Texas Commission on Environmental Quality

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1 Method EPA 1311 TCLP TX Method EPA 1312 SPLP TX Method EPA ph TX Method EPA Residue-filterable (TDS) TX Method EPA 1664 n-hexane Extractable Material (HEM) (O&G) TX Silica Gel Treated n-hexane Extractable Material (SGT-HEM) TX Method EPA Aluminum TX Antimony TX Arsenic TX Barium TX Beryllium TX Cadmium TX Calcium TX Chromium TX Cobalt TX Copper TX Iron TX Lead TX Lithium TX Page 1 of 21

2 Magnesium TX Manganese TX Molybdenum TX Nickel TX Potassium TX Selenium TX Silica as SiO2 TX Silver TX Sodium TX Strontium TX Thallium TX Tin TX Titanium TX Vanadium TX Zinc TX Method EPA Mercury TX Method EPA Chloride TX Method EPA Total residual chlorine TX Method EPA Sulfate TX Method EPA Biochemical oxygen demand (BOD) TX Carbonaceous BOD, CBOD TX Page 2 of 21

3 Method EPA Chemical oxygen demand (COD) TX Method EPA 6010 Aluminum TX Antimony TX Arsenic TX Barium TX Beryllium TX Boron TX Cadmium TX Calcium TX Chromium TX Cobalt TX Copper TX Iron TX Lead TX Lithium TX Magnesium TX Manganese TX Molybdenum TX Nickel TX Potassium TX Selenium TX Silica as SiO2 TX Silver TX Sodium TX Strontium TX Thallium TX Tin TX Page 3 of 21

4 Titanium TX Vanadium TX Zinc TX Method EPA 624 1,1,1-Trichloroethane TX ,1,2,2-Tetrachloroethane TX ,1,2-Trichloroethane TX ,1-Dichloroethane TX ,1-Dichloroethylene TX ,2-Dibromoethane (EDB, Ethylene dibromide) TX ,2-Dichlorobenzene TX ,2-Dichloroethane (Ethylene dichloride) TX ,2-Dichloropropane TX ,3-Dichlorobenzene TX ,4-Dichlorobenzene TX Butanone (Methyl ethyl ketone, MEK) TX Chloroethyl vinyl ether TX Acetone (2-Propanone) TX Acrolein (Propenal) TX Acrylonitrile TX Benzene TX Bromodichloromethane TX Bromoform TX Carbon tetrachloride TX Chlorobenzene TX Chlorodibromomethane TX Chloroethane (Ethyl chloride) TX Chloroform TX cis-1,2-dichloroethylene TX Page 4 of 21

5 cis-1,3-dichloropropene TX Ethylbenzene TX m+p-xylene TX Methyl bromide (Bromomethane) TX Methyl chloride (Chloromethane) TX Methyl tert-butyl ether (MTBE) TX Methylene chloride (Dichloromethane) TX Naphthalene TX o-xylene TX Tetrachloroethylene (Perchloroethylene) TX Toluene TX Total trihalomethanes TX trans-1,2-dichloroethylene TX trans-1,3-dichloropropylene TX Trichloroethene (Trichloroethylene) TX Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) TX Vinyl chloride TX Xylene (total) TX Method EPA 625 2,2'-Oxybis(1-chloropropane) (bis(2-chloro-1-methylethyl)ether) TX ,2,4-Trichlorobenzene TX ,2-Dichlorobenzene TX ,3-Dichlorobenzene TX ,4-Dichlorobenzene TX ,4,5-Trichlorophenol TX ,4,6-Trichlorophenol TX ,4-Dichlorophenol TX ,4-Dimethylphenol TX ,4-Dinitrophenol TX Page 5 of 21

6 2,4-Dinitrotoluene (2,4-DNT) TX ,6-Dinitrotoluene (2,6-DNT) TX Chloronaphthalene TX Chlorophenol TX Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol) TX Methylphenol (o-cresol) TX Nitrophenol TX ,3'-Dichlorobenzidine TX Bromophenyl phenyl ether (BDE-3) TX Chloro-3-methylphenol TX Chlorophenyl phenylether TX Methylphenol (p-cresol) TX Acenaphthene TX Acenaphthylene TX Anthracene TX Benzo(a)anthracene TX Benzo(a)pyrene TX Benzo(b)fluoranthene TX Benzo(g,h,i)perylene TX Benzo(k)fluoranthene TX bis(2-chloroethoxy)methane TX bis(2-chloroethyl) ether TX bis(2-ethylhexyl) phthalate (Di(2-Ethylhexyl) phthalate, DEHP) TX Butyl benzyl phthalate TX Chrysene TX Dibenz(a,h) anthracene TX Diethyl phthalate TX Dimethyl phthalate TX Di-n-butyl phthalate TX Di-n-octyl phthalate TX Page 6 of 21

