Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005

Transcription

1 Deutsche Akkreditierungsstelle GmbH Annex to the Accreditation Certificate D-PL according to DIN EN ISO/IEC 17025:2005 Period of validity: to Holder of certificate: FIZ GmbH Tannenstraße 2, Düsseldorf Tests in the fields: Determination of inorganic and organic gaseous or particulate airborne substances Special sampling of substances requiring additional effort for sampling or analysis (airborne polyhalogenated dibenzo-p-dioxins and dibenzofurans and dioxin-like PCBs); determination of combustion conditions Calibration and functional tests of continuously operating emission measuring equipment for inorganic and organic gas or particulate airborne substances; calibration and functional tests of continuously operating emission measuring equipment for inorganic and organic gas or particulate airborne substances in systems in accordance with 4. BImSchV, Annex column 1 Determination of noise and vibrations Analytical determination of selected heavy metals in immission samples Measurement and calculation of noise Immission control module Abbreviations used: see last page This is a translation. The definitive version is the original German annex to the accreditation certificate. 1/14

2 1. Determination of emissions in areas regulated by immission control law Measurement procedure as per immission control module and Annex A2 to VDI 4220 The fulfilment of the requirements of CEN/TS 15675:2007 is hereby confirmed. The requirements for emission measurements in accordance with DIN EN 15259:2008 (Measurement of stationary source emissions Requirements for measurement sections and sites and for the measurement objective, plan and report) are fulfilled. Task area G: Gaseous inorganic compounds SO 2 continuous SO 2 Measurement of gaseous emissions I Measurement of sulphur dioxide concentration I Infrared absorption devices UNOR 6 and URAS 2 concentration of sulphur dioxide Reference method VDI 2462 Blatt (guideline withdrawn) DIN EN A A A A Proof-tested NDIR analyser type NO x continuous NOx HCl Determination of mass concentration of nitrogen oxides (NOx) Reference method Chemiluminescence Measurement of gaseous emissions Reference method for the determination of the sum of nitrogen monoxide and nitrogen dioxide Ion chromatographic method Determination of mass concentration of gaseous chlorides expressed as HCl Standard reference method DIN EN VDI DIN EN A A A A A A A NO x continuous Gaseous emission measurement; measurement of nitrogen monoxide in flue gas with the NDUV resonance analyzer (RADAS 1) VDI 2456 Blatt (guideline withdrawn) A Proof-tested NDIR analyser type: Limas CO continuous DIN EN A Determination of mass concentration of carbon monoxide (CO) Reference method: Nondispersive infrared spectrometry Period of validity: to Translation - 2/14

3 Task area G: Gaseous inorganic compounds O 2 Determination of volume concentration of oxygen (O₂) Reference method Paramagnetism DIN EN A O 2, CO, CO 2 Determination of carbon monoxide, carbon dioxide and oxygen Performance characteristics and calibration of automated measuring systems ISO A HF Determination of mass concentration of gaseous fluorine compounds In-house method A As per DIN EN 1911: , validated for HF HF Measurement of gaseous emissions; Measurement of gaseous fluorine compounds / Absorption method VDI 2470 Blatt A A NH 4 + NH 4 + Gaseous emission measurement; determination of basic nitrogen compounds seizable by absorption in sulphuric acid Ammonium VDI 3496 Blatt A A A Biogenic 14 CO 2 Discontinuous sampling of biogenic 14 CO 2 DIN EN ISO A Water vapour Determination of the water vapour in ducts DIN EN A N 2O Gaseous emission measurement Measurement of nitrous oxide Manual gas chromatographic method VDI 2469 Blatt A A SO 3 Measurement of gaseous emissions Determination of sulphur trioxide in water vapour containing exhaust gas Condensation method VDI 2462 Blatt A A A Volume flow Manual and automatic determination of velocity and volume flow rate in ducts Part 1: Manual reference method DIN EN A Period of validity: to Translation - 3/14

4 *) Total of at least 5 different compounds Task area G: Gaseous organic chemical compounds Benzene Tetrachloroethe ne PAH concentration of individual gaseous organic compounds Sorptive sampling method followed by solvent extraction or thermal desorption concentration of individual gaseous organic compounds Sorptive sampling method followed by solvent extraction or thermal desorption Measurement of emissions Determination of polycyclic aromatic hydrocarbons (PAHs) GC/MS method DIN EN DIN EN VDI A A A A A A Period of validity: to Translation - 4/14

