Analytical Test Report

Transcription

1 Sample Name: Vanilla Haze Laboratory ID: Batch ID: EVH41416 Client: Cascadia Herbals Tamper bags: na Science First. Analytical Test Report SE Division St Date Received: 4/14/2016 Cannabinoids Analytical Batch: Pesticides Analytical Batch: Harvest Date n/a Report Filed: 4/19/2016 Harvest Lot n/a Equipment: HPLC Shimadzu LC2010AHT "Franz" Analyte Detection LOQ Expected Determined Expected Determined THC-Acid 0.056% 0.002% 0.00% 0.02% 100% 103.1% D9-THC 1.012% 0.003% 0.00% 0.00% 100% 97.7% D8-THC 0.000% 0.002% 0.00% 0.00% 100% n/a Total THC 1.068% LOQ = Limit of quantification decarboxylated THC 1.061% CBD-ACID 0.000% 0.007% 0.00% 0.00% 100% 97.7% CBDV 0.000% 0.001% 0.00% 0.00% 100% n/a CBD 0.010% 0.001% 0.00% 0.00% 100% 106.8% Total CBD 0.010% decarboxylated CBD 0.010% CBGA 0.004% 0.002% 0.00% 0.00% 100% 105.0% CBG 0.022% 0.002% 0.00% 0.00% 100% 97.2% CBN 0.010% 0.006% 0.00% 0.00% 100% 85.2% CBC 0.012% 0.001% 0.00% 0.00% 100% 91.2% Total Other 0.048% Acid form of THC/CBD are decarboxylated by combustion, lose 12% original mass. Result = bioactive Cannabinoids per 1.00 gram serving (1mL) LCS control data upon request THC-A 0.56 mg CBD-A 0.00 mg CBG 0.26 mg D9-THC mg CBD 0.10 mg CBN 0.10 mg D8-THC 0.00 mg mg CBC 0.12 mg Total THC mg Total CBD 0.10 mg Total Other 0.48 mg Moisture Content Detection None Cannabinoids Client Sample Method Blank Lab Control Sample Limit CFU=Colony forming units 10,000 CFU/g Moisture Analysis Adjusted Total THC Adjusted Total CBD Water Activity (A w ) A w Pass/Fail Mold / Mildew / Yeast Pass/Fail Pass Equipment: 3M Petrifilm RYM; 48 hour incubation detection limit < 1,000 cfu/g Biologist Chemist Lab Director OAR / (HB3460) Dave Melander Zev Feinstein Chris Nielsen 4/19/2016 page 1

2 11119 SE Division St Analytical Test Report Batch ID EVH41416 Lab ID Vanilla Haze Analyte Limit (ppm) LOQ Detection Pass/Fail Acephate none Pass Acetamiprid none Pass Aldicarb none Pass Azoxystrobin none Pass Bifenazate none Pass Bifenthrin none Pass Boscalid none Pass Carbaryl none Pass Carbofuran none Pass Chlorfenapyr none Pass Chlorpyrifos none Pass Clofentezine none Pass Cyfluthrin none Pass Cypermethrin none Pass DDVP (Dichlorvos) none Pass Diazinon none Pass Dimethoate none Pass Ethoprophos none Pass Etofenprox none Pass Etoxazole none Pass Fenoxycarb none Pass Fipronil none Pass Flonicamid none Pass Fludioxonil none Pass Hexythiazox none Pass Imazalil none Pass Imidacloprid none Pass Kresoxim-methyl none Pass Malathion none Pass Metalaxyl none Pass Methiocarb none Pass Methomyl none Pass Methyl parathion none Pass MGK none Pass Myclobutanil none Pass Naled none Pass Oxamyl none Pass Paclobutrazol none Pass Permethrins none Pass Phosmet none Pass Piperonyl butoxide none Pass Prallethrin none Pass Propiconazole none Pass Propoxur none Pass Pyrethrins none Pass Pyridaben none Pass Spiromesifen none Pass Spiroxamine none Pass Tebuconazole none Pass Thiacloprid none Pass Thiamethoxam none Pass Trifloxystrobin none Pass Equipment: GC/MS Shimadzu GCMS-QP2010 Pesticides Blank Result LCS (% of Expected) LCS = Laborator Control Sample (spiked) LOQ = Limit of quantification page 2 LOD = Limit of detection 4/19/2016 LCS control Data available upon request.

3 11119 SE Division st Analyte Limit (ppm) LOQ Detection Pass/Fail 1,2-dimethoxyethane 100 1,4-Dioxane Butanol Pentanol Propanol Butanol Butanone Ethoxyethanol Methylbutane Propanol (IPA) 5000 Acetone 5000 Acetonitrile 410 Benzene 2 Butane 5000 Cumene 70 Cyclohexane 3880 Dichloromethane 600 2,2-Dimethylbutane 290 2,3-Dimethylbutane 290 1,2-Dimethylbenzene ,3-Dimethylbenzene ,4-Dimethylbenzene 2170 Dimethyl sulfoxide 5000 Ethanol 5000 Ethyl Acetate 5000 Ethylbenzene 2170 Ethyl ether 5000 Ethylene Glycol 620 Ethylene Oxide 50 Heptane 5000 n-hexane 290 Isopropyl acetate 5000 Methanol 3000 Methylpropane Methylpentane Methylpentane 290 N,N-Dimethylacetamide 1090 N,N-Dimethylformamide 880 Pentane 5000 Propane 5000 Pyridine 200 Sulfolane 160 Tetrahydrofuran 720 Toluene 890 Xylenes 2170 Equipment: GC/MS Shimadzu GCMS-QP2010 Analytical Test Report Residual Solvent Blank Result Duplicate Result

4

5 11119 SE Division st Analyte alpha-pinene camphene beta-pinene p-myrcene d-3-carene alpha-terpinene p-cymene d-limonene cis+trans ocimene g-terpinene terpinolene Linalool neo-allo-ocimene Isopregol Geraniol Caryophyllene a-humulene c-nerolidol t-nerolidol guaiol bisbolol Terpenes LOQ Result (%) Method Blank Duplicate Result Equipment: GC/MS Shimadzu GCMS-QP2010 4/19/2016 page 4