EuroDist System ScienDist TBP, Potstill, Combi

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1 EuroDist System ScienDist TBP, Potstill, Combi Automatic distillation plants according to ASTM standards D 2892 and D 5236 (conforming to last version) from 1 to 80 litres

2 ScienDist stands for a new generation of distillation plants with sizes from 1 to 80 litres. The modular construction gives maximum flexibility, simplifies maintenance and service. ScienDist s flexible framework can be installed in many different ways, so that it fits in any laboratories. For laboratories with less height, the oversized main condenser can be reclined, without loss of performance. The new type of distillation line is flexible and can be teperature-controlled between 5º and 100 C. The new construction of the column allows easy assembling and disassembling in less than 30 min. without moving reflux divider and main condenser. An infrared heated mantle guarantees good temperature control and fast cooling between the stages. There are gas- and coldtraps placed in an insulated stainless steel vessel. They can be cooled by dry ice or optionally by a cryostat right down to 70 C. ScienDist Potstill, 10 l with control cabinet ScienDist TBP, 20 l Direct connection to valve and volume follower reduces the length of distillation line. Line and valve are heated by heating tapes or infrared heaters. The Volume follower system controls distillation speed and separates the system to atmospheric pressure. Flasks are made of stainless steel. A magnetic stirrer provides a constant distillation process. The control cabinet contains a PC-system, ScienDist-Control hardware and all necessary power supplies.

3 ScienDist-Control Software For distillation control and data processing for manual, semiautomatic or fully automatic operation access to all input and output functions ScienDist Control runs under Windows (latest Version) On request also available for Windows NT easy to handle all data are collected in adjustable time intervals data can be transferred to spreadsheet programs distillation can be interrupted at any time. After continuation, data are combined to one data file. Also several interruptions are possible generates distillation reports according to ASTM D 2892 and D modes: manual, semi- and fully automatic operation calibration software for all probes safety control allows unsupervised operation external watchdog supervises software control software in English, French, Italian, Spanish and German (other languages on request) (not all screenpages are shown in this leaflet) input of cuts (volume or temperature). Changing of cuts during distillation is possible. Up to 99 cuts are possible loads and saves parameter settings

4 ScienDist Volume Follower System stepper motor moves light barrier limit switches for upper and lower postion double mantle glass cylinder, operation range from 5º 100 C pneumatic operated sampler and outlet valve ventilator for preventing condensation on glass cylinder ScienDist Volume Follower can be easily disassembled for service. Pneumatic cylinders guarantee safe operation ScienDist Chart Recorder complete distillation data are stored on harddisk shows all temperatures, pressures and volumes possible to manipulate x and y axes prints chart on colour printer ScienDist Conveyor Belt Typical combined distillation curve standard conveyor belt carries 28 receivers. Number of receivers can be enlarged easily option: weighting system for weighing each cut can be added

5 Nitrogen, 2 Bar RV Torr 10 Torr PIC PIC 1 2 MV4 Technical Data TBP: 15 theoretical plates MV1 Cryostat -25ºC PIOC 3 TIA 4 MV12 Gastraps/ Coldtraps Max. temp flask: 450º C MV3 minimum operation pressure: 1 Torr MV7 TLA+ 5 TLA+ 9 MV5 RV1 max. temp AET: 420º C MV6 MV6a No. of receivers: 28 MV MV8 LIC 10 MV9 Thermostat -20ºC-+100ºC Dimensions: Length: 190 cm Depth: 100 cm Heigth: 230 cm Water, 2 Bar M 8 Electrical data: 3*230V, 16A, N, PE Nitrogen, 2 Bar Buffervessel 8 MV3 MV7 MV4 Coldtrap MV6a MV6 RV1 Thermostat -20 C-+100 C MV1 2 LIC PIC 1 3 Technical Data Potstill: Max. temp flask: 500º C minimum operation pressure: 0.01 Torr max. temp AET: 600º C No. of receivers: 16 Dimensions: Length: 130 cm Depth: 100 cm Heigth: 230 cm MV2 MV5 Elektrical data: 3*230V,16A,N,PE 5 M water, 2 Bar options: dehydration according to D 2892 fire extinguishing gas detectors internal balance for automatic cut weighting automatic testing equipment for Annex D 2892 and D 5236 automatic report generation on customized spreadsheet programms automatic density measuring system cryostat (min.-70º) for gas and coldtraps

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