7 Fluoranthene TX Fluorene TX Hexachlorobenzene TX Hexachlorobutadiene TX Hexachlorocyclopentadiene TX Hexachloroethane TX Indeno(1,2,3-cd) pyrene TX Isophorone TX Naphthalene TX Nitrobenzene TX n-nitrosodi-n-propylamine TX n-nitrosodiphenylamine TX Pentachlorophenol TX Phenanthrene TX Phenol TX Pyrene TX Pyridine TX Method EPA 7470 Mercury TX Method EPA 7471 Mercury TX Method EPA 8015 Diesel range organics (DRO) TX Ethanol TX Ethylene glycol TX Methanol TX Propylene Glycol TX Page 7 of 21

8 Method EPA ,1,1,2-Tetrachloroethane TX ,1,1-Trichloroethane TX ,1,2,2-Tetrachloroethane TX ,1,2-Trichloroethane TX ,1-Dichloroethane TX ,1-Dichloroethylene TX ,1-Dichloropropene TX ,2,3-Trichlorobenzene TX ,2,3-Trichloropropane TX ,2,4-Trichlorobenzene TX ,2,4-Trimethylbenzene TX ,2-Dibromo-3-chloropropane (DBCP) TX ,2-Dibromoethane (EDB, Ethylene dibromide) TX ,2-Dichlorobenzene TX ,2-Dichloroethane (Ethylene dichloride) TX ,2-Dichloropropane TX ,3,5-Trimethylbenzene TX ,3-Dichlorobenzene TX ,3-Dichloropropane TX ,4-Dichlorobenzene TX Chlorohexane TX ,2-Dichloropropane TX Butanone (Methyl ethyl ketone, MEK) TX Chloroethyl vinyl ether TX Chlorotoluene TX Hexanone (MBK) TX Chlorotoluene TX Isopropyltoluene (p-cymene) TX Page 8 of 21

9 4-Methyl-2-pentanone (MIBK) TX Acetone (2-Propanone) TX Acrolein (Propenal) TX Acrylonitrile TX Benzene TX Bromobenzene TX Bromochloromethane TX Bromodichloromethane TX Bromoform TX Carbon disulfide TX Carbon tetrachloride TX Chlorobenzene TX Chlorodibromomethane TX Chloroethane (Ethyl chloride) TX Chloroform TX cis-1,2-dichloroethylene TX cis-1,3-dichloropropene TX cis-1,4-dichloro-2-butene TX Dibromomethane (Methylene bromide) TX Dichlorodifluoromethane (Freon-12) TX Di-isopropylether (DIPE) TX Ethanol TX Ethylbenzene TX Ethyl-t-butylether (ETBE) (2-Ethoxy-2-methylpropane) TX Hexachlorobutadiene TX Isopropylbenzene (Cumene) TX m+p-xylene TX Methyl bromide (Bromomethane) TX Methyl chloride (Chloromethane) TX Methyl tert-butyl ether (MTBE) TX Page 9 of 21

10 Methylene chloride (Dichloromethane) TX Naphthalene TX n-butylbenzene TX n-propylbenzene TX o-xylene TX sec-butylbenzene TX Styrene TX T-amylmethylether (TAME) TX tert-butyl alcohol TX tert-butylbenzene TX Tetrachloroethylene (Perchloroethylene) TX Toluene TX Total trihalomethanes TX trans-1,2-dichloroethylene TX trans-1,3-dichloropropylene TX trans-1,4-dichloro-2-butene TX Trichloroethene (Trichloroethylene) TX Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) TX Vinyl chloride TX Xylene (total) TX Method EPA ,2'-Oxybis(1-chloropropane) (bis(2-chloro-1-methylethyl)ether) TX ,2,4-Trichlorobenzene TX ,2-Dichlorobenzene TX ,2-Diphenylhydrazine TX ,3-Dichlorobenzene TX ,4-Dichlorobenzene TX ,4,5-Trichlorophenol TX ,4,6-Trichlorophenol TX Page 10 of 21

