MACTEC Engineering & Consulting 5628 East Slauson Avenue 12-Nov-09 14:21 ANALYTICAL REPORT FOR SAMPLES
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1 Figure G-1.24
2 Figure G-1.25
3 Figure G-1.26
4 MACTEC Engineering & Consulting Project: MAC East Slauson Avenue Project Number: Metro Westside Ext. / Wilshire Blvd. Reported: Los Angeles, CA Project Manager: Mr. Curt Welty 12-Nov-09 14:21 ANALYTICAL REPORT FOR SAMPLES Sample ID Laboratory ID Matrix Date Sampled Date Received M7-25 E Vapor 04-Nov Nov-09 M13-65 E Vapor 04-Nov Nov-09 Page 1 of 4 Figure G-1.27
5 MACTEC Engineering & Consulting Project: MAC East Slauson Avenue Project Number: Metro Westside Ext. / Wilshire Blvd. Reported: Los Angeles, CA Project Manager: Mr. Curt Welty 12-Nov-09 14:21 Soil Gas and Vapor Analysis H&P Mobile Geochemistry Analyte Result Reporting Limit Units Dilution Factor Batch Prepared Analyzed Method Notes M7-25 (E ) Vapor Sampled: 04-Nov-09 Received: 04-Nov-09 Methane ppmv 125 EK Nov Nov-09 EPA 8015M M13-65 (E ) Vapor Sampled: 04-Nov-09 Received: 04-Nov-09 A Methane ppmv 125 EK Nov Nov-09 EPA 8015M Page 2 of 4 Figure G-1.28
6 MACTEC Engineering & Consulting Project: MAC East Slauson Avenue Project Number: Metro Westside Ext. / Wilshire Blvd. Reported: Los Angeles, CA Project Manager: Mr. Curt Welty 12-Nov-09 14:21 Soil Gas and Vapor Analysis - Quality Control H&P Mobile Geochemistry Analyte Result Reporting Limit Units Spike Level Source Result %REC %REC Limits RPD RPD Limit Notes Batch EK GC Blank (EK90608-BLK1) Methane ND 10 ppmv Prepared & Analyzed: 05-Nov-09 Page 3 of 4 Figure G-1.29
7 MACTEC Engineering & Consulting Project: MAC East Slauson Avenue Project Number: Metro Westside Ext. / Wilshire Blvd. Reported: Los Angeles, CA Project Manager: Mr. Curt Welty 12-Nov-09 14:21 Notes and Definitions A DET ND NR dry RPD The determined value was ppmv but the value was changed to ppmv since it is assumed to be pure methane. Analyte DETECTED Analyte NOT DETECTED at or above the reporting limit Not Reported Sample results reported on a dry weight basis Relative Percent Difference Page 4 of 4 Figure G-1.30
8 Figure G-1.31
9 Figure G-1.32
10 Figure G-1.33
11 Figure G-1.34
12 Figure G-1.35
13 Figure G-1.36
14 Figure G-1.37
15 Figure G-1.38
16 Figure G-1.39
17 Figure G-1.40
18 Figure G-1.41
19 Figure G-1.42
20 Figure G-1.43
21 Preliminary Geotechnical and Environmental Report Appendix G Subsurface Gas Investigation FIGURES G-2.1 THROUGH G-2.28 ANALYTICAL TEST RESULTS (PE PHASE) December 21, 2011 WESTSIDE SUBWAY EXTENSION PROJECT
22 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site 241 Moreno Drive Beverly Hills, CA Method: 1664, Revision A, Oil and Grease (HEM) QC Batch No: Our Lab I.D Client Sample I.D. G-166-D G-165-D Date Sampled 04/22/ /22/2011 Date Prepared 04/26/ /26/2011 Preparation Method Date Analyzed 04/26/ /26/2011 Matrix Water Water Units mg/l mg/l Dilution Factor 1 1 Analytes PQL Results Results Conventionals Oil and Grease 5.00 ND ND Analytes Conventionals LCS QUALITY CONTROL REPORT QC Batch No: LCS DUP LCS RPD LCS/LCSD LCS RPD % REC % REC % REC % Limit % Limit Oil and Grease <20 ASL Job Number Submitted Client /22/2011 MACTEC FIGURE G-2.1
23 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site Method: 418.1, TRPH 241 Moreno Drive Beverly Hills, CA QC Batch No: W Our Lab I.D Client Sample I.D. G-166-D G-165-D Date Sampled 04/22/ /22/2011 Date Prepared 04/27/ /27/2011 Preparation Method Date Analyzed 04/28/ /28/2011 Matrix Water Water Units mg/l mg/l Dilution Factor 1 1 Analytes PQL Results Results Total Recoverable Petroleum Hydrocarbons ND ND Analytes Total Recoverable Petroleum Hydrocarbons MS QUALITY CONTROL REPORT QC Batch No: W MS DUP RPD MS/MSD MS RPD % REC % REC % % Limit % Limit < ASL Job Number Submitted Client /22/2011 MACTEC FIGURE G-2.2