5 Task area G: Gaseous organic chemical compounds Toluene concentration of individual gaseous organic compounds Sorptive sampling method followed by solvent extraction or thermal desorption DIN EN A A Xylenes concentration of individual gaseous organic compounds Sorptive sampling method followed by solvent extraction or thermal desorption DIN EN A A Ethyl benzene concentration of individual gaseous organic compounds Sorptive sampling method followed by solvent extraction or thermal desorption DIN EN A A Total carbon, continuous concentration of total gaseous organic carbon at low concentrations in flue gases Continuous flame ionisation detector method DIN EN A Hydrocarbons, continuous Determination of the proportion of short-chain hydrocarbons in the TOC of exhaust gases on the basis of VDI 3481 Blatt 2 (C 1/C 2 determination) In-house method A Phenols Measurement of gaseous emissions; Measurement of phenols In-house method A Period of validity: to Translation - 5/14

6 Task area G: Gaseous organic chemical compounds Aldehydes, ketones Measurement of gaseous emissions Measurement of aliphatic and aromatic aldehydes and ketones using the DNPH method Gas washing bottle method VDI 3862 Blatt A A Methane Manual method for the determination of the methane concentration using gas chromatography *) Total of at least 5 different compounds DIN EN A A Task area P: Particulate compounds and chemical compounds adsorbed on particles Dust, Filter head unit Measurement of particles Dust measurement in flowing gases Gravimetric determination of dust load VDI 2066 Blatt A A Dust, plan filter head unit Determination of low range mass concentration of dust Part 1: Manual gravimetric method DIN EN A A PAH Measurement of emissions Determination of polycyclic aromatic hydrocarbons (PAHs) GC/MS method VDI A A Emission analytics Arsenic (As) EN Cadmium (Cd) EN Period of validity: to Translation - 6/14

7 Task area P: Particulate compounds and chemical compounds adsorbed on particles Nickel (Ni) EN Lead (Pb) EN Mercury (Hg) Air quality Stationary source emissions Manual method of determination of the concentration of total mercury DIN EN and Corrigendum A Chromium (Cr) EN Cobalt (Co) EN Copper (Cu) EN Manganese (Mn) EN Antimony (Sb) EN Period of validity: to Translation - 7/14

8 Task area P: Particulate compounds and chemical compounds adsorbed on particles Thallium (Tl) EN Vanadium (V) EN Metals / semimetals, particulate and filterable Cd, Tl, As, Co, Ni, Se, Te, Sb, Pb, Cr, Cu, Mn, V, Sn, Be, Zn VDI 3868 Blatt Soot Measurement of particles Dust measurement in flowing gases Measurement of smoke number in furnaces designed for EL-type fuel oil VDI 2066 Blatt Valid guideline is used PM 10 and PM 2,5 Particulate matter measurement Dust measurement in flowing gases Measurement of PM 10 and PM 2,5 emissions at stationary sources by impaction method *) Total of at least 7 dust components (without PAH) VDI 2066 Blatt A Task area Sp: Special sampling of substances requiring additional effort for sampling or analysis Component Standard / Guideline / Technical rule SRM QM PCDD/PCDF concentration of PCDDs/PCDFs and dioxin-like PCBs Part 1: of PCDDs/PCDFs PCB concentration of PCDDs/PCDFs and dioxin-like PCBs Part 4: and analysis of dioxin-like PCBs DIN EN DIN EN A A A A Period of validity: to Translation - 8/14

9 Test area / ID Group I.2: Determination of emissions Special sampling of substances requiring additional effort for sampling or analysis Component Standard / Guideline / Technical rule SRM QM Determination of minimum temperature Bundeseinheitliche Praxis bei der Überwachung der Emissionen (German federal uniform practice for the monitoring of emissions) BEP In-house method A A Functional testing of thermal elements for the monitoring of minimum temperature Test area / ID Group II.1 and II.2: Verification of proper installation and function and calibration of continuous emission measuring equipment Measurement objective Standard / Guideline / Technical rule SRM QM Certificate of proper installation Quality assurance of automated measuring and electronic data evaluation systems VDI A Functional tests Quality assurance of automated measuring systems Quality assurance of automated measuring and electronic data evaluation systems Calibration Quality assurance of automated measuring systems Quality assurance of automated measuring and electronic data evaluation systems DIN EN VDI DIN EN VDI A A A A A A Period of validity: to Translation - 9/14

10 Test area / ID Group II.1 and II.2: Verification of proper installation and function and calibration of continuous emission measuring equipment Measurement objective Standard / Guideline / Technical rule SRM QM Calibration TNBZ (only for II.2) Functional testing and calibration of measuring instruments for the continuous monitoring of minimum temperature BEP A Functional testing of thermal elements for the monitoring of minimum temperature In-house method A Electronic evaluation of continuous emission measurements BMU circulars of and A Test area / ID Group II.1 and II.2: Verification of proper installation and function and calibration of continuous emission measuring equipment Measurement objective Standard / Guideline / Technical rule SRM QM Calibration of an AMS for the determination of the volume flow Manual and automatic determination of velocity and volume flow rate in ducts Part 2: Automated measuring systems DIN EN ISO , A Dust, plan filters Calibration of an AMS for the determination of the dust content Determination of low range mass concentration of dust Part 2: Automatic measuring systems DIN EN A A Mercury (Hg) Calibration of an AMS for the determination of mercury (Hg) Air quality Stationary source emissions Determination of total mercury: Automated measuring systems DIN EN A Period of validity: to Translation - 10/14

