Analysis of 209 PCBs by HRGC/HRMS Analysis of Chlorinated Dioxins/Dibenzofurans by HRGC/HRMS

Transcription

1 Method Description 1668A Analysis of 209 PCBs by HRGC/HRMS 8290A Analysis of Chlorinated Dioxins/Dibenzofurans by HRGC/HRMS AFNOR NFE Filterability - Mineral Oils (Dry) AFNOR NFE Filterability - Mineral Oils (Wet) AlcoholExtract/GC Fuel Dilution - Ethanol, Methanol, t-butanol ASTM Proposed Free and Total Glycerin in B100 and Biodiesel Blends by Ion Chromotography Burlington Northern Oxidation Test - Paddle - Burlington Northern C-4 Viscosity Characteristics (Test 228 and D and E) CARB 429A Analysis of Polycyclic Aromatic Hydrocarbon (PAH) (up to 19) by GC/MS with PI/EI/SIM CARB 429B Analysis of Polycyclic Aromatic Hydrocarbon (PAH) (up to 19) by HRGC/HRMS CARB 429C Analysis of PAH (MW 250) by HRGC/HRMS Micro Oxidation Test Seal Test - AT-1 (All elastomers at all temperatures and durations) Seal Test - AT-1 AEM 1E1798A elastomer (168 Seal Test - AT-1 AEM 1E1798A elastomer (70 Seal Test - AT-1 FKM 1E0944 elastomer ( C) Seal Test - AT-1 FKM 1E0944 elastomer (70 150C) Seal Test - AT-1 FKM 1E1039B elastomer ( C) Seal Test - AT-1 FKM 1E1039B elastomer (70 150C) Seal Test - AT-1 FKM 1E2865A elastomer ( C) Seal Test - AT-1 FKM 1E2865A elastomer (70 150C) Seal Test - AT-1 HNBR 1E2719A elastomer ( C) Seal Test - AT-1 HNBR 1E2719A elastomer (70 120C) Seal Test - AT-1 NBR 1E0741 elastomer (168 Seal Test - AT-1 NBR 1E0741 elastomer (70 Fluid Compatibility Foam Test - with and without water Homogeneity Low-Temperature Storage Rust Test (175 hours) Rust Test (Test duration per client request) Seal Test - Compatibility - Fluoroelastomer (1E2827) Seal Test - Compatibility - Fluoroelastomer (1Y0530) CEC F06A96 Lubricity - High Frequency Reciprocating Rig CEC L-14-A Shear Stability - Mechanical (30 passes) CEC L-36-A Viscosity - High Temperature High Shear - 150C - Ravenfield Instrument CEC L-36-A Viscosity - High Temperature High Shear - 150C - TBS Instrument Seal Test - Includes all four rubbers Seal Test - Fluoroelastomer - RE1 FPM Seal Test - Polyacrylate - RE2 ACM Seal Test - Silicon - RE3 VMQ Seal Test - Nitrile - RE4 NBR CEC L-40-A Volatility - NOACK (1 hours at 250C) Tapered Roller Bearing Shear Test (VW Shear) 4 hrs. Tapered Roller Bearing Shear Test (VW Shear) 8 hrs. Tapered Roller Bearing Shear Test (VW Shear) 20 hrs. Tapered Roller Bearing Shear Test (VW Shear) 30 hrs. Tapered Roller Bearing Shear Test (VW Shear) 40 hrs. Tapered Roller Bearing Shear Test (VW Shear) 48 hrs. Tapered Roller Bearing Shear Test (VW Shear) 60 hrs. Tapered Roller Bearing Shear Test (VW Shear) 80 hrs. Tapered Roller Bearing Shear Test (VW Shear) 100 hrs. Tapered Roller Bearing Shear Test (VW Shear) 192 hrs. Tapered Roller Bearing Shear Test (VW Shear) 200 hrs. CEC L-48-A Oxidation Test - Method A (GFC) Oxidation Test - Method B at 150C (DKA) Oxidation Test - Method B at 160C (DKA) Oxidation Test - Method B at 170C (DKA) Oxidation Test - Method B at 180C (DKA) CEC L-82-A Soot CEC L-85 Hot Surface Oxidation by Pressure Differential Scanning Calorimeter (120 minute duration) CEC L-85M Hot Surface Oxidation by Pressure Differential Scanning Calorimeter (120 minute duration. Each additional 3 hour increment are billed at $100 per increment) CEC L-105 Low Temperature Pumpability CETOP RP 124H Filterability - Hydraulic and Lubricating Oils Cincinnati Milacron - Mod Thermal Stability - Cincinnati Milacron - Method A - Modified (Micro 90 vs KCN) Cincinnati Milacron - Mod Thermal Stability - Cincinnati Milacron - Method B - Modified (Micro 90 vs KCN) CMS M1135 Foam Resistance CMS M1135 Seal Test - Compatibility Cognis Friction Analysis using HFRR Instrument (Cognis) Conrail Oxidation Test - Conrail Railroad D56 Flash Point - Tag Closed D86 Distillation - Gasoline, Kerosene, Gas, Oil D91 Precipitation Number D92 Fire Point - Cleveland Open Cup D92 Flash Point - Cleveland Open Cup D93 Flash Point - Pensky-Martins D94 Saponification Number (Color Indicator) (Single Run) D95 Water Content - Azeotropic Distillation D96 Water and Sediment - Crude Oil D97 Pour Point - Manual D129 