Introduction Engine Test Solutions Industrial Plant Solutions Fleet Maintenance Solutions

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1 Fluid Analysis Solutions 2018

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3 Table of Contents Introduction Engine Test Solutions Industrial Plant Solutions Fleet Maintenance Solutions Portable Oil Analysis Tools FieldLab FluidScan FerroCheck MiniVisc FDM Soot Meter...59 Oil Analysis Laboratory Instruments SpectroTrack...63 SpectrOil M Series...65 SpectrOil LaserNet T2FM Application Specific Instruments BioDiesel/Ethanol...81 Oil in Water...83 SpectrOil M/N-W...85 FluidScan 1210 BN Analyzer...87 CoolCheck SpectrOil M/F-W...91 Service and Support...93 Product Catalog 3

4 Introduction About Spectro Scientific Inc. Spectro Scientific, an ISO 9001:2008 company, specializes in analytical tools and software for machine condition monitoring. Founded in 1983, the company is one of the largest suppliers of oil, fuel and fluid analysis instruments to industry and the military worldwide. The company headquarters is in Chelmsford, MA, United States, and a research & development and sales/ marketing branch is located in Beijing, China. With the support of over 50 global sales and service representative companies, Spectro Scientific products are used in over 100 countries. Industry clients include petrochemical, mining, transportation, oil & gas exploration and power generation companies as well as commercial testing laboratories. Spectro Scientific company timeline Spectro Inc. founded Acquired by Qinetiq NA Acquired by SFW Acquired Wilks Enterprise Spectro Scientific rebrand launch Completed industry oil analysis solution offering Spectroil M was approved by JOAP with first contract Acquired 5200 MiniLab from Emerson Acquired On-Site Analysis Inc. Acquired LaserNet Fines from LMCO 4 Product Catalog

5 Oil & Grease Analysis Solutions Oil in Water/Soil Analyzers Fuel Analysis Instruments Applications and technologies Spectro Scientific s focus in fluid analysis can be divided into three areas: n Fluid nondestructive testing (NDT) and machine condition based maintenance (CBM). This includes new and in-service fluid analysis for lubricants and greases, coolants and hydraulic fluids. We provide lab instruments, on-site oil analysis systems, and portable tools for a variety of customer needs. n Fuel and biofuel analysis for quality control and incoming inspection for blending plants (producers) and power plants (consumers) of fuels to ensure quality fuel is produced and delivered. n Oil in water or soil for environmental compliance testing of discharged water for EPA agencies, oil drilling sites and industrial plants. Spectro Scientific has focused on providing quick and high quality fluid analysis in labs, on-site, or in the field with easy to use, environmental friendly solutions. This mission is supported by our extensive and growing intellectual property portfolio. Spectro Scientific currently owns and exclusively licenses over 70 patents covering all product lines. They can be divided into several core measurement technologies including: n Optical Emission Spectroscopy (OES) for elemental analysis of oil, fuel, coolant and water n FPQ-XRF for wear particle analysis in oil n LaserNet Fines laser imaging particle analysis and ferrous particle analysis in oil n InfraRed absorption spectroscopy for fluid property analysis n Solvent free kinematic viscosity for temperature controlled viscosity measurement in the field n Headspace fuel vapor analysis using Surface Acoustic Wave sensor n UV-Vis and NIR dual absorption spectroscopy for coolant and diesel exhaust fluid analysis n Sample introduction technologies that enable high quality test data with small sample volume and no need for solvent use This unique set of IPs in hardware design and measurement technologies, combined with software and expert systems for diagnostics and recommendations, enables Spectro Scientific to provide comprehensive and easy to use systems, such as the MiniLab EL Series, MiniLab Series, MicroLab Series, and FieldLab Series, that are a fraction of the cost of setting up a full laboratory with comparable data quality for test reporting and analysis. Product Catalog 5

6 Our commitment to quality and performance Over the years Spectro Scientific has contributed greatly to the advancement of oil analysis by initiating and publishing new ASTM standards. With recent publication of several new standards majority of the products now have designated ASTM standards.this gives our customers the peace of mind of instrument performance and data integrity when they use the products in various environments and applications. Below is a list of products and their designated ASTM standards. PRODUCT METHOD TITLE SpectrOil M or 100 Series D6595 Standard Test Method for Determination of Wear Metals and Contaminants in Used Lubricating Oils or Used Hydraulic Fluids by Rotating Disc Electrode Atomic Emission Spectrometry SpectrOil M or 100 Series D6728 Standard Test Method for Determination of Contaminants in Gas Turbine and Diesel Engine Fuel by Rotating Disc Electrode Atomic Emission Spectrometry LaserNet 200 Series D7596 Standard Test Method for Automatic Particle Counting and Particle Shape Classification of Oils Using a Direct Imaging Integrated Tester SpectroVisc 300 Series D7279 Standard Test Method for Kinematic Viscosity of Transparent and Opaque Liquids by Automated Houillon Viscometer Fluidscan 1000 Series D7889 Standard Test Method for Field Determination of In-Service Fluid Properties Using IR Spectroscopy T2FM 500 D7690 Standard Practice for Microscopic Characterization of Particles from In-Service Lubricants by Analytical Ferrography FDM 6000 Series D8004 Standard Test Method for Fuel Dilution of In-Service Lubricants Using Surface Acoustic Wave Sensing MiniVisc 3000 Series D8092 Test Method for Coupled Particulate and Elemental Analysis using XRF for In-Service Lubricants FerroCheck 2000 Series D8120 Standard Test Method for Ferrous Debris Quantification FieldLab 58 FPQ-XRF D8127 Test Method for Coupled Particulate and Elemental Analysis using XRF for In- Service Lubricants MicroLab Series D7417 Standard Test Method for Automatic Particle Counting of Lubricating and Hydraulic Fluids Using Dilution Techniques to Eliminate the Contribution of Water and Interfering Soft Particles by Light Extinction Spectro 5200 D7416 Standard Practice for Analysis of In-Service Lubricants Using a Particular Five-Part (Dielectric Permittivity, Time-Resolved Dielectric Permittivity with Switching Magnetic Fields, Laser Particle Counter, Microscopic Debris Analysis, and Orbital Viscometer) Integrated Tester Soot Meter D7686 Standard Test Method for Field-Based Condition Monitoring of Soot in In-Service Lubricants Using a Fixed-Filter Infrared (IR) Instrument InfraCal Trans-SP D7066 Standard Test Method for dimer/trimer of chlorotrifluoroethylene (S-316) Recoverable Oil and Grease and Nonpolar Material by Infrared Determination 6 Product Catalog

7 High Performance Engine Test Solutions Optimize performance Detect problems early Ensure safety in operation

8 Engine Oil Analysis: A Reliable Technique for Engine Condition Monitoring Engine oil analysis is a reliable and mature non-destructive testing (NDT) technique used to monitor the condition of the engine in development, on the production line and for in-service maintenance. High performance reciprocating engines and jet turbines are complicated mechanical systems with many high-speed moving parts. Comprehensive engine oil analysis provides a complete picture of engine wear and other mechanical failures in addition to lubricant condition and contamination, in almost real time with a small amount of oil. This information advances engine design and development, ensures quality in production and reduces maintenance and repair costs. CONTAMINATION ENGINE WEAR Elemental wear analysis Total ferrous measurement Fuel dilution Coolant leak Water Soot Sand and dirt OIL CONDITION Viscosity Total Base Number (TBN) Oxidation, Sulfation, Nitration Antiwear additive depletion Total Acid Number (TAN natural gas engines only) 2 8 MiniLab Product Catalog EL Series

9 ENGINE TEST SOLUTIONS The need for real time engine oil analysis for high performance engines Achieving and maintaining optimal performance from high performance engines in airplanes, racing cars or locomotives requires much care in engineering, production, and maintenance due to size, high speed or high power output. They also need great sensitivity in oil analysis as only a few parts per million (ppm) of trace metals in the oil can indicate abnormal wear of a critical part. Near real time, lab quality engine oil analysis can significantly improve the productivity of research and development, production quality, and performance and reliability of these engines. MiniLab EL Series: A new non-destructive tool for use throughout an engine s lifecycle The new MiniLab EL Series oil analyzer is an ideal non-destructive testing (NDT) tool for engineers in research and development, production QC or in-service maintenance. The MiniLab EL system allows organizations to gain deep insights into engine and lubricant condition when and where it is needed. HIGH PERFORMANCE n Comprehensive (up to 36 parameters) n Full ASTM compliance n Wear, contamination, oil condition CONVENIENT n Fast (less than 5 minutes) n No sample preparation n No special facility requirements ENVIRONMENTALLY FRIENDLY n Low waste (total 4ml of oil used) n No solvent n No hazardous chemicals EXPANDABLE n Extended metals (up to 31 elements) n Coolant analysis n Fuel analysis MiniLab EL Series Product Catalog 93

10 MiniLab EL Series 5 simple tests to comprehensive engine oil analysis Oil Chemistry ASTM D microliters of oil with no sample preparation 1 minute test time No solvent or chemicals Viscosity ASTM D microliters of oil with no sample preparation 2 sec- 6 min, viscosity dependent Temperature controlled at 40C No solvent or chemicals Elements ASTM D ml of oil with no sample preparation 30 seconds test time No solvent or chemicals 24 elements by default 4 10 MiniLab Product EL Catalog Series

11 ENGINE TEST SOLUTIONS Location: Unit ID: Model: Machine Type: P42 LE Ciara Stbd Main Engine E Engine, Diesel: Liquid-Cooled Viscosity at 40 is not consistent with the stated grade. Edward O'Dwyer, 20 Jun 2017 Oil Maxol HD Marine 1240 Sample ID 671F23 R F67 R BE R R R4703 Note: Sampled on 08 Jun Jun May May Apr 2017 Received on 15 Jun Jun May May May 2017 Km Total Km Oil Top up (l.) Fuel Dilution Total Ferrous Warning Limits Iron ppm Chromium ppm 10 <1 <1 <1 <1 <1 Nickel ppm <1 <1 <1 <1 <1 Molybdenum ppm <1 1 <1 <1 <1 Aluminium ppm ASTM D WEAR METALS Lead ppm 10 <1 <1 <1 <1 <1 Copper ppm 10 <1 <1 <1 <1 <1 Tin ppm 5 <1 <1 <1 <1 <1 Silver ppm <1 <1 <1 <1 <1 Titanium ppm <1 <1 <1 <1 <1 Silicon ppm ASTM D CONTAMINANT Sodium ppm S Vanadium ppm <1 <1 <1 <1 <1 Calcium ppm Magnesium ppm Phosphorus ppm ASTM D ADDITIVES Zinc ppm Barium ppm <1 <1 <1 <1 <1 Boron ppm <1 <1 <1 <1 <1 Viscosity cst ASTM D445 at 40 C Viscosity at 100Â C cst TBN mg KOH/g < Water ppm < <10.0 ASTM E2412 Oxidation By-Products abs/mm Glycol (Antifreeze) % Soot %wt Fuel Dilution % ASTM D8004 ASTM D8120 Date 29 Aug ml of sample with no sample preparation 2 ml sample with no sample preparation Sample report 1 minute test time 30 sec test time No solvent or chemicals No solvent or chemicals MiniLab EL Series Product Catalog 115

12 MiniLab Software Suite The MiniLab Software Suite is powerful yet easy to use and includes two components: the MiniLab Device Console (MDC) and the MiniLab LIMS. The MiniLab Device Console is installed on a local PC and controls: n Sample or asset ID entry n Instrument operation n Data acquisition n Automatic data transfer to LIMS system MiniLab device console Analysis Trend Charts Irish Naval Service Location: P42 LE Ciara Location: Unit ID: Model: Machine Type: P42 LE Ciara Stbd Main Engine E Engine, Diesel: Liquid-Cooled Viscosity at 40 is not consistent with the stated grade. Edward O'Dwyer, 20 Jun 2017 Oil Maxol HD Marine 1240 Sample ID 671F23 R F67 R BE R R R4703 The MiniLab LIMS is a browser-based tool; it can be installed on local PCs, local networks, or hosted in the cloud server. MiniLab LIMS includes: n Asset management n Alarm limits and alarm management n Customizable reports, including multi-parameter trend graphs n Enhanced notification and options n Option to support multiple MiniLab EL Series analyzers in different locations across an enterprise Sampled on 08 Jun Jun May May Apr 2017 Note: Received on 15 Jun Jun May May May 2017 Km Total Km Oil Top up (l.) Warning Limits Iron ppm Chromium ppm 10 <1 <1 <1 <1 <1 Nickel ppm <1 <1 <1 <1 <1 Molybdenum ppm <1 1 <1 <1 <1 Aluminium ppm ASTM D WEAR METALS Lead ppm 10 <1 <1 <1 <1 <1 Copper ppm 10 <1 <1 <1 <1 <1 Tin ppm 5 <1 <1 <1 <1 <1 Silver ppm <1 <1 <1 <1 <1 Titanium ppm <1 <1 <1 <1 <1 Silicon ppm ASTM D CONTAMINANT Sodium ppm S Vanadium ppm <1 <1 <1 <1 <1 Calcium ppm Magnesium ppm Phosphorus ppm ASTM D ADDITIVES Zinc ppm Barium ppm <1 <1 <1 <1 <1 Boron ppm <1 <1 <1 <1 <1 ASTM D445 Viscosity at 40 C cst Viscosity at 100Â C cst TBN mg KOH/g < Water ppm < <10.0 ASTM E2412 Oxidation By-Products abs/mm Glycol (Antifreeze) % Soot %wt Fuel Dilution % Date 29 Aug MiniLab Product EL Catalog Series

13 MiniLab 143EL or 123EL Two MiniLab EL Series models are available: MiniLab 143EL Elements, Oil Chemistry, Viscosity, Fuel Dilution, Total Ferrous MiniLab 123EL Elements, Oil Chemistry, Viscosity PARAMETER Elements ASTM D6595 MiniLab 123EL Oil Chemistry ASTM D7889 MiniLab 143EL Viscosity ASTM D8092 Fuel Dilution ASTM D8004 Total Ferrous ASTM D8120 ENGINE TEST SOLUTIONS Contamination Boron, Sodium, and Potassium Water Soot Glycol Fuel dilution Chemistry Total Base Number (TBN) Oxidation, Nitration, and Sulfation Additive depletion (ZDDP) Total Acid Number (TAN) for NatGas engines and lube oils Magnesium, Calcium, Barium, Zinc, Molybdenum, and Phosphorus Viscosity Wear Total Ferrous Copper, Silver, Chromium, Titanium, Aluminum, Nickel, Iron, Manganese, Lead, Tin, Cadmium, and Vanadium Optional Accessories Two other instruments complement the MiniLab EL Series: The SootMeter extends MiniLab EL soot in engine oil measurement up to 15% by measuring infrared absorption at a fixed wavelength. n ASTM Method D7686 n 1 ml sample volume with no sample preparation n 30 seconds test time n No solvent needed for cleaning n Battery powered n Measurement range: 0-15% soot The CoolCheck 2 provides measurement and profiling of coolant condition with a near IR (NIR) and UV/Visible dual spectrometer design that measures 8 different properties in less than 45 seconds. n 15 ml sample volume with no sample preparation n 45 second test time n No solvents needed for cleaning n Parameters reported are: Type of coolant Clarity Contamination Freeze point Glycol content Boiling point Nitrites MiniLab EL Series Product Catalog 137

