CUSTOM MANUFACTURING CAPABILITIES AND EQUIPMENT

Transcription

1 3324 Chelsea Avenue Memphis, TN 3808 Toll Free: PENN Fax: CUSTOM MANUFACTURING CAPABILITIES AND EQUIPMENT

2 CONTENTS SITE INFORMATION LOCATION EXPERIENCE TYPES OF SERVICES AVAILABLE TRANSPORTATION UTILITIES OVERVIEW OF AVAILABLE UNITS EQUIPMENT LISTS FOR AVAILABLE UNITS Page 2 of 27

3 SITE INFORMATION LOCATION Northeast section of Memphis, Tennessee Contact: Tom Colanero at EXPERIENCE 50 years of hydrogenation reactions experience using a variety of copper and nickel based catalysts at conditions ranging from psi and F. 40 years of de-carbonylation reaction experience using precious metal-based catalysts at pressures ranging from psi and temperatures from F. 40 years of strong acid catalyst-based polymerization reaction and processing experience. 50 years experience in steam and high-purity hydrogen generation. Up to 20 years experience in the following: Reductive animations Condensation reactions Oxidations Esterifications Neutralizations Solvent stripping Air stripping of waste water Recovery of precious metals catalyst Pressure and vacuum distillations Blending ISO 900:2000 Certified and PSM/RMP covered site. Page 3 of 27

4 Experience with both large and small clients. TYPES OF SERVICES AVAILABLE Batch distillations at pressures ranging from full vacuum to 200 psi. Single and multi-column continuous distillations at pressures ranging from full vacuum to 00 psi. Reactions including but not limited to: Liquid phase hydrogenations from atmospheric up to 500 psi Liquid phase de-carbonylations at temperatures up to 500 F Aminations Esterifications Oxidations Blending and packaging operations ranging from bulk to 5-gallon pails. Filtrations. Full service QA/QC laboratory. R&D facilities with an extensive array of equipment and expertise. Pilot plant with a large assortment of equipment and capabilities. Other - Specific needs/requirements can be discussed in detail by inquiry. TRANSPORTATION Rail - X switchyard directly across the street from site. Railcar loading/unloading facilities on-site. 3+ miles of on-site track. Truck - Serviced by all major truck lines. Located ½ mile off I-240. Bulk truck loading/unloading facilities. Drum/ pail filling, handling and shipping facilities. Barge - Service available via tank car shuttle between the site and the barge terminal located downtown on the river. Page 4 of 27

5 UNIT (Bldg 84) OVERVIEW OF AVAILABLE UNITS Original Use: Purification and recovery distillation system. Consists of two vacuum distillation columns (one available 00% of time and one 70%) with associated ancillary equipment, including vessels, pumps, vacuum pumps, exchangers, receivers, etc. UNIT 2 (Bldg 78) Note: This process currently operates approximately 4 months/yr on a campaign basis. It is idle/unused for approximately 8 months each year. The parallel small reactor noted below is not used in this operation. It, along with its hot oil system, etc, is idle/unused 00% of the time. However, it is still currently connected to and coupled with the operating process. Original Use: Continuous liquid phase endothermic reaction (50-75 psi/ F) process with feed pretreatment and post reaction purification. Consists of: A feedstock reactant treatment system with hold tanks. Two vacuum distillation columns with associated ancillary equipment, including vessels, pumps, vacuum pumps, exchangers, receivers, etc. Originally used for purification of the feed to the reactor. Two parallel reactors (one large, one small) with distillation columns flanged to the heads and condensers, vessels, pumps, etc., for purification of the vapor out-flow, internal coils with hot-oil recirculation systems, including vessels, pumps, gas fired heaters, etc., for heating the reactors. (See Note above regarding small reactor) Three pressure distillation columns with associated ancillary equipment, including vessels, pumps, exchangers, receivers, etc., for recovery of the feedstock exiting the reactor and purification of the product. Two scrubbing columns with associated ancillary equipment, including vessels, exchangers, pumps, receivers, etc., for removing and recovering the product from the waste non-condensable gas stream that exits the reactor. A system for collection of all the waste streams from the process and recovery of the feedstock contained in them via a vacuum distillation column with its associated ancillary equipment, including vessels, pumps, vacuum pumps, exchangers, receivers, etc. A centrifuge system and a parallel filtration system for recovery of the catalyst used in the reactor, which in the original use was a precious metal-based material. Includes feed and filtrate vessels, pumps, etc. Page 5 of 27

6 Two gas-fired hot-oil (550 F) recirculation systems for heating the reactors. Includes expansion tanks, pumps, gas-fired heaters, etc. (See note above regarding the small reactor and oil system) UNIT 3 (Bldg 54) Note: A portion of the equipment in this area is currently 00% utilized for another project. The Detailed Equipment List reflects only the specific equipment that is currently available. Original Use: Reaction of a ring compound to a chain polyol with subsequent processing and purification of the polyol. Consists of: An agitated, jacketed TR system with vent condenser, cooling, pumps, exchangers, etc. Parallel Teflon lined batch still pots with Hastalloy steam spargers and Teflon lined distillation columns for recovery of the unreacted feedstock. Neutralization and distillation system for purification of the recovered feedstock including columns, reboilers, vessels, exchangers, pumps, etc. Teflon lined neutralization and decant vessels with pumps, etc. Dehydration system consisting of distillation columns with associated periphery equipment. Parallel filtration systems with precoat tanks and body feed systems. Two stage solvent stripping system with each stage consisting of an evaporator and a stripper. The second stage operates under a vacuum. 4 stage steam jet vacuum system capable of 0 mm Hg abs. Solvent recovery and purification system consisting of two distillation towers with associated reboilers, reflux drums, pumps, etc. Waste water air stripping system consisting of tower, air blower and preheater, overheads condenser, tanks, pumps, etc. UNIT 4 (Bldg 45) Original Use: This unit was designed and constructed to be a multi-purpose pilot plant scale reaction and processing facility. Consists of small-scale multiple reactors, specialized equipment, and vessels of varying materials of construction and design conditions. By rerouting of piping and hoses, a wide variety of processing configurations can be obtained. Specific needs or requirements can be discussed upon inquiry. Page 6 of 27