Sulfur - Bomb Method Corrosion - Copper C Corrosion - Copper - Fuels C Corrosion - Copper - Provide Conditions Corrosion - Copper Strip - 3 hours at 150C Mod Corrosion - Copper - C4 qualification 3 hrs at 150C Mod Corrosion - Copper - With Specimen Weight Loss D156 Color - Saybolt D189 Carbon Residue - Conradson Cone Penetration - Worked 60 Strokes Cone Penetration - Worked 10,000 Strokes Cone Penetration - Worked 100,000 Strokes Cone Penetration - Unworked D240 Heat of Combustion - Gross D240 Heat of Combustion - Net D287 Density, Specific and API Gravity by Hydrometer at 60F D287 Mod Density, Specific and API Gravity by Hydrometer measured at other temperatures than 60F D322 Fuel Dilution - Crankcase Oils D381 Existent Gum Content - Fuels D412 Vulcanized Rubber and Thermoplastic Elastomers-Tension D413 Rubber Property-Adhesion to Flexible Substrate Viscosity - Kinematic - Non-Standard Temperatures Viscosity - Kinematic at 100C (cst) Viscosity - Kinematic at 100C (cst) - Mack T8 Test Procedure M Viscosity - Kinematic at 100C (cst) - TOST test Viscosity - Kinematic at 100F (SuS) Viscosity - Kinematic at 210F (SuS) Viscosity - Kinematic at 40C (cst) Viscosity - Stripped - Includes Stripping and Viscosity Seal Test - Parameters may vary Seal Test - Package for LRI Qualification includes Nitrile, Polyacrylate and Viton run for 1000 hours at 100C Seal Test - Nitrile (Buna N) for LRI Qualification (1000 hours at 100C includes sampling intervals at every 100 hrs. Seal Test - Polyacrylate for LRI Qualification (1000 Hours at 100C includes sampling intervals at every 100 hrs. Seal Test - Viton (Fluoroelastomer) for LRI Qualification 1000 hours at 100C includes sampling intervals at every 100 hrs. D473 Sediment in Crude and Fuel Oil by Extraction D482 Ash D524 Carbon Residue - Ramsbottom D524 / D86 Mod Carbon Residue - Ramsbottom (10% Bottoms) D525 Oxidation Stability - Gasoline D566 Dropping Point

2 D611 Aniline Point OR Mixed Aniline Point D613 Cetane Number - CFR D638 Standard Test Method for Tensile Properties of Plastics D664 Acid Number D664 Base Number - GE Method D664 ph - Initial D664 Method B Acid Number - Bio-diesel Fuel D664 Mod Acid Number - ABOT (1 gram sample) D664 Mod Acid Number - ABOT (5 gram sample) D664 Mod Acid Number - Strong D Base Number D665A Rust Preventing Characteristics - DI-Water - 24 hours D665A Rust Preventing Characteristics - DI-Water - 4 hours D665B Rust Preventing Characteristics - Synthetic Sea Water - 24 hours D665B Rust Preventing Characteristics - Synthetic Sea Water - 4 hours D808 Chlorine - Lubricating Oils D873 Oxidation Stability - Aviation Fuels - Potential Residue Method D874 Ash - Sulfated D892 Foaming Characteristics D892 Mod Foaming Characteristics - Individual Sequence I, II or III D892 Mod Foaming Characteristics - Individual Sequence II or IV - (Option A) D892 Opt. A Foaming Characteristics - Option A D893A Insolubles - Normal - Pentane D893A Insolubles - Normal - Toluene D893B Insolubles - Coagulated - Pentane D893B Insolubles - Coagulated - Toluene D942 Oxidation Stability - (Greases and Oils) D943 Oxidation Stability - Inhibited Mineral Oils - up to 1000 hours ($70 for each additional 168 hour increment up to 3000 hours. $70 for each 500 hour increment after 3000 hours.) D971 Interfacial Tension of Oil Against Water by the Ring Method D972 Evaporation Loss of Lubricating Grease and Oils D974 Acid Number - Color Indicator Titration D974 Base Number - Color Indicator Titration D974 Strong Acid Number - Color Indicator Titration D976 Cetane Index (Calculated from D86 and D4052) D1094 Water Reaction of Aviation Fuels D1119 Ash - Coolants D1120 Boiling Point - Coolants D1121 Reserve Alkalinity - Coolants D1122 Specific Gravity - Coolants D1123 Water Content - Karl Fisher Reagent - Coolants D1159 Bromine Number - Electrometric Titration Method D1160 Distillation - Vacuum Distillation of Petroleum Products D1177 Freeze Point - Coolants D1218 Refractive Index D1264 Water Washout - One Temperature D1275 Corrosive Sulfur in Electrical Insulating Oils D1287 ph - Coolants D1298 Density, Specific and API Gravity