24 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site Method: 600, General Minerals 241 Moreno Drive Beverly Hills, CA ASL Job Number Submitted Client /22/2011 MACTEC QC Batch No: Our Lab I.D Client Sample I.D. G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/2011 Date Prepared 04/22/ /22/ /22/2011 Preparation Method Date Analyzed 04/22/ /22/ /22/2011 Matrix Water Water Water Units mg/l mg/l mg/l Dilution Factor Analytes PQL Results Results Results Conventionals Alkalinity,Total Bicarbonate (as CaCO3) Carbonate (as CaCO3) 10.0 ND ND ND Hydroxide (as CaCO3) 10.0 ND ND ND Chloride Conductivity Fluoride Hardness (Ca,Mg) as CaCO Nitrate as N ph Sulfate Surfactants(MBAS) ND ND ND Total Dissolved Solids(TDS) ICP Metals Calcium Copper ND ND Iron Magnesium Manganese Potassium Sodium Zinc Analytes Conventionals LCS LCS/LCSD % REC % Limit QUALITY CONTROL REPORT QC Batch No: FIGURE G-2.3
25 ANALYTICAL RESULTS Page: Project ID: Project Name: G MTA Westside Extension ASL Job Number Submitted Client /22/2011 MACTEC Method: 600, General Minerals QUALITY CONTROL REPORT Analytes LCS LCS/LCSD % REC % Limit Conventionals Alkalinity,Total Bicarbonate (as CaCO3) Carbonate (as CaCO3) Hydroxide (as CaCO3) Chloride Conductivity Fluoride Hardness (Ca,Mg) as CaCO Nitrate as N ph Sulfate Surfactants(MBAS) Total Dissolved Solids(TDS) ICP Metals Calcium Copper Iron Magnesium Manganese Potassium Sodium Zinc QC Batch No: FIGURE G-2.4
26 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site 241 Moreno Drive Beverly Hills, CA Method: 6010B/7470A, CCR Title 22 Metals (TTLC) ASL Job Number Submitted Client /22/2011 MACTEC QC Batch No: Our Lab I.D Client Sample I.D. G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/2011 Date Prepared 04/26/ /26/ /26/2011 Preparation Method Date Analyzed 04/26/ /26/ /26/2011 Matrix Water Water Water Units mg/l mg/l mg/l Dilution Factor Analytes PQL Results Results Results AA Metals Mercury ND ND ND ICP Metals Antimony ND ND ND Arsenic Barium Beryllium ND ND ND Cadmium ND ND ND Chromium ND ND ND Cobalt ND Copper ND ND Lead ND ND ND Molybdenum ND Nickel Selenium ND Silver ND ND ND Thallium ND ND ND Vanadium ND ND ND Zinc Analytes AA Metals LCS LCS/LCSD % REC % Limit Mercury ICP Metals Antimony Arsenic QUALITY CONTROL REPORT QC Batch No: FIGURE G-2.5
27 ANALYTICAL RESULTS Page: Project ID: Project Name: G MTA Westside Extension ASL Job Number Submitted Client /22/2011 MACTEC Method: 6010B/7470A, CCR Title 22 Metals (TTLC) QUALITY CONTROL REPORT Analytes LCS LCS/LCSD % REC % Limit ICP Metals Barium Beryllium Cadmium Chromium Cobalt Copper Lead Molybdenum Nickel Selenium Silver Thallium Vanadium Zinc QC Batch No: FIGURE G-2.6
28 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site 241 Moreno Drive Beverly Hills, CA ASL Job Number Submitted Client /22/2011 MACTEC Method: 8015B, TPH DROs and OROs (Diesel and Oil Range Organics) QC Batch No: W P Our Lab I.D Client Sample I.D. G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/2011 Date Prepared 04/27/ /27/ /27/2011 Preparation Method Date Analyzed 04/27/ /27/ /27/2011 Matrix Water Water Water Units mg/l mg/l mg/l Dilution Factor Analytes PQL Results Results Results TPH DROs (C10 to C28) ND ND ND TPH OROs (C28+) ND ND ND. Our Lab I.D Surrogates % Rec.Limit % Rec. % Rec. % Rec. Surrogate Percent Recovery Chlorobenzene Analytes MS QUALITY CONTROL REPORT QC Batch No: W P MS DUP RPD MS/MSD MS RPD % REC % REC % % Limit % Limit Diesel < <20 FIGURE G-2.7
29 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site 241 Moreno Drive Beverly Hills, CA Method: 8081A, Organochlorine Pesticides QC Batch No: Our Lab I.D Client Sample I.D. G-166-D G-165-D Date Sampled 04/22/ /22/2011 Date Prepared 04/27/ /27/2011 Preparation Method Date Analyzed 04/27/ /27/2011 Matrix Water Water Units ug/l ug/l Dilution Factor 1 1 Analytes PQL Results Results Aldrin ND ND alpha-hexachlorocyclohexane (Alpha-BHC) ND ND Beta-Hexachlorocyclohexane (Beta-BHC) ND ND Gamma-Chlordane ND ND alpha-chlordane ND ND 4,4'-DDD (DDD) ND ND 4,4'-DDE (DDE) ND ND 4,4'-DDT (DDT) ND ND delta-hexachlorocyclohexane (Delta-BHC) ND ND dieldrin ND ND Endosulfan ND ND Endosulfan ND ND Endosulfan sulfate ND ND Endrin ND ND Endrin aldehyde ND ND Endrin ketone ND ND gamma-hexachlorocyclohexane (Gamma-BHC, Lindane) ND ND Heptachlor ND ND Heptachlor epoxide ND ND Methoxychlor ND ND Toxaphene 10.0 ND ND. Our Lab I.D Surrogates % Rec.Limit % Rec. % Rec. Surrogate Percent Recovery Decachlorobiphenyl ASL Job Number Submitted Client /22/2011 MACTEC FIGURE G-2.8