7 UNIT 5 (Bldg 85) Original Use: Dehydrolysis or dewatering reaction of a diol to form H2O and product with subsequent drying and purification of the product. Consists of: A large kettle type high alloy reactor with a distillation column flanged to the top with a condenser, reflux drum and pump, etc. Rx equipped with an internal bayonet type U-bundle for heating. A small tank and pump system for feeding liquid catalyst to the reactor and a small neutralization system for treating the blowdown waste from the reactor. A drying and purification system downstream of the reactor consisting of three large, very tall, tray columns with associated reboilers, exchangers, vessels, pumps, etc. First column - Dewatering column: Removed the bulk of the water from the reaction by a solvent stripping distillation. Second column - Solvent drying column: Removed the water from the solvent from the first column and returned the solvent back to the first column. Operated under vacuum provided by a vacuum pump. System includes solvent storage and supply system and a waste blowdown collection system. Third column Purification column: Completed drying and purification of the overhead product from the first (dewatering) column. A product work tank system consisting of two large day tanks with a system for adding inhibitor to the product before transferring to storage. A vent collection and scrubbing system. UNIT 6 (Bldg 55) Original Use: Reaction of a ring compound to a chain polyol with subsequent processing and purification of the polyol. Consists of: An agitated, jacketed TR system with vent condenser, cooling, pumps, exchangers, etc. Parallel Teflon lined batch still pots with Hastalloy steam spargers and Teflon lined distillation columns for recovery of the unreacted feedstock. Neutralization and distillation system for purification of the recovered feedstock including columns, reboilers, vessels, exchangers, pumps, etc. Teflon lined neutralization and decant vessels with pumps, etc. Dehydration system consisting of distillation columns with associated periphery equipment. Parallel filtration systems with precoat tanks and body feed systems. Page 7 of 27

8 Two stage solvent stripping system with each stage consisting of an evaporator and a stripper. The second stage operates under a vacuum. Combination pump and steam jet vacuum system capable of 5 mm Hg abs operating pressure. Solvent recovery and purification system consisting of two distillation towers with associated reboilers, reflux drums, pumps, etc. Waste water air stripping system consisting of tower, air blower and preheater, overheads condenser, tanks, pumps, etc. Page 8 of 27

9 UNIT (Bldg 84) Columns Size MOC Type Internals 6" x 0' 8' Pall Ring Packed Sect 8" x 2' 8' Pall Ring Packed Sect 3' x 38' 2 5' Fleximax Packed Sect 6.5' x 72' Sieve Tray 30 Trays Design Press Design Temp Comments 5 psi/fv 300 F Base level tank. No reboiler. 5 psi/fv 350 F Base level tank. No reboiler. 5 psi/fv 400 F Bottom tank integral with column. External thermosiphon reboiler. 5 psi/fv 400 F Bottom tank integral with column. External thermosiphon reboiler. Exchangers Area (sq. ft.) # Tubes MOC Design Press (PSI) Design / # Passes (All ") Shell Tube Shell Tube Temp Comments 33 / /FV 50/FV 400F Insulated 07 / 46 00/FV 00/FV 350F 228 / /FV 00/FV 300F 365 / L SS 200/FV 50/FV 400F Insulated 380 / L SS 200/FV 50/FV 400F Insulated 564 / 42 00/FV 00/FV 400F Insulated 6 / L SS 200/FV 50/FV 400F Insulated 653 / /FV 00/FV 400F 677 / /FV 00/FV 400F 53 / /FV 00/FV 400F Vessels Nom Cap Nom MOC Design Press Design Comments (gals) Dimen Temp 20 2 x 2.5 V 4 psi/fv 350F 70 2 x 3 H 4 psi/fv 350F x 4 H 4 psi/fv 350F X 4.5 V 200 psi/fv 400F Insulated X 5 V 4 psi/ - psi 350F X 5 V 4 psi/fv 350F X 5 V 4 psi/fv 350F X 6 H 4 psi/fv 350F 00 5 X 7.5 V 36L SS 20 psi/fv 350F 00 5 X 7.5 V 4 psi/ -4 psi 350F X 4 V 4 psi/ -4 psi 350F X 0 H 4 psi/ -7 psi 350F X 20 V 4 wc/ - 0 wc 350F Page 9 of 27

10 Other One liquid seal ring vacuum pumps. Ductile iron, 5 hp, 66 rpm, 250 icfm D control system. UNIT 2 (Bldg 78) Columns Size MOC Type Internals Design Press (psi) Design Comments Temp ' x 8' Flexring Pkg 00/FV 350 F Bottom pot integral with column. External thermosiphon reboiler 8"/4" x 28' 2 Sections Flexring Pkg 4/ - psi 350 F Base level tank. No reboiler. 6"/20"x 32' 2 Sections Flexring Pkg 00/FV 350 F Base level tank. No reboiler. 2" x 5.5" 304 SS Pall Ring Pkg F No base pot or reboiler. Flanged to small reactor head. Available 00% of time, but still tied to process. 2' x 2' IMPT Pkg 00/FV 250 F Base level tank. No reboiler 2' x 5' Flexipack Pkg 4/FV 350 F Base level tank. No reboiler 2' x 55' 2 Sections Flexpack Pkg 00/FV 350 F Bottom pot integral with column. External thermosiphon reboiler 2.5' x 6.5' Pall Rings 4/FV 350 F Base level tank. No reboiler 2.5' x 6.5' Pall Rings 4/FV 350 F Base level tank. No reboiler 3' x 35' 2 Sections Flexpack Pkg 00/FV 375 F Bottom pot integral with column. External thermosiphon reboiler 4' x 3' Flexring Pkg 00/FV 500 F No base pot or reboiler. Flanged to large reactor head 4.5' x 72.7' Flexivalve Trays 4/FV 350 F Bottom pot integral with column. 30 Trays 5' x 55.5' Sieve Tray 20 Trays Exchangers External thermosiphon reboiler 4/FV 350 F Bottom pot integral with column. External thermosiphon reboiler Area (sq ft) / # Tubes MOC Design Press (psi) Design Comments # Passes (All ") Shell Tube Shell Tube Temp 6 / 5 75/FV 25/FV 350 F Insulated 20 / 5 00/FV 25/FV 350 F Insulated 2 / 27 36L SS 75/FV 00/FV 375 F Insulated 29 / 00/FV 00/FV 250 F Insulated 29 / 00/FV 00/FV 250 F Insulated 30 / 2 50/FV 50/FV 375 F Insulated 30 / 2 50/FV 50/FV 375 F Insulated 30 / 2 50/FV 50/FV 375 F Insulated 30 / 2 50/FV 50/FV 375 F Insulated 54 / 36L SS 36L SS 200/FV 200/FV 600 F Insulated 63 / /FV 25/FV 350 F Insulated 79 / L SS 25/FV 00/FV 300 F Insulated 0 / 48 36L SS 75/FV 00/FV 375 F Insulated 9 / /FV 50/FV 425 F Insulated Page 0 of 27