14 MiniLab EL Series Product Information PART NUMBER MiniLab 123EL with SpectroTrack LIMS, 115VAC, 60Hz MiniLab 123EL with SpectroTrack LIMS, 230VAC, 50Hz MiniLab 123EL with SpectroTrack LIMS, 115VAC, 50Hz MiniLab 123EL with SpectroTrack LIMS, 230VAC, 60Hz MiniLab 143EL with SpectroTrack LIMS, 115VAC, 60Hz MiniLab 143EL with SpectroTrack LIMS, 230VAC, 50Hz MiniLab 143EL with SpectroTrack LIMS, 115VAC, 50Hz MiniLab 143EL with SpectroTrack LIMS, 230VAC, 60Hz ACCESSORIES AND CONSUMABLES MiniLab 123EL standard accessories MiniLab 123EL consumables kit for 500 samples MiniLab 143EL standard accessories MiniLab 143EL consumables kit for 500 samples MiniLab 123EL validation standards kit MiniLab 143EL validation standards kit M99903 Coolant analysis capability program for SpectrOil 120C (factory install) MiniLab tray assembly for FluidScan and MiniVisc Coolcheck 2, 115/220VAC, Coolcheck 2 standard accessories InfraCal 2 Soot Meter PRODUCT INFORMATION Applications Methodology Calibration OPERATIONAL SPECIFICATIONS Environmental requirements: Sample volume Mineral and synthetic lubricants including gear, engine, hydraulic, turbine and distillate fuels ASTM D6595, D8120, D8092, D7889, D8004 Factory calibrated, field calibration not required. Validation and standardization fluids supplied C ambient temperature, 10-80% RH non-condensing < 5 ml POWER REQUIREMENTS Power MECHANICAL SPECIFICATIONS Dimensions (H x W x D) Weight COMPLIANCE CE Mark-EMC directive, RoHS. ANALYTICAL RANGE 1 phase power, 1200W maximum (123EL and 143EL) MiniLab 123EL: 71 cm x 183 cm x 66 cm (28 x 72 x 26 ) MiniLab 143EL: 71 cm x 214 cm x 66 cm (28 x 84 x 26 ) MiniLab 123EL: 76 kg (167 lbs) MiniLab 143EL: 82 kg (180 lbs) Output Analytical Range Repeatability Elemental concentration of 24 elements, ppm Range and repeatability varies with element Total ferrous, ppm 0-10,000 ppm 3% RSD Fuel dilution % 5% RSD + 0.2% fuel dilution 40 C Kinematic viscosity, cst 100 C kinematic viscosity calculated from V40C and Viscosity Index cst at 40 C cst at 40 C 3% RSD 5% RSD Total Acid Number (TAN), mg KOH/g 0-6 mg KOH/g 3% RSD Total Base Number (TBN), mg KOH/g 0-70 mg KOH/g 3% RSD Oxidation, abs/0.1 mm % RSD Nitration, abs/cm % RSD Sulfation, abs/0.1 mm % RSD Soot 0-2% 3% RSD Glycol % 3% RSD Additive depletion (ZDDP) 0-100% 3% RSD Water, dissolved ppm *Oil specific. RSD = Relative Standard Deviation. 100 ppm-saturation* 3% RSD Solvents: None required USER INTERFACE SPECIFICATIONS Software/operating system Personal computer with Windows 7 Pro or Win 10, 32 or 64 bit, US English version. Quad core microprocessor speed 2.6 GHz or higher and 8 GB RAM minimum. Validation standards for MiniLab 143EL Consumables for MiniLab 143EL To learn more about Spectro Scientific products please call or visit us online at Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 14 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. Engine_BRv1_

15 Industrial Plant Solutions Maximize machine uptime Extend oil drains Prevent premature failures

16 In-service Oil Analysis for Machine Condition Monitoring Since the reliable operation of high value, fixed assets is critical to all industrial plants, predictive maintenance programs are implemented to manage machinery uptime. In-service oil analysis is a key machine condition monitoring technique for Condition Based Maintenance (CBM) and Reliability programs. It complements vibration analysis, thermography and other predictive maintenance technologies. In the time it takes external laboratories to return oil sample results, machinery condition can change significantly. On-site oil analysis eliminates this wait and enables immediate decision making. Corrosion and wear cause surface degradation of the lubricated surfaces in machinery and are the root causes of most mechanically-induced equipment downtime. Corrosion is caused by water or other fluids reacting with metal surfaces, while wear is caused by surface abrasion, adhesion and fatigue. Oil analysis provides early indications of equipment wear and identifies the root causes of corrosion. ONSET OF FAILURE The P-F Curve (Potential- Failure Curve) illustrates how in-service oil analysis provides critical information on machine condition in both Proactive and Predictive Maintenance periods. In the Proactive period, oil condition and contamination monitoring help prevent the onset of the root causes of machine failure. In the Predictive period, monitoring the increasing severity of wear particles allows maintenance work orders to be executed for component replacement or repair before catastrophic failure. OPTIMAL WORKING CONDITION FAILURE EQUIPMENT CONDITION PROACTIVE MAINTENANCE Monitor Oil Condition & Contamination: Viscosity, oil chemistry, water Particle count with ISO codes Elemental analysis of normal wear particles Total ferrous PREDICTIVE MAINTENANCE Monitor for Abnormal Wear: Total ferrous Wear particle analysis Elemental analysis EQUIPMENT FAILS COST TO REPAIR OPERATING HOURS 2 Industrial Solutions 16 Product Catalog

17 As part of a proactive maintenance program, on-site oil analysis delivers rapid results with immediate decision making to: n Lower operating costs n Reduce unscheduled downtime n Increase machine availability n Extend equipment life n Decrease total lifecycle equipment costs n Provide immediate retest capability Trivector oil and machine health simplified The TriVector is a simple representation of the integrity of the lubrication system and the health of the machine itself. The Trivector indicates the degree of health in each vector. Each vector is a representation of Alarm Limits based on underlying parameters, such as viscosity, water contamination, acid number, oxidation, total ferrous, particle count and ISO code, large ferrous particle count, etc. The following questions can be answered: INDUSTRIAL PLANT SOLUTIONS Is the machine healthy? Can I predict when the machinery will fail? Is the oil dry? Is the oil clean/ free of dirt? Is it the right oil? Is the oil fit for use? Industrial Solutions 3 *Trivector is a trademark of Emerson Process Systems Product Catalog 17

18 MiniLab Series 4 simple tests and less than 15 minutes to comprehensive oil analysis Can be operated on-site by plant staff; no chemist required. ELEMENTAL ANALYSIS The elemental analyzer provides measurement of 24 elements to identify individual contaminants, wear metals and the elemental composition of additives. PARTICLE COUNT AND FERROUS MONITOR The direct imaging particle counter and ferrous monitor provides particle counts and ISO codes, wear classification, ferrous particle counts & size distribution, and total ferrous measurement. VISCOSITY The portable viscometer provides high accuracy 40 C kinematic viscosity measurements. 4 Industrial Solutions 18 Product Catalog

19 Trivector reports on machinery health Easy to interpret results with Trivector sample and trend reports. Sample Trend - Spectro Scientific Database Area Plant Boston.rbm U1 - Unit One Reference Oil Chevron - GST - 32 Sample Date 11/29/2016 9/27/2016 7/28/2016 4/25/2016 1/3/2016 Sample ID Machine Wear Total Fe, ppm Fe >25, pml Fe >38, pml Fe >50, pml Fe >100, pml Wear Class MxD Ct >20, pml MxD Ct >50, pml MxD Ct >100, pml MxD Sl >20, pml MxD Sl >50, pml MxD Sl >100, pml MxD Ft >20, pml MxD Ft >50, pml MxD Ft >100, pml Contamination ISO > ISO > ISO > MxD Ox >20, pml Equipment Point U1 Turbine - Unit 1 Turbine P1 - Before Filter Machine Wear Contamination INDUSTRIAL PLANT SOLUTIONS MxD Ox >50, pml MxD Ox >100, pml Cnts >4, pml Cnts >6, pml Cnts >10, pml Cnts >14, pml Cnts >18, pml Cnts >21, pml Cnts >26, pml Cnts >32, pml Chemistry Cnts >38, pml Cnts >56, pml Cnts >70, pml Water, ppm Chemistry Visc 40C, cst TAN, mg KOH/g IR Oxid., Abs/mm CHEMICAL ANALYSIS The infrared spectrometer measures Total Acid Number (TAN), oxidation and water for machinery oils and hydraulics. Industrial Solutions Product Catalog 195

20 MiniLab Series Software The MiniLab Series software is based on a Laboratory Information Management System (LIMS) designed for oil analysis. It includes an asset management database, a reference oil database and reports. The software supports multiple databases and is available with single user or optional network configurations. Simple, easy to use GUI Asset management Each asset in a database is structured as an Area/ Equipment/Point/Sample. A Sample has a time stamp and unique Sample ID and is created at the Point asset level. Reference oil database. A reference oil is assigned to each asset to allow trending comparison to new oil properties. Schedule oil samples for routine sampling intervals. Alarms Color-coded Trivector reports provide a clear snapshot of machinery health by identifying parameters that are outside normal limits. Several parameters in each category of Wear-Chemistry-Contamination are assigned limits. The measured values of these parameters compared to these limits are used to generate the Trivector plot of machinery health. Alarm Limits are initially established for key parameters from the templates provided in the software, machinery component specifications, industry standard recommendations or from user-defined criteria. Industry best practice is to refine Alarm Limits based on machine history. Once a series of measurements is made, the initial alarm limits can be analyzed and adjusted. ALARM ALERT WITHIN LIMITS The Trivector shown has chemistry & viscosity within normal limits, wear in an alert condition, and contamination in an alarm condition Industrial Product Catalog Solutions

21 Reports Standard and user configurable reports can be automatically generated. The following Spectro Scientific trend report provides a concise report with multiple parameter trend plots. Sample Trend - Spectro Scientific Database Plant Boston.rbm Area U1 - Unit One Reference Oil Chevron - GST - 32 Sample Date 11/29/2016 9/27/2016 7/28/2016 4/25/2016 1/3/2016 Sample ID Machine Wear Total Fe, ppm Fe >25, pml Fe >38, pml Fe >50, pml Fe >100, pml Wear Class MxD Ct >20, pml MxD Ct >50, pml MxD Ct >100, pml MxD Sl >20, pml MxD Sl >50, pml MxD Sl >100, pml Equipment Point U1 Turbine - Unit 1 Turbine P1 - Before Filter Sample Trend - Spectro Scientific Database Plant Boston.rbm Area U1 - Unit One Machine Wear Equipment Point U1 Turbine - Unit 1 Turbine P1 - Before Filter INDUSTRIAL PLANT SOLUTIONS MxD Ft >20, pml MxD Ft >50, pml MxD Ft >100, pml Contamination ISO > ISO > ISO > MxD Ox >20, pml Contamination MxD Ox >50, pml MxD Ox >100, pml Cnts >4, pml Cnts >6, pml Cnts >10, pml Cnts >14, pml Cnts >18, pml Cnts >21, pml Cnts >26, pml Cnts >32, pml Chemistry Cnts >38, pml Cnts >56, pml Cnts >70, pml Water, ppm Chemistry Visc 40C, cst TAN, mg KOH/g IR Oxid., Abs/mm Trend Report Provides data and multiple parameter plots for a series of samples from the same component. Thumbnail images of wear particles Industrial Solutions Product Catalog 217

22 MiniLab Evolution 5200 MiniLab vs MiniLab 153 The MiniLab Series is the next generation of Trivector on-site oil analyzers replacing the 5200 MiniLab MINILAB MINILAB 153 Wear Large Ferrous content, trending only Total ferrous particle content (ppm) Wear Debris Analysis (WDA) (Optional) Wear Debris Analysis (WDA) (Optional) Automatic wear particle shape classification, count & distribution Ferrous particle count & distribution (> 25 µm) Wear elements: Fe, Cu, Pb, Mg, Ag, Sn Contamination Particle count & distribution, ISO codes Particle count & distribution, ISO codes Emulsified water only Dissolved water (ppm) Free water (ppm) Glycol contamination for engine oils Contaminate elements: Si, Na Chemistry Dynamic room temperature Kinematic 40 C Dielectric, trending only Oxidation Total Acid Number (TAN) Nitration, Sulfation, Anti-wear additive, Total Base Number (TBN), and soot for engine oils Additive elements: Ca, P, Zn, Mg, Ba, Mo Application Typical mineral and synthetic lubricant and hydraulics oils for industrial rotating machinery. Not suitable for backup generators. Mineral and synthetic lubricant and hydraulics for industrial rotating machinery, plus engine oil for backup generators and ground fleet, and special lubricants such as phosphate esters and PAG. Oil library database The MiniLab Series includes an extensive industrial oil library database to analyze in-service oils as a variety of lubricants and fluids are used in industrial equipment. The following fluid categories can be tested: FLUIDS ELEMENTAL CHEMISTRY PARTICLE COUNT & FERROUS Mineral oil based Hydraulic fluids and lubricants Y Y Y Y Synthetic hydrocarbon based hydraulic fluids and lubricants Y Y Y Y Ester-based Lubricant blends Y Y Y Y Oil Soluble Polyglycols (OSP) Y Y Y Y Organic Esters (OE) Y Y Y Y Phosphate Esters (Fyrquel/Skydrol) Y Y Y 1 Y Polyalkylene Glycols (PAG) Y Y Y 1 Y Poly Alpha Olefins (PAO) Y Y Y Y Polyinternal Olefins Y Y Y Y Polyol Esters (POE) Y Y Y Y Grease Y Y 2 N N Mineral Transformer Oil Y N Y Y 1: Require factory installed Skydrol tube and fitting kits and compatible solvent 2: Oxidation and water (absorbance units) for trending VISCOSITY 8 22 Industrial Product Catalog Solutions