30 ANALYTICAL RESULTS Page: Project ID: Project Name: G MTA Westside Extension ASL Job Number Submitted Client /22/2011 MACTEC Method: 8081A, Organochlorine Pesticides QUALITY CONTROL REPORT QC Batch No: LCS LCS DUP LCS RPD LCS/LCSD LCS RPD Analytes % REC % REC % REC % Limit % Limit Aldrin <30 4,4'-DDT (DDT) <30 dieldrin <30 Endrin <30 gamma-hexachlorocyclohexane <30 (Gamma-BHC, Lindane) Heptachlor <30 FIGURE G-2.9
31 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site 241 Moreno Drive Beverly Hills, CA QC Batch No: Our Lab I.D Client Sample I.D. G-166-D G-165-D Date Sampled 04/22/ /22/2011 Date Prepared 04/27/ /27/2011 Preparation Method Date Analyzed 04/27/ /27/2011 Matrix Water Water Units ug/l ug/l Dilution Factor 1 1 Analytes PQL Results Results ASL Job Number Submitted Client /22/2011 MACTEC Method: 8082, Polychlorinated Biphenyls(PCBs) by Gas Chromatography Aroclor-1016 (PCB-1016) ND ND Aroclor-1221 (PCB-1221) 1.00 ND ND Aroclor-1232 (PCB-1232) ND ND Aroclor-1242 (PCB-1242) ND ND Aroclor-1248 (PCB-1248) ND ND Aroclor-1254 (PCB-1254) ND ND Aroclor-1260 (PCB-1260) ND ND. Our Lab I.D Surrogates % Rec.Limit % Rec. % Rec. Surrogate Percent Recovery Decachlorobiphenyl Analytes LCS QUALITY CONTROL REPORT QC Batch No: LCS DUP LCS RPD LCS/LCSD LCS RPD % REC % REC % REC % Limit % Limit Aroclor-1260 (PCB-1260) <30 FIGURE G-2.10
32 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site 241 Moreno Drive Beverly Hills, CA Method: 8260B, Volatile Organic Compounds ASL Job Number Submitted Client /22/2011 MACTEC QC Batch No: W B Our Lab I.D Client Sample I.D. G-165-S G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/ /22/2011 Date Prepared 04/27/ /27/ /27/ /27/2011 Preparation Method Date Analyzed 04/27/ /27/ /27/ /27/2011 Matrix Water Water Water Water Units ug/l ug/l ug/l ug/l Dilution Factor Analytes PQL Results Results Results Results Acetone 5.00 ND ND ND ND Benzene 1.00 ND ND ND ND Bromobenzene (Phenyl bromide) 1.00 ND ND ND ND Bromochloromethane (Chlorobromomethane) 1.00 ND ND ND ND Bromodichloromethane (Dichlorobromomethane) ND 1.23 ND Bromoform (Tribromomethane) 5.00 ND ND ND ND Bromomethane (Methyl bromide) 3.00 ND ND ND ND 2-Butanone (MEK, Methyl ethyl ketone) 5.00 ND ND ND ND n-butylbenzene 1.00 ND ND ND ND sec-butylbenzene 1.00 ND ND ND ND tert-butylbenzene 1.00 ND ND ND ND Carbon disulfide 1.00 ND ND ND ND Carbon tetrachloride (Tetrachloromethane) 1.00 ND ND ND ND Chlorobenzene 1.00 ND ND ND ND Chloroethane 3.00 ND ND ND ND 2-Chloroethyl vinyl ether 5.00 ND ND ND ND Chloroform (Trichloromethane) ND Chloromethane (Methyl chloride) 3.00 ND ND ND ND 4-Chlorotoluene (p-chlorotoluene) 1.00 ND ND ND ND 2-Chlorotoluene (o-chlorotoluene) 1.00 ND ND ND ND 1,2-Dibromo-3-chloropropane (DBCP) 5.00 ND ND ND ND Dibromochloromethane ND 2.43 ND 1,2-Dibromoethane (EDB, Ethylene dibromide) 1.00 ND ND ND ND Dibromomethane 1.00 ND ND ND ND 1,2-Dichlorobenzene (o-dichlorobenzene) 1.00 ND ND ND ND 1,3-Dichlorobenzene (m-dichlorobenzene) 1.00 ND ND ND ND 1,4-Dichlorobenzene (p-dichlorobenzene) 1.00 ND ND ND ND Dichlorodifluoromethane 3.00 ND ND ND ND 1,1-Dichloroethane 1.00 ND ND ND ND FIGURE G-2.11
