REPORT OF LABORATORY ANALYSIS FOR PFAAs
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- Domenic Walter Bates
- 5 years ago
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1 Pace Analytical Services, Inc Elm Street Minneapolis, MN Phone: Fax: Report Prepared for: ToddRea PASI Florida 8 East Tower Circle Ormond Beach FL Report Information: Pace Project #: Sample Receipt Date: 07/18/2018 Client Project #: Universal Engineering Client Sub PO #: N/A State Cert #: N/A REPORT OF LABORATORY ANALYSIS FOR PFAAs Invoicing & Reporting Options: The report provided has been invoiced as a Level 2 PFAA Report. If an upgrade of this report package is requested, an additional charge may be applied. Please review the attachedinvoice for accuracy and forward any questions tokirsten Hogberg, your Pace Project Manager. This report has been reviewed by: August 03, 2018 Kirsten Hogberg, Project Manager (612) (612) (fax) kirsten.hogberg@pacelabs.com Report Prepared Date: August 3, 2018 Report of Laboratory Analysis Thisreportshouldnotbereproduced,exceptinfull, withoutthewrittenconsentofpaceanalyticalservices,inc. Theresultsrelateonlytothesamplesincludedinthisreport. Page 1 of 32
2 DISCUSSION This report presents the results from the analyses performed on fifteen of forty-one samples submitted by a representative of Pace Analytical-Ormund Beach. The samples were analyzed for the presence or absence of twenty-one perfluorinated compounds using a modified version of USEPA Method 537. Reporting limits were set to the quantitation limits. The remaining samples were placed on hold pending review of the first fifteen. The recoveries of the isotopically-labeled surrogate standards in the sample extracts ranged from %. With two exceptions, flagged "failed", the labeled surrogate standard recoveries obtained for this project were within the target ranges specified in the method. The labeled EtFOSAA in samples SE-1 and CV-1 extract were below the 70% limit. This could indicate a slight low bias in the results for these two samples. All internal standards in sample SH-1 failed low, which could result in a high bias for the target analytes in this sample. Sample SH-1 will be reanalyzed to verify the results. A laboratory method blank was prepared and analyzed with the sample batch as part of our routine quality control procedures. The results show the blank was free of the target perfluorinated compounds at the reporting limits. This indicates that the sample processing procedures did not significantly contribute to the analyte content determined for the sample material. Laboratory spike samples were also prepared with the sample batch using clean reference matrix that had been fortified with native standards. The results show that the spiked native compounds in the laboratory spikes were recovered at %, with relative percent differences of 0-9%. These results were within the method limits. It should be noted that Pace Analytical has not yet completed the certification process for all analytes in this method. Therefore, the results have been marked "N2" as qualified. Results for the low level spikes that were below the calibration range were flagged "J". Page 2 of 32