23 Typical limits for machinery The most common oil analysis tests and typical alarm limits for several component types are shown below. Component manufacturers establish alarm limits for their equipment for specified parameters. MEASUREMENT TURBINES GEAR BOXES HYDRAULICS ENGINES Particle Count / ISO Code < 18/14/12 < 19/16/13 < 15/13/11 Water < 100 ppm < 1,000 ppm < 150 ppm < 2,500 ppm Glycol 0.1% max Fuel dilution 5% max Viscosity + 15% / - 10% of nominal ISO + 15% / - 10% of nominal ISO + 15% / - 10% of nominal ISO + 20% to - 10% of nominal SAE TAN Baseline mg KOH/g max Baseline mg KOH/g max Baseline mg KOH/g max TBN 20% of Baseline mg KOH/g min Sodium < 40 ppm Boron < 20 ppm Aluminum, Chromium, Tin < 15 ppm Iron, Lead < 100 ppm Silicon < 10 ppm Copper < 30 ppm < 40 ppm Zinc < 2 ppm INDUSTRIAL PLANT SOLUTIONS Particle analysis and wearing mechanism With total ppm, ferrous particles, LaserNet total particles and the wear classifier results, users can make informative actionable decisions by identifying oil drain points, corrosive wear and the onset of a serious abnormal machine wear mechanism. MONITORING TOTAL Fe PPM FERROUS PARTICLES >20 µm LASERNET LARGE PARTICLES >20 µm LASERNET CLASSIFIER Oil change interval Onset of corrossive wear Transition into abnormal wear mode Ongoing severe wear mechanism (breakdown shear mixed layer) Temporary wear rate change due to increased load and speed Establish constant wear rate Dynamic equilibrium levels Dynamic equilibrium levels Dynamic equilibrium levels Reaches limit level Increase in rate Increase in rate Same or decrease in rate NA No change Increase Increase NA No change Increase Increase NA No change Increase in rate No change No change No change Increase cutting/sliding/fatigue Increase cutting /sliding/ fatigue Onset of external contamination No change No change Increase Increase non-metallic 3 Body abrasive mechanism iron No change Increase Increase Increase cutting/sliding 3 Body abrasive mechanism non-ferrous (copper, aluminum) No change No change Increase Increase cutting/sliding Onset of rolling contact failure No change Increase Increase Increase fatigue Industrial Solutions Product Catalog 239

24 Wear particle by metal type Contamination ID by source Oil additive levels Elemental Analysis The SpectrOil 100 Series analyzes small particulate wear, lubricant additives and contaminants for trace quantities of elements dissolved or suspended as fine particles. Using the proven rotating disc electrode (RDE) technique, the SpectrOil 100 Series has become the workhorse of industrial, commercial and military oil analysis laboratories requiring rapid analysis of wear metals, contaminants and additives in lubricants. Coolant, wash-down water and JOAP calibrations are available in addition to in-service lubricating oil and hydraulic fluid analysis. n Measures ppm levels of up to 32 elements in less than 30 seconds n Easy to operate no sample preparation, gases, coolants or solvents needed n Compliant with ASTM D6595 for used oil analysis On-site oil analysis provides greater insight into contaminant sources by linking elemental parameters with the probable source: Grating Exit Slits SpectrOil 100 Series instrument can be purchased separately. ELEMENT Sodium Boron Magnesium Calcium Oil Chemistry metallic additives possible sources Corrosion inhibitor additive, also indicates coolant leak into oil, can also be road salt, sea water, ingested dirt Corrosion inhibitor additive, antiwear/antioxidant additive; can indicate coolant leak, grease contamination Detergent/dispersive additive, can also be alloying element in steels Detergent/dispersant additive, alkaline reserve additive for high sulfur fueled engines, can be grease contamination, Fixed Electrode AC Arc Rotating Electrode Entrance Slit Fiber Optic Cable Sample Cup Optics & diffraction grating produce a spectrum SpectrOil 100 Series rotating disc electrode optical emission spectrometer schematic CCDs Molybdenum Solid/liquid antiwear additive, alloy in bearing and piston rings Barium Corrosion inhibitors, detergents, rust inhibitors Emission spectrum of hydrogen Sample consumed using RDE technology is optically analyzed with AE spectroscopy to detect elements. Zinc Phosphorus Antiwear, corrosion inhibitors, anti-oxidants, alloying element for bearings, thrust washers, galvanized cases Antiwear, corrosion inhibitors, anti-oxidants additives, EP additives Emission spectrum of iron Industrial Product Catalog Solutions

25 Particle Count and Ferrous Monitor The LaserNet 200 Series provides particle counts and codes, large wear particle classification and ferrous wear monitoring. n Particle count, size distribution and codes (ISO 4406, NAS 1638, NAVAIR 01-1A-17, SAE AS 4059, GOST, ASTM D6786, HAL, and user defined bins). n Differentiates contaminants (silica and fibers from machine wear metal) n Classifies wear particles, stores images, and reports particle count and size distribution for each wear type of Cutting, Sliding, Fatigue, Fibers and Nonmetallics n Ferrous Monitor measures total ferrous content in the sample and provides Ferrous particle count and size distribution n Widest range up to 5,000,000 particles/ml n Test oil viscosity up to ISO320 without dilution n Images through dark fluids containing up to 2% soot n Error corrections for water and air bubbles Options include an autosampler for high throughput sample processing as well as configurations without the ferrous monitor and wear classification. Ferrous content Wear particle shape Particle count and codes INDUSTRIAL PLANT SOLUTIONS Ferrous Particle Count & Size FILTER SCREEN LaserNet 200 Series instrument can be purchased separately. FLOW CELL CCD CAMERA 640 x 480 resolution 100 frames/s SMALL COIL SET Particle size distribution ISO 4406 cleanliness codes Particle shape classification CUTTING SLIDING CUTTING WEAR FATIGUE WEAR SLIDING WEAR NONMETALLIC FATIGUE x4 Lens Actual Pixel Resoluion NON METALLIC WATER LARGE COIL SET LaserNet 230 flow diagram Ferrous PPM PUMP WASTE Industrial Solutions Product Catalog 25 11

26 Water TAN TBN Oxidation Nitration Sulfation Soot Additive depletion Glycol Chemical Analysis The FluidScan 1000 Series oil chemistry analyzer determines when in-service oil is no longer fit for use due to oil degradation or the ingress of water or glycol. It is fast and easy to use, with just one drop of oil needed for the sample and less than one minute for test results. The analyzer includes an extensive oil library; additional oils can be added by the user. n Compliant to ASTM D7889 Standard Test Method for Field Determination of In-service Fluid Properties Using IR Spectroscopy n High correlation to TAN and TBN laboratory tests conducted with ASTM D664 and D4739 n Patented, Comprehensive Water Measurement option extends range to 6.5%. (Included with all MiniLab systems.) FluidScan 1000 Series handheld infrared spectrometer can be purchased separately. The oil library contains various categories of fluids. The industrial library provided with the MiniLab series includes the Comprehensive Water Solution and the Industrial Fluid Oil Library. CATEGORY ASTM EP Gear/Hydro ASTM Petroleum Crankcase ASTM Polyol Ester BIODIESEL FEEDSTOCK CHILLER ENGINE ENGINE-HEAVY DUTY ENGINE-HFO ENGINE-NAT GAS ETHANOL IN GASOLINE FAME FAME in DIESEL GEAR-PRESSURE GEAR-SPLASH HEAT TRANSFER HYDRAULIC HYDRAULIC-FIRE RESISTANT SLIDEWAY TRANSMISSION TURBINE-AERO TURBINE-CCGT TURBINE-STEAM Industrial Fluid Library FluidScan operating principle COMPREHENSIVE WATER SOLUTION Dissolved and Free Water Measurement Up to 6.5% water 0.03% Water measurement range 6.5% Saturation Limit (Oil Specific) STANDARD RANGE Dissolved Water Measurement Up to saturation limit Industrial Product Catalog Solutions

27 Viscosity Viscosity The MiniVisc 3000 Series provides fast, accurate 40 C kinematic viscosity measurements for easy detection of viscosity variations caused by contamination, mix-up and oil degradation. n Solvent free, portable, and easy to use n Viscosity range C n Accuracy +/- 3% to NIST viscosity standards n Fast results: ISO 15 ~10 seconds, ISO 320 ~ 3 minutes For machinery oils, the 40 C kinematic viscosity is used as the reference value. Engine oils operate at higher temperatures than rotating machinery, so they require V100 C kinematic viscosity. The Viscosity Index of an oil is a parameter that relates the V40 C measurement value to the V100 C value. A reference Viscosity Index value can be entered in the viscometer and both the measured V40 C viscosity and the calculated V100 C viscosity values are displayed. Positive displacement pipette MiniVisc 3000 Series portable viscometer can be purchased separately. INDUSTRIAL PLANT SOLUTIONS Open the two parallel plates for easy cleaning. MiniVisc 3000 Series kinematic viscometer schematic Total Ferrous The MiniLab 33 includes the FerroCheck, a portable ferrous analyzer that measures the total ferrous content of a sample. It is easy to operate; simply insert the sample vial with fluid sample to measure. n Small sample requirement with results in 30 seconds n No sample preparation and no solvents required to clean n Measurement range 0-10,000 ppm for oil, ,000 ppm for grease FerroCheck 2000 Series portable ferrous analyzer can be purchased separately. Grease boat and sample introduction vials Industrial Solutions Product Catalog 27 13

28 Four MiniLab Options. Which One is for You? MiniLab 153 provides a complete oil analysis report with elemental analysis, comprehensive wear particle analysis, solid and water contamination, fluid chemistry and viscosity. It is ideal for large power plants and manufacturing plants with many assets. MiniLab 53 provides a Trivector report with comprehensive wear particle analysis, solid and water contamination, fluid chemistry and viscosity. MiniLab 33 provides a basic Trivector report with total ferrous wear, fluid chemistry, water in oil and viscosity. MiniLab 23 provides basic oil condition information including viscosity, chemistry and water in oil. MiniLab tests MiniLab 53 3 tests MiniLab 33 3 tests MiniLab 23 2 tests PARAMETER Elemental ASTM METHOD D6595 Contamination Particle count and ISO codes Non-metallic particle count, distribution and images Sodium and Silicon Total Water Particle Count and Ferrous ASTM METHOD D7596 Ferrous ASTM METHOD D8120 Chemistry Viscosity Total Acid Number (TAN) Oxidation Total Base Number (TBN), Oxidation, Nitration, and Sulfation for engine oils Viscosity ASTM METHOD D8092 Chemical ASTM METHOD D7889 Magnesium, Calcium, Barium, Zinc, Molybdenum, and Phosphorus Wear Wear particle images, counts and distribution Total Ferrous content, ppm Ferrous particle count and size distribution Copper, Silver, Chromium, Titanium, Aluminum, Nickel, Iron, Manganese, Lead, Tin, Cadmium, and Vanadium Industrial Product Catalog Solutions

29 Accessories & Consumables Sample Preparation Equipment Sample preparation equipment such as the Homogenizer, Ultrasonic Deaerator, Electrode Sharpener and Consumables for 100 samples is included with each MiniLab 153 system. SAMPLE PREPARATION 3 SIMPLE STEPS 1. Sharpen electrode 2. Homogenize the sample for better water measurement 3. Ultrasonically degas the sample for particle analysis Validation Standards and ASTM Standards Validation standards are supplied for all MiniLab Series instrumentation. These NIST traceable standards support internal quality programs and compare current instrument performance against factory calibration. All instruments in the MiniLab Series have an associated ASTM Standard Test Method. Consumables Spectro Scientific consumables are selected and carefully tested with all Spectro Scientific instruments to ensure consistent, repeatable results. Always use Spectro Scientific certified consumables for best results. Accessories A variety of accessories to support your oil analysis program are available, from drawing a sample from an oil sump to preparing it for analysis. INDUSTRIAL PLANT SOLUTIONS PARTICLE COUNTER STANDARD LNF-509 calibration checkfluid SPECTROMETER STANDARDS CS ppm, 900ppm, baseoil FERROUS PARTICLE ANALYZER LNF-545 Ferrous Validation Standard for Magnetometer Total Ferrous Content, nominal 100 ppm Large Ferrous particle count, nominal 42 µm particles FLUIDSCAN IR CHECK FLUID FL310 FluidScan CheckFluid VISCOSITY STANDARDS PV1025 Visc 30 standard PV1026 Visc120 standard Solvent Filtration and Dispenser (A5051SF) Sampling Pump ( ) Wear Debris Anlaysis Kits: 115V ( ) 220V ( ) Service Contracts and Repair Spectro Scientific s service offerings for the MiniLab Series include: System Installation & Training for instrument operation and routine maintenance. Service Contracts for extended warranty and preventive maintenance. Field Repair by certified customer service engineers on site. In-house Instrument Calibration, Maintenance, Repair, and Upgrades performed at our facility near Boston, MA. Industrial Solutions Product Catalog 29 15

