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1 SpectrAA Report. 2:04 AM 11/25/2014 Page 1 of 22 Analyst Date Started Worksheet Comment Methods Computer name Serial Number: 9:21 PM 11/24/2014 CH461 - Pb 11_21_14 cp 02 Pb,Pb E3ED16988D8C4E9 AA1110M047 Method: Pb (Zeeman) Element - Matrix: Pb - Instrument Type: Zeeman Conc. Units: ug/l Instrument Mode: orbance Sampling Mode: Autonormal Calibration Mode: Concentration Measurement Mode: Peak Height Replicates Standard: 2 Replicates Sample: 2 Expansion Factor: 1.0 Minimum Reading: Disabled Smoothing: 7 point Conc. Dec. Places: 2 Wavelength: nm Slit Width: 0.5 nm Gain: 74 % Lamp Current: 10.0 ma Lamp Position: 2 Background Correction: BC On STANDARD 1: ug/l STANDARD 2: 3 ug/l STANDARD 3: ug/l Reslope Rate: 10 Reslope Standard No.: 2 Reslope Lower Limit: 75.0 % Reslope Upper Limit: % Recalibration Rate: 20 Calibration Algorithm: New Rational Cal. Low er Limit: 20.0 % Cal. Upper Limit: % Workhead Height: 0.0 mm Total Volume: 15 ul Sample Volume: 10 ul Vol. Reduction Factor: 2 Bulk Conc.: 5 ug/l Bulk Vial No.: 50 Makeup Vial No.: 49 Sample No. of Injections: 1 Sample Last Dry Step: 1
2 SpectrAA Report. 2:04 AM 11/25/2014 Page 2 of 22 Step Temp (C) (s) Flow (L/min) Gas Type Read Signal Storage Normal No No Normal No No Normal No No Normal No No Normal No No Normal No Yes Normal Yes Yes Normal Yes Yes Normal No Yes Sample ID Conc ug/l %RSD SD Mean BG CAL ZERO /24/ :09:36 PM STANDARD /24/ :12:54 PM CAL ZERO 0.17 STANDARD STANDARD /24/ :16:10 PM STANDARD /24/ :19:28 PM
3 SpectrAA Report. 2:04 AM 11/25/2014 Page 3 of STANDARD STANDARD 3 Curve Fit = New Rational Characteristic Conc = 0.49 ug/l r = Calculated Conc = Residuals = Conc = A (-890 x A x A x A + 893) 0.38 New Rational - Cal. Set Pb ug/l Sample ID Conc ug/l %RSD SD Mean BG SRM /24/ :22:44 PM G1 S /24/ :26:00 PM
4 SpectrAA Report. 2:04 AM 11/25/2014 Page 4 of SRM G1 S Sample ID Conc ug/l %RSD SD Mean BG G1 TW 0.28 > /24/ :29:16 PM G2 S /24/ :32:32 PM G1 TW 0.11 G2 S G2 TW /24/ :35:50 PM chk std 20 OVERD b 11/24/ :48:00 PM DF = 1
5 SpectrAA Report. 2:04 AM 11/25/2014 Page 5 of G2 TW chk std Sample ID Conc ug/l %RSD SD Mean BG G3 S /24/ :55:02 PM DF = 2.00 G3 TW > /24/ :58:22 PM 0.13 G3 S2 G3 TW G4 S /24/ :01:42 PM G4 TW /24/ :05:02 PM
6 SpectrAA Report. 2:04 AM 11/25/2014 Page 6 of G4 S G4 TW Sample ID Conc ug/l %RSD SD Mean BG CAL ZERO /24/ :08:18 PM Reslope /24/ :11:36 PM CAL ZERO 0.28 Re slope - - Curve Fit = New Rational Characteristic Conc = 0.58 ug/l r = Calculated Conc = Residuals = Conc = A (-890 x A x A x A + 893)
7 SpectrAA Report. 2:04 AM 11/25/2014 Page 7 of New Rational - Cal. Set Pb ug/l Sample ID Conc ug/l %RSD SD Mean BG G5 S /24/ :14:54 PM G5 TW /24/ :18:14 PM G5 S G5 TW chk std > /24/ :21:34 PM G6 S > /24/ :24:54 PM
8 SpectrAA Report. 2:04 AM 11/25/2014 Page 8 of 22 3 chk std 20 G6 S Sample ID Conc ug/l %RSD SD Mean BG G6 TW /24/ :28:12 PM G7 S /24/ :31:30 PM G6 TW G7 S G7 TW 0.12 > /24/ :34:48 PM SRM /24/ :38:04 PM
9 SpectrAA Report. 2:04 AM 11/25/2014 Page 9 of G7 TW 0.26 SRM Sample ID Conc ug/l %RSD SD Mean BG Blank f or DL /24/ :41:22 PM Blank f or DL /24/ :44:38 PM Blank for DL Blank for DL CAL ZERO /24/ :47:54 PM STANDARD /24/ :51:10 PM
10 SpectrAA Report. 2:04 AM 11/25/2014 Page 10 of CAL ZERO 0.13 STANDARD Sample ID Conc ug/l %RSD SD Mean BG STANDARD /24/ :54:28 PM STANDARD /24/ :57:44 PM 0.27 STANDARD STANDARD Curve Fit = New Rational Characteristic Conc = 0.66 ug/l r = Calculated Conc = Residuals = Conc = A (422 x A x A x A + 667)