3 Pace AnalyticalServices, LLC 1700 Elm Street - Suite 200 Minneapolis, MN Tel: Fax: Minnesota Laboratory Certifications Authority Certificate # Authority Certificate # A2LA Minnesota - Pet 1240 Alabama Mississippi MN00064 Alaska - DW MN00064 Montana CERT0092 Alaska - UST Nebraska NE-OS Arizona AZ0014 Nevada MN00064 Arkansas - DW MN00064 New Hampshire 2081 Arkansas - WW New Jersey (NE MN002 CNMI Saipan MP0003 New York California 2929 North Carolina Colorado MN00064 North Carolina Connecticut PH-0256 North Carolina EPA Region 8+ via MN North Dakota R-036 Florida (NELAP E87605 Ohio - DW Georgia 959 Ohio - VAP CL101 Guam r Oklahoma 9507 Hawaii MN00064 Oregon - Primar MN Idaho MN00064 Oregon - Secon MN Illinois Pennsylvania Indiana C-MN-01 Puerto Rico MN00064 Iowa 368 South Carolina Kansas E South Dakota NA Kentucky - DW Tennessee TN02818 Kentucky - WW Texas T Louisiana - DE Utah (NELAP) MN00064 Louisiana - DW MN00064 Virginia Maine MN00064 Washington C486 Maryland 322 West Virginia Massachusetts M-MN064 West Virginia C Michigan 9909 Wisconsin Minnesota Wyoming - UST Minnesota - De via MN REPORTOFLABORATORYANALYSIS This report shall not be reproduced, except in full, withoutthewrittenconsentofpace AnalyticalServices, Inc. Page 3 of 32
4 Appendix A Sample Management Pace Analytical Services, Inc. Page 4 of 32
5 Page 5 of 32
6 Page 6 of 32
7 Page 7 of 32
8 Page 8 of 32
9 Page 9 of 32
10 7/20/2018 Page 10 of 32
11 Pace AnalyticalServices, LLC 1700 Elm Street - Suite 200 Minneapolis, MN Tel: Fax: Reporting Flags A = B = C = D = E = I = J = L = Nn = P = R = S = U = V = X = Y = * = Reporting Limit based on signal to noise Less than 10x higher than method blank level Result obtained from confirmation analysis Resultobtainedfromanalysis ofdilutedsample Exceeds calibration range Interferencepresent Estimated value Suppressive interference, analyte may be biased low Value obtained from additional analysis PCDEInterference Recovery outside target range Peak saturated Analyte not detected Result verified by confirmation analysis %DExceedslimits Calculated using average of daily RFs SeeDiscussion REPORTOFLABORATORYANALYSIS This report shall not be reproduced, except in full, withoutthewrittenconsentofpace AnalyticalServices, Inc. Page 11 of 32
12 Appendix B Sample Analysis Summary Pace Analytical Services, Inc. Page 12 of 32
13 PFAA Sample Analysis Summary Client's Sample ID Collected 07/10/2018 Received 07/18/2018 GE LCMS02_180730A_031 Drinking_Water Total Amount Extracted 251 ml A02 10LCMS02_180730A_029 10LCMS02_180730A_042 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA /30/201815: N2 PFPeA ND /30/201815: N2 PFBS ND /30/201815: N2 PFHxA ND /30/201815: N2 PFPrOPrA ND /30/201815: N2 PFHpA ND /30/201815: N2 NaDONA ND /30/201815: N2 PFHxS ND /30/201815: N2 PFOA ND /30/201815: N2 PFNA ND /30/201815: N2 PFOS ND /30/201815: N2 PFDA ND /30/201815: N2 PFUdA ND /30/201815: N2 N-MeFOSAA ND /30/201815: N2 N-EtFOSAA ND /30/201815: N2 PFDS ND /30/201815: N2 PFDoA ND /30/201815: N2 PFTrDA ND /30/201815: N2 PFTeDA ND /30/201815: N2 PFHxDA ND /30/201815: N2 PFODA ND /30/201815: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 13 of 32
