Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005
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1 Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005 Period of validity: to Holder of certificate: Salzgitter Flachstahl GmbH Chemische Laboratorien, Immissionsschutz und Werkstoffprüfung Eisenhüttenstraße 99, Salzgitter Tests in the fields: physical, physico-chemical and chemical investigations of crude iron, steels, metals and alloys and of iron ores and basic pig iron sinter; investigation of slags and oxidic raw materials, materials and waste materials; selected investigations of water and process waters; investigations of fuels and oils and of coke by-products; determination of airborne substances at workplaces; determination of selected inorganic and organic gaseous or particle-form airborne substances; airborne substances of emissions; mechanical-technological investigations of metallic materials; chemical and microbiological investigations in accordance with the drinking water regulations; sampling of raw and drinking water Terms and abbreviations used: see last page The testing laboratory is permitted, without being required to inform and obtain prior approval from DAkkS, to use standards or equivalent testing methods listed here with different issue dates. The testing laboratory maintains a current list of all testing methods within the flexible scope of accreditation. This document is a translation. The definitive version is the original German annex to the accreditation certificate. 1/15
2 1 Investigations of crude irons, steels, metals and alloys 1.1 RFA determinations of elements DIN X-ray spectrometry - X-ray emission and X-ray fluorescence analysis (XRF) - Part 2: Definitions and basic principles for measurements, calibration and evaluation of results (Matrix: crude iron, zinc, sheet metal coatings) 1.2 ICP-OES determination of elements DIN EN ISO DIN EN DIN EN Zinc and zinc alloys - Part 2: Analysis by inductively coupled plasma optical emission spectrometry Chemical analysis of ferrous materials - Inductively coupled plasma optical emission spectrometric analysis of unalloyed and low alloyed steels - Determination of Mn, P, Cu, Ni, Cr, Mo, V, Co, Al (total) and Sn (also: Determination of Si, Ti, As, Zn, Nb, Ca, B) Aluminium and aluminium alloys - Chemical analysis - Inductively coupled plasma optical emission spectral analysis 1.3 IR determination of elements and compounds DIN EN ISO DIN EN Steel and iron - Determination of total carbon and sulfur content - Infrared absorption method after combustion in an induction furnace (routine method) (also: Determination of surface carbon at 550 C) Chemical analysis of ferrous materials - Determination of oxygen content in steel and iron - Part 2: Infrared method after fusion under inert gas 1.4 Spark-OES determination of elements ASTM E Standard Test Method for Atomic Emission Vacuum Spectrometric Analysis of Carbon an Low-Alloy Steel (extended element and working range) Period of validity: to Translation - 2/15
3 1.5 Other investigations DIN EN ISO DIN EN AV TCCO O089 Rev Handbuch für das Eisenhüttenlaboratorium Vol. 2, Part 1, 1st edition, 2004, p. 63 Handbuch für das Eisenhüttenlaboratorium Vol. 2,.Part 2, 1998 edition, p. 235 Handbuch für das Eisenhüttenlaboratorium - Vol. 1 principles and methods (2009 edition) p. 432 NACE TM NACE TM PSA D Steel and iron - Determination of nitrogen content - Thermal conductimetric method after fusion in a current of inert gas (Routine method) Cold rolled low carbon steel flat products for vitreous enamelling - Technical delivery conditions (Matrix: cold and warm strip) Determination of surface oil film (Matrix: cold strip) Determination of silicon content, gravimetric determination, perchloric acid method Determination of hydrogen in steel by hot extraction The activity measurement in the iron works - Determination of the radioactivity concentration in steel Evaluation of Pipeline and Pressure Vessel Steels for Resistance to Hydrogen-Induced Cracking Laboratory Testing of Metals for Resistance to Sulfide Stress Cracking and Stress Corrosion Cracking in H 2S Environments Zinc coatings on steel plating Gravimetric analysis of different elements and weights per unit area (atomic absorption or plasma torch method) 2 Investigation of iron ores and basic pig iron sinter ISO nd edition Iron ores - Determination of total iron content - Part 1: Titrimetric method after tin(ii) chloride reduction Period of validity: to Translation - 3/15