11 28 / 55 75/FV 25/FV 350 F Insulated 32 / /FV 25FV 375 F 36 / /FV 75/FV 350 F Insulated 45 / 69 36L SS 75/FV 00/FV 375 F Insulated 5 / /FV 00/FV 250 F 82 / 78 75/FV 75/FV 350 F Insulated 98 / /FV 20/FV 250 F 300 / /FV 00/FV 250 F Insulated 33 / /FV 25/FV 300 F Insulated 338 / /FV 25/FV 250 F Insulated 39/ /FV 25/FV 425 F Insulated 43 / 97 00/FV 00/FV 425 F Insulated 693 / L SS 75/FV 00/FV 375 F Insulated 783 / /FV 25/FV 300 F Insulated 6 / 45 36L SS 75/FV 00/FV 375 F Insulated 348 / /FV 00/FV 300 F Insulated 567 / L SS 75/FV 00/FV 375 F Insulated Vessels Nom Cap Nom MOC Design Design Comments (gals) Dimens Press Temp 30.5' X 2' V 50 psi 200 F 30.5' X 2' V 0" wc 200 F Flat Head 60 2' x 2.5' V 4 psi/fv 300 F ' x 2.5' V 304 SS 00 psi 200 F 00.5' x 7' V 00 psi 400 F Insulated 00 2' x 4.5' V 36L SS 4 psi/fv 300 F Column base level tank 00 2' x 4.5' V 4 psi/fv 250 F ' x 4' V 0" wc 200 F Flat Bottom ' x 4' V 304 SS 50 psi 400 F 200 2' x 8 ' H 4 psi/fv 300 F ' x 8' H 4 psi/fv 350 F ' x 8' H 4 psi/fv 300 F 350 4' x 3.5' V 50 psi 400 F Agitated, Insulated 450 3' x 8' H 00 psi 375 F Vertical Perforated Baffle 450 3' x 8' H 00 psi 350 F Vertical Perforated Baffle 500 4' x 5' V 50 psi 400 F Insulated ' x 8' V 36L SS 4 psi/fv 300 F Column Base Level Tank 750 5' x 4.5' V 00 psi 200 F Agitated ' x 0.5' H 4 psi/fv 350 F Vertical Baffle, Two Chambers SS 00 psi 400 F Insulated 000 5' x 6.5' V 0" wc 300 F Flat Bottom 770 6' X 7.5' V 304 SS 00 psi 500 F Reactor. Insulated. Agitated, Int Coil. Available 00% of time, but still tied to process ' x 8' V 0" wc 200 F Flat Bottom ' x 8' V 0" wc 200 F Flat Bottom ' x 9' V 00 psi 500 F Reactor. Insulated. Agitated, Int Coil ' x 20' V 00 psi 250 F ' x 4' V 4 psi/fv 250 F Agitated ' x 4' V 0" wc 300 F Flat Bottom Page of 27

12 5500 8' x 4' V 4 psi 500 F Cone Bottom, Insulated ' x 0' V 0" wc 300 F Flat Bottom Insulated ' x 5' V 00 psi 300 F 7000 ' x 0.5' V 0" wc 250 F Flat Bottom 7800 ' x ' V 0" wc 300 F Flat Bottom Insulated ' x 4' V 0" wc 350 F Flat Bottom ' x 8.7' V 304 SS 0" wc 200 F 0,000 0' x 7' V 00 psi 350 F 0, ' x ' V 0" wc 200 F Flat Bottom 5,000 2' x 8' V 0" wc 200 F Flat Bottom Other Two Liquid Seal Ring vacuum pumps. Ductile Iron, 50 Hp, 70 RPM, 200 ICFM. 80 mm Hg. One Liquid Seal Ring vacuum pump. Ductile Iron, 20 Hp, 70 RPM, 50 ICFM. 40 mm Hg. One Hot Oil recirculation system including expansion tank, overflow tank, pump, etc. 5MM BTU/hr capacity. One Hot Oil recirculation system including expansion tank, overflow tank, pump, etc. 5MM BTU/hr capacity. Available 00% of time, but still tied to process. One 6 sq meter candle type filtration system One process centrifuge. 0 gpm feed rate. Single Loop Control System UNIT 3 (Bldg 54) Columns Size MOC Internals Design Press 6" x 9' Derakane 470 3' x 23' TFE Lined 3' x 23' TFE Lined Design Temp Comments Random Polypro 4 psi/fv 200F Includes bottom pot Random Polypro 2 psi/ - psi 270F Loose liner Random Polypro 2 psi 270F Loose liner 4 x.5' 36L SS Random SS 4 psi/fv 250F 4' x 40.5' Hetron 980 Random Polypro 6 psi/ - psi 200F Page 2 of 27

13 32" x 24' 304LSS Sieve Trays 30 psi/fv 350F 2' x 6' 304LSS Random SS 4 psi/fv 250F Includes bottom pot 0" x 4' 304LSS Random SS 4 psi/fv 300F 2' x 5' 304LSS Sieve Trays 4 psi/fv 300F Sections Bot.5' x 32.5 Mid 2' x 5 Top 2.5' x 5' 304LSS Random SS 50 psi/fv 350F Exchangers Area(sq ft) # Tubes/ /# Pass Size (") 400 / / / / / 20 8 / 5? /? /? / / / 3 36 / 3 23 / 2 (U) / / 7? / 7? / / 27 MOC Shell Tube Alloy 20 36L SS 36L SS Graphite Block Graphite Block Graphite Block 36L SS 36L SS 36L SS 36L SS 36L SS Graphite Block Graphite Block Karbate 36L SS Press Shell/Tube 200 psi-fv 00 psi/fv TEMP (F) Nom Shell Dimens 340 5" x 8' 340 2" x 7' 340 6' x 4' 340 6' x 4' 340 8" x 0' " x 8' " x 5' " x 5' x x x x x x x " x 7' " x 4' 340 8" x 8 ' Comments Page 3 of 27