14 PFAA Sample Analysis Summary Client's Sample ID Collected 07/10/2018 Received 07/18/2018 IE LCMS02_180730A_032 Drinking_Water Total Amount Extracted 249 ml A02 10LCMS02_180730A_029 10LCMS02_180730A_042 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA /30/201815: N2 PFPeA ND /30/201815: N2 PFBS ND /30/201815: N2 PFHxA ND /30/201815: N2 PFPrOPrA ND /30/201815: N2 PFHpA ND /30/201815: N2 NaDONA ND /30/201815: N2 PFHxS ND /30/201815: N2 PFOA ND /30/201815: N2 PFNA ND /30/201815: N2 PFOS ND /30/201815: N2 PFDA ND /30/201815: N2 PFUdA ND /30/201815: N2 N-MeFOSAA ND /30/201815: N2 N-EtFOSAA ND /30/201815: N2 PFDS ND /30/201815: N2 PFDoA ND /30/201815: N2 PFTrDA ND /30/201815: N2 PFTeDA ND /30/201815: N2 PFHxDA ND /30/201815: N2 PFODA ND /30/201815: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 14 of 32
15 PFAA Sample Analysis Summary Client's Sample ID Collected 07/10/2018 Received 07/18/2018 HM LCMS02_180730A_033 Drinking_Water Total Amount Extracted 247 ml A02 10LCMS02_180730A_029 10LCMS02_180730A_042 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA /30/201815: N2 PFPeA ND /30/201815: N2 PFBS ND /30/201815: N2 PFHxA ND /30/201815: N2 PFPrOPrA ND /30/201815: N2 PFHpA ND /30/201815: N2 NaDONA ND /30/201815: N2 PFHxS ND /30/201815: N2 PFOA ND /30/201815: N2 PFNA ND /30/201815: N2 PFOS ND /30/201815: N2 PFDA ND /30/201815: N2 PFUdA ND /30/201815: N2 N-MeFOSAA ND /30/201815: N2 N-EtFOSAA ND /30/201815: N2 PFDS ND /30/201815: N2 PFDoA ND /30/201815: N2 PFTrDA ND /30/201815: N2 PFTeDA ND /30/201815: N2 PFHxDA ND /30/201815: N2 PFODA ND /30/201815: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 15 of 32
16 PFAA Sample Analysis Summary Client's Sample ID Collected 07/10/2018 Received 07/18/2018 OB LCMS02_180730A_034 Drinking_Water Total Amount Extracted 249 ml A02 10LCMS02_180730A_029 10LCMS02_180730A_042 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA /30/201816: N2 PFPeA ND /30/201816: N2 PFBS ND /30/201816: N2 PFHxA ND /30/201816: N2 PFPrOPrA ND /30/201816: N2 PFHpA ND /30/201816: N2 NaDONA ND /30/201816: N2 PFHxS ND /30/201816: N2 PFOA ND /30/201816: N2 PFNA ND /30/201816: N2 PFOS ND /30/201816: N2 PFDA ND /30/201816: N2 PFUdA ND /30/201816: N2 N-MeFOSAA ND /30/201816: N2 N-EtFOSAA ND /30/201816: N2 PFDS ND /30/201816: N2 PFDoA ND /30/201816: N2 PFTrDA ND /30/201816: N2 PFTeDA ND /30/201816: N2 PFHxDA ND /30/201816: N2 PFODA ND /30/201816: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 16 of 32