4 ISO DIN EN ISO (E 22) Handbuch für das Eisenhüttenlaboratorium Vol. 3, Part 1, 3rd edition, 2011, p.42 Iron ores - Determination of various elements by X-ray fluorescence spectrometry - Part 1: Comprehensive procedure Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) (Modification for sinter: Element determination of sinter material in acid solution borate digestions) Determination of iron(ii) oxide and iron(iii) oxide 3 Investigation of slags and oxidic raw materials, materials and waste materials DIN EN ISO DIN EN ISO (E 22) DIN D DIN S DIN Supplementary Sheet Handbuch für das Eisenhüttenlaboratorium Vol. 2, Part 1, 1st edition, 2004, p. 65 Chemical analysis of refractory products by X-ray fluorescence (XRF) - Fused cast-bead method (Matrix: refractory material, slags, olivine, dunite) Water quality - Determination of selected elements by inductively coupled plasma optical emission spectrometry (ICP-OES) (Modification for slags, lime and alloying agents: Element determination of slags in acid solution borate digestions and of lime and alloying agents following acid digestion) Determination of chloride ions (Modification for solid materials: Aqueous extraction from the sample) Determination of leachability by water (Matrix: Land fill samples) (withdrawn standard) X-ray spectrometry - X-ray emission and X-ray fluorescence analysis (XRF) - Part 2: Definitions and basic principles for measurements, calibration and evaluation of results (Matrix: Blast furnace slag, converter slag) Determination of silicon content, titrimetric method (Modification for alloying agents: only Fe-Si, Si-Mn, Fe-Nb) Period of validity: to Translation - 4/15
5 4 Selected investigations of water and process waters DIN EN ISO (D 6) DIN EN (E 4) DIN EN ISO (F 4) DIN (F 7) DIN EN ISO 9562 (H 14) DIN EN ISO (H 53) Handbuch für das Eisenhüttenlaboratorium Vol. 3, Part 1, 3rd edition, 2011, p. 75 Water quality - Determination of total cyanide and free cyanide using flow analysis (FIA and CFA) - Part 2: Method using continuous flow analysis (CFA) Water quality - Determination of trace elements using atomic absorption spectrometry with graphite furnace Water quality - Determination of highly volatile halogenated hydrocarbons - Gas-chromatographic methods Determination of six polycyclic aromatic hydrocarbons (PAH) in drinking and mineral water by high performance thin layer chromatography (HPTLC) (withdrawn standard) Water quality - Determination of adsorbable organically bound halogens (AOX) Water quality - Determination of hydrocarbon oil index - Part 2: Method using solvent extraction and gas chromatography Determination of sulfide sulfur 5 Investigations of fuels DIN EN ISO DIN EN ISO DIN Chemical analysis of refractory products by X-ray fluorescence (XRF) - Fused cast-bead method Water quality - Determination of adsorbable organically bound halogens (AOX) (Deviation of the method: Fuels with additive module) Testing of lubricants - Determination of elements content in additives, wear and other contaminations - Part 1: Direct determination by optical emission spectral analysis with inductively coupled plasma (ICP OES) (Modification: Digestion in microwave oven) Period of validity: to Translation - 5/15