by Hydrometer D1319 FIA - Aromatics, Olefins and Saturates D1322 Smoke Point D1331A Surface Tension D1331B Interfacial Tension D1384 Corrosion Test in Glassware - Coolants D1401 Emulsion Characteristics - Oil D1403 Cone Penetration - Unworked - Quarter Scale D1403 Cone Penetration - Worked - Quarter Scale - 60 Strokes D1405 Heat of Combustion - Net - Aviation Fuels - Calculated D1414 Standard Test Methods for Rubber O-Rings D1500 Color - ASTM D1533 Water Content - Insulating Materials (Method B) D1613 Acidity - Solvents and Chemical Intermediates D1662 Sulfur - Active - Cutting Fluids D1688M Copper in Water (D4806 modification) by AA D1742 Oil Separation From Lubricating Grease D1743 X2 Corrosion Preventative Properties of Lubricant Grease - Alternate Procedure D1748 Rust Protection - Humidity Cabinet - 49C/120F - Specify duration D1796 Water and Sediment - Petroleum Products D1838 Copper Strip Corrosion by Liquefied Petroleum (LP) Gases D1840 Naphthalene Content - Jet Fuel D1881 Foaming Characteristics - Coolants D1882 Effect on Automotive Finishes - Coolants D1903 Coefficient of Thermal Expansion of Electrical Insulating Liquids D2007 Clay Gel Analysis D2007 Clay Gel Analysis - Asphaltenes D2008 UV Absorbance and Absorptivity D2068 Filter Blocking Tendency D2070 Thermal Stability - Hydraulic Fluids D2140 Carbon Type D2158 Residues in Liquefied Petroleum (LP) Gases D2265 Dropping Point - Grease D2266 Four Ball - Wear Properties - Grease D2270 Viscosity Index - Extrapolated Various Temperatures (Calculation only) D2272 Rotating Bomb Oxidation Test (Single Run) D2272 Mod Rotating Bomb Oxidation Test Appendix X1 D2273 Trace Sediment D2274 Accelerated Stability D A2 Particulate Contamination in AV Turbine Fuel D2386 Freeze Point - Aviation Fuels D2425 Sep FIA Separation used for D2425 Hydrocarbon Types D2425 Hydrocarbon types in Middle Distillates D2500 Cloud Point - Petroleum Products D2509 Timken - OK Load - Grease D2509 Timken - OK Load - Grease - 1 Load D2532 Viscosity and Viscosity Change of Turbine Lubricants After Standing at Low Temperature D2570 Simulated Service - Corrosion - Coolants D2595 Evaporation Loss of Lubricating Grease D2596 Four Ball - Extreme Pressure Properties - Grease D2603 Sonic Shear Stability - Oils D2619 Beverage Bottle Test - Hydrolytic Stability D2622 Mod Chlorine - Petroleum Products D2622_07 Sulfur - Xray Florescence (Up to 100 ppm) D2624 Electrical Conductivity - Fuels D2670 Falex Pin and Vee Block - Wear Properties D2699 Octane Number - CFR (Research Rating)(Dual Pass) D2700 Octane Number - CFR (Motor Rating)(Dual Pass) D2709 Water and Sediment - Fuels - Centrifuge D2710 Bromine Index of Petroleum Hydrocarbons D2711 Demulsibility Characteristics - Oils D2711 Demulsibility Characteristics Extreme Pressure - Oils D2782 Timken - OK Load - Extreme-Pressure Properties D2783 Four Ball - Extreme Pressure Properties D2809 Cavitation Characteristics - Coolants D2887 Simulated Distillation - Diesel Fuels/Solvents D2893 Oxidation Characteristics - Extreme-Pressure Lubrication Oils D2896 Base Number/Alkalinity Value - Perchloric Acid Titration D2982 Glycol - Used Oil - Semi-Quantitative D2983 Viscosity - Low Temperature Brookfield - per temperature D3227 Sulfur - Mercaptan D3228 Mod Nitrogen - Kjeldahl D3231 Phosphorus - Gasoline D3233 Falex Pin and Vee-Block - Extreme Pressure - Method A

3 D3233 Falex Pin and Vee-Block - Extreme Pressure - Method B D3237 Lead - Gasoline - Atomic Absorption D3237 Mod Lead - Unleaded Gasoline - Atomic Absorption D3238 Carbon Type - Calculated D3241 JFTOT - Jet Fuel Thermal Oxidation Test D3241 JFTOT Breakpoint D3242 Acidity - Aviation Fuels D3321 Freeze Point - Coolants - Refractometer D3338 Estimation of Net Heat of Combustion of Aviation Fuels D3339 Acid Number - Petroleum Products by Semi-Micro Color Indicator Titration D3427 Gas Bubble Separation Time (Single Run) D3524 Mod Fuel Dilution - Diesel D3525 Mod Fuel Dilution - Gasoline D3606 Benzene with EPA modifications D3701 Hydrogen by Nuclear Magnetic Resonance D3703 Peroxide Number D3828A SetaFlash - Flash/No Flash D3828B Actual Flash