17 PFAA Sample Analysis Summary Client's Sample ID Collected 07/10/2018 Received 07/18/2018 SE LCMS02_180730A_035 Drinking_Water Total Amount Extracted 249 ml A02 10LCMS02_180730A_029 10LCMS02_180730A_042 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA /30/201816: N2 PFPeA ND /30/201816: N2 PFBS ND /30/201816: N2 PFHxA ND /30/201816: N2 PFPrOPrA ND /30/201816: N2 PFHpA ND /30/201816: N2 NaDONA ND /30/201816: N2 PFHxS ND /30/201816: N2 PFOA ND /30/201816: N2 PFNA ND /30/201816: N2 PFOS ND /30/201816: N2 PFDA ND /30/201816: N2 PFUdA ND /30/201816: N2 N-MeFOSAA ND /30/201816: N2 N-EtFOSAA ND /30/201816: N2 PFDS ND /30/201816: N2 PFDoA ND /30/201816: N2 PFTrDA ND /30/201816: N2 PFTeDA ND /30/201816: N2 PFHxDA ND /30/201816: N2 PFODA ND /30/201816: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Fail 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 17 of 32
18 PFAA Sample Analysis Summary Client's Sample ID Collected 07/10/2018 Received 07/18/2018 CV LCMS02_180730A_036 Drinking_Water Total Amount Extracted 247 ml A02 10LCMS02_180730A_029 10LCMS02_180730A_042 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA ND /30/201816: N2 PFPeA ND /30/201816: N2 PFBS ND /30/201816: N2 PFHxA ND /30/201816: N2 PFPrOPrA ND /30/201816: N2 PFHpA ND /30/201816: N2 NaDONA ND /30/201816: N2 PFHxS ND /30/201816: N2 PFOA ND /30/201816: N2 PFNA ND /30/201816: N2 PFOS ND /30/201816: N2 PFDA ND /30/201816: N2 PFUdA ND /30/201816: N2 N-MeFOSAA ND /30/201816: N2 N-EtFOSAA ND /30/201816: N2 PFDS ND /30/201816: N2 PFDoA ND /30/201816: N2 PFTrDA ND /30/201816: N2 PFTeDA ND /30/201816: N2 PFHxDA ND /30/201816: N2 PFODA ND /30/201816: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Fail 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 18 of 32
19 PFAA Sample Analysis Summary Client's Sample ID Collected 07/10/2018 Received 07/18/2018 RE LCMS02_180802C_016 Drinking_Water Total Amount Extracted 251 ml B02 10LCMS02_180802C_013 10LCMS02_180802C_029 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA ND /03/201803: N2 PFPeA ND /03/201803: N2 PFBS ND /03/201803: N2 PFHxA ND /03/201803: N2 PFPrOPrA ND /03/201803: N2 PFHpA ND /03/201803: N2 NaDONA ND /03/201803: N2 PFHxS ND /03/201803: N2 PFOA ND /03/201803: N2 PFNA ND /03/201803: N2 PFOS ND /03/201803: N2 PFDA ND /03/201803: N2 PFUdA ND /03/201803: N2 N-MeFOSAA ND /03/201803: N2 N-EtFOSAA ND /03/201803: N2 PFDS ND /03/201803: N2 PFDoA ND /03/201803: N2 PFTrDA ND /03/201803: N2 PFTeDA ND /03/201803: N2 PFHxDA ND /03/201803: N2 PFODA ND /03/201803: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 19 of 32
20 PFAA Sample Analysis Summary Client's Sample ID Collected 07/10/2018 Received 07/18/2018 RE DUP 10LCMS02_180802C_028 Drinking_Water Total Amount Extracted 248 ml B02 10LCMS02_180802C_013 10LCMS02_180802C_029 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA ND /03/201809: N2 PFPeA ND /03/201809: N2 PFBS ND /03/201809: N2 PFHxA ND /03/201809: N2 PFPrOPrA ND /03/201809: N2 PFHpA ND /03/201809: N2 NaDONA ND /03/201809: N2 PFHxS ND /03/201809: N2 PFOA ND /03/201809: N2 PFNA ND /03/201809: N2 PFOS ND /03/201809: N2 PFDA ND /03/201809: N2 PFUdA ND /03/201809: N2 N-MeFOSAA ND /03/201809: N2 N-EtFOSAA ND /03/201809: N2 PFDS ND /03/201809: N2 PFDoA ND /03/201809: N2 PFTrDA ND /03/201809: N2 PFTeDA ND /03/201809: N2 PFHxDA ND /03/201809: N2 PFODA ND /03/201809: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 20 of 32