6 DIN DIN DIN DIN DIN DIN DIN DIN DIN DIN Corrigendum DIN DIN ASTM D Testing of solid fuels - Determination of the water content and the moisture of analysis sample Testing of solid fuels - Solid mineral fuels - Determination of ash content Testing of solid fuels - Determination of volatile matter content Solid mineral fuels - Determination of sulfur content - Part 3: Instrumental methods Solid fuels - Determination of chemical composition of fuel ash - Part 8: Determination of soda and potash (Na 2O, K 2O) contents Testing of solid mineral fuels - Determination of total carbon, hydrogen and nitrogen - Instrumental methods Testing of solid fuels - Determination of plastic properties of coal with the Gieseler Plastometer Testing of solid fuels - Determination of the dilatation of coal Testing of solid fuels - Determination of the crucible swelling number of coal Testing of solid and liquid fuels - Determination of gross calorific value by the bomb calorimeter and calculation of net calorific value - Part 1: Principles, apparatus, methods Testing of solid and liquid fuels - Determination of gross calorific value by the bomb calorimeter and calculation of net calorific value - Part 3: Method using adiabatic jacket Investigations of the raw material in hard-coal-mining - Microscopical examinations of hard coal, coke and briquettes - Part 5: Reflectance measurements on vitrinites Test Methods for Determination of Trace Elements in Coal, Coke, & Combustion Residues from Coal Utilization Processes by Inductively Coupled Plasma Atomic Emission, Inductively Coupled Plasma Mass, & Graphite Furnace Atomic Absorption Spectrometry Period of validity: to Translation - 6/15
7 UN Test N Test ("Spontaneous heating - capable Materials" according to the UN Testing Manual (UN Recommendation on the Transport of Dangerous Goods, Manual of Tests and Criteria, Fifth Revision Edition 2009, Test Method for self-heating substances) 6 Investigations of oils DIN EN ISO DIN EN ISO DIN EN DIN EN DIN DIN DIN SEB DIN DIN Determination of flash point - Pensky-Martens closed cup method Petroleum products - Determination of ash Petroleum products and used oils - Determination of PCBs and related products - Part 1: Separation and determination of selected PCB congeners by gas chromatography (GC) using an electron capture detector (ECD) Petroleum products and used oils - Determination of PCBs and related products - Part 2: Calculation of polychlorinated biphenyl (PCB) content Testing of petroleum products and related products - Analysis by infrared spectrometry - General working principles Testing of mineral oils and related materials - Determination of density Viscometry - Measurement of viscosity by means of the rolling ball viscometer by Höppler Tribotechnology - Testing of lubricants - Determination of solid substances in oils, greases and cooling lubricants by membrane filtration Testing of Mineral Oils; Determination of the Neutralization Number, Colour-indicator titration (withdrawn standard) Testing of mineral oils; determination of neutralization number; color-indicator titration, insulating oils Period of validity: to Translation - 7/15
8 DIN DIN Testing of mineral oils - Determination of the saponification number - Part 1: Saponification numbers above 2, color indicator titration Testing of mineral oils - Determination of saponification number - Part 2: Color-indicator titration, insulating oils 7 Investigations of coke by-products (tar, oil) ISO DIN EN ISO Carbonaceous materials for the production of aluminium; Pitch for electrodes; Determination of content of toluene-insoluble material Petroleum products - Determination of water - Coulometric Karl Fischer titration method 8 Determination of airborne substances at workplaces BIA 6068/ BIA 6068/ BIA BIA BIA BIA BIA BIA Alveolar fraction - Measurement method 1 (Matrix: Dust samples) Alveolar fraction - Measurement method 2 (Matrix: Dust samples) Inhalable fraction - Measurement method 1 (Matrix: Dust samples) Quartz (sampling only) Hydrocarbons, aliphatic Hydrocarbons, aromatic Mixtures of hydrocarbons - reciprocal calculation procedure Diesel motor emissions - Determination of total carbon in the fine dust (in addition: Determination of carbon by infrared absorption following combustion) Period of validity: to Translation - 8/15