14 380 / LSS 735 / LSS 440 / / / / / LSS 304LSS / LSS 304LSS 247 / / 6 (U) / / / / / 5 93 / 36 Bayonet U / / / / / 90 Bayonet U 325 / / / 90 Bayonet U 200 psi-fv 200 psi-fv 200 psi-fv 50 psi-fv 50 psi-fv 5 psi-fv 200 psi-fv 50 psi-fv 5 psi-fv Page 4 of " x 6' 340 2" x2' 340 6" x 8' 340 7" x 8' 400 8" x 6' 400 9" x 2' 300 9" x 20' 340 8" x 6' Disc & Donut Falling Film Evap 400 7" x 6' 340 8" x ' Disc & Donut Falling Film Evap 304LSS 350 3" x 0' 304LSS x 304LSS 200 psi-fv 370 4" x 8' 304LSS 250 psi-fv 200 psi-fv 370 7" x 7' 304LSS 200 psi-fv 370 7" x 7' 304LSS 340 4" x 0' 304LSS 340 0" x 6' 304LSS 36L SS 200 psi-v 390 6" x 4' Reboiler 304LSS 430 6" x 8' 340 9" x 6' 304LSS 340 " x 4' 304LSS 304LSS 340 8" x 3' 304LSS 36L SS 200 psi-fv 390 5" x 5' Reboiler 340 8" x 0' 200 psi-fv 340 " x 3' 36L SS 200 psi/fv 390 5" x 5' Reboiler

15 74 / / / / / / LSS 304LSS 200 psi-fv 200 psi-fv 340 5" x 9' 340 9" x 0' 370 9" x 7' 340 9" x 5' 370 9" x 7' 390 " x 3' Vessels Nom Cap (gals) Nom Dimen Orient MOC Design Press Page 5 of 27 Design Temp (F) 5,000 2' x 4' H 50 psi/fv ' x 5' H 00 psi/fv ' x 4' V 304 SS 4 psi / - psi 250 Comments ' x 0' V TFE Lined 2 psi / - psi 270 Loose liner. Hastalloy Sparger ' x 0' V TFE Lined 2 psi / -psi 270 Loose liner. Hastalloy Sparger 600 4' x 6.5' H TFE Lined 2 psi / -psi 270 Loose liner 600 4' x 6.5' H TFE Lined 2 psi / -psi 270 Loose liner ' x 8.5' V 00 psi/fv ' x 7' V 36L SS 4 psi / - psi 250 With agitator 000 5' x 7' V 36L SS 4 psi / - psi 250 With agitator 0,000 ' x 4' V Kynar lined 2 psi -psi 220 Hetron 500 4' x 5' V Kynar lined 2 psi / -psi 220 Hetron 000 5' x 8' V Hetron psi / - psi ' x 8' V Kynar line 4 psi / - psi 250 Tefzel coated 36SS Agitator ' x 4' V 36L SS 4 psi / - psi ' x 5' V HETRON psi / - psi ' x 6' V Derakane 4 4 psi / - psi ' x 0' V TFE Lined 2 psi / -psi 270 Loose liner. With Agitator 900 5' x 8' V 30 psi/fv 350 Column Base 750 4' x 8' H 4 psi/fv ' x 7' V 304 SS 4 psi / -psi 200 With Agitator 000 5' x 7' V 304 SS 4 psi / -psi 200 With Agitator 200 3' x 4 V 304 SS 4 psi / -psi 340 With Agitator 200 3' x 4' V 304 SS 4 psi / -psi 340 With Agitator ' x 8' V 304 SS 4 psi / -psi ' x 2' V 304 SS 4 psi / -psi ,000 V 2" wc/ -4"wc 250 With Side Mount Agitator 26,000 V 2" wc/ -4"wc 250 With Side Mount Agitator 2,000 V 2" wc/ -4"wc 300 With Side Mount Agitator 200 5' x 8' V 4 psi / -psi ' x 5' V 4 psi/fv ' x 7' H 4 psi/fv ' x 0' V 4 psi / -psi 250 With Agitator

16 'x4' V 4 psi/fv 'x 7' H 4 psi/fv ' x 4' H 304 SS 50 psi 350 Column Base ' x 8' V 20"wc/ -6"wc ' x 3' V 4 psi/fv ' x 5.5' V Alloy 20 Vessel 4 psi/fv Jckt 00 psi 350 Jacketed with Agitator Other 4 stage steam jet vacuum system capable of 0 mm Hg abs. Vertical leaf filter. 00 psi, 304SS, 350F, 00 sq ft. Vertical leaf filter. 00 psi, 304SS, 350F, 200 sq ft. UNIT 4 (Bldg 45) Columns Size MOC Type Internals Design Design Comments Press Temp 8" x 304 SS 50 psi 500 F 25 Theoretical Stages Exchangers Area (sq ft) # Tubes MOC Design Press Design Comments # Passes Diam Shell Tube Shell Tube Temp 34 / 3/8" SS 50 psi 50 psi 350 F 65 / 84 ¾" 36 SS 50 psi 50 psi 350 F Vessels Nom Cap Nom MOC Design Design Comments (gals) Dimens Press Temp 5 2" x 27" V 36 SS 600 psi 500 F Reactor. Agitated, jacketed, insulated, gas sparge ring. 20 8" x 6" V Glass Lined 200 psi 500 F Not installed. Reactor. Agitated, jacketed, 20 sq ft overhead condenser - 75 psi Des press. 26 3/4" SS tubes " x 5" V 36L SS 50 psi 350 F Not installed. Reactor. Agitated, jacketed, 34 sq ft overhead condenser - 50 psi design press. 3/8" SS tubes 35 6" x 43" V SS 50 psi 200 F Receiver 35 6" x 43" V SS 50 psi 200 F Receiver 50 24" x 25" V 36L SS 50 psi 350 F Reactor. Jacketed. Scraped wall agitator, 34 sq ft overhead condenser - 50 psi design press. 3/8" SS tubes. Inclds 25 stage column listed above " x 27" V Glass 50 psi 650 F Agitated, jacketed, reactor. 3" 5 stage column Page 6 of 27