21 PFAA Sample Analysis Summary Client's Sample ID Collected 07/10/2018 Received 07/18/2018 CB LCMS02_180802C_017 Drinking_Water Total Amount Extracted 247 ml B02 10LCMS02_180802C_013 10LCMS02_180802C_029 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA ND /03/201803: N2 PFPeA ND /03/201803: N2 PFBS ND /03/201803: N2 PFHxA ND /03/201803: N2 PFPrOPrA ND /03/201803: N2 PFHpA ND /03/201803: N2 NaDONA ND /03/201803: N2 PFHxS ND /03/201803: N2 PFOA ND /03/201803: N2 PFNA ND /03/201803: N2 PFOS ND /03/201803: N2 PFDA ND /03/201803: N2 PFUdA ND /03/201803: N2 N-MeFOSAA ND /03/201803: N2 N-EtFOSAA ND /03/201803: N2 PFDS ND /03/201803: N2 PFDoA ND /03/201803: N2 PFTrDA ND /03/201803: N2 PFTeDA ND /03/201803: N2 PFHxDA ND /03/201803: N2 PFODA ND /03/201803: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 21 of 32
22 PFAA Sample Analysis Summary Client's Sample ID Collected 07/10/2018 Received 07/18/2018 F LCMS02_180802C_018 Drinking_Water Total Amount Extracted 248 ml B02 10LCMS02_180802C_013 10LCMS02_180802C_029 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA ND /03/201803: N2 PFPeA ND /03/201803: N2 PFBS ND /03/201803: N2 PFHxA ND /03/201803: N2 PFPrOPrA ND /03/201803: N2 PFHpA ND /03/201803: N2 NaDONA ND /03/201803: N2 PFHxS ND /03/201803: N2 PFOA ND /03/201803: N2 PFNA ND /03/201803: N2 PFOS ND /03/201803: N2 PFDA ND /03/201803: N2 PFUdA ND /03/201803: N2 N-MeFOSAA ND /03/201803: N2 N-EtFOSAA ND /03/201803: N2 PFDS ND /03/201803: N2 PFDoA ND /03/201803: N2 PFTrDA ND /03/201803: N2 PFTeDA ND /03/201803: N2 PFHxDA ND /03/201803: N2 PFODA ND /03/201803: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 22 of 32
23 PFAA Sample Analysis Summary Client's Sample ID Collected 07/11/2018 Received 07/18/2018 SP LCMS02_180802C_019 Drinking_Water Total Amount Extracted 248 ml B02 10LCMS02_180802C_013 10LCMS02_180802C_029 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA /03/201803: N2 PFPeA ND /03/201803: N2 PFBS ND /03/201803: N2 PFHxA ND /03/201803: N2 PFPrOPrA ND /03/201803: N2 PFHpA ND /03/201803: N2 NaDONA ND /03/201803: N2 PFHxS ND /03/201803: N2 PFOA ND /03/201803: N2 PFNA ND /03/201803: N2 PFOS ND /03/201803: N2 PFDA ND /03/201803: N2 PFUdA ND /03/201803: N2 N-MeFOSAA ND /03/201803: N2 N-EtFOSAA ND /03/201803: N2 PFDS ND /03/201803: N2 PFDoA ND /03/201803: N2 PFTrDA ND /03/201803: N2 PFTeDA ND /03/201803: N2 PFHxDA ND /03/201803: N2 PFODA ND /03/201803: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 23 of 32
24 PFAA Sample Analysis Summary Client's Sample ID Collected 07/11/2018 Received 07/18/2018 HE LCMS02_180802C_020 Drinking_Water Total Amount Extracted 243 ml B02 10LCMS02_180802C_013 10LCMS02_180802C_029 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA /03/201804: N2 PFPeA ND /03/201804: N2 PFBS ND /03/201804: N2 PFHxA ND /03/201804: N2 PFPrOPrA ND /03/201804: N2 PFHpA ND /03/201804: N2 NaDONA ND /03/201804: N2 PFHxS ND /03/201804: N2 PFOA ND /03/201804: N2 PFNA ND /03/201804: N2 PFOS ND /03/201804: N2 PFDA ND /03/201804: N2 PFUdA ND /03/201804: N2 N-MeFOSAA ND /03/201804: N2 N-EtFOSAA ND /03/201804: N2 PFDS ND /03/201804: N2 PFDoA ND /03/201804: N2 PFTrDA ND /03/201804: N2 PFTeDA ND /03/201804: N2 PFHxDA ND /03/201804: N2 PFODA ND /03/201804: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 24 of 32