9 BIA Mineral oils, vapour and aerosol (aliphatic hydrocarbons with high boiling points 9 Selected emission measurements DIN EN DIN EN DIN EN DIN EN DIN EN DIN EN DIN EN DIN EN DIN DIN Stationary source emissions - Determination of mass concentration of gaseous chlorides expressed as HCl - Standard reference method (sampling only) Stationary source emissions - Determination of the mass concentration of PCDDs/PCDFs and dioxin-like PCBs - Part 1: Sampling of PCDDs/PCDFs Stationary source emissions - Determination of the mass concentration of total gaseous organic carbon - Continuous flame ionisation detector method Stationary source emissions - Determination of low range mass concentration of dust - Part 1: Manual gravimetric method Stationary source emissions - Determination of the total emission of As, Cd, Cr, Co, Cu, Mn, Ni, Pb, Sb, TI and V (sampling only) Stationary source emissions - Determination of volume concentration of oxygen (O 2) - Reference method - Paramagnetism Stationary source emissions - Determination of mass concentration of sulphur dioxide - Reference method (sampling only) Stationary source emissions - Determination of the mass concentration of carbon monoxide (CO) - Reference method: Nondispersive infrared spectrometry Measurement of gaseous emissions - Automatic measurement systems for single measurements of nitrogen monooxide and nitrogen dioxide (withdrawn standard) Testing of gaseous fuels and other gases; determination of the components; gaschromatographic procedure Period of validity: to Translation - 9/15
10 AA TU VDI 2470 Sheet VDI 2066 Sheet VDI 3499 Sheet Continuous measurement of SO 2 on the basis of the withdrawn standard VDI 2462, Sheet 4 ( ) Gaseous emission measurement; measurement of gaseous fluorine compounds; absorption method (sampling only) Particulate matter measurement - Dust measurement in flowing gases - Gravimetric determination of dust load Emission measurement - Determination of polychlorinated dibenzo-p-dioxins (PCDDs) and dibenzofurans (PCDFs) - Cooled probe method; Example of application of DIN EN 1948 for the concentration range < 0.1 ng I-TEQ/m 3 and supplement for the concentration range > 0.1 ng I-TEQ/m 3 (sampling only) 10 Mechanical-technological investigations of metallic materials 10.1 Tensile testing DIN ISO DIN ISO DIN EN ISO DIN EN ISO DIN EN ASTM A Metallic materials - Sheet and strip - Determination of plastic strain ratio Metallic materials - Sheet and strip - Determination of tensile strain hardening exponent Metallic materials - Tensile testing - Part 1: Method of test at room temperature Metallic materials - Tensile testing - Part 2: Method of test at elevated temperature Steel - Determination of yield strength increase by the effect of heat treatment (Bake-Hardening-Index) Standard Test Methods and Definitions for Mechanical Testing of Steel Products 10.2 Notch impact bend testing DIN EN ISO Metallic materials - Charpy pendulum impact test - Part 1: Test method Period of validity: to Translation - 10/15
11 10.3 Drop weight testing DIN EN API RP 5L Metallic materials - Drop weight tear test Recommended Practice for Conducting Drop-Weight Tear Tests on Line Pipe 10.4 Hardness measurement DIN EN ISO DIN EN ISO DIN EN ISO Metallic materials - Brinell hardness test - Part 1: Test method Metallic materials - Vickers hardness test - Part 1: Test method Metallic materials - Rockwell hardness test - Part 1: Test method (Scales A, B, C, D, E, F, G, H, K, N, T) 10.5 Roughness measurement DIN EN Measurement of roughness average Ra and peak count RPC on metallic flat products 10.6 Bend testing DIN EN ISO DIN EN ISO Destructive tests on welds in metallic materials - Bend tests Metallic materials - Bend test Period of validity: to Translation - 11/15