17 Lined flanged to head. 4 sq ft thimble style Glasteel overhead condenser. 50 psi design press. 50 Glass Lined 25 psi 500 F Receiver 00 32" x 64" V Glasslined 50 psi 450 F Not installed. Agitated, insulated jacketed Rx 50 40" x 28" V 36 SS 75 psi Not installed. Agitated, insulated jacketed reactor " x 5" V 36L SS 300 psi 350 F Reactor. Var speed agitator, jacketed, insulated. Gas sparge ring. 20 gpm recirc pump. 8" diam column with 2 theor stages - Atm press or vac only. Includes 65 sq ft exchanger listed above. Other 5 Ton Chilled Water System. Two -tube fixed bed vapor reactor systems. Includes vaporizers, condensers, receivers, and pumps. Tubes are.25" x 6'. Vacuum pump system Tolhurst basket centrifuge. 20" Diam. 5 sq ft. 36 SS sq ft Sparkler pressure leaf filter. 304 SS F. 8 sq ft Sparkler pressure leaf filter. 304 SS F. 26 sq ft Sparkler horizontal pressure leaf filter. 304 SS F. Steam jacketed. 2 weigh scales. 000 lb capacity 50 KW hot oil system. 36 SS Two 304 SS vacuum pumps 2 SS Pope Wiped Film Evaporator 0.35 sq ft. 6 36SS Jacketed Pope Wiped Film Evaporator 2.35 sq ft. Also have glass body for unit. BTRS-90 unit for vapor phase studies Pilot scale operation. Control system is a mix of single loop and manual controls Page 7 of 27

18 UNIT 5 (Bldg 85) Note This list arranged alphanumerically by equipment #. Equip # Service Qty SIZE OR TYPE Design Cap A60 D0 INHIBITOR TANK AGITATOR Feedstock Storage Tank Design Conditions Press. PSIG Temp F Materials Of Construction HP MOTOR ENCL 3.5' IMPELER /3 TEFC 48'ID x 3' 49,629 gal W/LINER D200 REACTOR HEAVIES 4'ID X 8' T/T -- 50/FV 400 DUPLEX D20 D202 D30 D40 REACTOR REFLUX DRUM REACTOR B.D.NEUT. DRUM SOLVENT STRIPPER REFLUX DRUM SOLVENT STRIPPER REFLUX DRUM 5'ID X 7' 6'T/T -- 50/FV L SS ' ID X 6' - "T/T -- 50/FV L SS HORIZONTAL 4' 6" ID X 2' T/T -- 50/FV 'ID X 6' T/T -- 4/FV D404 Solvent Storage Tank 8'-6"ID X 9'H --.5/ D50 LIGHTS REMOVAL COL.REFLUX DRUM 4'6" ID X 2' T/T -- 50/FV D502 PRODUCT K.O.DRUM 24" OD X 6' T/T -- 50/FV D503 D600 PRODUCT PUMP SUCTION DRUM PRODUCT STORAGE TANK 36"ID X 4'6" T/T /FV 'ID X 5' T/T -- D60 INHIBITOR TANK 2'-6"OD X 2' D900 CONDENSATE FLASH DRUM 4/6" VAC 0"wc/ -6"wc 'ID X 9' T/T /FV 300 E0 Feedstock Storage Tank Heater AEL sq.ft. 4,000 BTU/HR 00/FV Page 8 of 27

19 E200 REACTOR HEATER U-TUBE 3 sq.ft. 7.6 MM BTU/HR 4/FV CODE HASTELLOY B /FV CODE HASTELLOY B3 E20 REACTOR O.H. CONDENSOR BEU sq.ft MM BTU/HR 00/FV /FV 400 DUPLEX 2205 E202 NEUTRALIZATION DRUM COOLER AEM sq.ft BTU/HR 00/FV 300 / /FV 250 / L SS E300 DEHYDRATOR COLUMN REBOILER AEL sq.ft MM BTU/HR 50/FV 400 / /FV 400 / E30 DEHYRATOR COLUMN CONDENSER AJM sq.ft MM BTU /HR 00/FV 350 / /FV 300 / 300 TUBES/ CHANNEL E400 SOLVENT STRIPPER REBOILER BKU 40/ sq.ft MM BTU/HR 00/FV 50/FV 400 / / 350 TUBES/ CHANNEL E40 SOLVENT STRIPPER CONDENSER AJM sq.ft. 6.64MM BTU/HR 00/FV 250/ /FV 300 / 300 TUBES/ CHANNEL E402 SOLVENT STRIPPER BOTTOMS COOLER AFM sq.ft MM BTU/HR 50/FV 400 / /FV 300 / 300 TUBES/ CHANNEL --- E404 Solvent Storage Tank BEU MM Page 9 of 27

20 Heater 33 sq.ft. BTU/HR 50/FV 420 / E500 LIGHTS REMOVAL COLUMN REBOILER AEL sq.ft. 8.65MM BTU/HR 50/FV 400 / /FV 300 / 300 TUBES/ CHANNEL E50 LIGHTS REMOVAL COLUMN CONDENSER AEM sq.ft MM BTU/HR 350/35 00/FV 0 00/FV 300 / E502 PRODUCT CONDENSER AEL sq.ft..95 MM BTU/HR 200/FV /FV L SS EJ20 NEUTRALAZATION DRUM EDUCTOR 2" 88 GPM F202 FILTER 2 SIMPLEX 40 GPM SS P00 RAILCAR UNLOADING PUMP VERTICAL 3 X 4-0 ANSI 200 GPM SS 7.5 TEFC P0 Feedstock Storage Pumps 2 VERTICAL 3 X 4-0 ANSI 300 GPM SS 30 TEFC P02 Catalyst Feed Pumps 2 METERING PUMP 0.27 GPH ALLOY 20 /3 P03 Catalyst Charging Pump AIR DIAPHRAGM 2.4 GPM TEFLON P09 PROCESS SUMP PUMP P200A/ REACTOR BOTTOMS B PUMPS P20 REACTOR REFLUX PUMPS 2 2 HORIZONTAL X.5-6 ANSI VERTICAL.5 X 3-3 ANSI VERTICAL.5 X 2-6 ANSI 40 GPM DI / 36 SS 7.5 TEFC 26 GPM HASTELLOY B3 0 TEFC 55 GPM SS 7.5 TEFC P202 REACTOR NEUT. PUMPS 2 HORIZONTAL X.5-6 ANSI 40 GPM SS 7.5 TEFC P300 DEHYDRATOR COL BOTTOMS PUMPS 2 VERTICAL.5 X 2-8 ANSI 55 GPM SS 3 TEFC P30 DEHYDRATOR COL.REFLUX PUMPS 2 VERTICAL.5 X 3-8 ANSI 70 GPM SS 0 TEFC Page 20 of 27