33 ANALYTICAL RESULTS Page: Project ID: Project Name: G MTA Westside Extension ASL Job Number Submitted Client /22/2011 MACTEC Method: 8260B, Volatile Organic Compounds QC Batch No: W B Our Lab I.D Client Sample I.D. G-165-S G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/ /22/2011 Date Prepared 04/27/ /27/ /27/ /27/2011 Preparation Method Date Analyzed 04/27/ /27/ /27/ /27/2011 Matrix Water Water Water Water Units ug/l ug/l ug/l ug/l Dilution Factor Analytes PQL Results Results Results Results 1,2-Dichloroethane 1.00 ND ND ND ND 1,1-Dichloroethene (1,1-Dichloroethylene) 1.00 ND ND ND ND cis-1,2-dichloroethene 1.00 ND ND ND ND trans-1,2-dichloroethene 1.00 ND ND ND ND 1,2-Dichloropropane 1.00 ND ND ND ND 1,3-Dichloropropane 1.00 ND ND ND ND 2,2-Dichloropropane 1.00 ND ND ND ND 1,1-Dichloropropene 1.00 ND ND ND ND cis-1,3-dichloropropene 1.00 ND ND ND ND trans-1,3-dichloropropene 1.00 ND ND ND ND Ethylbenzene 1.00 ND ND ND ND Hexachlorobutadiene (1,3-Hexachlorobutadiene) 3.00 ND ND ND ND 2-Hexanone 5.00 ND ND ND ND Isopropylbenzene 1.00 ND ND ND ND p-isopropyltoluene (4-Isopropyltoluene) 1.00 ND ND ND ND MTBE 2.00 ND ND ND ND 4-Methyl-2-pentanone (MIBK, Methyl isobutyl ketone) 5.00 ND ND ND ND Methylene chloride (Dichloromethane, DCM) 5.00 ND ND ND ND Naphthalene 1.00 ND ND ND ND n-propylbenzene 1.00 ND ND ND ND Styrene 1.00 ND ND ND ND 1,1,1,2-Tetrachloroethane 1.00 ND ND ND ND 1,1,2,2-Tetrachloroethane 1.00 ND ND ND ND Tetrachloroethene (Tetrachloroethylene) 1.00 ND ND ND ND Toluene (Methyl benzene) 1.00 ND ND ND ND 1,2,3-Trichlorobenzene 1.00 ND ND ND ND 1,2,4-Trichlorobenzene 1.00 ND ND ND ND 1,1,1-Trichloroethane 1.00 ND ND ND ND 1,1,2-Trichloroethane 1.00 ND ND ND ND Trichloroethene (TCE) 1.00 ND ND ND ND Trichlorofluoromethane 1.00 ND ND ND ND 1,2,3-Trichloropropane 1.00 ND ND ND ND 1,2,4-Trimethylbenzene 1.00 ND ND ND ND 1,3,5-Trimethylbenzene 1.00 ND ND ND ND Vinyl acetate 5.00 ND ND ND ND FIGURE G-2.12
34 ANALYTICAL RESULTS Page: Project ID: Project Name: G MTA Westside Extension ASL Job Number Submitted Client /22/2011 MACTEC Method: 8260B, Volatile Organic Compounds QC Batch No: W B Our Lab I.D Client Sample I.D. G-165-S G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/ /22/2011 Date Prepared 04/27/ /27/ /27/ /27/2011 Preparation Method Date Analyzed 04/27/ /27/ /27/ /27/2011 Matrix Water Water Water Water Units ug/l ug/l ug/l ug/l Dilution Factor Analytes PQL Results Results Results Results Vinyl chloride (Chloroethene) 3.00 ND ND ND ND o-xylene 1.00 ND ND ND ND m- & p-xylenes 2.00 ND ND ND ND. Our Lab I.D Surrogates % Rec.Limit % Rec. % Rec. % Rec. % Rec. Surrogate Percent Recovery Bromofluorobenzene Dibromofluoromethane Toluene-d QUALITY CONTROL REPORT QC Batch No: W B MS MS DUP RPD MS/MSD MS RPD Analytes % REC % REC % % Limit % Limit Benzene Chlorobenzene ,1-Dichloroethene (1,1-Dichloroethylene) MTBE < Toluene (Methyl benzene) Trichloroethene (TCE) FIGURE G-2.13
35 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site 241 Moreno Drive Beverly Hills, CA Method: 8260B, TPH GROs(Gasoline Range Organics) ASL Job Number Submitted Client /22/2011 MACTEC QC Batch No: W B Our Lab I.D Client Sample I.D. G-165-S G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/ /22/2011 Date Prepared 04/27/ /27/ /27/ /27/2011 Preparation Method Date Analyzed 04/27/ /27/ /27/ /27/2011 Matrix Water Water Water Water Units ug/l ug/l ug/l ug/l Dilution Factor Analytes PQL Results Results Results Results TPH GROs (C6 to C10) 50.0 ND ND ND ND. Our Lab I.D Surrogates % Rec.Limit % Rec. % Rec. % Rec. % Rec. Surrogate Percent Recovery Bromofluorobenzene Dibromofluoromethane Toluene-d Analytes MS QUALITY CONTROL REPORT QC Batch No: W B MS DUP RPD MS/MSD MS RPD % REC % REC % % Limit % Limit Benzene Chlorobenzene ,1-Dichloroethene (1,1-Dichloroethylene) Toluene (Methyl benzene) Trichloroethene (TCE) FIGURE G-2.14
36 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site 241 Moreno Drive Beverly Hills, CA Method: 8270C, Semivolatile Organics ASL Job Number Submitted Client /22/2011 MACTEC QC Batch No: Our Lab I.D Client Sample I.D. G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/2011 Date Prepared 04/27/ /27/ /27/2011 Preparation Method Date Analyzed 04/27/ /27/ /27/2011 Matrix Water Water Water Units ug/l ug/l ug/l Dilution Factor Analytes PQL Results Results Results Acenaphthene 10.0 ND ND ND Acenaphthylene 10.0 ND ND ND Anthracene 10.0 ND ND ND Benz(a)anthracene (Benzo(a)anthracene) 10.0 ND ND ND Benzo(a)pyrene 10.0 ND ND ND Benzo(b)fluoranthene 10.0 ND ND ND Benzo(ghi)perylene 10.0 ND ND ND