Point D3829 Borderline Pumpability (Viscosity MRV) D3831 Manganese in Gasoline by Atomic Absorption Spectrometry D3948 Micro Separation - Water in Fuel - (Single Run) D4007 Water and Sediment in Crude Oils D4048 Corrosion - Copper - Grease D4052 Mod Density by Meter (Temperatures between 20 and 90C) D4052 Density/API by Meter (15.5C/60F) D4053 Benzene in Motor and Aviation Gasoline by D4054 Qualification and Approval of New Aviation Turbine Fuels and Fuel Additives D4055 Mod Insolubles Millipore D4055 Mod Insolubles - Coagulated - using a 1.2 micron filter membrane D4055 Insolubles - Millipore Filtration D4172 Mod Four Ball - Wear Properties - Modified (Specify Conditions) D4172 OptA Four Ball - Wear Properties - Option A D4172 OptB Four Ball - Wear Properties - Option B D4176 Free Water and Particulate Contamination (Distillate Fuels) D4291 Glycol - Lube Oils - Quantitative D4294 Sulfur - Energy Dispersive - Petroleum Products D4308 Electrical Conductivity of Hydrocarbons (Precision) D4310 Oxidation - Sludging Tendencies of Mineral Oils (Up to 1000 hours) D4340 Corrosion of Aluminum Alloys by Coolants (In Duplicate) D4529 Estimation of Net Heat of Combustion of Aviation Fuels D4530 Carbon Residue - Micro D4539 Low Temperature Flow Test - Full Range D4539 Low Temperature Flow Test - Per Temperature D4625 Middle Distillate Fuel Storage Stability at 43C (110F) for three (3) storage periods D4627 Corrosion - Iron Chip D4629 Nitrogen - Chemiluminescence D4636 Alt 2 Corrosion and Oxidation Stability - Alternate Procedure 2 D4681 A1 Rust - with Reference D4682 Miscibility - - with Reference - Specify Category or Temperature D4683 Viscosity - Tapered Bearing Simulator - New Oils at 150C D4683 Mod Viscosity - Tapered Bearing Simulator - Used Oils D4684 Viscosity - Apparent D4737A Cetane Index (Calculated from D86 and D4052) D4737B Cetane Index (Calculated from D86 and D4052) D4739 Base Number D4741 Viscosity - High Temperature High Shear by Tapered Plug Viscometer - 150C D4742 Thin Film Oxygen Uptake (Single Run) D4808 Hydrogen by Nuclear Magnetic Resonance D4809 Heat of Combustion - Gross - Intermediate - (includes D2622 and D4809) D4809 Heat of Combustion - Net - Intermediate - (includes D2622, D4809 and D5291) D4814 X2 V/L Ratio - Gasoline (Calculated using D86 and D5191) D4815 Oxygenates and Oxygen - Gasoline D4927B Elements - (Ba, Ca, P, S, Zn) in unused oils (Wavelength Dispersive) D4928 Water Coulometric - Karl Fischer - Crude Oils D4951M Elements - (B, Ba, Ca, Cu, Mg, Mo, P, Si, Zn) by ICP D4951 Elements - (B, Ba, Ca, Cu, Mg, Mo, P, Zn) by ICP D4951 Sulfur - ICP D4952 Doctor Test D5001 Lubricity - Aviation Fuels - Ball on Cylinder Lubricant Evaluation (BOCLE) - Wear Properties D5006 Fuel System Icing Inhibitor D5133 Brookfield - Scanning D5183 Four Ball - Coefficient of Friction Elements - (Al, Ag, B, Ba, Ca, Cd, Cr, Cu, Fe, K, Mg, Mn, Mo, Na, Ni, P, Pb, Sb, Si, Sn, Sr, Ti, V, Zn) by ICP Elements - Special for Sequence IIIG testing - price per run - 2 runs minimum required by test procedure. Elements - Specialized (As, Be, Bi, Co, L, Se, W) by ICP Sulfur - ICP D5186 Aromatics - Diesel Fuel (SFC) D5188 V/L Ratio - Determination/Instrument D5191 Vapor Pressure - Reid (Automatic) D5291 Carbon/Hydrogen in Petroleum Products D5291 Nitrogen - Carlo Erba D5293 Cold Cranking Simulator - Automatic D5304 Stability of Fuel by Oxygen Overpressure D5305 Determination of Ethyl Mercaptan in LP-Gas Vapor D5452 Particulate Contamination in Aviation Fuels by Filtration D5453 Sulfur - UV (Antek) D5481 Viscosity - High Temperature High Shear D5483 Oxidation Induction Time by DSC D5501 Ethanol Content of Denatured Fuel D5580 Aromatics - Total by Gas Chromatography D5599 Oxygenate and Oxygen Content by Oxygen Selective Flame Ionization Detection D5621 Sonic Shear Stability - Hydraulic Fluids D5662 Seal Test - Nitrile (BUNA N) for PG-2 Qualification (240 hours at 100C) D5662 Seal Test - Polyacrylate for PG-1/PG-2/MT-1 Qualification (240 hours at 150C) D5662 Seal Test - Viton (Fluoroelastomer) for PG-1/PG- 2/MT-1 Qualification (240 Hours at 150C) D5762 Nitrogen - Chemiluminescence - by Boat-Inlet D5769 Aromatics - Gas Chromagraphy/Mass Spectrometry (Wt%) D5773 Cloud Point - Automated D5800 Volatility - NOACK (1 hour at 250C) D5827 Ion Chromatography - Includes Chloride, Nitrate, Nitrite, Phosphate and Sulfate D5845 Oxygenate and Oxygen Content by Petrospec D5949 Pour Point - Automated D5968 Corrosion Bench Test (CBT) (250F) D5972 Freeze Point D6045 Color, ASTM by Automatic Method D6045 Color, Saybolt by Automatic Method D6078A Lubricity - Diesel Fuels - Ball On Cylinder Lubricant Evaluation (BOCLE) - Scuffing Load D6079 Ball on Cylinder Lubricant Evaluation (HFRR) - Friction/Wear Properties D6079 Lubricity - Diesel Fuels - High Frequency Reciprocating Rig (HFRR) D6079 Lubricity - Gasoline - High Frequency Reciprocating Rig (HFRR) D6079 Mod Lubricity - Used Oils - High Frequency Reciprocating Rig (HFRR) (MACK Specification Requirement) D6082 Foam, High Temperature D6082 Foam, High Temperature - Optional Blending D6130 Elements - Aqueous (Al, Ag, B, Ba, Ca, Cd, Cr, Cu, Fe, K, Mg, Mn, Mo, Na, Ni, P, Pb, S, Sb, Si, Sn, Sr, Ti, V, Zn) by ICP ($100 for first 5 elements - $17 each additional element) D6186 Oxidation Induction Time of Lube Oils by PDSC D6186 Oxidation Induction Time of Lube Oils by PDSC at 175C D6217 Particulate Contamination in Middle Distillate Fuels by Laboratory Filtration D6278 Shear Stability (30 cycles) D6278M Shear Stability (90 cycles) D6304 Water Coulometric - Karl Fisher D6335 Thermo-Oxidation Engine Oil Simulation Test (TEOST)

4 D6352 Simulated Distillation - Oils D6371 Cold Filter Plugging Point D6378 Vapor Pressure (Triple Expansion) D6379 Aromatic Types in Aviation and Distillates by HPLC/RI D6417 Volatility - Simulated Distillation - Oils D6421 PFI Bench Rig Test - Keep Clean D6421M PFI Bench Rig Test Dirty Up/Clean Up D6423 phe - Ethanol, Denatured Fuel Ethanol and Fuel Ethanol D6443 Chlorine - Unused Oils and Additives for ATF fluids only D6443 Elements - (Ca, Cl, Cu, Mg, P, S, Zn) in Unused Oils and Additives by WDXRF D6450 Flash Point by Continuously Closed Cup (CCCFP) Tester D6468 Stability of Distillate Fuels by High Temperature (90 or 180 minutes) D6550 Olefin Content of Gasolines by SFC D6584 Free and Total Glycerin (B100) D6594 Corrosion Bench Test (HTCBT) (275F) D6616 Viscosity - Tapered Bearing Simulator - New Oils at 100C D6616 Viscosity - Tapered Bearing Simulator - Used Oils at 100C D6729 Detailed Hydrocarbon Analysis D6751 Cold Soak Filtration of B100 D6756 Red Dye 26 in Diesel Fuel by Petrospec D6793 Determination of Isothermal Secant and Tangent Bulk Modulus D6794 Filterability of Engine Oils after Treatment with Various Water amounts and a Long Heating Time (6 hr) (EOWTT) D6795 Filterability of Engine Oils after Treatment with Water and Dry Ice and a Short Heating Time (EOFT) D6811 Thermal Stability - Aviation Turbine Fuels - HiReTS Method D6890 Derived Cetane Number D6896 Viscosity - Apparent - Used Diesel Oils D6922 Homogeneity and Miscibility D6922 Mod Homogeneity and Miscibility - Modified - 1 Reference Fluid - GM Method D7039 Sulfur - Monochromatic Wavelength Dispersive XRF D7094 Flash Point by Modified Continuously Closed Cup (MCCCFP) Tester D7097 Thermo-Oxidation Engine Oil Simulation Test - MTEOST D7098 Thin Film Oxygen Uptake (Single Run) D7109 Shear Stability - Includes 30 and 90 Passes D7111 Elements - (Al, Ba, Ca, Cr, Cu, Fe, Li, Pb, Mg, Mn, Mo, Ni, K, Na, Si, Ag, Ti, V, Zn) D7111 Mod Elements - (Ca, K, Mg, Na) D7214 Oxidation of Used Lubricants by FT using Peak Area Increase Calculation Seal Test - Nitrile - NBR Seal Test - Polyacrylate - ACM Seal Test - Silicon - VMQ Seal Test - Vamac - MAC Seal Test - Viton - FKM D7224 Water Separation Characteristics of Kerosine-Type Aviation Turbine Fuels Containing Additives by Portable Separometer D7261 DSEP-Diesel Fuels D7317 Insolubles - Coagulated Pentane - Used lubricating oils by filtration (LMOA Method) D7319 Sulfate and Chloride in Ethanol D7321 Particulate Contamination of Biodiesel B100 Blend Stock Biodiesel Esters and Biodiesel Blends by Laboratory Filtration D7328 Sulfate and Chloride by IC using