30 MiniLab Series Product Information PART NUMBER MiniLab 153 with OilView LIMS and PC, 115 VAC, 60 Hz MiniLab 153, 115 VAC, 60 Hz. Requires OilView LIMS MiniLab 153 with OilView LIMS and PC, 220 VAC, 50 Hz MiniLab 153, 220 VAC, 50 Hz. Requires OilView LIMS MiniLab 153 with OilView LIMS and PC, 240 VAC, 60 Hz Minilab 153, 240 VAC, 60 Hz. Requires Oilview LIMS MiniLab 153 with OilView LIMS and PC, 120 VAC, 50 Hz Minilab 153, 120 VAC, 50 Hz. Requires Oilview LIMS MiniLab 53, 115 VAC, 50/ 60 Hz. Requires OilView LIMS MiniLab 53, 220 VAC, 50/60 Hz. Requires OilView LIMS MiniLab 53, 115 VAC, 50/60 Hz with OilView LIMS MiniLab 53, 220 VAC, 50/60 Hz with OilView LIMS MiniLab 33, 115 VAC, 50/60 Hz. Requires OilView LIMS MiniLab 33, 220 VAC, 50/60 Hz. Requires OilView LIMS MiniLab 33, 115 VAC, 50/60 Hz with OilView LIMS MiniLab 33, 220 VAC, 50/60 Hz with OilView LIMS MiniLab 23, 115 VAC, 50/60 Hz. Requires Oilview LIMS MiniLab 23, 220 VAC, 50/60 Hz. Requires Oilview LIMS MiniLab 23, 115 VAC, 50/60 Hz with Oilview LIMS MiniLab 23, 220 VAC, 50/60 Hz with Oilview LIMS. *OilView LIMS v5.61 or v5.7 is required for MiniLab operation. ACCESSORIES AND CONSUMABLES MiniLab 153 Standard Accessories Kit MiniLab 153 Consumables Kit for 500 samples MiniLab 53 Standard Accessories Kit MiniLab 53 Consumables Kit for 500 samples MiniLab 33 Standard Accessories Kit MiniLab 33 Consumables Kit for 500 samples SA1022 MiniLab 23 Standard Accessories Kit MiniLab 23 Consumables Kit for 500 samples Minilab 153 Validation standards kit Minilab 53 Validation standards kit Minilab 33 Validation standards kit Minilab 23 Validation standards kit MiniLab 153 with Skydrol kit standard accessories MiniLab 53 with Skydrol kit standard accessories LNF-905 Skydrol kit (phosphate ester fluids) for LaserNet 230 only; factory installation FL360 All Libraries license for FluidScan PRODUCT INFORMATION Applications Mineral and synthetic lubricants including gear, engine, hydraulic, turbine and distillate fuels Methodology ASTM D7596, ASTM D7889, ASTM ASTM D6595 Calibration Factory calibrated, field calibration not required. Validation and standardization fluids supplied. OPERATIONAL SPECIFICATIONS Environmental Requirements Sample Volume 5-40 C ambient temperature, 10-80% RH non-condensing, 2000 m maximum altitude ml, varies with viscosity Solvents Lamp oil, odorless kerosene, or Electron 22 USER INTERFACE SPECIFICATIONS Software/Operating System Personal computer with Windows 10 Pro or Windows 7 Pro, 32 or 64 bit, US English version. Quad core microprocessor speed 2.6 GHz or higher and 8 GB RAM minimum. POWER REQUIREMENTS Power MiniLab 153: 1 Phase power, 1200 W (max) MiniLab 53/33/23: 1 Phase power, 110 W (max) MECHANICAL SPECIFICATIONS Dimensions (H x W x D) Weight COMPLIANCE CE Mark-EMC directive, RoHS MiniLab 153: 71 cm x 214 cm x 66 cm (28 x 84 x 26 ) MiniLab 53: 35 cm x 50 cm x 53 cm (13.8 x 19.7 x 21 ) Minilab 33: 14 cm x 69 cm x 48 cm (5.5 x 27 x 19 ) Minilab 23: 10 cm x 51 cm x 48 cm (4 x 20 x 19 ) MiniLab 153: 84 kg (185 lbs) MiniLab 53: 14 kg (31 lbs) MiniLab 33: 9 kg (22 lbs) MiniLab 23: 6 kg (14 lbs) ANALYTICAL RANGE AND REPEATABILITY Output Analytical Range Repeatability Particle count and size distribution Particle count 6% RSD ISO codes per 4402/4406, other codes selectable µm Ferrous particle count and size µm 5% RSD distribution Total Ferrous, ppm 10-2,000 ppm 5% RSD Wear particle counts and size distribution by wear mode : fatique, sliding, cutting,non-metallic, fibers µm 40 C Kinematic viscosity, cst cst at 40 C cst at 40 C 3% RSD 5% RSD Total Acid Number (TAN), mg KOH/g 0-6 mg KOH/g 3% RSD Total Base Number (TBN), mg KOH/g 0-70 mg KOH/g 3% RSD Oxidation, abs/0.1 mm % RSD Nitration, abs/cm % RSD Sulfation, abs/0.1 mm % RSD Water, dissolved ppm 100 ppm-saturation* 3% RSD Water, free, ppm % (300-65,000 ppm) 25% RSD Elemental concentration of 23 elements, ppm *Oil specific. RSD = Relative Standard Deviation. SUPPORT RESOURCES SVC019 Service Contract MiniLab 33 SVC015 Service Contract MiniLab 53 SVC057 Service Contract MiniLab 153 Elemental analysis range and repeatability vary with element Spectro Scientific offers On- and Off-site Product Training, Field Repair, In-house Instrument Calibration, Maintenance, Repair, and Upgrades and Service Contracts. See previous page for more information about service and customer support. To learn more about Spectro Scientific products please call or visit us online at Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 30 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. Industrial_BRv3_

31 Fleet Maintenance Solutions Maximize machine uptime Extend oil drains Prevent premature failures

32 Oil Analysis for Vehicle Preventative Maintenance The reliable operation of vehicles in a fleet is critical in virtually every industry that depends on equipment powered by engines including: n Automotive n Trucking n Energy n Mining n Construction n Government (military and municipal) Maintenance programs are implemented to keep this equipment operating and performing its required work. Downtime not only costs money to repair the equipment but also lost productivity and loss of customer confidence. Oil analysis is a critical part of vehicle maintenance, providing valuable information on the condition of the oil and the health of the vehicle. To be most effective, oil analysis must be used when the mechanic is working on the vehicle so the technician can take immediate action and, if necessary, retest the oil for confirmation. An oil analysis program lowers the risk of a vehicle roadside failure and eliminates the costs involved with having equipment out of service. ONSET OF FAILURE OPTIMAL WORKING CONDITION The longer it takes to identify a problem along the failure curve, the more expensive it becomes to fix the equipment. Oil analysis is used for proactive maintenance to help prevent the onset of failures. In the predictive maintenance stage, oil analysis can identify problems before they become catastrophic failures. FAILURE EQUIPMENT CONDITION PROACTIVE MAINTENANCE PREDICTIVE MAINTENANCE EQUIPMENT FAILS COST TO REPAIR OPERATING HOURS 2 32 Fleet Product Solutions Catalog

33 As part of a proactive maintenance program, on-site oil analysis delivers rapid results with immediate decision making to: n Lower operating costs n Reduce unscheduled downtime n Increase vehicle availability and extend vehicle life Achieving green initiatives with oil analysis Reduction in new oil fill and used oil disposal by extending oil drains can greatly contribute to achieving eco-goals. On-site oil analysis provides information about the oil health while the equipment is being serviced so the mechanic knows instantly if the oil can be safely extended. Extending just one oil drain per vehicle per year can have a significant impact on oil usage and disposal across an entire fleet. 500 HEAVY DUTY TRUCKS Oil analysis can help answer the following questions x 6 = 3000 LESS GALLONS OF OIL LESS USED & LESS DISPOSED EXAMPLE: With an average oil drain of 6 gallons per vehicle, reduction of 1 oil drain per vehicle in a fleet of 500 heavy duty trucks saves 3000 gallons of oil per year. FLEET MAINTENANCE SOLUTIONS SERVICEABLE LIFE OF THE OIL MECHANICAL ISSUES WITH THE EQUIPMENT Is it the right oil? (Right viscosity and additive package) Is the oil clean? (No dirt or dust) Can the oil drain be extended? (Degradation of viscosity or oil chemistry) Is there mechanical failure allowing contamination to enter? (Coolant or dirt) Are the vehicle components in good condition? (Free of abnormal wear debris) Can I predict when a component will fail? (Wear metals present) Is there a coolant or a fuel leak? (Elemental contamination or degradation of viscosity) Fleet Solutions Product Catalog 33 3

34 MicroLab Series FULLY AUTOMATED OIL ANALYSIS The MicroLab combines automation and artificial intelligence in an all-in-one oil analysis tool. 15 minutes to comprehensive oil analysis n Can be operated by maintenance staff, no chemist required n Fully automated operation and cleaning n Easy to understand reports with color-coded alarm limits and diagnostic statements 4 34 Fleet Product Solutions Catalog

35 Four automated oil tests CHEMISTRY The MicroLab Infrared Spectrometer measures six key parameters which indicate potential oil degradation and contamination. Both the MicroLab 30 and 40 provide: Oil degradation: oxidation, nitration, total base number Oil contamination: soot, water, glycol VISCOSITY The MicroLab Dual Temperature Viscometer provides kinematic viscosity analysis which can help identify potential oil degradation or contamination. Both the MicroLab 30 and 40 provide: Kinematic viscosity at 40 C and 100 C Viscosity Index (VI) ELEMENTAL ANALYSIS The MicroLab Optical Emission Spectrometer quantifies wear metals cause from mechanical components, as well as other elements from oil additives or sources of contamination. MicroLab 30 analyzes 10 basic metals: aluminum, chromium, copper, iron, lead, molybdenum, potassium, silicon, sodium, and tin. It is upgradable to include all 20 elements. MicroLab 40 analyzes 20 elements including the basic metals listed above and the extended metals: barium, boron, calcium, magnesium, manganese, nickel, phosphorous, titanium, vanadium, and zinc. PARTICLE COUNT The MicroLab 40 model is equipped with a particle counter to measure particle contamination which is crucial for maintaining hydraulic systems, compressors and turbines. The MicroLab 40 measures: Gross particle count ISO particle size Monitoring equipment and oil health with oil analysis The four automated MicroLab tests provide a complete look at equipment and oil condition. Mechanical condition parameters indicate potential equipment failure: Wear metal analysis Contamination (glycol, dirt, water) Oil condition parameters indicate potential degradation and contamination: Viscosity Oil chemistry (Total Base Number, oxidation, nitration) Contamination (glycol, water, soot, particle count) Oil additive levels Infrared spectrometer Kinematic viscometer OES elemental analyzer Particle counter MicroLab 40 For engines, transmissions, power steering, generators, hydraulics, gear oils MicroLab 30 For engines, transmissions, power steering, generators FLEET MAINTENANCE SOLUTIONS Fleet Solutions Product Catalog 35 5

36 Converting Test Data into Maintenance Actions MicroLab Reports Comprehensive MicroLab report includes color-coded alarm limits, diagnostic statements and trending history. The MicroLab has an embedded expert system that translates chemistry results into diagnostic statements specific to the type of equipment and guides the technician on necessary maintenance actions. The diagnostic statements can indicate whether an oil change is required or if the oil drain interval can be extended. It can also direct the technician to potential mechanical problems to investigate. The comprehensive reports: Save time compiles and analyzes all test data Take the guess work out of interpreting results provides suggested maintenance actions Save money no need to hire an analytical resource Sample history for trending analysis Account: Address: Phone: Vehicle ID: Vehicle Make: Vehicle Model: MICROLAB SYSTEM TEST 1 EXECUTIVE DR CHELMSFORD MA OVER-ROAD FORD Vehicle Year : 2017 Component ID: Component Type : Oil Brand: Oil Type: Oil Weight: Sump Capacity: EXPLORER LIMITED OVER-ROADGSGENERAL GASOLINE ENGINE MOBIL MOBIL 1 FORMULA 5W30 6 QUARTS Viscosity Limit 40 Deg C Viscosity Limit 100 Deg C Diagnosis for current sample HEAVY CONCENTRATION OF WATER PRESENT. CHECK FOR SOURCE OF WATER ENTRY. OIL DRAIN AND REFILL MAY BE NECESSARY. CONSULT SERVICE PROVIDER FOR FURTHER RECOMMENDATIONS. TO CONFIRM, RESAMPLE AT 5,000 MILES (8,000 KM) OR 100 HOURS. Diagnostic statements with maintenance recommendations Legend ABNORMAL SEVERE X = NOT TESTED / - = NOT DETECTED NOT APPLICABLE Analysis Results: Units Current Sample Sample ID Date Analyzed 9/19/2017 9/19/2017 9/19/2017 9/19/2017 Date Sample Taken 9/19/2017 9/19/2017 9/19/2017 9/19/2017 Top Up qt/gal/l Miles on Oil Miles on Component Oil Changed Y/N No Yes No No Oil Condition: Nitration abs <2.0 < Oxidation abs <2.0 < Total Base Number mg KOH/g C (M) cst C (M) cst Viscosity Index Contamination: Glycol % Potassium ppm <2 <2 <2 <2 Silicon ppm <2 <2 <2 3 Sodium ppm <2 < Soot % <0.1 <0.1 <0.1 <0.1 Water % 2.0 < >3 Wear Metals: Aluminium ppm <2 <2 <2 <2 Chromium ppm <2 <2 <2 <2 Copper ppm < Iron ppm <2 < Manganese ppm Molybdenum ppm <2 < Nickel ppm Lead ppm <2 <2 <2 <2 Tin ppm <2 <2 <2 <2 Titanium ppm Vanadium ppm Additives: Barium ppm Boron ppm Calcium ppm Magnesium ppm Phosphorus ppm Zinc ppm Additional Tests: Fuel Dilution % Total Acid Number mg KOH/g Total Ferrous ppm Water % Color-coded alarm limits NA = NOT AVAILABLE C = CALCULATED M = MEASURED Results from external devices 6 36 Fleet Product Solutions Catalog

37 EXPERT SYSTEM Sample Input User Interface Rules Engine Knowledge Base Non-expert User Advice Knowledge from an Expert The user inputs information about: the equpment, the component and the oil being tested... The Expert System does the rest. Embedded Expert System The Expert System is the brains of the MicroLab, translating analytical data into maintenance actions so the technician or mechanic do not need to interpret the chemistry behind the report; they simply read the service recommendations on the report. Built from over 20 years of industry knowledge and more than 10,000 individual software scripts, the MicroLab s Expert System generates diagnostics that are specific to the: equipment application (e.g., automotive, on-road trucking, off-road trucking, generators) component type (e.g., diesel engine, gasoline engine, hydraulic) and often the equipment manufacturer The Expert System utilizes Rule Sets which are specific to each component type. These Rule Sets contain the threshold levels and diagnostic scripts that are applied to sample results to generate diagnostic statements. The Expert System grades individual sample results as Normal, Abnormal or Severe, using color-coding of the results on the report. Before comparing the results to custom threshold levels stored in the system s database, the system automatically factors in: usage time on the component time on the oil break-in periods FLEET MAINTENANCE SOLUTIONS FOR EXAMPLE Report Results: 25 ppm Lead, 20 ppm Tin Time on Engine Time on Oil Alarm Diagnostic Statement 35,000 miles 15,000 miles NORMAL WEAR METALS DETECTED FOR BREAK-IN OR OVERHAUL PERIOD 375,000 miles 15,000 miles ABNORMAL BEARING WEAR DETECTED 375,000 miles 5,000 miles SEVERE BEARING WEAR DETECTED Given the same results for wear metals but varying the time on the component and oil, the resulting diagnostic statements will be different. Fleet Solutions Product Catalog 37 7

38 Converting Oil Reports into Fleet Decisions LubeTrak Data Management Software LubeTrak compiles individual oil reports into a consolidated database of historical information. This allows fleet managers to view and manage the oil analysis results across the entire fleet. This fleet-level view can be used to assess the health of the entire fleet to optimize maintenance program and practices. LubeTrak s web-based, subscription data management system provides pre-configured reports and the option to custom-design reports. LubeTrak offers companies an on-line reporting solution to view, track, trend and share oil analysis results throughout your organization. The dashboard graphics provide an equipment overview, consolidates the latest results, and shows red-flag problems. Data from MicroLab and CoolCheck instruments can be uploaded to LubeTrak. COMPLETE SAMPLE HISTORY IN ONE PLACE Dashboard summary data for quick assessments Sort by date, equipment type, condition (severity) or site Mobile access CUSTOMIZABLE alerts Customized reports 8 38 Fleet Product Solutions Catalog