Benzo(k)fluoranthene 10.0 ND ND ND Benzidine 20.0 ND ND ND Benzoic acid 10.0 ND ND ND Benzyl alcohol 10.0 ND ND ND Bis(2-chloroethoxy)methane 10.0 ND ND ND Bis(2-chloroethyl)ether 10.0 ND ND ND Bis(2-chloroisopropyl) ether 10.0 ND ND ND Bis(2-ethylhexyl) phthalate 10.0 ND ND ND 4-Bromophenyl phenyl ether 10.0 ND ND ND Butyl benzyl phthalate (Benzyl butyl phthalate) 10.0 ND ND ND 4-Chloro-3-methylphenol (p-chloro-m-cresol) 1.00 ND ND ND 4-Chloroaniline 10.0 ND ND ND 2-Chloronaphthalene 10.0 ND ND ND 2-Chlorophenol (o-chlorophenol) 1.00 ND ND ND 4-Chlorophenyl phenyl ether 10.0 ND ND ND Chrysene 10.0 ND ND ND Di-n-butyl phthalate 10.0 ND ND ND Di-n-octyl phthalate (Dioctyl ester) 10.0 ND ND ND Dibenz(a,h)anthracene 10.0 ND ND ND Dibenzofuran 10.0 ND ND ND 1,3-Dichlorobenzene (m-dichlorobenzene) 10.0 ND ND ND 1,2-Dichlorobenzene (o-dichlorobenzene) 10.0 ND ND ND FIGURE G-2.15
37 ANALYTICAL RESULTS Page: Project ID: Project Name: G MTA Westside Extension ASL Job Number Submitted Client /22/2011 MACTEC Method: 8270C, Semivolatile Organics QC Batch No: Our Lab I.D Client Sample I.D. G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/2011 Date Prepared 04/27/ /27/ /27/2011 Preparation Method Date Analyzed 04/27/ /27/ /27/2011 Matrix Water Water Water Units ug/l ug/l ug/l Dilution Factor Analytes PQL Results Results Results 1,4-Dichlorobenzene 10.0 ND ND ND 3,3'-Dichlorobenzidine 20.0 ND ND ND 2,4-Dichlorophenol 1.00 ND ND ND Diethyl phthalate (Diethyl ester) 10.0 ND ND ND 2,4-Dimethylphenol 1.00 ND ND ND Dimethyl phthalate (Dimethyl ester) 10.0 ND ND ND 2,4-Dinitrophenol 1.00 ND ND ND 2,4-Dinitrotoluene 10.0 ND ND ND 2,6-Dinitrotoluene (2,6-DNT) 10.0 ND ND ND 1,2-Diphenylhydrazine 10.0 ND ND ND Fluoranthene 10.0 ND ND ND Fluorene 10.0 ND ND ND Hexachlorobenzene 10.0 ND ND ND Hexachlorobutadiene (1,3-Hexachlorobutadiene) 20.0 ND ND ND Hexachlorocyclopentadiene 10.0 ND ND ND Hexachloroethane 10.0 ND ND ND Indeno(1,2,3-cd)pyrene 10.0 ND ND ND Isophorone 10.0 ND ND ND 2-methyl-4,6-Dinitrophenol 1.00 ND ND ND 2-Methylnaphthalene 10.0 ND ND ND 2-Methylphenol (o-cresol, 2-Cresol) 1.00 ND ND ND 4-Methylphenol (p-cresol, 4-Cresol) 1.00 ND ND ND N-Nitroso-Di-n-propylamine 10.0 ND ND ND N-Nitrosodimethylamine (NDMA) 10.0 ND ND ND N-Nitrosodiphenylamine 10.0 ND ND ND Naphthalene 10.0 ND ND ND 2-Nitroaniline 10.0 ND ND ND 3-Nitroaniline 10.0 ND ND ND 4-Nitroaniline 10.0 ND ND ND Nitrobenzene (NB) 10.0 ND ND ND 2-Nitrophenol (o-nitrophenol) 1.00 ND ND ND 4-Nitrophenol 1.00 ND ND ND Pentachlorophenol 1.00 ND ND ND Phenanthrene 10.0 ND ND ND Phenol 1.00 ND ND ND FIGURE G-2.16
38 ANALYTICAL RESULTS Page: Project ID: Project Name: G MTA Westside Extension ASL Job Number Submitted Client /22/2011 MACTEC Method: 8270C, Semivolatile Organics QC Batch No: Our Lab I.D Client Sample I.D. G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/2011 Date Prepared 04/27/ /27/ /27/2011 Preparation Method Date Analyzed 04/27/ /27/ /27/2011 Matrix Water Water Water Units ug/l ug/l ug/l Dilution Factor Analytes PQL Results Results Results Pyrene 10.0 ND ND ND 1,2,4-Trichlorobenzene 10.0 ND ND ND 2,4,5-Trichlorophenol 1.00 ND ND ND 2,4,6-Trichlorophenol 1.00 ND ND ND. Our Lab I.D Surrogates % Rec.Limit % Rec. % Rec. % Rec. Surrogate Percent Recovery 2-Fluorophenol Phenol-d ,4,6-Tribromophenol Nitrobenzene-d Fluorobiphenyl Terphenyl-d QUALITY CONTROL REPORT QC Batch No: LCS LCS DUP LCS RPD LCS/LCSD LCS RPD Analytes % REC % REC % REC % Limit % Limit Acenaphthene <30 4-Chloro-3-methylphenol <30 (p-chloro-m-cresol) 2-Chlorophenol (o-chlorophenol) <30 1,4-Dichlorobenzene <30 2,4-Dinitrotoluene < <30 N-Nitroso-Di-n-propylamine <30 4-Nitrophenol <30 Pentachlorophenol <30 Phenol <30 Pyrene <30 1,2,4-Trichlorobenzene <30 FIGURE G-2.17