12 11 Investigations in accordance with the drinking water regulations (TrinkwV 2001) Sampling Method DIN ISO DIN EN ISO DIN EN ISO (K 19) Title Water quality - Sampling - Part 5: Guidance on sampling of drinking water from treatment works and piped distribution systems Water quality - Sampling - Part 3: Preservation and handling of water samples Water quality - Sampling for microbiological analysis ANNEX 1: MICROBIOLOGICAL PARAMETERS PART I: General requirements for drinking water No. Parameter Method 1 Escherichia coli (E. coli) with Colilert -18/Quanti-Tray 2 Enterococci Enterolert -DW PART II: Requirements for drinking water intended for dispensing from closed containers not applicable ANNEX 2: CHEMICAL PARAMETERS PART I: Chemical parameters for which as a rule the concentration no longer rises in the supply network, including the drinking water installation No. Parameter Method 1 Acrylamide not measured 2 Benzene DIN F (withdrawn standard) 3 Boon DIN EN ISO (E22) Bromate DIN EN ISO (D34) Chromium DIN EN ISO (E22) Cyanide DIN EN ISO (D3) ,2-dichloroethane DIN EN ISO (F4) Fluoride DIN D Nitrate DIN EN ISO (D 20) Active ingredients of pesticide and biocide products DIN EN ISO 6468 (F1) Total active ingredients of pesticide and biocide products DIN EN ISO 6468 (F1) Mercury DIN EN ISO (E12) Selenium DIN EN ISO (E4) Period of validity: to Translation - 12/15
13 No. Parameter Method 14 Tetrachloroethene and trichloroethene DIN EN ISO (F4) Uranium DIN EN ISO (E22) PART II: Chemical parameters for which the concentration in the supply network, including the drinking water installation, can rise No. Parameter Method 1 Antimony DIN EN ISO (E4) Arsenic DIN EN ISO (D18) (withdrawn standard) 3 Benzo-(a)-pyrenes DIN (F7) (withdrawn standard) 4 Lead DIN EN ISO (E4) Cadmium DIN EN ISO (E22) Epichlorohydrin not measured 7 Copper DIN EN ISO (E22) Nickel DIN EN ISO (E22) Nitrite DIN EN (D10) Polycyclic aromatic hydrocarbons DIN (F7) (withdrawn standard) 11 Trihalomethanes DIN EN ISO (F4) Vinyl chloride not measured ANNEX 3: INDICATOR PARAMETERS Part I: General indicator parameters No. Parameter Method 1 Aluminium DIN EN ISO (E22) Ammonium DIN E Chloride DIN EN ISO (D20) DIN (D1) Clostridium perfringens (including spores) not measured 5 Coliform bacteria Colilert -18/Quanti-Tray 6 Iron DIN EN ISO (E22) Colouring (spectral absorption coefficient for Hg 436 nm) DIN EN ISO 7887 (C1) Odour DIN EN 1622 (B3) Flavour DIN EN 1622 (B3) Colony count at 22 C TrinkwV 2001 (2011) Anl. 5 I d) bb) 11 Colony count at 2236 C TrinkwV 2001 (2011) Anl. 5 I d) bb) 12 Electrical conductivity DIN EN (C8) Manganese DIN EN ISO (E22) Period of validity: to Translation - 13/15
14 No. Parameter Method 14 Sodium DIN EN ISO (E22) Organically bound carbon (TOC) DIN EN 1484 (H3) Oxididizability DIN EN ISO 8467 (H5) Sulfate DIN EN ISO (D 20) Turbidity DIN EN ISO 7027 (C2) Hydrogen ion concentration DIN EN ISO Calcite solubility DIN (C10) (calculation method 3) 21 Tritium not measured 22 Total indicative dose not measured Part II: Special requirements for drinking water in drinking installation systems not applicable Parameters not included in Annexes 1 to 3 of the drinking water Regulations of 2001 Further periodic investigations Parameter Method Calcium DIN EN ISO (E22) Potassium DIN EN ISO (E22) Magnesium DIN EN ISO (E22) Acid capacity DIN (H7) The accreditation does not replace the recognition or approval procedures of the responsible regulatory authorities in accordance with Article 15, Paragraph 4 of the drinking water regulations. Period of validity: to Translation - 14/15
15 Abbreviations used: AA TU API RP ASTM AV TCCO BIA DIN EN IEC ISO NACE TM PSA SEB TrinkwV VDI Arbeitsanweisung Hausmethode der Salzgitter Flachstahl GmbH (In-house work instruction of the Salzgitter Flachstahl GmbH) American Petroleum Institute Recommended Practice American Society for Testing and Materials Analysenvorschrift Hausmethode der Salzgitter Flachstahl GmbH (In-house analytical specification of the Salzgitter Flachstahl GmbH) Berufsgenossenschaftliches Institut für Arbeitsschutz (German Occupational Insurance Institute) Deutsches Institut für Normung (German Institute for Standardization) Europäische Norm (European standard) International Electrotechnical Commission International Organization for Standardization Standard Method of NACE International - The Corrosion Society Peugot Société Anonyme (Anonymous Peugot Society) Stahleisenbetriebsblatt (Basic Pig Iron Works Sheet) Trinkwasserverordnung (drinking water regulations) Verein Deutscher Ingenieure (Association of German Engineers) Period of validity: to Translation - 15/15
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