11 SpectrAA Report. 2:04 AM 11/25/2014 Page 11 of New Rational - Cal. Set Pb ug/l Sample ID Conc ug/l %RSD SD Mean BG Blank f or DL 0.04 > /25/ :01:02 AM 0.36 > /25/ :04:18 AM Blank for DL Method: Pb (Zeeman) Element - Matrix: Pb - Instrument Type: Zeeman Conc. Units: ug/l Instrument Mode: orbance Sampling Mode: Autonormal Calibration Mode: Concentration Measurement Mode: Peak Height Replicates Standard: 2 Replicates Sample: 2 Expansion Factor: 1.0 Minimum Reading: Disabled Smoothing: 7 point
12 SpectrAA Report. 2:04 AM 11/25/2014 Page 12 of 22 Conc. Dec. Places: 2 Wavelength: nm Slit Width: 0.5 nm Gain: 75 % Lamp Current: 10.0 ma Lamp Position: 2 Background Correction: BC On STANDARD 1: ug/l STANDARD 2: 3 ug/l STANDARD 3: ug/l Reslope Rate: 10 Reslope Standard No.: 2 Reslope Lower Limit: 75.0 % Reslope Upper Limit: % Recalibration Rate: 20 Calibration Algorithm: New Rational Cal. Low er Limit: 20.0 % Cal. Upper Limit: % Workhead Height: 8.5 mm Total Volume: 15 ul Sample Volume: 10 ul Vol. Reduction Factor: 2 Bulk Conc.: 5 ug/l Bulk Vial No.: 50 Makeup Vial No.: 49 Sample No. of Injections: 1 Sample Last Dry Step: 1 Modifier 1 Mode: Co Inject Modifier 1 Vol.: 5 ul Last Dry Step: 0 Injection Rate: 1 Modifier 1 Pos.: 48 No. of Injections: 1
13 SpectrAA Report. 2:04 AM 11/25/2014 Page 13 of 22 Step Temp (C) (s) Flow (L/min) Gas Type Read Signal Storage Normal No No Normal No No Normal No No Normal No No Normal No No Normal No Yes Normal Yes Yes Normal Yes Yes Normal No Yes Sample ID Conc ug/l %RSD SD Mean BG CAL ZERO /25/ :08:06 AM STANDARD /25/ :11:38 AM 0 CAL ZERO STANDARD STANDARD /25/ :15:12 AM STANDARD /25/ :18:44 AM
14 SpectrAA Report. 2:04 AM 11/25/2014 Page 14 of STANDARD STANDARD 3 Curve Fit = New Rational Characteristic Conc = 0.97 ug/l r = Calculated Conc = Residuals = Conc = A (265 x A x A x A + 457) New Rational - Cal. Set Pb ug/l Sample ID Conc ug/l %RSD SD Mean BG chk std /25/ :22:06 AM SRM /25/ :29:30 AM DF = 2.00
15 SpectrAA Report. 2:04 AM 11/25/2014 Page 15 of chk std SRM Sample ID Conc ug/l %RSD SD Mean BG G1 S /25/ :32:52 AM G1 TW 0.13 > /25/ :36:14 AM G1 S2 2 G1 TW G2 S /25/ :39:36 AM G2 TW /25/ :42:58 AM
16 SpectrAA Report. 2:04 AM 11/25/2014 Page 16 of G2 S G2 TW Sample ID Conc ug/l %RSD SD Mean BG chk std /25/ :46:20 AM G3 S /25/ :49:42 AM chk std G3 S G3 TW /25/ :53:06 AM G4 S /25/ :56:32 AM
17 SpectrAA Report. 2:04 AM 11/25/2014 Page 17 of G3 TW 1 G4 S Sample ID Conc ug/l %RSD SD Mean BG CAL ZERO /25/2014 1:00:02 AM Reslope /25/2014 1:03:36 AM CAL ZERO 0.15 Re slope Curve Fit = New Rational Characteristic Conc = 1.05 ug/l r = Calculated Conc = Residuals = Conc = A (265 x A x A x A + 457)
18 SpectrAA Report. 2:04 AM 11/25/2014 Page 18 of 22 New Rational - Cal. Set Pb ug/l Sample ID Conc ug/l %RSD SD Mean BG G4 TW /25/2014 1:06:56 AM G5 S /25/2014 1:10:18 AM 1 G4 TW 7 G5 S G5 TW 1.13 > /25/2014 1:13:42 AM chk std /25/2014 1:17:04 AM
19 SpectrAA Report. 2:04 AM 11/25/2014 Page 19 of G5 TW chk std Sample ID Conc ug/l %RSD SD Mean BG G6 S /25/2014 1:20:26 AM G6 TW /25/2014 1:23:46 AM G6 S3 6 G6 TW G7 S /25/2014 1:27:08 AM G7 TW /25/2014 1:30:30 AM
20 SpectrAA Report. 2:04 AM 11/25/2014 Page 20 of 22 0 G7 S3 6 G7 TW Sample ID Conc ug/l %RSD SD Mean BG SRM /25/2014 1:37:52 AM DF = 2.00 Blank f or DL /25/2014 1:41:14 AM 0.16 SRM 0 Blank for DL CAL ZERO /25/2014 1:44:40 AM STANDARD /25/2014 1:48:14 AM
21 SpectrAA Report. 2:04 AM 11/25/2014 Page 21 of CAL ZERO STANDARD Sample ID Conc ug/l %RSD SD Mean BG STANDARD /25/2014 1:51:46 AM STANDARD /25/2014 1:55:20 AM 0.14 STANDARD STANDARD 3 Curve Fit = New Rational Characteristic Conc = 1.48 ug/l r = Calculated Conc = Residuals = Conc = A (904 x A x A x A + 295)
22 SpectrAA Report. 2:04 AM 11/25/2014 Page 22 of 22 New Rational - Cal. Set Pb ug/l Sample ID Conc ug/l %RSD SD Mean BG Blank f or DL > /25/2014 1:58:40 AM Blank f or DL > /25/2014 2:02:00 AM 9 Blank for DL Blank for DL
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