39 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site 241 Moreno Drive Beverly Hills, CA Method: RSKSOP-175, Dissolved Gases ASL Job Number Submitted Client /22/2011 MACTEC QC Batch No: Our Lab I.D Client Sample I.D. G-165-S G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/ /22/2011 Date Prepared 04/29/ /29/ /29/ /29/2011 Preparation Method Date Analyzed 04/29/ /29/ /29/ /29/2011 Matrix Water Water Water Water Units ug/l ug/l ug/l ug/l Dilution Factor Analytes PQL Results Results Results Results Methane 1.00 ND Analytes LCS QUALITY CONTROL REPORT QC Batch No: LCS DUP LCS RPD LCS/LCSD LCS RPD % REC % REC % REC % Limit % Limit Methane <30 FIGURE G-2.18
40 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site 241 Moreno Drive Beverly Hills, CA Method: SM2540-D, Total Suspended Solids (TSS) ASL Job Number Submitted Client /22/2011 MACTEC QC Batch No: Our Lab I.D Client Sample I.D. G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/2011 Date Prepared 04/27/ /27/ /27/2011 Preparation Method Date Analyzed 04/27/ /27/ /27/2011 Matrix Water Water Water Units mg/l mg/l mg/l Dilution Factor Analytes PQL Results Results Results Conventionals Solids, Total Suspended (TSS) Analytes Conventionals LCS QUALITY CONTROL REPORT QC Batch No: LCS DUP LCS RPD LCS/LCSD LCS RPD % REC % REC % REC % Limit % Limit Solids, Total Suspended (TSS) FIGURE G-2.19
41 Ordered By MACTEC Engineering & Consulting Inc 5628 East Slauson Ave. Los Angeles, CA Telephone: (323) Marty Hudson Attn: Page: Project ID: Project Name: G MTA Westside Extension ANALYTICAL RESULTS Site 241 Moreno Drive Beverly Hills, CA Method: SM4500-S-2-D, Sulfide (Methylene Blue Method) ASL Job Number Submitted Client /22/2011 MACTEC QC Batch No: Our Lab I.D Client Sample I.D. G-166-D G-166-S G-165-D Date Sampled 04/22/ /22/ /22/2011 Date Prepared 04/22/ /22/ /22/2011 Preparation Method Date Analyzed 04/22/ /22/ /22/2011 Matrix Water Water Water Units mg/l mg/l mg/l Dilution Factor Analytes PQL Results Results Results Conventionals Sulfide, total ND ND ND Analytes Conventionals SM QUALITY CONTROL REPORT SM DUP RPD Result Result % QC Batch No: SM RPD % Limit Sulfide, total ND ND <1 20 FIGURE G-2.20
42 2655 Park Center Drive, Suite A, Simi Valley, CA LABORATORY REPORT May 6, 2011 Molky Brar American Scientific Laboratories 2520 North San Fernando Road Los Angeles, CA RE: Dear Molky: Enclosed are the results of the samples submitted to our laboratory on April 25, For your reference, these analyses have been assigned our service request number P All analyses were performed according to our laboratory s NELAP and DoD-ELAP-approved quality assurance program. The test results meet requirements of the current NELAP and DoD-ELAP standards, where applicable, and except as noted in the laboratory case narrative provided. For a specific list of NELAP and DoD-ELAPaccredited analytes, refer to the certifications section at Results are intended to be considered in their entirety and apply only to the samples analyzed and reported herein. Columbia Analytical Services, Inc. is certified by the California Department of Health Services, NELAP Laboratory Certificate No CA; Arizona Department of Health Services, Certificate No. AZ0694; Florida Department of Health, NELAP Certification E871020; New Jersey Department of Environmental Protection, NELAP Laboratory Certification ID #CA009; New York State Department of Health, NELAP NY Lab ID No: 11221; Oregon Environmental Laboratory Accreditation Program, NELAP ID: CA20007; The American Industrial Hygiene Association, Laboratory #101661; United States Department of Defense Environmental Laboratory Accreditation Program (DoD-ELAP), Certificate No. L10-3; Pennsylvania Registration No ; TX Commission of Environmental Quality, NELAP ID T ; Minnesota Department of Health, NELAP Certificate No ; Washington State Department of Ecology, ELAP Lab ID: C946. Each of the certifications listed above have an explicit Scope of Accreditation that applies to specific matrices/methods/analytes; therefore, please contact me for information corresponding to a particular certification. If you have any questions, please call me at (805) Respectfully submitted, Columbia Analytical Services, Inc. Sue Anderson Project Manager FIGURE G-2.21