Aqueous Sample Injection D7347 Olefin Content of EtOH by SFC D7419 Saturate and Aromatic content of Lube Basestock by HPLC/RI D7462 Accelerated Stability - B100 and BioDiesel D7462 Mod Accelerated Stability - B100 and BioDiesel w/isooctane Insolubles D7463 Hy-LiTE Microbial Test - water D7463 Hy-LiTE Microbial Test - fuel D7501 Cold Soak D7525 Standard Test Method for Oxidation Stability of Spark Ignition Fuel - Rapid Small Scale Oxidation Test (RSSOT) D Oxidation Test - Romaszewski Oil Bench D7545 Standard Test Method for Oxidation Stability of Middle Distillate Fuels - Rapid Small Scale Oxidation Test (RSSOT) D7563 E85 Emulsion D7576 Benzene and Aromatics in EtOH by GC D7603 Storage Stability and Compatibility D7671A Silver Corrosion D7756 Residues in Liquefied Petroleum (LP) Gases by Gas Chromatography with Liquid, On-Column Injection Detroit Diesel (Enhanced) Soot by TGA - LUBRICANTS ONLY Foam Test - Foam Test - Foam Test - - Option A Foam Test - VI Miscibility Rust Protection - - Humidity Cabinet-50 hours Seal Test - Nitrile - GRN1386 Seal Test - Polyacrylate - A ETI Seal Test - Polyacrylate - GRA2256 Seal Test - Polyacrylate Seal Test - Vamac - A ETI Seal Test - Vamac - FML-69 Seal Test - Vamac - P-250 Seal Test - Viton - 7V2127 Seal Test - Viton - V150B Seal Test - ACM C Seal Test - AEM C Seal Test - NBR C Seal Test - Diamler Chrysler AK C Dielectric Constant Dielectric Constant DIN Part 1 Aging Characteristics of Lubricating Oils (Part 1) DIN Part 2 Aging Characteristics of Lubricating Oils in the Presence of Iron Oxide (Part 2) DIN A Corrosion Test DIN B Corrosion Test DIN Insolubles - Centrifuge DIN Viscosity - Kinematic - (Specify Temperature) DIN Shear Stability - Hydraulic (250 passes) DIN Elements - (Al, Cr, Cu, Fe, Pb, Si, Sn) DIN Infrared Spectra - Analysis of Oxidation and Nitration of Used Engine Oils DIN Infrared Spectra - Determination of Soot content in Used Diesel Oil by Infrared Spectroscopy DIN Carbon Residue DIN Viscosity - Kinematic - Ubbelohde Viscometer - Specify Temperature E202 Mod. Glycol - Engine Coolant - Composition (Modified) E203 Water by Coulometric Karl Fisher Titration E659 Auto Ignition Temperature of Liquid Chemical Products E1064 Water Content - Organic Liquids (Coulometric) E1269 Specific Heat E2680 Appearance E2716 Specific Heat Capacity by MTDSC EI th Edition (2008) Specifications and Qualification Procedures for Aviation Jet Fuel Filter/Separators EI th Edition (2010) Laboratory Tests and Minimum Performance Levels for Aviation Fuel Filter Monitors EMD LO.201 Rev. C Silver Corrosion - EMD Revision C EN14078 FAME Content () EN14112 Oxidation Stability of Biodiesel by Rancimat EN15751 Oxidation Stability - FAME and FAME/Diesel Blends EPA 3051A Microwave Digestion EU-PAHA Analysis of 8 PAH in oil by HRGC/LRMS EU-PAHB Analysis of 8 PAH in oil by HRGC/HRMS EXT-A Extraction of One Filter (up to 20" by 20") EXT-B Extraction of One PUF/XAD/PUF Canister Ferrography Ferrography Aluminum Beaker Oxidation Test (300 Hours) - BJ110-4 Appearance of Additive by Visual Inspection - AMS Extreme Pressure Properties of Lubricants - BJ1-2 (A) Extreme Pressure Properties of Lubricants - BJ1-2 (B) Filterability - Engine Oil - BJ Oxidation - Water Tolerance Test (Modified) - BJ110-3 Sediment - Determination of Initial and Extended Sediment in Additive

5 FTM 203 Cycle C Pour Point - Stable FTM Oil Separation From Lubricating Grease - Static Technique FTM Induction System Deposits Bench Test FTM 791C.6053 Manifold Ignition Test FTM 2540C Dissolved Solids in Engine Coolants FTM 3013 Particulates FTM Compatibility Characteristics of Universal Gear Lubricants FTM 3430/3440 Storage Stability and Compatibility FTM 3430/3440 Mod Storage Stability and Compatibility-Modified-1 Reference Fluid FTM Channeling Characteristics FTM 3462 Panel Coker Test (8 Hour Interval) FTM Salt Spray FTM Mod Corrosion and Oxidation Stability (Modified) FTM Corrosion and Oxidation Stability FTM MIL Corrosion and Oxidation Stability FTM 5321 Corrosion - Lead FTM Corrosiveness of Oil on a Bi-Metallic Couple FTM 5329 Humidity Resistance Gas Chromatography