11 2,4-Dichlorophenol TX ,4-Dimethylphenol TX ,4-Dinitrophenol TX ,4-Dinitrotoluene (2,4-DNT) TX ,6-Dinitrotoluene (2,6-DNT) TX Chloronaphthalene TX Chlorophenol TX Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol) TX Methylnaphthalene TX Methylphenol (o-cresol) TX Nitroaniline TX Nitrophenol TX ,3'-Dichlorobenzidine TX Methylphenol (m-cresol) TX Nitroaniline TX Bromophenyl phenyl ether (BDE-3) TX Chloro-3-methylphenol TX Chloroaniline TX Chlorophenyl phenylether TX Methylphenol (p-cresol) TX Nitroaniline TX Nitrophenol TX Acenaphthene TX Acenaphthylene TX Aniline TX Anthracene TX Azobenzene TX Benzidine TX Benzo(a)anthracene TX Benzo(a)pyrene TX Page 11 of 21

12 Benzo(b)fluoranthene TX Benzo(g,h,i)perylene TX Benzo(k)fluoranthene TX Benzoic acid TX bis(2-chloroethoxy)methane TX bis(2-chloroethyl) ether TX bis(2-ethylhexyl) phthalate (Di(2-Ethylhexyl) phthalate, DEHP) TX Butyl benzyl phthalate TX Chrysene TX Dibenz(a,h) anthracene TX Dibenzofuran TX Diethyl phthalate TX Dimethyl phthalate TX Di-n-butyl phthalate TX Di-n-octyl phthalate TX Diphenylamine TX Fluoranthene TX Fluorene TX Hexachlorobenzene TX Hexachlorobutadiene TX Hexachlorocyclopentadiene TX Hexachloroethane TX Indeno(1,2,3-cd) pyrene TX Isophorone TX Naphthalene TX Nitrobenzene TX n-nitrosodi-n-propylamine TX n-nitrosodiphenylamine TX Pentachlorophenol TX Phenanthrene TX Page 12 of 21

13 Phenol TX Pyrene TX Pyridine TX Method SM 2340 B Total hardness as CaCO3 TX Method SM 2540 C Residue-filterable (TDS) TX Method SM 4500-Cl C Chloride TX Method SM 4500-H+ B ph TX Method SM 5210 B Biochemical oxygen demand (BOD) TX Carbonaceous BOD, CBOD TX Method SM 5220 D Chemical oxygen demand (COD) TX Method TCEQ 1005 Total Petroleum Hydrocarbons (TPH) TX Page 13 of 21

14 Matrix: Solid & Chemical Materials Method ASTM D2216 Moisture TX ASTM D Method EPA 1311 TCLP TX Method EPA 1312 SPLP TX Method EPA 6010 Aluminum TX Antimony TX Arsenic TX Barium TX Beryllium TX Boron TX Cadmium TX Calcium TX Chromium TX Cobalt TX Copper TX Iron TX Lead TX Lithium TX Magnesium TX Manganese TX Molybdenum TX Nickel TX Potassium TX Selenium TX Page 14 of 21

15 Matrix: Solid & Chemical Materials Silica as SiO2 TX Silver TX Sodium TX Strontium TX Thallium TX Tin TX Titanium TX Vanadium TX Zinc TX Method EPA 7470 Mercury TX Method EPA 7471 Mercury TX Method EPA 8015 Diesel range organics (DRO) TX Ethanol TX Ethylene glycol TX Methanol TX Propylene Glycol TX Method EPA ,1,1,2-Tetrachloroethane TX ,1,1-Trichloroethane TX ,1,2,2-Tetrachloroethane TX ,1,2-Trichloroethane TX ,1-Dichloroethane TX ,1-Dichloroethylene TX ,1-Dichloropropene TX Page 15 of 21

16 Matrix: Solid & Chemical Materials 1,2,3-Trichlorobenzene TX ,2,3-Trichloropropane TX ,2,4-Trichlorobenzene TX ,2,4-Trimethylbenzene TX ,2-Dibromo-3-chloropropane (DBCP) TX ,2-Dibromoethane (EDB, Ethylene dibromide) TX ,2-Dichlorobenzene TX ,2-Dichloroethane (Ethylene dichloride) TX ,2-Dichloropropane TX ,3,5-Trimethylbenzene TX ,3-Dichlorobenzene TX ,3-Dichloropropane TX ,4-Dichlorobenzene TX Chlorohexane TX ,2-Dichloropropane TX Butanone (Methyl ethyl ketone, MEK) TX Chloroethyl vinyl ether TX Chlorotoluene TX Hexanone (MBK) TX Chlorotoluene TX Isopropyltoluene (p-cymene) TX Methyl-2-pentanone (MIBK) TX Acetone (2-Propanone) TX Acrolein (Propenal) TX Acrylonitrile TX Benzene TX Bromobenzene TX Bromochloromethane TX Bromodichloromethane TX Bromoform TX Page 16 of 21