39 Fleet and Enterprise Solutions Oil analysis with the MicroLab can help fleets to achieve an effective maintenance program which plays a critical role in asset management goals to: Optimize the lifecycle of the vehicles Minimize equipment downtime Control the costs of replacement parts and service Ensure the safety of the equipment and operators MicroLab Network Solution FLEET MAINTENANCE SOLUTIONS Network solutions for multi-site fleets When a fleet is managing assets across multiple sites, it is important to have an overall view of the entire maintenance program. Some fleets also may have vehicles that access any of their service locations; in those cases it is important that the vehicle s oil analysis history is accessible regardless of which site they visit. Our network solutions allow multiple MicroLabs to be connected via a central server and LubeTrak to provide fleets the ability to: Generate reports locally at each site Synchronize assets and oil history across all sites Upload data from all sites to compare maintenance activities and issues across locations CENTRAL SERVER These network solutions are customized to meet the needs and configurations of many types of fleets to ensure information on the entire fleet is available whenever and wherever it is needed. SITE 1 SITE 2 SITE 3 Fleet Solutions Product Catalog 39 9

40 MICROLAB COMPANION TOOLS The MicroLab is truly an all-in-one solution designed to provide a complete oil analysis with one sample, however, for some specific situations an additional instrument may provide more information as a step two analysis. There are three companion products that fleets might consider depending on their needs. The MicroLab can screen for fuel dilution through a drop in viscosity, however, if a specific fuel dilution amount is needed then the Fuel Dilution Meter can be added to the analysis. The MicroLab detects iron wear particles below 10µm, however, when larger iron wear particles need to be detected such as in transmissions and gearboxes the FerroCheck can be added. The MicroLab can detect contamination from a coolant leak but it cannot be used to test coolants. The CoolCheck 2 provides analysis on coolant condition as well as DEF purity. Results from external devices for fuel dilution, TAN, water and total ferrous can be manually entered to consolidate data into the MicroLab report. FDM 6000 Series AUTOMATED FUEL DILUTION METER Fuel dilution in lubrication oil can cause serious engine damage. In diesel engine crankcases, for example, fuel contamination can be caused by excessive idling, defective injectors or loose connections. The Fuel Dilution Meter 6000 Series detects fuel contamination in minutes which allows for rapid maintenance actions. The device requires just a small sample size in a disposable vial. In addition, the touchscreen and audio prompts guide the operator through the testing process making it simple for any operator to use. Result in % fuel (0.2 to 15%) Small sample required in disposable vial no solvents needed for cleaning Test results within a minute for direct measurement of fuel dilution. FerroCheck 2000 Series AUTOMATED FERROUS WEAR ANALYZER Magnetic wear metal measurement in lubricants can be useful in determining the condition of the gearbox itself. Oil analysis can be used to determine wear conditions in the gears or bearings so corrective actions can be taken to prevent premature failures. Quick and easy measurements with a lightweight, battery operated system make the FerroCheck 2000 Series an essential tool for measurements in the field. Highly repeatable (3 ppm) Reports 0-10,000 ppm iron concentrations Rapid response (30 seconds) Small sample requirement (2 ml) No sample prep or solvents required Fleet Product Solutions Catalog

41 CoolCheck 2 AUTOMATED COOLANT AND DIESEL EXHAUST FLUIDS ANALYSIS SYSTEM Coolant Analyzer Cooling systems play a vital role in preserving the overall engine heat balance and in protecting engine components against corrosion and other problems. CoolCheck offers an easy and fast way to test a fleet s coolant to ensure optimum performance of the cooling system by identifying the most common problems such as, mixed fluid types, depletion of key performance additives and system contamination. Testing coolant and maintaining systems at optimum levels will help prevent corrosion, overheating, engine seize up, and engine damage from freezing. The automated analyzer performs 8 different tests in less than a minute with a simple user interface designed to be run by non-laboratory personnel. The CoolCheck confirms: Glycol% Boil point and freeze point Nitrites Coolant type Color Contamination and clarity FLEET MAINTENANCE SOLUTIONS Diesel Exhaust Fluid (DEF) Analyzer As an added benefit, CoolCheck tests for correct DEF levels. An incorrect DEF mixture can reduce engine efficiency and negate emission reduction systems. The CoolCheck DEF test confirms % urea and total % DEF. Normal Sample All readings within acceptable range CoolCheck reports can be uploaded to LubeTrak Abnormal Sample Freeze Point, Glycol Content and Boil Point all below acceptable range additives depleted Fleet Solutions Product Catalog 11 41

42 MicroLab Series Product Information PART NUMBER (115v) (230v) (115v) (230v) (115v) (230v) COMPANION KITS (115v) (230v) (115v) (230v) (115v) (230v) MicroLab 30 Requires Standard Accessory Kit MicroLab 30, extended metals. Requires Standard Accessory Kit MicroLab 40 Requires (115v) or (230v) Standard Accessory Kit MicroLab 31 Includes: MicroLab 30, CoolCheck, 5YR LubeTrak License MicroLab 42 Includes: MicroLab 40, FerroCheck, FDM6001, 5YR LubeTrak License MicroLab 43 Includes: MicroLab 40, FerroCheck, FDM6001, CoolCheck, 5YR LubeTrak License ACCESSORIES & CONSUMABLES ABS 5 oz sample bottle w/cap (box of 300) Long sipper straw (350 pcs) Cleaning wipe for IR Cell (280 wipes) Clean swabs packages (100 pcs) Sample Extraction Tubing (100 foot roll) Upper Electrode Lower Electrode Filter Screen, 1/2 Dia, #60 x 60 MESH, 304S Check Flush (One Gallon) Basic Metal Test Standard Fluid High (32 oz) - Blue Extended Metal Low Test Standard (32 oz) LCS - Yellow Extended Metal High Test Standard (32 oz) HCS - Brown Low Viscosity Test Standard (32 oz) - Red High Viscosity Test Standard (32 oz) - Green Accessories (Included with instrument and accessory kit) Power conditioner/surge protector, universal cable kit, sample bottles (300), sample straws (1 box), Kimwipes (1 box), cleaning swabs (15 bags), waste bottle, sample extractor and tubing, best practices poster, metals test standards, high and low viscosity standards, check flush (8 gal), wire brush, filter screens (25), remote drain port, allen wrenches PRODUCT INFORMATION Methodology Per ASTM D7417 Repeatability Per ASTM D7417 OPERATIONAL SPECIFICATIONS Sample Volume 1-5 oz. depending on analyses performed Required Sample Time Required Oil range specs Calibration Ambient Operating Temperature Operational Humidity Ambient Altitude 5-15 minutes, depending on analyses selected Up to 680 cst at 40C particle counter limited to 320cSt at 40C Standardization (analyzer metals detection) dependent on application typically required every 50 samples (software-changeable) 0 to 25 C 0-85% non-condensing up to 3000 meters USER INTERFACE SPECFICATIONS Computer OS Win10 32-bit; SQL server database Display 15 (diag.) touchscreen Data Entry Touchscreen / keyboard / USB port for computer mouse Data Storage 512 GB hard drive; 32 GB MSATA drive for database backups Data Transfer FTP (for online reporting) Security AVG 2015 Communication Network port 25 ( of reports) ; Port 21 (online reporting); Remote access software (LogMeIn) for support/training POWER REQUIREMENTS Power 115/230V 50/60 Hz (single-phase) Spec. by part number (top) Power Consumption 1100 Watts continuous; 1700 Watts instantaneous max. MECHANICAL SPECIFICATIONS Dimensions 29 (L) x 30 (W) x 26 (H) (74cm x 76cm x 66cm) Weight 130 lbs (59 kg) COMPLIANCE CE Mark / RoHS To keep your MicroLab running in top condition, it is important to use the recommended consumables including cleaning and standardization fluids. Spectro Scientific certified consumables are selected and carefully tested with all our instruments to ensure consistent, repeatable results. Always use Spectro Scientific supplied consumables for best results. CheckFlush is specially designed to clean the lines in the MicroLab between samples. This prevents cross-over contamination and keeps your instrument running its best. Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 42 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. Fleet_BRv2_

43 Portable Oil Analysis Tools

44 Tools for Service Professionals Conducting oil analysis in the field right next to the high value assets provides unparalleled advantage to reliability professionals and military personals to assess the condition of the assets in real time. Spectro Scientific offers a wide range of portable devices with field simplicity and lab accuracy. The product combinations are powerful for different applications as together they provide more comprehensive analysis of oil condition, contamination and machine wear condition. All Spectro portable devices are battery powered, use small amounts of oil, and do not require solvents or chemicals to clean and fully in compliance to ASTM standards. They are light weighted and ideal for field use. Different combinations are recommended based on the type of asset (engines vs rotating machines such as gear boxes, transmissions, or compressors), and users. Even though devices can be purchased, there are three essential combinations and applications. COMBINATION KIT DEVICES APPLICATIONS Basic Oil Analysis Kit MiniVisc, FerroCheck Used by OEM and service professional for basic oil condition and machine wear condition check in various industries. Oil Condition Kit MiniVisc, FluidScan Primary for engine oil condition checking. Great for marine, aerospace, railway and transportation industries MiniLab 33 MiniVisc, FluidScan, FerroCheck Basic Trivector MiniLab for small and mid-size industrial plant or power plant to start an on-site oil analysis program Portable Oil Analysis Lab FieldLab 58 A battery powered lab in a suitcase that provides elemental analysis, particle count, viscosity and oil condition. It is fully in compliance to ASTM standards and designed for Military personals and reliability professionals to conduct oil analysis next to the high value assets 44 Product Catalog

45 FieldLab 58 EXPEDITIONARY FLUID ANALYSIS SYSTEM Owners of critical assets in the military, mining and marine industries need immediate information about oil and equipment condition. The portable FieldLab 58 oil analyzer eliminates the wait for lab results, so you won t miss early signs of contamination or abnormal wear. Key applications include: In-service oil analysis for engines, gearboxes, hydraulics and turbines Comprehensive oil analysis report Grease analysis for bearings, couplings and motor operated valves Wear metals Oxidation Water (trending only) FieldLab 58 is a battery-powered, integrated oil analysis system that provides quick and comprehensive oil analysis in the field. Military and commercial field service professionals managing fleets of high-value assets require portable, lightweight devices that provide rapid oil analysis results with quality similar to oil analysis labs. Funded by the United States Department of Defense (DoD) in 2009, then developed and commercialized by Spectro Scientific, the FieldLab 58 Expeditionary Fluid Analysis System (EFAS) was designed. The FieldLab 58 integrated system requires only a few milliliters of oil to complete four comprehensive tests to help maintain readiness of critical assets while economically managing maintenance costs. Key Features Rugged design with battery power for on-site field use No solvents or chemicals required Complete oil analysis lab with 4 technologies integrated into a small case X-Ray Florescence (XRF) spectrometer for elemental analysis Filter Particle Quantifier (FPQ) pore blockage particle counter Infrared (IR) spectrometer Kinematic viscometer (40 C) 4 tests generate more than 20 oil analysis parameters in 5 to 7 minutes Built-in controller for measurement, data, and asset with touch screen interface Uses only 3 ml of oil ASTM compliant PORTABLE OIL ANALYSIS TOOLS Product Catalog 45

46 FieldLab 58 Complete in-service oil analysis lab in the field KEY PARAMETERS MACHINE WEAR 13 elements for particles > 5 µm (Si, Al, Cr, Ti, Fe, Ni, Pb, Cu Sn, Mo,Ag, Zn, V) CONTAMINATION Particle count, ISO codes Water, glycol, soot OIL CONDITION Oxidation, nitration, sulfation, TAN, TBN C, calculated C Link with LIMS software Connects directly to the cloud-based SpectroTrack LIMS using the FluidManager software Data transfer with the push of button Fleet level oil analysis tracked and reported in SpectroTrack notifications, trending reports and asset management readily available to reliability managers FieldLab 58 data can also be imported into AMS OilView software SpectroTrack 46 Product Catalog

47 PRINCIPLES OF OPERATION Particle count and elemental analysis ASTM D8127 Particle counts are generated using our patented FPQ pore blockage particle counter (ISO ). It captures the particles of interest for severe wear detection onto a unique filtergram. This debris may now be measured on the companion XRF spectrometer for immediate results in ppm for 13 elements. Wear and contamination particles larger than 4 microns deposit on the filtergram, and are tested using an X-Ray Florescence (XRF) spectrometer. The concentration (in ppm) for thirteen different elements is reported. The filtergram coupon can be stored for future analysis, such as microscopic wear debris analysis of particle colors and shapes. Oil Insertion Particles Filtergram Fluid chemistry and contamination ASTM D7889 The IR spectrometer measures the chemistry of the lubricant and contamination in one minute using only one drop of oil; no chemicals or solvents are required. It combines ease of use, ruggedness and laboratory precision in a small package, which is ideal for field use. The oil condition parameters measured by FluidScan include oxidation, nitration, sulfation, anti-wear additive, Total Base Number (TBN), glycol, soot, and water for engine oil; and oxidation, Total Acid Number, and water for rotating machine lubricants such as gear oil, transmission oil and hydraulic oil. PORTABLE OIL ANALYSIS TOOLS Viscosity ASTM D8092 Viscosity is measured using a temperature-controlled kinematic viscometer with a patented split-cell design. A funnel, with a 100 micron gap, is formed in the center of the cell. Optical sensors in the cell detect the flow of oil under the influence of gravity. The time it takes the oil to flow through the cell is proportional to the viscosity of the oil. When open, the cells can be cleaned using a non-abrasive wipe. No solvents are required. Kinematic Viscosity (40C) = A* (t 1 -t 0 ) + B *A and B are calibration coefficients Product Catalog 47