21 P400 SOLVENT STRIPPER BOTTOMS PUMPS 2 VERTICAL.5 X 2-8 ANSI 70 GPM SS 5 TEFC P40 SOLVENT STRIPPER REFLUX PUMPS 2 VERTICAL.5 X 2-6 ANSI 20 GPM SS 7.5 TEFC P404 Solvent Storage Pumps 2 LIGHTS REMOVAL P500A/ COL. BOTTOMS 2 B PUMPS P50 LIGHTS REMOVAL COL.REFLUX PUMPS 2 VERTICAL.5 X 2-6 ANSI HORIZONTAL X.5-8 ANSI VERTICAL.5 X 3-8 ANSI 50 GPM SS 7.5 TEFC 0 GPM TEFC 00 GPM SS 0 TEFC P502 PRODUCT PUMPS 2 VERTICAL.5 X 2-8 ANSI 30 GPM SS 3 TEFC P600 Work Tank Pumps 2 VERTICAL.5 X 3-8 ANSI 75 GPM SS 5 TEFC P700 VENT SCRUBBER PUMPS 2 HORIZONTAL X.5-8 ANSI 0 GPM SS 7.5 TEFC P900 CONDENSATE FLASH TANK PUMP VERTICAL.5 X 3-6 ANSI 00 GPM DI / 36 SS 0 TEFC P975 PLANT DRAINAGE SUMP PUMPS 2 HORIZONTAL 3 X 3-0 ANSI 00 GPM DI / 36 SS 7.5 TEFC PK403 SOLVENT STRIPPER VACUUM SYSTEM 6' X '-6" 80 LB/HR 36 SS 7.5 TEFC R200 REACTOR 0'ID X 22' T/T -- 50/FV 400 DUPLEX T200 REACTOR SCRUBBER 48"ID X 8'6" T/T -- 50/FV 400 DUPLEX T300 DEHYDRATOR COLUMN 48"ID X 0'3" T/T -- 50/FV T400 SOLVENT STRIPPER 60"ID X 50'6" T/T -- 50/FV 400/ T500 LIGHTS REMOVAL COL. 54"ID X 03'3" T/T -- 50/FV 400/ T700 VENT SCRUBBER 8"/24" DIA X 22' T/T UNIT 6 (Bldg 55) Columns TAG # SIZE MATRL TYPE TEMP PRESS Comments T0 6" X 9' Derakane 470 Dumped Polypro packing 200 4psi/fv Includes bottom pot T20A 3'X23' TFE Lined Dumped Polypro packing 270 2psi/-psi Loose liner Page 2 of 27

22 T20B 3'X23' TFE Lined Dumped Polypro packing 270 2psi/-psi Loose liner T2 4"X.5' 36L SS Dumped SS packing PSI/FV T23 4'X40.5' Hetron 980 Dumped PP packing PSI/- PSI T303 32"X24' 304LSS SIEVE TRAYS PSI/FV T702 2'X6' 304LSS Dumped SS packing PSI/FV Includes bottom pot T703 0"X4' 304LSS Dumped SS packing PSI/FV T706 2'X5' 304LSS SIEVE TRAYS PSI/FV T802 Sect.5',2',2.5' X32.5' 304LSS Dumped SS packing PSI/FV T805 2'X4' 304LSS Dumped SS packing PSI/FV Exchangers AREA (sq ft) / # TUBES / PRESS: SHELL / Nom Shell TAG # # PASS SIZE (") TUBE TEMP (F) Dimens MATRL: SHELL / TUBE E0 400 / 45 / 00 PSI-FV/50 PSI-FV 340 5" x 8' /Alloy 20 E / 273 / 00 PSI-FV/50 PSI-FV " x 8' /36L SS E03 4 / 555 / PSI-FV/50 PSI-FV " x 8' /36L SS E05A 74 / 2 48 / 00 PSI-FV/50 PSI-FV 340 2" x 7' / E07 22 / 27 / 00 PSI-FV/50 PSI-FV 340 6' X 4' /36L SS E08 22 / 27 / 00 PSI-FV/50 PSI-FV 340 6' X 4' /36L SS E09 39 / 20 / 50 PSI-FV/00 PSI-FV 340 8" X 0' / E20 8 / 5 / PSI-FV/00 PSI-FV " X 8' Graphite Block E202A 734 / / PSI-FV/00 PSI-FV " x 5' Graphite Block E202B 734 / / PSI-FV/00 PSI-FV " x 5' Graphite Block E204A 22 / 29 / 00 PSI-FV/50 PSI-FV 340 8" x 4' /36L SS E204B 22 / 29 / 00 PSI-FV/50 PSI-FV 340 8" x 4' /36L SS E206A 36 / 3 / 00 PSI-FV/00 PSI-FV 340 0" x 6' /36L SS E206B 36 / 3 / 00 PSI-FV/00 PSI-FV 340 0" x 6' /36L SS E / 2 (U) 30 / 200 PSI-FV/50 PSI-FV 390 2" x 2' / E / 27 / 00 PSI-FV/50 PSI-FV 340 8" x 4' /36L SS E / 7 / PSI-FV/00 PSI-FV " x 7' Graphite Block E22 45 / 7 / PSI-FV/00 PSI-FV " x 7' Graphite Block E / 439 / PSI-FV/00 PSI-FV " x 4' /Karbate E30 4 / 27 / 00 PSI-FV/50 PSI-FV 340 8" x 8 ' /36L SS E / 320 / 200 PSI-FV/50 PSI-FV 370 2" x 6' /304LSS E / 36 / 00 PSI-FV/50 PSI-FV 340 2" x2' /304LSS E / 2 60 / 00 PSI-FV/50 PSI-FV 340 6" x 8' / E / 95 / 00 PSI-FV/50 PSI-FV 340 7" x 8' / E50 75 / 8 24 / 200 PSI-FV/50 PSI-FV 400 8" x 6' / E / 3 / PSI-FV/50 PSI-FV 400 9" x 2' / E / 55 / 00 PSI-FV/50 PSI-FV 300 9" x 20' / 304LSS/304LSS E PSI-FV/50 PSI-FV 340 8" x 6' Disc&Donut Evap E505 / 7 / PSI-FV/50 PSI-FV 400 7" x 6' / E PSI-FV/50 PSI-FV 340 8" x ' 304LSS/304LSS Disc&Donut Evap E / 26 / 00 PSI-FV/50 PSI-FV 350 3" x 0' /304LSS E509 8 / 2 00 PSI-FV/50 PSI-FV 430 /304LSS Page 22 of 27