11 Requirements in accordance with immission control modules and DIN 45688:2014 Group V Determination of noise Standard / Guideline / Technical rule QM TA Lärm Sixth general administrative provision to the Federal Immission Control Act; technical guidance on protection against noise TA Lärm including the standards and guidelines specified therein A A BImSchV of (BGBl. I p. 1036) 16th Ordinance on the implementation of the Federal Immission Protection Law (Traffic Noise Ordinance) A AVwV Baulärm General administrative provision on protection against construction noise Noise immissions Valid provision is used Akustik Guideline for noise-related analysis in the planning of shunting and handling stations Valid provision is used Group VI: Determination of vibrations 1) Standard Standard / Guideline / Technical rule QM DIN DIN DIN LAI- Erschütterungs-LL 2000 Vibrations in buildings Part 1: Prediction of vibration parameters Vibrations in buildings Part 2: Effects on persons in buildings Vibrations in buildings Part 3: Effects on structures Notes on the measurement, assessment and reduction of vibration immissions 1) Only for the determination and assessment of short-term effects (blast vibrations) A A A A A Period of validity: to Translation - 11/14

12 2. and analytical determination of particulate immission samples and chemical compounds adsorbed thereon VDI 4320 Blatt VDI 2267 Blatt VDI 2267 Blatt Measurement of atmospheric depositions Determination of dust precipitation according to the Bergerhoff method Determination of suspended matter in ambient air Measurement of the mass concentration of Al, As, Ca, Cd, Co, Cr, Cu, K, Mn, Ni, Pb, Sb, V, Zn as part of dust precipitation by mass spectrometry (ICP-MS) Determination of suspended matter in ambient air Measurement of the mass concentration of As, Cd, Co, Cr, Cu, Ni, Pb, Sb, V and Zn as part of dust precipitation by atomic absorption spectrometry (AAS) 3. Measurement and calculation of noise DIN ISO DIN DIN VDI VDI DIN Parkplatzlärmstudie 2007 VDI DIN ISO DIN and Corrigendum Acoustics Determination of sound power levels of multisource industrial plants for evaluation of sound pressure levels in the environment Engineering method Measurement of noise emitted by machines; airborne noise emission; enveloping surface method; basic method, divided into 3 grades of accuracy Measurement of noise emitted by machines; airborne noise emission; enveloping surface method; chimneys Noises at pipes Computation and measurement of sound propagation in workrooms Measurement and assessment of low-frequency noise immissions in the neighbourhood lfu series: Noise emissions from car parks Sound radiation from industrial buildings (guideline withdrawn) Acoustics Attenuation of sound during propagation outdoors Part 2: General method of calculation Determination of tonal components of noise and determination of a tone adjustment for the assessment of noise immissions Period of validity: to Translation - 12/14

13 The listed methods comply with the requirements of the "Specialist customer certificate for determination in the area of immission control" ("Immission control module") in the version of Competence is confirmed for the testing and technical areas of activity regulated by immission control law Group I No. 1: G, P, Sp; Group I No. 2; Group II No. 1; Group II No. 2; Group V; Group VI The following are authorised to sign for the listed areas regulated by law: Technical responsibility Dr.-Ing. Ute Zunzer Dipl.-Ing. Andreas Wieczorek For the areas [code letters] Group I No. 1: G, P, Sp Group I No. 2: G Group II No. 1:P, G Group II No. 2: G Group V Group VI Dipl.-Ing. Hartmut Prömper Group I No. 2 Deputy with technical responsibility Dipl.-Ing. Michael Heydemann Dipl.-Ing. Hartmut Prömper Dipl.-Ing. Peter Küllertz Dipl.-Ing. Andreas Wieczorek Dipl.-Ing. Stanislav Janz For the areas [code letters] Group I No. 1: G, P, Sp Group II No. 1: P, G Group I No. 1: G, P, Sp Group I No. 2: G Group II No. 1: G Group II No. 2: G Group V Group VI Group I No. 1: G, P, Sp Group I No. 1: G, P, Sp Period of validity: to Translation - 13/14

14 Abbreviations used: BEP BImSchV BMU VDI Bundeseinheitliche Praxis bei der Überwachung der Emissionen (German federal uniform practice for the monitoring of emissions) Federal Immission Control Ordinance Bundesministerium für Umweltschutz (Federal Ministry for the Environment) Verein Deutscher Ingenieure (Association of German Engineers) Period of validity: to Translation - 14/14