GC Fingerprint - Gasoline GC/MS Benzene, Toluene, EthylBenzene and Xylenes by GC/MS GC/MS GCMS Fingerprint GE Bronze Friction - GE GE Oxidation Test - GE GFC T021 x 88 Oxidation Test - GFC Seal Test - Fluoroelastomer - FKM-1 Seal Test - Nitrile - HNBR-1 Seal Test - Polyacrylate - ACM-1 Seal Test - Silicon - VMQ-1 GMN10060 Filtration GS1000 Full Analysis (Vol%) by PetroSpec GS1000 plus GS1000 Full Analysis (Wt%) by PetroSpec GS1000 plus Honda Corrosion - Copper Strip - Honda Honda Seal Test - Honda - (price is per elastomer/per interval/per temperature) InfraCal Biodiesel (%) in Diesel Fuel by InfraCal Analyzer IP 48 Oxidation Test - Lubes IP 306 Oxidation Stability IP 309 Cold Filter Plugging Point IP 585 FAME in Aviation Turbine Fuels FT Oil Analyzer Infrared Spectra - Fingerprint using 0.10 mm NaCl cell Infrared Spectra - Oxidation - Total Absorbance - (0.1 mm cell uncorrected) Infrared Spectra - Oxidation - Peak Area Infrared Spectra - Oxidation - Peak Height Infrared Spectra - Oxidation - Peak Height - ABOT Infrared Spectra - Oxidation and Nitration - Peak Area Infrared Spectra - Oxidation and Nitration - Peak Height Infrared Spectra - Oxidation - Peak Height (NaCl cell) Infrared Spectra - Fingerprint Infrared Spectra - Fingerprint - (Unknown Analysis) Infrared Spectra - for Mack T12 (Includes Method 5 and PE method) Infrared Spectra - (MACK) FT Method 5 Infrared Spectra - Oxidation - Peak Height - ( Friction Test) Infrared Spectra - Nitration - Area (Subjective) and Peak Height Infrared Spectra - Nitration - Area (Fixed) and Peak Height Infrared Spectra - Fingerprint on Unwashed Gum Residue Isentropic Bulk Modulus Isentropic Bulk Modulus of Petroleum Fluids ISO (Proposed) Particle Count - Class 8 Specification ISO 4406 Particle Size Count (Reports ISO Code and specific particle counts) ISO 4406 Particle Size Count (Reports ISO Code Only) ISO 4407 Optical Particle Counting ISO Filtration Efficiency Using Particle Counting and Contaminant Retention Capacity ISO Inlet and Outlet Anti-Drain Valve Tests ISO Filterability (Dry) ISO Filterability (Wet) ISO Multi-Pass Method for Evaluating Filtration Performance of a Filter Element ISO Filtration Efficiency using Particle Counting and Contaminant Retention Capacity ISO Manifold Ignition Test ISO UREA for AUS 32 ISOT Oxidation Test - Indiana Stirring JDQ-9 Seal Test - Compatibility (all elastomers) JDQ-16 Oxidation Test JDQ-19 Water Sensitivity JDQ-22 Rust Protection - Humidity Cabinet hours JDQ-22 Rust Protection - Humidity Cabinet hours JDQ-23/ JDM Compatibility - With other Oil JDQ-24 Cold Flow Properties of Lube Oil JDQ-33 Foaming Characteristics with Option A JDQ-71 Pour Point - Stable JDQ-72 Pour Point JDQ-73 Low Temperature Fluidity - Per Temperature JDQ-74 Low Temperature Fluidity - Per Temperature JIS D 1611:1995 Lubricating Oil Filters for Internal Combustion Engines - Part 1: General Test Methods JIS D 1617:1998 Fuel Filters for Diesel Engines - Test Methods JIS K D893A Insolubles - Normal - Includes Pentane, Tolulene, Resins JIS K D893B Insolubles - Coagulated - Includes Pentane, Tolulene, Resins JIS K 2001 Viscosity Classification for Industrial Liquid Lubricants JIS K 2252 Reaction JIS K 2272 Ash JIS K 2272 Ash - Sulfated JIS K 2275 Water - Coulometric JIS K 2283 Viscosity - Kinematic at 100C (cst) JIS K 2283 Viscosity - Kinematic at 40C (cst) JIS K 2501 Acid Number JIS K 2501 Base Number - HCl JIS K 2501 Base Number - Perchloric Acid JIS K 2513 Corrosion - Copper - Copper Strip Test JIS K 2514 Oxidation Test - Indiana Stirring JIS K 2536 Kerosene in Gasoline by GC (Clause 6) JPI-5S-23 Fuel Dilution - Diesel JPI-5S-41 Procedure B Volatility - NOACK (1 hour at 250C) Seal Test - All Elastomers (HNBR-1, ACM-1, FKM-1, VMQ-1, AEM-1) Seal Test - Nitrile - HNBR-1 Seal Test - Polyacrylate - ACM-1 Seal Test - Silicon - VMQ-1 Seal Test - Vamac - AEM-1 Seal Test - Viton - FKM-1 Liqui-cult Test Kit Liqui-cult Micro Organism - Fuels M2C a Viscosity - Stability M2C b Corrosion - Copper M2C Seal Test - Compatibility M2C Water Sensitivity M2C Homogeneity and Compatibility Mercedes-Benz Seal Test - AK6 - Mercedes-Benz Falex Pin and Vee-Block - Extreme Pressure ( 100C and 150C in duplicate) Foaming Characteristics - Sequence I, II, III and IV - () Four Ball - (100 and 150C in duplicate) Miscibility - V Noack (2 150C) Seal Test - BUNA N ATRR (with references and T and E) Seal Test - Polyacrylate ATRR (with references and T and E) Seal Test - Viton ATRR (with references and T and E)