48 FieldLab 58 Product Information PRODUCT INFORMATION Part Number Applications Mineral and synthetic lubricants including gear, engines, transmissions, hydraulics, turbine as well as military, marine and mining applications In-service grease for industrial plants ELEMENTAL MODULE Detector 25 mm 2 SDD detector; Peltier cooled Resolution 122 ev FWHM resolution at 5.9 kev Excitation Source X-ray tube with Rhodium target; max voltage 50 kv OPERATIONAL SPECIFICATIONS Sample Volume 3 ml Required (all tests) Sample Time Required Viscosity: 20 secs to 10 mins, dependent on grade Fluid Chemistry: less than 60 secs Particle Count: 20 secs to 3 minutes, sample dependent XRF: 3-4 minutes Ambient Operating Temperature Operational Humidity Ambient Altitude 0 to 40 C RH< 80% non-condensing Up to 5,000 meters (16,404 feet) USER INTERFACE SPECIFICATIONS Instrument OS SQL database on Windows CE Display Fixed-angle 7 color touch screen display Data Storage Internal flash memory (SD card expansion) Data Transfer Ethernet, mini USB Data Entry Touch screen, FluidManager desktop software (asset loading and synchronization) POWER REQUIREMENTS Battery Power Source Lithium-ion battery pack Charge Power 120/240 Vac, 50/60 Hz, 10 watts Typical Runtime 4-6 hours Recharge Time 2.5 hours MECHANICAL SPECIFICATIONS Dimensions 48 cm (L) x 39 cm (W) x 23 cm (H); 19.2 x 15.2 x 9 Weight 16.5 kg (36.4 lbs); 20 kg (44.4 lbs with backpack and power supply) COMPLIANCE CENELEC EN :2010 EN CENEIEC EN MIL-STD 461 EMI MIL-PRF 28800F Class II Drop Test OUTPUTS Elemental Concentration (ppm) Fluid Chemistry Viscosity Particle Count Methodology Calibration Silicon (Si); Aluminum (Al); Chromium (Cr); Titanium (Ti); Iron (Fe); Nickel (Ni); Lead (Pb); Copper (Cu); Tin (Sn); Molybdenum (Mo); Silver (Ag); Zinc (Zn); Vanadium (V) TAN & TBN (mg KOH/g); Oxidation, Nitration, Sulfation (Abs/.1mm); Water (parts per million); Glycol (% by weight); Soot (% by weight); Incorrect fluid (% by weight); Antioxidant Depletion (% remaining); Antiwear Depletion (% by weight) Kinematic 40C Calculated 100C Particle count #/ml (> 4 µm) ISO Codes 4/6/14 ISO codes >6 and >14 are extrapolated ASTM D7889 (IR), ASTM D8092 (viscosity), ASTM D8127 (FPQ-XRF) Factory, verification standards: NIST traceable verification standards provided CONSUMABLES P ml syringe (100 pack) PV ml disposable pipettes & non-abrasive cleaning pad kit (100 pack) FPQ waste container (3 pack) FieldLab 58 verification standards (6 bottles) FL310 IR Check Fluid 5 ml FPQ filtergrams (50 pack) FPQ filtergrams Grease (50 pack) OPTIONAL ACCESSORIES XRF calibration standard set FieldLab 58 consumables and standards Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 48 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. FieldLab 58_DSv4_

49 FluidScan 1000 Series PORTABLE FLUID CONDITION MONITOR Handheld, Solvent-free, Immediate Results The FluidScan 1000 Series provides quantitative measurement of a lubricant s condition and plays an important role in predictive maintenance. Using the device, you can eliminate unnecessary oil changes or service by testing not just servicing the oil. Applications include: Mineral and synthetic oils used in gear boxes, engines, transmissions Hydraulic systems, turbines and other machinery components Biodiesel/Fuel Quality assurance of new oils FluidScan 1000 Color Yellow Blue Default library Upgradable to full library Total water license Route base analysis OilView Interface Intended application One free library from FL364 to FL371 at time of purchase Yes Optional No No Fleet, marine, military, aerospace, fuel QC FluidScan 1100 Industrial Yes Optional Yes Yes Industrial manufacturing plants, power plants Rugged Direct Infrared Spectrometer No moving parts, designed for handheld and field use applications High signal to noise ratio (>7000:1) to ensure high accuracy and repeatability Easy to use Needs just one drop of oil and one minute to test No solvents required to clean Color-coded, user adjustable alarm limits Determine when in service oil is no longer fit for use due to liquid contamination or degradation Direct immediate measurement of water, TAN and oxidation for lubricants used in gearboxes, turbines and hydraulic systems Also measures TBN, water, glycol, soot, additive depletion and oxidation for engine oil Highly repeatable and reproducible results ASTM D7889 Compliant Standard Test Method for Field Determination of In-service Fluid Properties Using IR Spectroscopy High correlation to KF water, TAN and TBN laboratory tests Reproducibility and repeatability comparable to benchtop FTIR method ASTM E2412 Data analysis compliant to ASTM E1655 Comprehensive Fluid Library Over 700 fluids for immediate, out-of-the-box operation Results for critical properties such as TAN and water contamination for industrial lubricants or TBN, water, glycol and soot for engine oils Easy dissolved water & free water measurement For both dissolved and free water using homogenization technique Solvent free alternative to Karl Fischer titration Patented total water algorithm for both dissolved and free water Ideal for turbine oil, hydraulic fluids, and rotating machinery oils such as gear oil and compressor oil Product Catalog 49 PORTABLE OIL ANALYSIS TOOLS

50 Multivariate Calibrations The FluidScan classifies fluids into groups called families based on their chemical makeup, usage and spectral signature. The spectrum of all fluids in each family changes in a similar way with a given amount of degradation or contamination. Family-specific algorithms are assigned that accurately quantify these amounts. These algorithms yield quantitative results for the most critical properties of the most common oil types. Multivariate calibrations are applied so that quantitative readings can be obtained, even with complex, contaminated samples. Innovation in hardware and calibration At the core of the FluidScan is a patented, mid-infrared spectrometer with grating optics and a linear detector array. The spectrometer collects the infrared light transmitted through the fluid in the flip top cell into a waveguide. The waveguide then carries the light to a prism-like diffraction grating that reflects the light into a high-performance array detector which registers the infrared spectrum of the fluid. It provides more than adequate spectral range, resolution and signal-to-noise ratio for the rapid analysis of in-service lubricants. The FluidScan Applications Library includes over 700 oils and growing. Parameters for the oils differ based on oil type so engine oil parameters are different from gear oils. Parameters such as water, TAN or TBN are calibrated according to ASTM methods used in common oil analysis labs with excellent correlation using multivariate calibration methods. Fresh oils not in the library can be matched and added as user fluids, and existing calibration can be applied to the user fluid with custom slope and offset adjustments, if needed. Correlation with ASTM D664 Correlation with ASTM D6304 A typical IR spectrum from FluidScan TAN correlation to titration Dissolved water correlation to Karl Fischer 50 Product Catalog

51 Comparison of FluidScan ASTM D7889 and corresponding IR ASTM methods OIL PROPERTY FLUIDSCAN REPEATABILITY IR REPEATABILITY IR ASTM Oxidation (abs/0.1 mm) D7414 Nitration (abs/cm) D7624 Sulfation (abs/0.1 mm) D7415 Antiwear Additive (abs/0.1 mm) D7412 Soot (abs/cm) D7844 Oil category and properties APPLICATION CATEGORIES Transmission Hydraulic Fire resistant (Phosphate Ester) Hydraulic Aerospace (Synthetic Hydraulic Fluid) Heat Transfer (Quenching Oil) Industrial (Steam and CCGT Turbine, Hydraulic, compressor, Chiller, Gear, etc.) Turbine Aerospace (Synthetic Gas Turbine Oil) Engines (Engine oil for different engine types, including Gasoline, Diesel, Heavy Duty Diesel, HFO, Natural Gas, etc) Ethanol in Gasoline Ethanol (%) FAME in Diesel FAME (%) PROPERTIES MEASURED BY FLUIDSCAN Water (ppm), Oxidation (Abs/0.1mm) Water (ppm), TAN (mg KOH/g) Water (ppm), Oxidation (Abs/0.1mm), Alien Fluid mineral based (MIL-H-2304) (%), and Alien Fluid engine oil (MIL-H-23699) (%) Water (ppm), Oxidation (Abs/0.1mm) Biodiesel Feedstock Water (ppm), FFA % Water (ppm), Oxidation (Abs/0.1mm), TAN (mg KOH/g) Water (ppm), TAN (mg KOH/g), Antioxidant (% depletion) Water (ppm), Oxidation (Abs/0.1mm), TBN (mg KOH/g), TAN (mg KOH/g) (Natural Gas only), Sulfation (Abs/0.1mm), Nitration (Abs/cm), Soot (%), Glycol (%), Anti Wear (%) Biodiesel Water (ppm), TAN (mg KOH/g), Total Glycerin (%) Fluid libraries and application categories included P/N LIBRARY OIL CATEGORIES INCLUDED FL364 Automotive Engine, Engine-Natural Gas, Hydraulic, Transmission FL365 Aviation Compressor, Engine, Hydraulic, Hydraulic Fire resistant, Hydraulic-Aero, Turbine-Aero FL366 Fuel QC Biodiesel, Biodiesel Feedstock, Ethanol in Gasoline, FAME in Diesel FL367 Industrial Chiller, Compressor, Engine, Engine-Heavy Duty, Engine-Natural Gas, Gear- Pressure, Gear-Splash, Heat Transfer, Hydraulic, Hydraulic-Fire Resistant, Slideway, Transmission, Turbine-Aero, Turbine-CCGT, Turbine-Steam FL368 Lab Trend ASTM Petroleum Engine, ASTM Polyol Ester (Turbine) FL369 Marine Chiller, Compressor, Engine, Engine-Heavy Duty, Engine-HFO, Gear-Pressure, Gear-Splash, Hydraulic, Transmission, Turbine-CCGT, Turbine-Steam FL370 Military Chiller, Compressor, Engine, Engine-Heavy Duty, Engine-HFO, Gear-Pressure, Gear-Splash, Hydraulic-Fire Resistant, Hydraulic-Aero, Turbine-Aero FL371 Railroad Compressor, Engine, Engine-Natural Gas, Hydraulic, Transmission FL360 All Libraries All Categories of oils included Examples of fluid chemistry types included in the library Mineral oil-based hydraulic, compression, transmission, turbine and gear blends Polyol Esters Phosphate Esters Organic Esters Synthetic hydrocarbon-based hydraulic, compression, transmission, turbine and gear blends Ester-based Blends Biodiesel Diesel Fuel Polyglycols Polyalkylene Glycols Polyalphaolefins Polyinternal Olefins Note: Fluid chemistry in the library is not inclusive. Call Spectro Scientific support for more details before ordering. Fluid properties and corresponding (compliance or correlation) methods PROPERTY Oxidation D Nitration D Sulfation D AW Additive D Soot D Gravimetric 2 TBN D TAN D664 2 Water D Glycol Gravimetric 2 Antioxidant E Gravimetric 2 Notes: 1. FluidScan complies with ASTM D FluidScan correlates to ASTM method for TBN, TAN, Water, and gravimetric method for Glycol, antioxidant PORTABLE OIL ANALYSIS TOOLS Product Catalog 51

52 FluidScan Series Product Information FluidScan can also be ordered in a combination kit with the MiniVisc 3050 portable viscometer. The battery-operated MiniVisc 3050 is a 40 C kinematic viscometer. It uses a few drops of oil to measure viscosity and does not require solvents to clean between samples. FluidScan 1000 & MiniVisc 3050 Combination Kit FluidScan 1100 & MiniVisc 3050 Combination Kit PART NUMBER FluidScan 1000 SA1001 Spectro 1000/3050 SA1004 SA1018 FluidScan 1100 Spectro 1100/3050 SA1022 FluidScan 1000 (requires SA1001 and Library license to operate) FluidScan standard accessories FluidScan 1000 & MiniVisc 3050 Combination Kit (requires SA1004 and Library license to operate) Spectro Combination Kit standard accessories FluidScan 1000/1100 & 3050 Combination Kit Standard Accessories 1100 FluidScan. Requires SA1001 Accessory Kit. FluidScan 1100 & MiniVisc 3050 Combination Kit. Requires SA1022 Accessory Kit. Spectro Combination Kit standard accessories Comprehensive Water Solution with Portable Homogenizer and license, 115 V, 60 Hz charger Comprehensive Water Solution with Portable Homogenizer and license, 220 V, 50 Hz charger Comprehensive Water Solution with table top Homogenizer and license, 115 V, 60 Hz Comprehensive Water Solution with table top Homogenizer and license, 220 V, 50 Hz PRODUCT INFORMATION Application Library Mineral and synthetic lubricants including gear, engine, transmission, hydraulics, turbine and biodiesels Output (varies by fluid type and application) Methodology Standard Analytical Range Accuracy Repeatability Calibration OPERATIONAL SPECIFICATIONS Sample Volume 100 μl (1 drop) Solvents/Reagents None TAN (mgkoh/g), TBN (mgkoh/g); Oxidation (abs/0.1 mm); Nitration (abs/cm); Sulfation (abs/0.1 mm); Water, ppm (dissolved, dissolved + free water with Comprehensive Water Solution option); Glycol (% by weight); Soot (% by weight); Incorrect Fluid (% by weight); Antioxidant Depletion (% remaining); Antiwear Depletion (% by weight). ASTM D7889, ASTM E1655, E2412 modified Mid infrared range cm -1 ± 3% of measured value, typical ± 6% of measured value, typical Factory calibrated to wet chemistry methods ASTM D664 for TAN and ASTM D4739 for TBN. Use Check Fluid for instrument validation. Ambient Operating Temperature Relative Humidity Ambient Altitude 10 C to 50 C (14 F to 122 F) 0 to 100%, non-condensing up to 5,000 meters (16,404 feet) USER INTERFACE SPECFICATIONS Software/Operating Microsoft Windows CE System Display Data Storage Data Transfer Data Entry 320 x 320 transflective color screen Up to 5,000 analyses USB for data updates and synchronization Directional pad and soft buttons POWER REQUIREMENTS Battery Power Source Built in Rechargeable Lithium Ion Battery Power AC 110/240 V, 50/60 Hz, 10 Watts Typical Runtime 6-8 hours Recharge Time 6.5 hours MECHANICAL SPECIFICATIONS Dimensions 24 cm (H) x 14 cm (W) x 7 cm (D) (9.5 in x 5.5 in x 2.75 in) Weight 1.4 kg (3 lbs) Shipping package dimensions Shipping pkg weight 45.7 cm (H) x 40.6 cm (W) x 35.6 cm (L) (18 in x 16 in x 14 in) 8.1 kg, (18 lbs) COMPLIANCE CE Mark: EMC Directive (2004/108/EC); RoHS ACCESSORIES & CONSUMABLES A OilView LIMS software FL310 IR Check Fluid 5 ml PV1011 Disposable Non-Abrasive Cleaning Pads; pkg of 500 P µl Disposable Pipettes, package of 500 PV µl Disposable Pipettes & Non-Abrasive Cleaning Pad Kit; package of 100 each FL360 Reference Fluid Application Library all categories P Pipette tips for positive displacement pipette (used with MiniVisc 3050), package of Tray Assembly and Charging Station, VAC, 50/60 Hz Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 52 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. FluidScan Series_DSv5_

