NITRIC ACID PLANT DETAILS
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1 NITRIC ACID PLANT DETAILS C & I Girdler (Wheatherly USA), mono pressure, High pressure Plant HNO3 content - minimum percent per weight 56% Design and actual cooling water temp Summer - Temp. In: 28 Deg. C; Temp. Out: 35 Deg. C; Winter - Temp. In: 26 Deg. C; Temp. Out: 33 Deg. C Operating pressure of the plant Air exit compressor: 8.0 barg Pressure at Converter head: 7.5 barg Pressure in Absorption column: 6.8 barg Tail gas exhaust inlet of gas turbine: 6.0 barg SPECIFIC CONSUMPTIONS (at 100% concentration actually produced) 160 MTPD NH3-310kg / Ton, 100 platinum catalyst 270mg / Ton, 100 export steam - pressure, temperature, 3.0 Ton / hr, 16 barg cooling water cubic metres / hr electricity 180kW / Ton, 100 / 1250kWh (average) import steam during start-up - via an oil fired boiler producing saturated 16 barg & 3 Tons / hr
2 AMMONIUM NITRATE SOLUTION PLANT LIST OF EQUIPMENT (APPENDIX I) AMMONIUM NITRATE SOLUTION PLANT 1. Ammonia Vapouriser 2. Ammonia Knock-out Pot 3. Acid Preheater 4. AN Reactor 5. AN Recirculation Pump 6. Vapour Separator 7. AN Neutralizer Tank 8. AN Storage Tank E AN ph Control System x Contaminated Steam Condenser 11. Steam Ejector 12. Contaminated Condensate Tank 13. Contaminated Condensate Cooler 14. Contaminated Condensate Transfer Pump 15. AN Solution Transfer Pumps x Interconnecting Process Pipings 17. Instrumentation & Control Equipment 18. One 4-level Steel Supporting Structure for ANS Plant LIST OF EQUIPMENT Equipment Item No. Equipment Description "#$"%&'%"(&)*'#& 1. Bunker C Tank 2. Fuel Preparation Unit 3. Demin Plant A & B
3 4. Demin Tank + Demin Pumps x 2 5. Oil Fired Boiler + 2 BFW Pumps 6. Boiler Feed Chemical Tank + Pump 7. Deaerator 8. AOP Burn Tank (Liquid Ammonia Storage Bullet) 9. Ammonia Water Vapourizer 10. Spare Waste Heat Exchanger 11. Spare Cooler Condenser x Air Intake Filter (Delbag) 13. Demag Compressor x Intercoolers 15. Process Air Filter (sintered metal) 16. Air Heater 17. Gas Mixer 18. Ammonia Superheater 19. Ammonia Filters x Converter (Ammonia Oxidation Reactor) 21. Tail Gas Reheater 22. Waste Heat Exchanger + Steam Drum 23. Platinum Filter 24. Tail Gas Preheater 25. Cooler Condensers A & B 26. Acid Separator 27. Absorption Column 28. HEA Column + HEA Pumps 29. Weak Acid Collector
4 30. Mist Separator 31. Tail Gas Tempering Heater 32. ABB Gas Turbine 33. Siemens (Synchronous) Motor 34. Epicyclic Gearbox.2/ Equipment Item No. Equipment Description "#$"%&'%"(&)*'#& 35. Oil Cooler 36. Dilution Fan 37. Exhaust Stack 38. Acid Storage Tank A 39. Acid Transfer Pumps 40. MCC A.O.P 41. Boiler Control Panel 42. AOP Control Panel 43. Demag Control Panel 44. Siemens Control Panel 45. Expander Control Panel 46. AOP Building 47. Overhead Crane 48. Process Pipings 49. Instrumentation and Control Equipment 50. Ammonia Stripper 51. WHE Blowdown Vessel
5 2.1.DEMAGCOMPRESSORSYSTEM TAGNo:01"V"1101 REQUISITIONNo:01"150 SUPPLIER:BECSA MANUFACTURER:DEMAG PURCHASE ORDER: 4018-Br-01-1 MANUFACTURER SREFERENCE:Orderno: "2609 Serialno:6492 TYPE GENERALDESCRIPTION: 4 Stage geared turbo compressor VK32 with motor drive TYPE GENERALDESCRIPTION: Provides compressed (~8.4 bars) air for ammonia oxidation TECHNICALDATA: ~104C A. Operation kp/cm 2 C@8.4 5kp/cm 2 bar ~87C ~72C C4 C3 C2 C1 ~58C kp/cm 2 32"35C Air1atm; 33800m 3 /h C.S.3 C.S.2 C.S.1
6 ~40C ~40C ~40C ~33C ~40C ~33C CoolingWaterIN 115m 3 CoolingWaterOUT 200 Kpa (+,-.&%/,01+22/1&345+,-674& 2.2.DEMAGCOMPRESSORSYSTEMCONTD. B. Speed (rpm) Stage I & II : 8441 Stage III & IV :13105 Drive Speed :1500 Power Requirement :3190 KW C. Oil (i) (ii) Lubrication Type : Viscosity : 4.5 degree 50 Quantity : 3000 Litres Oil Oil cooler Inlet :52.5 C Outlet :40 C D.PhysicalPropertiesofGas(Air) Constant :29.7 kpm/kp Relative Humidity :~67% Cp/Cv :1.4 TAGNo:01"A"1101 REQUISITIONNo:01"150