25 PFAA Sample Analysis Summary Client's Sample ID Collected 07/11/2018 Received 07/18/2018 DM LCMS02_180802C_021 Drinking_Water Total Amount Extracted 249 ml B02 10LCMS02_180802C_013 10LCMS02_180802C_029 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA /03/201804: N2 PFPeA ND /03/201804: N2 PFBS ND /03/201804: N2 PFHxA ND /03/201804: N2 PFPrOPrA ND /03/201804: N2 PFHpA ND /03/201804: N2 NaDONA ND /03/201804: N2 PFHxS ND /03/201804: N2 PFOA ND /03/201804: N2 PFNA ND /03/201804: N2 PFOS ND /03/201804: N2 PFDA ND /03/201804: N2 PFUdA ND /03/201804: N2 N-MeFOSAA ND /03/201804: N2 N-EtFOSAA ND /03/201804: N2 PFDS ND /03/201804: N2 PFDoA ND /03/201804: N2 PFTrDA ND /03/201804: N2 PFTeDA ND /03/201804: N2 PFHxDA ND /03/201804: N2 PFODA ND /03/201804: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 25 of 32
26 PFAA Sample Analysis Summary Client's Sample ID Collected 07/11/2018 Received 07/18/2018 SH LCMS02_180802C_022 Drinking_Water Total Amount Extracted 242 ml B02 10LCMS02_180802C_013 10LCMS02_180802C_029 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA /03/201804: N2 PFPeA ND /03/201804: N2 PFBS ND /03/201804: N2 PFHxA ND /03/201804: N2 PFPrOPrA ND /03/201804: N2 PFHpA ND /03/201804: N2 NaDONA ND /03/201804: N2 PFHxS ND /03/201804: N2 PFOA ND /03/201804: N2 PFNA ND /03/201804: N2 PFOS ND /03/201804: N2 PFDA ND /03/201804: N2 PFUdA ND /03/201804: N2 N-MeFOSAA ND /03/201804: N2 N-EtFOSAA ND /03/201804: N2 PFDS ND /03/201804: N2 PFDoA ND /03/201804: N2 PFTrDA ND /03/201804: N2 PFTeDA ND /03/201804: N2 PFHxDA ND /03/201804: N2 PFODA ND /03/201804: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Fail 13C2_PFOA Fail 13C4_PFOS Fail d3-mefosaa Fail Page 26 of 32
27 PFAA Sample Analysis Summary Client's Sample ID Collected 07/11/2018 Received 07/18/2018 FB LCMS02_180802C_023 Drinking_Water Total Amount Extracted 244 ml B02 10LCMS02_180802C_013 10LCMS02_180802C_029 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA ND /03/201804: N2 PFPeA ND /03/201804: N2 PFBS ND /03/201804: N2 PFHxA ND /03/201804: N2 PFPrOPrA ND /03/201804: N2 PFHpA ND /03/201804: N2 NaDONA ND /03/201804: N2 PFHxS ND /03/201804: N2 PFOA ND /03/201804: N2 PFNA ND /03/201804: N2 PFOS ND /03/201804: N2 PFDA ND /03/201804: N2 PFUdA ND /03/201804: N2 N-MeFOSAA ND /03/201804: N2 N-EtFOSAA ND /03/201804: N2 PFDS ND /03/201804: N2 PFDoA ND /03/201804: N2 PFTrDA ND /03/201804: N2 PFTeDA ND /03/201804: N2 PFHxDA ND /03/201804: N2 PFODA ND /03/201804: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 27 of 32
