen filter is not spent replace if necessary. Make sure detector temperature is higher than final column temperature if possible. Check cleanliness of detector clean if necessary. Recondition column re-run conditioning program. Cut 50 cm from the front end of the column. Check temperature program. Check injector temperature. Ensure manual injection technique is consistent. Check carrier gas flow rate / velocity. Check for injector leaks. Ensure same solvent being used. Column is contaminated - rinse or replace. Remove 50 cm from front of column. Phase breakdown replace column. Use correct column or phase. Use different temperature program. Check injector temperature is it correct for solvent and analytes. Check injection technique. Check carrier flow / velocity. Sample overload - dilute or change split ratio. Contaminated column rinse or replace. Phase breakdown replace column. Check for leaks and repair. Check oxygen traps and replace if necessary. Exceeded upper temperature limit of column for extended periods replace column. Column contamination replace column (perform extra clean up of samples). Damage due to sample do not inject strong acid or base samples. Correct injection technique for concentration of analyte. Check proper liner is used for injection technique. Check syringe needle not blocked or plunger is not leaking. Check split ratio if using split technique. Check injector temperature is correct. Check detector temperature is correct. Check flow rates of detector gas(es). Error in sample concentration verify concentrations. Detector Problems PID - Dirty window clean according to manufacturer s specifications. ELCD - Faulty reactor tube. - Contaminated alcohol. - Incorrect alcohol flow rate. ECD - Impurities in nitrogen. - Dirty detector; clean (bake) according to manufacturer s specifications. NPD - Bad bead. FID - Partially blocked jet. FPD - Incorrect gas flow rates. - Incorrect filter installed. - Clean filter. TCD - Balance flow rates. 22

23 Poor Peak Shape Problem Reason Resolution Peak Fronting Column overload. Reduce sample concentration or injection volume. Incorrect polarity of column for compound. Use correct column. Peak Tailing Column is active. Remove first meter of column; recheck; replace column if necessary. Split Peaks Active inlet liner. Incorrect column for analysis. Incorrect column installation. Poor injection technique. Mixed solvents. Replace liner with clean, deactivated liner. Use correct column. Check inlet and outlet connections, and for any cold spots. Refine injection technique. Use only single solvent system. Poor resolution. Use different column or change temperature profile. Ghost Peaks Run GC without injection; if ghost peaks disappear then the problem is probably the syringe or solvent; if ghost peaks are still evident then the problem is either the septum or the breakdown of the phase. Contaminated syringe or solvents. Clean syringe thoroughly and replace solvents. Septum bleed. Replace with new EC septum. Specific Peaks Low Response Breakdown of column phase. Too large an injection volume. Column is active. Active inlet liner. Incorrect calculation of sample. FID altered gas flows. Choose different phase which restricts breakdown. Decrease injection volume. Remove first meter of column; recheck; replace column if necessary. Replace liner with clean, deactivated liner. Verify calculations. Readjust gas flows. 23

24 GC Supplies - Instrument Quick Pick Guide Choose for Your Instrument SGE Analytical Science (SGE) is a world renowned brand for components and consumables used in scientific analysis. Primarily in the field of scientific glass engineering for liquid handling and separation science, since its beginnings in 1960, SGE has become the global market leader in niche areas such as autosampler syringes and GC inlet liners. Completing the transition into Trajan after acquisition in 2013, SGE products make up a solid foundation of Trajan s portfolio and will continue to be created and supported by Trajan customer service and distribution networks worldwide. For more information, visit vwr.com or contact your VWR representative. Approved Distribution Partner BR-0479-G Trajan Scientific and Medical 09/ M Lit. No