53 FerroCheck 2000 Series FERROUS METAL ANALYZER Solvent-free, simple to use, fast and accurate results Accurate total ferrous measurement for in-service lubricants The FerroCheck 2000 Series enables fast and simple measurement of the total ferrous wear content in oils and grease for condition based maintenance of machinery and engines. Typical components trended for wear as part of a condition based maintenance program include: Gear boxes Turbines Hydraulics Transmissions Engines Pumps and compressors Measure total ferrous content in parts per million (ppm) by weight Measures all ferrous material normal machine wear and large abnormal wear particles. Highly accurate and repeatable Wide range of measurement Validation standards included Easy to use Solvent-free operation and no sample preparation Requires less than 2 ml of sample to test Results in 30 seconds Expanded I/O capability Automated data storage, export files in CSV format or use AMS OilView software interface Portable, battery-powered design Lightweight and fits easily into a toolbox or carrying bag; capable of operation for over 4 hours before recharge. Unit plugs in for continuous use. ASTM compliance ASTM method D8120 Standard Test Method for Ferrous Debris Quantification FerroCheck 2000 FerroCheck 2100 Oil 0-10,000 ppm 0-10,000 ppm Grease NA 0-15% PORTABLE OIL ANALYSIS TOOLS SAMPLE VIAL MEASUREMENT COIL Schematic of Coil Around Sample REFERENCE COIL Principle of Operation The core of the FerroCheck 2000 is a pair of precision-rounded coils that when powered generate magnetic fields. When a small amount of in-service oil is inserted into one of the coils, ferrous particles such as iron, nickel and cobalt interact with the magnetic field and introduce current changes in the coils. The amount of current change is proportional to the amount of ferrous particles in the oil, calibrated in weight by parts per million (ppm). Product Catalog 53

54 FerroCheck 2000 Series Product Information PART NUMBERS FerroCheck 2000 ferrous monitor for oil USER INTERFACE SPECIFICATIONS Display 6, fixed-angle, color touchscreen display FerroCheck 2000 standard accessories kit. Includes instrument carrying case, dust cover, 1000 sample vials, 200 vial stoppers, and oil validation standards. Data Transfer Data Entry USB flashdrive or to OilView LIMS software Touchscreen FerroCheck 2100 ferrous monitor for oil and grease FerroCheck 2100 standard accessories kit. Includes instrument carrying case, dust cover, 1000 sample vials, 300 grease boats and blades, 200 vial stoppers, and oil and grease validation standards. PRODUCT INFORMATION Applications FerroCheck 2000: Lubricant oil FerroCheck 2100: Lubricant oil and grease Output Total ferrous, parts per million by weight Methodology Standard Calibrated Ranges Test Time Limit of detection Repeatability Calibration ASTM D8120 FerroCheck 2000: ppm, ,000 ppm FerroCheck 2100: ppm, ,000 ppm for oil ppm, 2000 ppm-15% for grease < 30 s 3 ppm 3% RSD Ferrous standards provided OPERATIONAL SPECIFICATIONS Sample Volume For oil with sampling vial: 1.5 ml With grease boat: 0.75 ml Ambient Operating 10 to 40C Temperature POWER REQUIREMENTS Power Source Built in rechargeable NiCd battery Power Typical Runtime MECHANICAL SPECIFICATIONS Dimensions (WxDxH) Weight 2.9 kg COMPLIANCE CE, FCC Class B, NEMA 2, IP VAC, 50/60 Hz, 3.5 watts for charger Battery life 4-6 h or plug in for continuous use 17 cm x 20 cm x 13.5 cm (6.6 in x 7.8 in x 5.2 in) CONSUMABLES FerroCheck 2000 consumables kit (500 samples). Includes 500 sample vials, 100 vial stoppers, and validation standards FerroCheck 2100 consumables kit (500 samples). Includes 500 sample vials, 100 vial stoppers, 150 grease boats and blades, and validation standards FerroCheck sample vials, qty Grease sample boats and blades, qty 50 each Grease boat, blade and vial kit, qty 50 each FerroCheck sample vial stoppers, qty 100 each ppm verification fluid for FerroCheck (oil) ppm verification fluid for FerroCheck (oil) Relative Humidity Internal Data Storage 10-90% RH, non-condensing 2,000 samples Verification standard for grease, high range Verification standard for grease, low range RSD: Relative Standard Deviation A recommended solution set includes the FluidScan 1000, MiniVisc 3000 and FerroCheck Grease boat and grease boat inserted into sample vial Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 54 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. FerroCheck_DSv1_

55 MiniVisc 3000 Series PORTABLE KINEMATIC VISCOMETERS Solvent-free, simple to use, fast and accurate results Applications include: Machine Condition Monitoring Increase availability of critical equipment by monitoring viscosity changes due to oil degradation and contamination. Avoid inadequate lubrication which causes adhesive wear in machinery and is a principal cause of equipment downtime. Quality Control for Fuel/Oil Production and Blending Incoming Inspection Quality Control High accuracy 40C kinematic viscosity measurements for new and in-service oils Lab-quality results when and where you need them Accuracy +/- 3% Relative Standard Deviation to NIST viscosity standards. Solvent-free operation Fewer consumables, lower disposal costs and less environmental impact. Easy cleaning with the patented split-cell design just wipe off the surfaces with a nonabrasive cleaning pad between samples. Requires only a few drops of oil to test Obtain samples without impacting lubricant level; only a few drops (60 μl) of oil required. A positive displacement pipette is provided for the most precise, repeatable measurements. Test even dark and sooty samples Innovative design allows testing of virtually any sample including dark and sooty or transparent samples without any pre-checks. Portable, battery-powered design Fits easily into a toolbox or carrying bag and capable of operation for over six hours before recharge. Expanded I/O capability Import sample lists and export measurement results via ViscTrack or AMS Oilview software. ASTM compliance ASTM D8092 Standard Test Method for Field Determination of Kinematic Viscosity Using a Microchannel Viscometer. PORTABLE OIL ANALYSIS TOOLS V40 = A* (t 1 -t 0 ) + B *A and B are calibration coefficients Principle of Operation MiniVisc 3000 Series viscometers use a patented split cell design that enables measurement of kinematic viscosity using only a few drops (60 µl) of oil. When closed, the center pieces of the split cell form a funnel with a 100 micron gap allowing oil to flow down by gravity. Sensors along the funnel are triggered when oil flows by and flow time between two sensors is measured. The kinematic viscosity is then calculated. When opened, the split cell can be easily cleaned with a non-abrasive cleaning pad and it is ready for the next sample. The split cell is controlled at 40 C throughout the measurement. Product Catalog 55

56 MiniVisc 3000 Series Product Information The MiniVisc 3000 includes the base viscometer, battery charger, USB cable, user s manual DVD and ViscTrack software. The recommended 3050 Standard Accessories Kit SA1021 includes a positive displacement pipette, disposable pipette tips and cleaning pads for 192 samples, and two viscosity standards kits. The recommended 3000 Standard Accessories Kit SA1002 includes disposable 60 μl pipettes and cleaning pads for 100 samples, and two viscosity standards kits. MiniVisc 3000 MiniVisc 3050 Range cst cst Outputs V40 V40 V100 (calculated) Pipette Disposable pipette Positive displacement pipette PART NUMBER SpectroVisc-Q3050 SpectroVisc-Q3000 Spectro-Q1100/Q3050 Spectro-Q1000/Q3050 MiniVisc 3050 Portable Viscometer, cst. Requires SA1021 Standard Accessories Kit. MiniVisc 3000 Portable Viscometer, cst. Requires SA1002 Standard Accessories Kit. FluidScan 1100 Lubricant Condition Monitor & MiniVisc 3050 Combo Kit. Requires SA1022 Standard Accessories for Combo Kit. FluidScan 1000 Lubricant Condition Monitor & MiniVisc 3050 Combo Kit. Requires SA1022 Standard Accessories for Combo Kit. PRODUCT INFORMATION Applications Lubricant oils (mineral and synthetic), coolants, glycol, and any Newtonian fluid within the measuring range Output Kinematic viscosity 40 C V100 viscosity calculation from VI index input (3050 only) Methodology ASTM D 8092 Standard Analytical Range 3000: C 3050: C Accuracy 3000: ± 3% of measured value over range cst 3050: ± 3% of measured value over range cst ± 5% of measured value for viscosity > 350 cst Accuracy specification is with use of user correction function. Repeatability 3000: ± 3% RSD of measured value, typical 3050: ± 3% RSD of value, typical, over range cst ± 5% RSD of measured value for viscosity > 350 cst Test Temperature Control Calibration RSD is Relative Standard Deviation. ± 0.1 C Not required OPERATIONAL SPECIFICATIONS Sample Volume 60 µl (about 3-4 drops) Solvents/Reagents None Ambient Operating 0 C to 40 C (32 F to 104 F) Temperature Relative Humidity Ambient Altitude 10% to 80% r.h. non-condensing Up to 5,000 meters (16,404 feet) USER INTERFACE SPECIFICATIONS Display Fixed angle color touchscreen display Data Transfer USB for software updates Data Entry Touchscreen POWER REQUIREMENTS Battery Power Source Built in rechargeable lithium ion battery Power AC 110/240 V, 50/60 Hz, 10 Watts Typical Runtime 6-8 hours with full charge Recharge Time 2.5 hrs MECHANICAL SPECIFICATIONS Dimensions 152 mm (H) x 127 mm (W) x 203 mm (D) (6.0 in x 5.0 in x 8.0 in) Weight 1.8 kg (4.0 lbs) Shipping Package Dimensions Shipping Package Weight 50.8 cm (H) x 40.6 cm (W) x 35.6 cm (L) (20 in x 16 in x 14 in) 4.9 kg (11 lbs) COMPLIANCE CE Mark: EMC Directive (2004/108/EC); RoHS CONSUMABLES P Positive displacement pipette, μl P Pipette tips for P-11177, package of 192 P Pipette tips for P-11177, package of 960 PV1011 Disposable non-abrasive cleaning pads, package of 500 P μl disposable pipettes, package of 500 PV1025 Visc 30 standard, 20 ml PV1026 Visc 120 standard, 20 ml A recommended solution set includes the FluidScan 1000, MiniVisc 3000 and FerroCheck Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 56 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. MiniVisc3000Series_DSv4_

57 FDM 6000 Series PORTABLE FUEL DILUTION METER Solvent-free, simple to use, fast and accurate results The Need for Fuel Dilution Measurement If left unchecked, fuel dilution in lube oil causes serious engine damage. In diesel engine crankcases, fuel dilution can be caused by: Excessive idling Defective injectors Loose connections Intercooler leakage (aircraft hydraulic systems) Therefore fuel dilution is a common test item for both on site and off site in-service engine oil analysis. FDM 6000 Series is a portable fuel dilution meter that measures direct fuel dilution in engine oil. Lab quality results where and when you need them 0.2 to 15% fuel dilution measurement range. Excellent repeatability ( 5% RSD). Disposable FDM vials eliminat e carryover contamination. Onboard memory allows use of up to three stored calibration profiles. Sample ID entry and data file export via USB cable. Battery powered, lightweight, optional hard case for transit. Complies to ASTM D8004. Fast and easy to use Small volume 0.5 ml of sample required. No solvent needed for cleaning. Less than one minute test time. Direct reading of fuel dilution percentage. Easy touch screen interface with voice guidance. PORTABLE OIL ANALYSIS TOOLS PATENTED FDM SAMPLING SYSTEM INLET PURGE PUMP AMBIENT AIR DISPOSABLE OIL SAMPLE CONTAINER VENT SAW SENSOR ARRAY SAMPLE PUMP Innovative design The FDM analyzer employ a Surface Acoustic Wave (SAW) vapor sensor to measure the concentration of fuel in used oil samples by sampling the headspace in the vial. The device assumes (based on Henry s Law) that the fuel concentration in the headspace vapor is directly related to the fuel present in the oil sample. The surface of the SAW sensor has a polymer coating with specific solubility to fuel vapors. The sample pump draws the headspace vapor through the SAW sensor where it is absorbed onto the polymer coating and detected. The purge pump then pushes air through the SAW to clean the system so it is ready for the next sample. Product Catalog 57

58 FDM 6000 Series Product Information Both the FDM 6000 and 6001 include the base fuel dilution meter, soft tip stylus, battery charger, USB cable, CD manual, FDM vials and disposable pipettes for 100 samples. FDM 6000 FDM 6001 Stored Calibration 1 3 PART NUMBER SpectroFDM-Q6001 SpectroFDM-Q6000 SA1019 FDM 6001 Fuel Dilution Meter System Multiple Calibration. Requires SA1019 Standard Accessory Kit. FDM 6000 Fuel Dilution Meter System Single Calibration. Requires SA1019 Standard Accessory Kit. Spectro-Q6000 Standard Accessories PRODUCT INFORMATION Application Mineral and Synthetic Lubricants used in liquid fueled engines Output Methodology Standard Analytical Range % (wt or vol) ) Fuel dilution ASTM D % fuel in oil (fuel dilution) Accuracy ± 0.2% fuel dilution in range 0.2-2% ± 10% of measurement in range 2-15% Repeatability Calibration ± 5% RSD of measurement + 0.2% fuel dilution Single point, User developed or Certified Check Standard (optional) OPERATIONAL SPECIFICATIONS Sample Volume 0.5 ml Solvents/Reagents None Ambient Operating 5 C to 35 C (41 F to 95 F) Temperature Relative Humidity Ambient Altitude 0 to 90%, non-condensing up to 2,000 meters (6561 feet) USER INTERFACE SPECFICATIONS Display 4.3 TFT color screen (480 X 272 ) Data Storage 4 GB Data Transfer USB Data Entry Touch-screen with stylus POWER REQUIREMENTS Battery Power Built in Rechargeable Lithium Ion Battery Source Power AC 110/240 V, 50/60 Hz, 9 Watts, 9 Volts Typical Runtime 3-4 hours Recharge Time 4 hours MECHANICAL SPECIFICATIONS Dimensions 15 cm (W) x cm (D) x 13.5 cm (H) (5.9 in x 7.77 in x 5.31 in) Weight Shipping Package Dimensions Shipping Package Weight 1.4 kg (3 lbs) 45.7 cm (H) x 40.6 cm (W) x 35.6 cm (L) (18 in x 16 in x 14 in) 8.1 kg, (18 lbs) COMPLIANCE CENELEC EN (2010/10/01 Ed:3 ); CENELEC EN (2006/05/01); FCC 47CFR 15B; RoHS CONSUMABLES AND STANDARDS FDM Vials Kit (50 pk) FDM Vials Kit (500 pk) μl Disposable Pipettes (50 pk) P ul Disposable Pipettes (500 pk) DSL5%DEV-100 5% Devolatized diesel in oil fuel dilution standard, NIST traceable, 100ml DSLBLK-15W GASFD-2P-100 Diesel blank standard for fuel dilution standard, 100 ml 2% Devolatized gasoline in oil standard, NIST traceable, 100 ml OPTIONAL ACCESSORIES P Positive Displacement Pipette μl P Pipette Tips μl (182 pk) P Transport Case FDM 6000 Series Standards and optional positive displacement pipette FDM consumable and preparation kit Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 58 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. FDM 6000_DSv3_