7 MOTORSYSTEM: 1.Compressor Make: 1.5MW"3PhasesynchronousSiemensMotor Type: 1DM3129"3"BE02"2serialno:D Ratings: 6.6Kv"150A"1500kw"1500rpm PowerFactor: 0.9cap Standstillheating: 220V 13A Excitation: 57V 250A StartingCurrent: 5.5xratedcurrent 2.HighPressurePump Make: AEG Type: AM90SZ4 Ratings:230/400V"4.75/2.15A"1.1KW 1400rpm 2.3.DEMAGCOMPRESSORSYSTEMCONTD. 3.Intercoolers Make: Siemens Serial#: Type: 1LA3166"4AA90Z Shell&Tubeheatexchanger(withgasonshellside)
8 4. Auxiliary Oil Pump Make: Siemens Type: 1LA3 166 (90S 160L) ACCESSORIES: Intakeguideunit(gas): Ref:DemagCat."Sect2 Overflowvalve(oil): Ref:DemagCat."Sect3 Couplingsforgearbox: IIIIII"Sect6 Silencers: IIIIII"Sect8 Gears: IIIIII"Sect10 Intakevane:IIIIII"Sect11&catalogue1929 Pumps(mainoil): IIIIII"Sect14 (Auxiliarygearpumps):IIIIII"Sect14 Filter(duplex): IIIIII"Sect15 OilCooler:IIIIII"Sect16 KKKTurbineforoilpump: IIIIII"Sect18+ file01"150 IntakeAirFilter: IIIIII"Sect20+ file01" ABSORPTIONCOLUMN TAGNo:01"K"1101 REQUISITIONNo:01"101 SUPPLIER:Phoenix"Rheinrohr PURCHASE ORDER: 4018-Br-01-3 of Jan, 1972
9 GENERAL DESCRIPTION: Vertical cylindrical tank with dished head and bottom EQUIPMENT PURPOSE: Absorption of nitrous oxide (from process gas) in water to form nitric acid. DIMENSIONSANDTECHNICALDATA: A. Dimensions 1.Shell: 2300"x13mmthickness Length:(a)excludingdishedheads :11990mm (b)withdishedheads :13106mm 2.Footshell:964x2326"x13mm 1. Accessories: No.oftrays:35bubbletrays 2bleachertrays Spacing :305mm Coolingcoils:~12100x26.9"x2.9mm Quantity:180(semiCircular) B.OperatingConditions 1.ProcessGas(IN) Pressure: 6.5kg/cm 2
10 Temperature: 40~42C 2.TailGas(OUT) Pressure: 6.1kg/cm 2 Temperature: 37C 22.2.ABSORPTIONCOLUMNCONTD. 3.Acid(OUT) Concentration: 50"54% Temperature: 40C 4.CoolingWater IN: 40C OUT: 38C@3.5kg/cm 2 RATE: 2700GPM 5.DeminWater(IN) Temperature: 36C RATE: 2700GPM 6.BleachingAir(IN) Temperature: 139.8C RATE: 5863Nm 3 /hr Pressure: 8.4kg/cm 2
11 C. Construction Material Acid out 22.3.ABSORPTIONCOLUMNCONTD. 1.Shell:Sicr18/8,Type304L 2.Footshell: C.Steel 3.Pipefittings:ASTMA120Gr.AorB(Ms.63.1) NOTES: 1.Selected Technical drawings available overleaf 2.Additionaldrawinginc.accessways&supportsavailableinAbsorptioncolumnarchives
12 22.4.ABSORPTIONCOLUMNCONTD. Absorptioncolumn(topsection)
13 22.5.ABSORPTIONCOLUMNCONTD.
14 Absorptioncolumn(bottomsection) 22.6.ABSORPTIONCOLUMNCONTD. AbsorptionColumn(Plan)
15 AbsorptionColumn(Internals) 23.1.HEACOLUMN SUPPLIER:ChaudronneriedesRoches(CDF) PURCHASE ORDER: , June 1990 CONTRUCTION CODE: CODAP 85 Categorie:C REFERENCE: FSP GENERAL DESCRIPTION: Vertical cylindrical tank with dished heads EQUIPMENT PURPOSE: Maximize No x absorption DIMENSIONSANDTECHNICALDATA:
16 A. Dimensions 1.Shell: 2800"x10mmthickness Length:(a)excludingdishedheads :11620mm (b)withdishedheads :13600mm 2.Footshell:2000x2800" 1. Accessories: No.oftrays:7sievetrays Spacing :1500mm Coolingtubes:33.7"x2mm B.OperatingConditions Temperature(C) Pressure(BarAbs) Design 60 8 Operating HEACOLUMNCONTD.
17 C. Construction Material D.Weight 1.Shell: 2.Skirt: Z2CN Trays+supports: 4.Vesselheads: 5.Internal+Externalbolting: Z6CN18.09 Empty: 19595kg Fullofwater: kg Capacity: 86800dm 3
18 NOTES: 1.Selected Technical drawings available overleaf 2.Alsoreferarchivesdwg" HEACOLUMNCONTD. HEAColumn(TopSection)
19 23.4.HEACOLUMNCONTD. HEAColumn(BottomSection)
20
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