43 2655 Park Center Drive, Suite A, Simi Valley, CA Client: American Scientific Laboratories CAS Project No: P Project: CASE NARRATIVE The samples were received intact under chain of custody on April 25, 2011 and were stored in accordance with the analytical method requirements. Please refer to the sample acceptance check form for additional information. The results reported herein are applicable only to the condition of the samples at the time of sample receipt. Hydrogen Sulfide Analysis The samples were analyzed for hydrogen sulfide using a gas chromatograph equipped with a sulfur chemiluminescence detector (SCD). The results of analyses are given in the attached laboratory report. All results are intended to be considered in their entirety, and Columbia Analytical Services, Inc. (CAS) is not responsible for utilization of less than the complete report. FIGURE G-2.22
44 2655 Park Center Drive, Suite A, Simi Valley, CA DETAIL SUMMARY REPORT Client: American Scientific Laboratories Service Request: P Project ID: Date Received: 4/25/2011 Time Received: 11:10 Client Sample ID Lab Code Matrix Date Collected Time Collected P Water 4/22/ :45 X P Water 4/22/ :35 X P Water 4/22/ :20 X P Water 4/22/ :35 X Sulfur Liq - Sulfur P _Detail Summary_ _RB.xls - DETAIL SUMMARY FIGURE G-2.23
45 2655 Park Center Drive, Suite A, Simi Valley, CA FIGURE G-2.24
46 2655 Park Center Drive, Suite A, Simi Valley, CA Sample Acceptance Check Form Client: American Scientific Laboratories Work order: P Project: Sample(s) received on: 4/25/11 Date opened: 4/25/11 by: SSTAPLES Note: This form is used for all samples received by CAS. The use of this form for custody seals is strictly meant to indicate presence/absence and not as an indication of compliance or nonconformity. Thermal preservation and ph will only be evaluated either at the request of the client and/or as required by the method/sop. Yes No N/A 1 Were sample containers properly marked with client sample ID? 2 Container(s) supplied by CAS? 3 Did sample containers arrive in good condition? 4 Were chain-of-custody papers used and filled out? 5 Did sample container labels and/or tags agree with custody papers? 6 Was sample volume received adequate for analysis? 7 Are samples within specified holding times? 8 Was proper temperature (thermal preservation) of cooler at receipt adhered to? Cooler Temperature 6 C Blank Temperature C 9 Was a trip blank received? 10 Were custody seals on outside of cooler/box? Location of seal(s)? Sealing Lid? Were signature and date included? Were seals intact? Were custody seals on outside of sample container? Location of seal(s)? Sealing Lid? Were signature and date included? Were seals intact? 11 Do containers have appropriate preservation, according to method/sop or Client specified information? Is there a client indication that the submitted samples are ph preserved? Were VOA vials checked for presence/absence of air bubbles? Does the client/method/sop require that the analyst check the sample ph and if necessary alter it? 12 Tubes: Are the tubes capped and intact? Do they contain moisture? 13 Badges: Are the badges properly capped and intact? Are dual bed badges separated and individually capped and intact? Lab Sample ID Container Required Received Adjusted VOA Headspace Receipt / Preservation Description ph * ph ph (Presence/Absence) Comments P P P P P P P P mL VOA NP 6 P 40mL VOA NP P 40mL VOA NP P 40mL VOA NP 6 P 40mL VOA NP P 40mL VOA NP P 40mL VOA NP 6 P 40mL VOA NP P Explain any discrepancies: (include lab sample ID numbers): Vials contained precipitate RSK - MEEPP, HCL (ph<2); RSK - CO2, (ph 5-8); Sulfur (ph>4) P _American Scientific Laboratories_Sulfur Analysis _ xls - Page 1 of 2 5/6/11 10:57 AM FIGURE G-2.25