28 PFAA Sample Analysis Summary Client's Sample ID Collected Received 07/18/ LCMS02_180802C_024 Water 07/11/2018 Total Amount Extracted 250 ml B02 10LCMS02_180802C_013 10LCMS02_180802C_029 Method Blank 10LCMS02_180731A_021 Concentration PQL MDL CAS No. Qual. PFBA ND /03/201804: N2 PFPeA ND /03/201804: N2 PFBS ND /03/201804: N2 PFHxA ND /03/201804: N2 PFPrOPrA ND /03/201804: N2 PFHpA ND /03/201804: N2 NaDONA ND /03/201804: N2 PFHxS ND /03/201804: N2 PFOA ND /03/201804: N2 PFNA ND /03/201804: N2 PFOS ND /03/201804: N2 PFDA ND /03/201804: N2 PFUdA ND /03/201804: N2 N-MeFOSAA ND /03/201804: N2 N-EtFOSAA ND /03/201804: N2 PFDS ND /03/201804: N2 PFDoA ND /03/201804: N2 PFTrDA ND /03/201804: N2 PFTeDA ND /03/201804: N2 PFHxDA ND /03/201804: N2 PFODA ND /03/201804: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 28 of 32
29 PFAA Blank Analysis Summary BLANK LCMS02_180731A_021 Water Total Amount Extracted 250 ml A02 10LCMS02_180731A_015 10LCMS02_180731A_022 Concentration PQL MDL CAS No. Qual. PFBA ND /31/201819: N2 PFPeA ND /31/201819: N2 PFBS ND /31/201819: N2 PFHxA ND /31/201819: N2 PFPrOPrA ND /31/201819: N2 PFHpA ND /31/201819: N2 NaDONA ND /31/201819: N2 PFHxS ND /31/201819: N2 PFOA ND /31/201819: N2 PFNA ND /31/201819: N2 PFOS ND /31/201819: N2 PFDA ND /31/201819: N2 PFUdA ND /31/201819: N2 N-MeFOSAA ND /31/201819: N2 N-EtFOSAA ND /31/201819: N2 PFDS ND /31/201819: N2 PFDoA ND /31/201819: N2 PFTrDA ND /31/201819: N2 PFTeDA ND /31/201819: N2 PFHxDA ND /31/201819: N2 PFODA ND /31/201819: N2 13C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 29 of 32
30 PFAA Laboratory Control Sample (LCS) LCS LCS Total Amount Extracted Start CCal End CCal Method Blank LCS LCMS02_180731A_ mL A02 10LCMS02_180731A_015 10LCMS02_180731A_022 10LCMS02_180731A_021 Extracted Injected By Water 1 07/20/ /31/ :28 QL Spiked Recovered Recovery % Limits PFBA J PFPeA J PFBS J PFHxA J PFPrOPrA J PFHpA J NaDONA PFHxS J PFOA J PFNA PFOS PFDA PFUdA N-MeFOSAA J N-EtFOSAA PFDS PFDoA PFTrDA PFTeDA PFHxDA J PFODA J C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 30 of 32
31 PFAA Laboratory Control Sample (LCS) LCS LCS Total Amount Extracted Start CCal End CCal Method Blank LCS LCMS02_180731A_ mL A02 10LCMS02_180731A_015 10LCMS02_180731A_022 10LCMS02_180731A_021 Extracted Injected By Water 1 07/20/ /31/ :40 QL Spiked Recovered Recovery % Limits PFBA PFPeA PFBS PFHxA PFPrOPrA PFHpA NaDONA PFHxS PFOA PFNA PFOS PFDA PFUdA N-MeFOSAA N-EtFOSAA PFDS PFDoA PFTrDA PFTeDA PFHxDA PFODA C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 31 of 32
32 PFAA Laboratory Control Sample Duplicate (LCSD) LCSD LCSD Total Amount Extracted Start CCal End CCal Method Blank LCSD LCMS02_180731A_ mL A02 10LCMS02_180731A_015 10LCMS02_180731A_022 10LCMS02_180731A_021 LCS Extracted Injected By 10LCMS02_180731A_018 Water 1 07/20/ /31/ :52 QL Spiked Recovered Recovery Recovery RPD % Limits % PFBA PFPeA PFBS PFHxA PFPrOPrA PFHpA NaDONA PFHxS PFOA PFNA PFOS PFDA PFUdA N-MeFOSAA N-EtFOSAA PFDS PFDoA PFTrDA PFTeDA PFHxDA PFODA C2_PFHxA Pass 13C2_PFDA Pass d5-etfosaa Pass 13C3_PFPrOPrA Pass 13C2_PFOA Pass 13C4_PFOS Pass d3-mefosaa Pass Page 32 of 32
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