23 E / 6 (U) 63 / PSI-FV/00 PSI-FV 300 3" x ' 304LSS/304LSS E606 6 / 2 04 / 200 PSI-FV/50 PSI-FV 370 4" x 8' /304LSS E / 2 80 / 200 PSI-FV/50 PSI-FV 370 7" x 7' /304LSS E / 2 80 / 200 PSI-FV/50 PSI-FV 370 7" x 7' /304LSS E70 82 / 2 94 / 00 PSI-FV/50 PSI-FV 340 4" x 0' /304LSS E / 5 / 00 PSI-FV/50 PSI-FV 340 0" x 6' /304LSS 93 / Bayonet 36 / E703 U PSI/FV 390 6" x 4' 36L SS E / 208 / 00 PSI-FV/50 PSI-FV 430 6" x 8' /304LSS E / 4 36 / 00 PSI-FV/50 PSI-FV 340 9" x 6' /304LSS E / 85 / 00 PSI-FV/50 PSI-FV 340 " x 4' /304LSS 392 / E80 77 / PSI-FV/50 PSI-FV 340 8" x 3' 304LSS/304LSS E / Bayonet U 90 / 200 PSI/FV 390 5" x 5' 36L SS E / 392 / PSI-FV/50 PSI-FV 340 8" x 0' / E / 2 / PSI-FV/50 PSI-FV 340 " x 3' / E / Bayonet U 90 / 200 PSI/FV 390 5" x 5' 36L SS E / 2 / PSI-FV/50 PSI-FV 340 5" x 9' / E / 55 / 00 PSI-FV/50 PSI-FV 340 9" x 0' /304LSS E / 8 24 / 00 PSI-FV/50 PSI-FV 370 9" x 7' /304LSS E / 24 / 00 PSI-FV/50 PSI-FV 340 9" x 5' / E / 6 43 / 200 PSI-FV/50 PSI-FV 370 9" x 7' / E / 2 72 / 200 PSI-FV/50 PSI-FV 390 " x 3' / Vessels TAG # NOM CAP MATRL PRESS TEMP DIMEN COMMENTS D66B 5,000 gal 50psi/FV 300 F 2' x4' H D66C 5,000 gal 50psi/FV 300 F 2' x4' H D04 A 4000 GAL Tefzel Lined 4 psi/- psi 250 8'x0' V With agitator D04 B 4000 GAL Tefzel Lined 4 psi/- psi 250 8'x0' V With agitator D GAL 4PSI/FV 250 3'x4' V D gal 00 psi/fv 300 4'X5' H D GAL 304 SS 4 psi/- psi 'X4' V D20 A 4000 GAL TFE Lined 2psi/-psi 270 8'x0' V Page 23 of 27 Loose liner. Hastalloy Sprager Loose liner. Hastalloy Sparger D20 B 4000 GAL TFE Lined 2psi/-psi 270 8'x0' V D202 A 600 GAL TFE Lined 2psi/-psi 270 4'X6.5' H Loose liner D202 B 600 GAL TFE Lined 2psi/-psi 270 4'X6.5' H Loose liner D GAL 00 PSI/FV 'X8.5' V D204 A 000 GAL 36L SS 4 psi/- psi 250 5'x7' V With agitator

24 D204 B 000 GAL 36L SS 4 psi/- psi 250 5'x7' V With agitator D206 A 4000 GAL TFE Lined 2psi/-psi 270 8'x0' V Loose liner. D206 B 4000 GAL TFE Lined 2psi/-psi 270 8'x0' V Loose liner. D208 0,000 GAL Kynar lined Hetron 2psi/-psi 220 'x4' V D GAL Kynar lined Hetron 2psi/-psi 220 4'x5' V D GAL Hetron 922 4psi/- PSI 220 5'x8' V D2 700 GAL Kynar lined 4psi/- PSI 250 5'x8' V Tefzel coated 36SS Agit D GAL 36L SS 4psi/- PSI 250 9'x4' V D GAL HETRON 980 4psi/- PSI 220 4'x5' V D GAL Derakane 4 4psi/- PSI 'x6'V D GAL TFE Lined 2psi/-psi 270 8'x0' V Loose liner. With Agitator D GAL 4psi/-psi 340 8'x0' V With Agitator D GAL 30psi/FV 350 5'x8' V COLUMN BASE D GAL 4psi/FV 250 4'x8' H D323 0,000 gal 0" wc/-6" wc 200 F 25.5'x29.5' V D40 A 000 GAL 304 SS 4psi/-psi 200 5'x7' V With Agitator D40 B 000 GAL 304 SS 4psi/-psi 200 5'x7' V With Agitator D GAL 304 SS 4psi/-psi 340 3'x4' V With Agitator D GAL 304 SS 4psi/-psi 340 3'x4' V With Agitator D GAL 304 SS 4psi/-psi 300 6'x8' V D GAL 304 SS 4psi/-psi 300 7'x8' V D GAL 304 SS 4psi/-psi 300 2'x2' V D GAL 4psi/-psi 250 8'x0' V With Agitator D GAL 4psi/-psi 250 8'x0' V With Agitator D GAL 4psi/-psi 250 8'x0' V With Agitator D606 20,000 GAL +2"wc/-4"wc 'x33' V With Side Mount Agitator D608 20,000 GAL +2"wc/-4"wc 'x33' V With Side Mount Agitator D609 26,000 GAL +2"wc/-4"wc 300 5'x20' V With Side Mount Agitator D70 20,000 GAL +20"wc/-3"wc 250 6'x6' V D GAL 4psi/- PSI 250 5'x8' V D GAL 4psi/FV 300 4'x5' V D GAL 4psi/FV 'x7' H D GAL 4psi/-psi 250 8'x0' V With Agitator D GAL 4psi/FV 'x4' V D GAL 4psi/FV 'x7' H D GAL 4psi/FV 'x2' V With Agitator D GAL 304 SS 50 psi/fv 350 3'x4' H COLUMN BASE D GAL 304 SS 50 psi/fv 350 3'x4' V D GAL 304 SS 4psi/FV 250 5'x6' V D GAL 304 SS 50psi/FV 390 4'x4' H COLUMN BASE D GAL 50psi/FV 300 3'x4' H D GAL 4psi/FV 'x2' V D GAL +20"wc/-6"wc 'x8' V D GAL 4psi/FV 'x3' V R0 500 GAL ALLOY 20 4PSI/FV Jkt 00 psi 350 4'x5.5' V Jacketed with Agitator Page 24 of 27