47 2655 Park Center Drive, Suite A, Simi Valley, CA Sample Acceptance Check Form Client: American Scientific Laboratories Work order: P Project: Sample(s) received on: 4/25/11 Date opened: 4/25/11 by: SSTAPLES Lab Sample ID Container Required Received Adjusted VOA Headspace Receipt / Preservation Description ph * ph ph (Presence/Absence) Comments P P P P mL VOA NP P 40mL VOA NP 6 A 40mL VOA NP A 40mL VOA NP A Explain any discrepancies: (include lab sample ID numbers): RSK - MEEPP, HCL (ph<2); RSK - CO2, (ph 5-8); Sulfur (ph>4) P _American Scientific Laboratories_Sulfur Analysis _ xls - Page 2 of 2 5/6/11 10:57 AM FIGURE G-2.26
48 2655 Park Center Drive, Suite A, Simi Valley, CA RESULTS OF ANALYSIS Page 1 of 1 Client: American Scientific Laboratories Client Project ID: CAS Project ID: P Hydrogen Sulfide Test Code: GC/SCD Reduced Sulfur Analysis Instrument ID: Agilent 6890A/GC13/SCD Date(s) Collected: 4/22/11 Analyst: Wade Henton/Lauryn Keeler Date Received: 4/25/11 Matrix: Water Date Analyzed: 4/26/11 Test Notes: Liquid Amount: Purge Injection Client Sample ID CAS Sample ID Amount Volume Volume Result MRL Data ml(s) Liter(s) ml(s) µg/l µg/l Qualifier P ND P ND P ND P ND 0.84 Method Blank P MB ND 0.84 ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method. P _GCSCD_ _SS.xls - GS-SCD LIQ-SOIL.XLT - Page No.: FIGURE G-2.27
49 2655 Park Center Drive, Suite A, Simi Valley, CA LABORATORY CONTROL SAMPLE / DUPLICATE LABORATORY CONTROL SAMPLE SUMMARY Page 1 of 1 Client: American Scientific Laboratories Client Sample ID: Duplicate Lab Control Sample CAS Project ID: P Client Project ID: CAS Sample ID: P DLCS Test Code: GC/SCD Reduced Sulfur Analysis Date Collected: NA Instrument ID: Agilent 6890A/GC13/SCD Date Received: NA Analyst: Wade Henton/Lauryn Keeler Date Analyzed: 4/26/11 Matrix: Water Liquid Amount: 10.0 ml(s) Test Notes: Purge Volume: 0.30 Liter(s) Injection Volume: 0.20 ml(s) Spike Amount Result CAS CAS # Compound LCS / DLCS LCS DLCS % Recovery Acceptance RPD RPD Data ug/l ug/l ug/l LCS DLCS Limits Limit Qualifier Hydrogen Sulfide P _GCSCD_ _SS.xls - DLCS LIQ-SOL.XLT - Page No.: FIGURE G-2.28
50 Preliminary Geotechnical and Environmental Report Appendix G Subsurface Gas Investigation FIGURES G THROUGH G VAPOR SAMPLE DATA (PE PHASE) December 21, 2011 WESTSIDE SUBWAY EXTENSION PROJECT
51 G 3.1 MTA Westside Extension PE Phase Vapor Sample Data Location: M 6
52 Figure G-3.1.1
53 Advanced Technology Laboratories Date: 20-May-11 CLIENT: MACTEC Project: MTA WESTSIDE EXTENSION, Lab Order: CASE NARRATIVE The sample for EPA 1516 analysis was subcontracted to Air Technology Lab. Page 1 of Walnut Avenue, Signal Hill, CA Tel: Fax: of 4 Figure G-3.1.2
54 Advanced Technology Laboratories CLIENT: MACTEC Lab Order: Project: MTA WESTSIDE EXTENSION, Lab ID: A Client Sample ID: M-6 / Wilshire Collection Date: 5/13/2011 1:35:00 PM Matrix: AIR ANALYTICAL RESULTS Print Date: 20-May-11 Analyses Result PQL Qual Units DF Date Analyzed GASES BY GAS CHROMATOGRAPHY RunID: GC18_110516A QC Batch: Z11A018 Methane ND ASTM D1946 PrepDate: 10 ppmv 1 Analyst: BB 5/16/ :12 PM Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference Results are wet unless otherwise specified DO Surrogate Diluted Out 3275 Walnut Avenue, Signal Hill, CA Tel: Fax: of 4 Figure G-3.1.3
55 Advanced Technology Laboratories CLIENT: MACTEC Work Order: Project: MTA WESTSIDE EXTENSION, Date: 20-May-11 ANALYTICAL QC SUMMARY REPORT TestCode: D1946 Sample ID: MB-Z11A018 Client ID: ZZZZZZ SampType: MBLK TestCode: D1946 Units: ppmv Prep Date: Batch ID: Z11A018 TestNo: ASTM D1946 Analysis Date: 5/16/2011 RunNo: SeqNo: Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Methane ND 10 Sample ID: LCS-Z11A018 Client ID: ZZZZZZ SampType: LCS TestCode: D1946 Units: ppmv Prep Date: Batch ID: Z11A018 TestNo: ASTM D1946 Analysis Date: 5/16/2011 RunNo: SeqNo: Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Methane Sample ID: LCSD-Z11A018 Client ID: ZZZZZZ SampType: LCSD TestCode: D1946 Units: ppmv Prep Date: Batch ID: Z11A018 TestNo: ASTM D1946 Analysis Date: 5/16/2011 RunNo: SeqNo: Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Methane Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values 3275 Walnut Avenue, Signal Hill, CA Tel: Fax: of 4 Figure G-3.1.4
56 Figure G-3.1.5
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