17 Matrix: Solid & Chemical Materials Carbon disulfide TX Carbon tetrachloride TX Chlorobenzene TX Chlorodibromomethane TX Chloroethane (Ethyl chloride) TX Chloroform TX cis-1,2-dichloroethylene TX cis-1,3-dichloropropene TX Dibromomethane (Methylene bromide) TX Dichlorodifluoromethane (Freon-12) TX Ethanol TX Ethylbenzene TX Hexachlorobutadiene TX Isopropylbenzene (Cumene) TX m+p-xylene TX Methyl bromide (Bromomethane) TX Methyl chloride (Chloromethane) TX Methyl tert-butyl ether (MTBE) TX Methylene chloride (Dichloromethane) TX Naphthalene TX n-butyl alcohol (1-Butanol, n-butanol) TX n-butylbenzene TX n-propylbenzene TX o-xylene TX sec-butylbenzene TX Styrene TX tert-butyl alcohol TX tert-butylbenzene TX Tetrachloroethylene (Perchloroethylene) TX Toluene TX Page 17 of 21

18 Matrix: Solid & Chemical Materials trans-1,2-dichloroethylene TX trans-1,3-dichloropropylene TX trans-1,4-dichloro-2-butene TX Trichloroethene (Trichloroethylene) TX Trichlorofluoromethane (Fluorotrichloromethane, Freon 11) TX Vinyl acetate TX Vinyl chloride TX Xylene (total) TX Method EPA ,2'-Oxybis(1-chloropropane) (bis(2-chloro-1-methylethyl)ether) TX ,2,4-Trichlorobenzene TX ,2-Dichlorobenzene TX ,2-Diphenylhydrazine TX ,3-Dichlorobenzene TX ,4-Dichlorobenzene TX ,4,5-Trichlorophenol TX ,4,6-Trichlorophenol TX ,4-Dichlorophenol TX ,4-Dimethylphenol TX ,4-Dinitrophenol TX ,4-Dinitrotoluene (2,4-DNT) TX ,6-Dinitrotoluene (2,6-DNT) TX Chloronaphthalene TX Chlorophenol TX Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol) TX Methylnaphthalene TX Methylphenol (o-cresol) TX Nitroaniline TX Nitrophenol TX Page 18 of 21

19 Matrix: Solid & Chemical Materials 3,3'-Dichlorobenzidine TX Methylphenol (m-cresol) TX Nitroaniline TX Bromophenyl phenyl ether (BDE-3) TX Chloro-3-methylphenol TX Chloroaniline TX Chlorophenyl phenylether TX Methylphenol (p-cresol) TX Nitroaniline TX Nitrophenol TX Acenaphthene TX Acenaphthylene TX Aniline TX Anthracene TX Azobenzene TX Benzidine TX Benzo(a)anthracene TX Benzo(a)pyrene TX Benzo(b)fluoranthene TX Benzo(g,h,i)perylene TX Benzo(k)fluoranthene TX Benzoic acid TX bis(2-chloroethoxy)methane TX bis(2-chloroethyl) ether TX bis(2-ethylhexyl) phthalate (Di(2-Ethylhexyl) phthalate, DEHP) TX Butyl benzyl phthalate TX Chrysene TX Dibenz(a,h) anthracene TX Dibenzofuran TX Diethyl phthalate TX Page 19 of 21

20 Matrix: Solid & Chemical Materials Dimethyl phthalate TX Di-n-butyl phthalate TX Di-n-octyl phthalate TX Diphenylamine TX Fluoranthene TX Fluorene TX Hexachlorobenzene TX Hexachlorobutadiene TX Hexachlorocyclopentadiene TX Hexachloroethane TX Indeno(1,2,3-cd) pyrene TX Isophorone TX Naphthalene TX Nitrobenzene TX n-nitrosodimethylamine TX n-nitrosodi-n-propylamine TX n-nitrosodiphenylamine TX Pentachlorophenol TX Phenanthrene TX Phenol TX Pyrene TX Pyridine TX Method EPA 9038 Sulfate TX Method EPA 9045 Corrosivity TX ph TX Method SM 2540 G Page 20 of 21

21 Matrix: Solid & Chemical Materials Residue-total (total solids) TX Method TCEQ 1005 Total Petroleum Hydrocarbons (TPH) TX Page 21 of 21

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