25 R GAL 36SS R GAL 36SS 4PSI/FV Jkt 00 psi 350 8'x0' V Jacketed with Agitator 4PSI/FV Jkt 00 psi 'x8' V Jacketed with Agitator Pumps TAG # CAPACITY MATRL Page 25 of 27 SEAL PURGE HP RPM TYPE B SCFM@5"wc FRP --- Exhaust vent fan B0 400 SCFM@9"wc FRP Exhaust vent fan B SCFM@ 5PSI NO BLOWER P0 A 75 GPM@00'TDH ALLOY 20 NO Pos Displac Dbl Mech Seal P0 B 75 GPM@00'TDH ALLOY 20 NO Pos Displac Dbl Mech Seal P02 A 75 GPM@30'TDH 36 SS NO Pos Displac Dbl Mech Seal P02 B 75 GPM@30'TDH 36 SS NO Pos Displac Dbl Mech Seal P03 A 50 GPM@290'TDH 36 SS NO Pos Disp Dbl Mech Seal VFD P03 B 50 GPM@290'TDH 36 SS NO Pos Disp Dbl Mech Seal VFD P SS NO P07 5 GPM@00'TDH 36 SS NO Canned P20 A 50 GPM@60'TDH TFE Lined DI Yes 5 800, single mech seal P20 B 50 GPM@60'TDH TFE Lined DI Yes 5 800, single mech seal P202 A 30 GPM@70'TDH 36 SS NO P202 B 30 GPM@70'TDH 36 SS NO P GPM@00'TDH 304 SS NO P204 A 40 GPM@65'TDH 36 SS NO P204 B 40 GPM@65'TDH 36 SS NO P206 A 200 GPM@60'TDH TFE Lined DI NO P206 B 200 GPM@60'TDH TFE Lined DI NO P GPM@30'TDH TFE Lined DI NO P GPM@60'TDH TFE Lined DI NO P20 90 GPM@75'TDH Tefzel Lined NO P2 20 GPM@60'TDH Tefzel Lined NO P22 00 GPM@25'TDH 36 SS NO

26 P SS NO P30 A 50 GPM@65'TDH 36 SS NO P30 B 50 GPM@65'TDH 36 SS NO P302 A 30 GPM@90'TDH 36 SS NO P302 B 30 GPM@90'TDH 36 SS NO P303 A 480 GPM@90'TDH 36 SS NO P303 B 480 GPM@90'TDH 36 SS NO Page 26 of 27 P GPM@80'TDH 36 SS NO P40 A 200 GPM@20'TDH 36 SS NO P40 B 200 GPM@20'TDH 36 SS NO P403 A 3 GPM@90'TDH TEFLON NO --- Metweing Diaphraghm P403 B 3 GPM@90'TDH TEFLON NO --- Metweing Diaphraghm P GPM@60'TDH 36 SS NO P50 60 GPM@300'TDH 36 SS NO P504 0 GPM@228'TDH 36 SS NO Pos Displac Var Freq Drive P506 0 GPM@228'TDH 36 SS NO Pos Displac Var Freq Drive Nash Liquid Seal Ring Vacuum pump. 36 SS. 4 mm Hg Abs Press 0 70 P508 Pos Displac Single Mech P60 00 GPM@250'TDH 36 SS NO Seal Pos Displac Single Mech P GPM@250'TDH 36 SS NO Seal Pos Displac Single Mech P GPM@250'TDH 36 SS NO Seal Pos Displac Single Mech P GPM@300'TDH 36 SS NO Seal Pos Displac Single Mech P GPM@300'TDH 36 SS NO Seal Pos Displac Single Mech P GPM@300'TDH 36 SS NO Seal, single mech P60 2 GPM@25'TDH 36 SS NO seal P70 A 00 GPM@40'TDH 36 SS NO P70 B 00 GPM@40'TDH 36 SS NO P GPM@00'TDH 36 SS NO P703 5 GPM@70'TDH 36 SS NO

27 P SS NO P705 5 GPM@20'TDH 36 SS NO P GPM@90'TDH 36 SS NO P708 5 GPM@70'TDH 36 SS NO P80 20 GPM@80'TDH 36 SS NO P GPM@20'TDH 36 SS NO P GPM@375'TDH 36 SS NO P GPM@00'TDH 36 SS NO P807 5 GPM@85'TDH 36 SS NO P80 5 GPM@75'TDH 36 SS NO P GPM@75'TDH DI NO P902 P903 P GPM@50'TDH 36 SS NO , single mech seal Filters F40A Horizontal leaf centrifugal discharge Funda filter. 440 sq ft. 304SS. 00 psi/fv. 300 F F40B Horizontal leaf centrifugal discharge Funda filter. 440 sq ft. 304SS. 00 psi/fv. 300 F F606A Basket with 5u felt sleeve. 00 gpm, 50 psi, 304 SS. F606B Basket with 5u felt sleeve. 00 gpm, 50 psi, 304 SS. F608A Basket with 5u felt sleeve. 00 gpm, 50 psi, 304 SS. F608B Basket with 5u felt sleeve. 00 gpm, 50 psi, 304 SS. Misc. M800 Solids Conveyor lbs/hr. 3 hp.. M400 Filter hydraulic unit. 25 hp 800 rpm X90 Water Chiller Refrigeration Unit. 262 tons. 600 gpm flow. Outlet temp 38 F. 20 hp 3600 rpm X907 Low Press Stm Gen. 483 sq ft. Shell 304SS, 00 psi/fv, 390F. Tube 304SS, 200 psi/fv, 390F For additional information please contact Tom Colanero at or tcolanero@pennakem.com. Page 27 of 27