Discipline Chemical Testing Issue Date Certificate Number T-1183 Valid Until Last Amended on - Page 1 of 6
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1 Quality Control of AVT McCormick Ingredients Private Last Amended on - Page 1 of 6 I. FOODS & AGRICULTURAL PRODUCTS 1. Spices and condiments a. Whole and Ground Moisture content AOAC 2012, 19 th Edition , McCormick Method M 200, Volatile oil AOAC 2012, 19 th Edition McCormick Method M 210, Issue Date:Mar-99 Ash ASTA Method 3 Revised 1997 McCormick Method M265, Acid insoluble ash ASTA Method 4 revised 1997 McCormick Method M265, Non volatile ether extract AOAC 2012, 19 th edition, McCormick Method M220, Granulation ASTA Method 10, Revised 2004 McCormick Method M110, Issue Date:Mar-03 1 % to 17 % 0.1 % to 25 % 0.8 % to 11 % 0.01 % to 0.6 % 1 % to 50 % 0.1 % to 100 % Bulk Index Bulk Density ASTA Analytical Method 25.1,Revised April 2001 McCormick Method M120, Issue Date:Dec-05 ASTA Analytical Method 25.1Revised April 2001 (100 to 1000) cc/100 g (100 to 1000) g/l
2 Quality Control of AVT McCormick Ingredients Private Last Amended on - Page 2 of 6 Whole and Ground Water Activity AOAC-2012,19 th Edition,978.18, McCormick Method M180, Heavy Filth AOAC 19 th edition 2012, 975.4, McCormick Method M602, Extraneous matter in spices (Excluding black and white pepper) ASTA Analytical Method- 14.1,Revised 1997 McCormick Method M600, 0.10 to % to 5 % 0.1 % to 5.0 % Relative Humidity AOAC2012,19 th Edition, % to 100 % Pesticide Residues Chlorfenapyr Chlorthalonil Dimethoate Mefenoxam Pendimethalin Lindane Carbofuran Profenofos Hexaconazole Kresoxim-Methyl AOAC, 2012, 19 th Edition,
3 Quality Control of AVT McCormick Ingredients Private Last Amended on - Page 3 of 6 Whole and Ground Lufenuron Pesticide Residues Dicofol Propargite Propiconazole Fenitrothion Ethion Myclobutanyl Malathion Triazophos Quinalphos Chlorpyrifos Ethyl Endosulfan-1 Endosulfan-2 Endosulfan sulfate AOAC, 2012, 19 th Edition, Cypermethrin op- DDT Indoxacarb Cyhalothrin Beta BHC Carbosulfan Phosalone
4 Quality Control of AVT McCormick Ingredients Private Last Amended on - Page 4 of 6 Whole and Ground b. Whole and spice blends-chilli Heptachlorepoxide Spiromesifen Pesticide Residues Thiametoxam Difenthiuron Fipronil Dieldrin Triadimefon Hexachlorobenzene AOAC, 2012, 19 th Edition, Aflatoxin- B1,B2, G1&G2 AOAC th edition Method no- DCQ-1129G, Issue Date:Sep-04 Ochratoxin A AOAC th edition Method no- DCQ- 1183K, Issue Date:Sep-04 Methyl parathion AOAC2012, 19 th Edition McCormick Method M 401, ASTA colour ASTA method revised 2004 McCormick Method M310, 0.4 µg/g to 3 µg/g 0.5 ng/g to 500 ng/g 2.5 ng/g to 500 ng/g 10 ASTA to 250 ASTA
5 Quality Control of AVT McCormick Ingredients Private Last Amended on - Page 5 of 6 Whole and spice blends-chilli Seed / Pod Method AMPH 1008/ developed method 1 % to 70 % c. Whole and spice blends-ginger, Cassia Ethoxyquin AOAC th edition, By HPLC Sulfite residue AOAC th edition McCormick Method M290, Issue Date:Mar µg/g to 100 µg/g 5 µg/g to 1000 µg/g d. Whole and spice blends-chilli, Turmeric Color Foreign Iron Dyes ASTM E308 McCormick Method M322, Issue Date:Feb-96 Euroma Analytical Method WILC027, (-) 50 to µg/g to 20 µg/g a) Sudan I ASTA Method No 28 Revised 1 µg/g to 100 µg/g b) Sudan II Aug µg/g to 100 µg/g c) Sudan III 1 µg/g to 100 µg/g d) Sudan IV 1 µg/g to 100 µg/g e. Whole & ground Black Pepper, White pepper & Green pepper Light Berries &Extraneous matter ASTA Analytical Method 14.0 McCormick Method M629, Issue Date: Sep-02 Piperine AOAC th Edition McCormick Method M300, Issue Date: Sep % to 10 % 0.2 % to 8 %
6 Quality Control of AVT McCormick Ingredients Private Last Amended on - Page 6 of 6 f. Whole and Ground spices- Turmeric Curcumin ASTA Method 18, 2004 revision McCormick Method M320, Issue Date:Dec % to 8 % g. Whole and Ground spices- Chilli, Turmeric, Fenugreek Light filth AOAC2012, 19thEdition, ; McCormick Method M0604, M0614, M615,M613, M623, M606, M617, (1 to 200) nos h. Whole and Ground spices- Cassia Coumarin A.W.Archer,J. Chromatog.447(1) (1988) McCormick Method M429, Issue Date:Dec µg/g to 2000 µg/g 2000 µg/g to µg/g -X-X-X-X-X-X-X-X-X-X-X-X-X-X-
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