6 Seal Test - Vamac ATRR (with references and T and E) Seal Test - ATRR (with references and T and E) Timken - OK Load - Extreme-Pressure Properties - MIL-L-21260/4.6.3 Humidity Cabinet Corrosion Protection MIL-L-21260/4.6.4 Salt Water Immersion MIL-L-21260/4.6.5 Acid Neutralization MIL-L Storage Stability (14 days) NACE TM Rust Preventing Properties (NACE) Foam Test Insoluble Deposit Test Corrosion Test Water Tolerance Rust Test Oxidation Test NFPA T Particle Count - Using Liquid Automatic Counter Compatibility - -TC-W3 Filter Plugging Test (Filterability) Identification Test - Includes 40C (), Sulfated Ash (D874), Cloud Point (D2500), Distillation (D6352), Base Number (D2896), Nitrogen, Kjeldahl (D3228M), Nitrogen, Carlo Erba (D5291) and FT (E168) Rust Test - FCW - (Includes one set of photos) Fluidity - Specify Testing Temperature Norfolk Oxidation - Norfolk NPAH-A Analysis of Nitro-Polycyclic Aromatic Hydrocarbon (N-PAH) by GC/MS with NI/CI/SIM NPAH-B Analysis of Nitro-Polycyclic Aromatic Hydrocarbon (N-PAH) by HRGC/HRMS PREP-A Preparation of 2" i.d. Glass PUF/XAD/PUF Sampling Canister PREP-B Preparation of 4" i.d. Stainless Steel PUF/XAD/PUF Sampling Canister SAE Air 4978 FZG Gear Screening Test SAE ARP 1400revB Recommended Practices for Lubricating Oil Filters, General Aviation Reciprocating Engine (Piston Type) Aircraft SAE ARP 1827A Measuring Aircraft Gas Turbine Engine Fine Fuel Filter Element Performance SAE ARP 901 Bubble Point Test Method SAE AS4059F Cleanliness Classification for Hydraulic Fluids SAE HS-806 SAE Oil Filter Test Procedure SAE J300 Pour Point - Stable SAE J905 Fuel Filter Test Methods SAE J1488 Emulsified Water/Fuel Separation Test SAE J1839 Coarse Droplt Water/Fuel Separation SAE J1985 Fuel Filter Initial Single-Pass Efficiency Test Method Speed of Sound Speed of Sound in Fluids SVOC-A Analysis of Engine Emissions for Semi-volatile Hydrocarbons by GC/MS PI/EI/full scan SVOC-B Semi-Volatile Hydrocarbon Speciation of Diesel or Jet fuels by GC/MS PI/EI/full scan SVOC-C Extraction of 2" I.d. Glass PUR/XAD/PUR Sampling Canister SVOC-D Extraction of 4" I.d. Stainless Steel PUR/XAD/PUR Sampling Canister Differential Scanning Calorimeter Scan FAME by Gas Chromotography Fuel Dilution - Ethanol High Pressure High Frequency Reciprocating Rig Intake Valve Deposit Screening Test - Dirty-Up/Clean-Up Intake Valve Deposit Screening Test - Keep Clean Isentropic Bulk Modulus (30C max.) ph Meter Lubricity - Silver - Falex 4Ball Tester Speed of Sound - Liquids Thermal Conductivity by Transient Hot Wire (Specify Temperature) Wire on Capstan TANNAS Viscosity - TANNAS Basic Rotary Viscosity TES-389 Aluminum Beaker Oxidation Test (300 Hours) TES-389 Seal Test - Allison TES-439 Aluminum Beaker Oxidation Test (300 Hours) Thermal Conductivity Thermal Conductivity by Transient Hot Wire TP Filterability - DENNISON Union Pacific Oxidation Stability Test - Union Pacific VDA Seal Test - NBR 34 (168 hours, 100C) VW Seal Test - Volkswagen - ACM1 (168 hours, 150C) VW Seal Test - Volkswagen - ACM1 (500 hours, 150C) VW Seal Test - Volkswagen - AEM - EAM1 (168 hours, 150C) VW Seal Test - Volkswagen - AEM - EAM1 (500 hours, 150C) VW Seal Test - Volkswagen - AEM - EAM2 (168 hours, 150C) VW Seal Test - Volkswagen - AEM - EAM2 (500 hours, 150C) VW Seal Test - Volkswagen - AK6 (168 hours, 150C) VW Seal Test - Volkswagen - AK6 (282 hours, 150C, oil changes) X-Ray Elements - Special Application Determination (Xray Fluorescence for Na thru Pb, Na and Mg >0.1%) Multi-element, Standardless, Qualitative Analysis X-Ray Elements - Special Application Determination (Xray Fluorescence for Na thru- Pb, Na and Mg >0.1%) Multi-element, Standards used, Semi-Quantitative (Pending) Blotter Test