59 InfraCal 2 Soot Meter PORTABLE, RUGGED INFRARED ANALYZER Soot, in diesel engines, is made up of nanometer size hard carbon particles and is deposited in the oil as combustion by-products. As soot globules coagulate into larger particles, engine wear will accelerate. At very high levels soot can cause an increase in the oil viscosity. Higher than normal levels can indicate an improper air/ fuel ratio, plugged or defective air intakes or leaking injectors. The InfraCal 2 Soot Meter measures the amount of suspended carbon (soot) in diesel engine lubricating oils by infrared absorption at a fixed wavelength. The Soot Meter is based on proven IR technology. Results correlate to the TGA (thermogravimetric analysis) reference method ASTM D7686 and FTIR methods. No solvents requiring special ventilation, expensive waste disposal or difficult to clean cells are needed. Ideal for: Oil testing labs achieve comparable results to TGA or FTIR in a fraction of the time Engine test labs obtain on-the-spot assessment of the engine test progress Fleet maintenance shops check soot level to know exactly when to schedule oil changes Construction or mining sites stay operational with oil condition checks On-board-ship no need to return to port to monitor oil condition Power generation stations monitor the quality of the lubricating oil without waiting for off-site lab results Measurement range: 0-15% soot Instrument repeatability: +/- 0.2 Complies with ASTM Method D7686 No dilution or sample preparation Rapid analysis less than 30 seconds per sample Multiple language interface with touch screen input Password protected settings PORTABLE OIL ANALYSIS TOOLS Principle of Operation Samples are applied to a zinc selenide (ZnSe) attenuated total reflectance (ATR) sample plate. Infrared light from a source bounces multiple times between the top and bottom surfaces of ZnSe crystal as it travels horizontally from one side to the other. It is then filtered and measured by the detector. The loss of the light at specific wavelengths is due to the absorption by the oil sample on the top plate and it is then calculated to percentage of soot based on calibration to gravimetric methods. Product Catalog 59

60 Soot Meter Product Information PART NUMBER InfraCal 2 Soot Meter, complete with HATR sample stage for direct measurement of suspended carbon (soot) level in diesel engine oils (factory calibrated to 12% soot concentration) set of reference oils and power supply. PRODUCT INFORMATION Analytical Wavelength/ Wave Number Outputs ASTM Method ASTM 7686 Analytical Range 0-15% Analysis Time Instrument Repeatability 3.9 micrometers, 2464 cm -1 % (by weight) soot in engine oil Less than 30 seconds ±0.2% USER INTERFACE SPECIFICATIONS User interface Data input 6 color display Touch screen Communication port USB, RS 232 POWER REQUIREMENTS Battery Power Source External Power Requirements Power Adaptor Input Battery Run Time 18 volt NiCad battery 18 volts DC, 3.3 amps Universal AC/DC 4-6 hours OPERATING SPECIFICATIONS Sample Volume Solvent/Reagent < 1 ml None Operating Temperature 5 C - 40 C Relative Humidity Altitude MECHANICAL SPECIFICATIONS Weight Dimensions Shipping Weight Shipping Dimensions COMPLIANCE CE, FCC Class B, NEMA 2, IP %, non-condensing Up to 5000 meters 7.0 lbs (3.2 kg) 6.7 x 7.8 x 5.2 (170 x 198 x 132 mm) 8.0 lbs (3.6 kg) CONSUMABLES AND STANDARDS 10 x 10 x 14 (254 x 254 x 355 mm) Set of 6 reference oils in dropper bottles, appropriate for calibration and verification of reproducibility 0-12% soot range. This set of reference oils has been correlated with the results obtained via thermal gravimetric analysis (TGA) of fresh used diesel oil samples. OPTIONAL ACCESSORIES Carrying case for InfraCal Analyzers with pre-diced pluck foam x 14.6 x 8 ; 10 lbs Dust cover The Soot Meter can be used as part of a solutions kit for engine oil condition. Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 60 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. InfraCal 2 Soot Meter_DSv1_

61 Oil Analysis Laboratory Instruments

62 Industrial Tribology Lab (ITL) The Spectro Scientific Industrial Tribology Laboratory (ITL) is a turnkey system that provides a complete lubricant analysis condition monitoring solution. The measurements made using the Industrial Tribology Laboratory determine lubricant and machine condition, the core of any effective predictive maintenance system. The ITL system is expandable and can incorporate testing and measurement solutions for other machinery fluids such as fuel, coolants, transformer oils and greases. The center piece of the ITL is the SpectrTrack LIMS software that helps use manage assets, oil sample life cycle, analytical results, reports and maintenance actions in one place. INDUSTRIAL TRIBOLOGY LAB SpectroTrack INFORMATION MANAGEMENT SYSTEM 62 Product Catalog

63 SpectroTrack INFORMATION MANAGEMENT SYSTEM SpectroTrack is an information management system (IMS) optimized for machine condition monitoring. The browser-based system is the ideal tool for accessing historical and trend information about an organization s high-value assets. The system provides a single end-to-end view of a sample lifecycle from sample submission and receipt to results entry. The software also provides all trending, imaging, numerical and textual asset data in one secure location. Clients and laboratory personnel can see a comprehensive, historical view of fluid condition for an engine, department or an entire fleet. Maintenance Operations Maintenance Management Benefits of SpectroTrack IMS Efficient Data Collection = Greater Expandability SpectroTrack offers a streamlined process for accepting oil analysis data from a variety of analytical instruments. Users have the flexibility to add new classes of analysis and additional parameters as needed, including trend analysis. Browser-based System = Easy Accessibility The system can be viewed on any browser-based device eliminating the need for installation on each workstation. Customers can access and view online interactive sample results anywhere and at any time to support them in making equipment maintenance decisions. Data Consolidation = Improved Accuracy and Consistency SpectroTrack brings information together with centralization of all oil analysis data as well as images from both Spectro Inc. s and other vendor s instrumentation. Simple System Deployment and Maintenance = Improved Productivity Once SpectroTrack is installed, operators only need browser access to begin using the software. With a zero footprint on the client machine and remote access support, the SpectroTrack minimizes the need for costly IT support and maintenance while giving the operator the information necessary to maintain the health of high-value assets. Assets Oil/Lubricant Samples Multi-lab Module = Enterprise-level Support with a Single Point of Contact SpectroTrack s multi-lab function integrates the workflow of multiple testing labs and enables each lab to view samples and support each other. Clients with assets deployed globally have visibility to all assets and conditions. Critical oil analysis test information is easily shared by all. Sample Management and Workflow = Removal of Gap Between Operator and Lab SpectroTrack facilitates the workflow between the equipment maintainer and the lab by managing the sample lifecycle. The system gives both customers and on-site labs the information critical to assess sample results, and ultimately, machine condition. OIL ANALYSIS LABORATORY INSTRUMENTS Test Results ITL Workshop Product Catalog 63

64 Feature Overview Self-contained installation on one server Automatically retrieves data from all Spectro Inc. instruments Designed specifically for oil analysis programs dedicated or contract testing Supports customer (private label) branding Remote Login Laboratory customer (interactive report viewers) can access defined data Remote portals can be connected to the Internet Accounts Laboratory user accounts and client accounts password protected Multi user accounts for distributor sales or corporate reliability grouping Equipment Assigned to accounts and can be searched, created, removed and reactivated with ease Detail includes manufacturer, application and components Maintenance feedback and notes visible to all stakeholders Components Rich customer component detail, complete with assigned test package Can be easily transferred to other equipment (engine change) Scheduling Schedule maintenance activities and analysis intervals Automatic reminders sent via Customer bottle labels printed prior to submittal Sample Login Auto-fill and drop-down selection Data Entry Bar code tracking bottle labels Shows status of each batch as it moves through the laboratory Automatic data collection from Spectro instruments Expandable with other vendor-supplied instruments Laboratory dashboard for easy workflow management Diagnostic Analysis User defined limits for each test Data rated as Notable, Abnormal, and Severe for both Hi and Lo limits Default and customizable diagnostic recommendations with historical trending Alarm Limits specific to Component Type, Manufacturer, Model, and Application Evaluation Results color-coded with severity level Evaluator assigns overall sample severity and comments Reports Mult-language support Printed or ed to assigned recipient or accessed by the web Test results, graphs, comments, and particle images Interactive portal reports SpectroTrack Product Information PART NUMBERS AND ADDITIONAL CONFIGURATION OPTIONS M90035 Base Product M90038 Additional Laboratory User License (each) M90036 SpectroTrack Custom Device Interface Import driver interface for lab instruments (Spectro products included in base product M90037 M90042 Client Portal Access Pack ( Clients) Multi Lab Option Resides on Main server Allows multiple labs to share and access SpectroTrack on main server. All laboratory users with rights can access and diagnose oil samples from all labs. Each lab must have P/N M90035 ACCESSORIES M90039 SpectroTrack Customer Reference Guide (Print ) M90041 SpectroTrack Laboratory Reference Guide (Print) P SpectroTrack Labelwriter P SpectroTrack Lab Barcode Labels (750/roll) P SpectroTrack Customer Labels (300/roll) I&T Installation & Training RECOMMENDED HARDWARE Server Processor RAM Hard Drive Operating systems x64 Processor: AMD Opteron, AMD Athlon 64, Intel Xeon with Intel EM64T support, Intel Pentium IV with EM64T support x86 Processor: Pentium III-compatible processor or faster 4 GB 500 GB Windows XP, Windows Server 2008 R2 Standard, Windows 7 Professional Edition or Higher, Windows Vista Professional Edition or Higher SpectroTrack oil analysis report of multi-site, power generation turbines. Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 64 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. SPECTROTRACK_DSv3_

65 SpectrOil M Series OIL ANALYSIS SPECTROMETER Standard for rugged spectrometric oil analysis in the field The SpectrOil M Series RDE-OES Elemental Analyzer is a compact, rugged, transportable spectrometer designed for accurate elemental analysis of a variety of fluids tested in the field or in a laboratory. Using the proven, reliable rotating disc electrode (RDE) technique, the analyzer measures trace quantities of elements dissolved or suspended as fine particles in natural or synthetic petroleum-based products. It includes new and in-service lubricants, hydraulic fluids, light (gasoline or diesel) or heavy fuels (HFO), coolants, industrial process water or washdown water for gas turbines. The SpectrOil M Series is widely used in commercial and military aviation, ground transportation, mining, power generation and commercial in service oil analysis laboratories. Originally designed for military applications in the mid 1990s, the SpectrOil M is the only in service oil analysis spectrometer approved by the US Department of Defense (DoD) Joint Oil Analysis Program (JOAP). Since its development, the SpectrOil M has been the industry standard for reliable, deployable spectrometers that perform the rapid analysis of wear metals, contaminants and additives in lubricants, hydraulic fluids, fuels, coolants and water. SpectrOil M Series key features Rugged frame and optics system that meets military shock and vibration and environmental test standards (JOAP CID-0191) Designed for remote locations and frequent transportation No sample preparation required 30 second analysis time Analyzes up to 31 elements simultaneously Self-sustained with built-in industrial touch panel PC Simple to operate; does not require special training No special utilities or gases required, only AC power Compliant to ASTM D6595 (In service Lubricant) and ASTM D6728 (Fuel) SpectrOil M Series includes the following models: MODEL APPLICATIONS DEFAULT CALIBRATION PROGRAM M/C-W M/F-W M/F-LD In service oil analysis for military, mining, oil & gas and commercial laboratories in remote locations Fuel quality control for power plant turbines and diesel/ gas engines No.2 diesel quality control for gas turbines, ultra low limits of detection for alkali metals and vanadium 24 elements for lubricant and hydraulics 15 elements for light fuel and heavy fuel 15 elements for No.2 Diesel, ultra low limits of detection OIL ANALYSIS LABORATORY INSTRUMENTS M/N-W Only approved oil analysis elemental spectrometer for aerospace, marine and ground support for US DoD Joint Oil Analysis Program (JOAP) 15 elements for JOAP Product Catalog 65

66 Laboratory Precision SpectrOil M is a rugged and precise Rotating Disc Electrode Optical Emission Spectrometer (RDE-OES). Measures sub-ppm elemental concentrations with high-purity carbon electrodes Detects elements in solution or particles as large as 10μm with RDE s precise pulsed-power, high-temperature plasma Accurately identifies elements in a wide variety of substances without sample preparation or dilution SpectrOil M Series consists of three main components 1. Excitation Source introduces energy to the sample. This includes a high voltage AC source that applies voltage across a small gap formed by the highly purified graphite rod and disc with the disc rotating and picking up oil from the sample holder under it. 2. Optical System At the core of the spectrometer is a Rowland circle grating optics system with 400 mm focal length. The temperature of the optics is tightly controlled at 40 C for the most stable result. Fourteen CCD array chips are precisely aligned on the edge of the optics. Light emitted from the burning sample is transmitted by optical fiber into the optics and diffracted by the grating into different wavelengths and picked up by the CCD chips. 3. Readout System detects and measures the light that has been separated into its component wavelengths by the optical system and presents this information to the operator in a usable fashion. A specific calibration program is applied to raw spectrum which eliminates the matrix effect, so results are compliant to ASTM standards. Then, the user only needs to select the calibration profile for specific fluids. So, switching from oil to fuel to coolant or water only takes seconds, not hours like ICP and other instruments. Grating Exit Slits CCDs Fixed Electrode AC Arc Rotating Electrode Entrance Slit Fiber Optic Cable Optics & diffraction grating produce a spectrum Sample Cup Schematic of how a SpectrOil analyzes a fluid sample to determine sub-ppm elemental content 66 Product Catalog

67 Available calibration programs (can be added to every model) CALIBRATION DESCRIPTION STANDARDS Lubricating oil (Commercial) Detects and quantifies elemental wear and additives in lubricants. Conforms to ASTM-D6595. Default 24 elements, up to 31 elements CS CS G SMA G Base oil 24 elements, 100 ppm 5 elements, 900 ppm Fuel (Light and heavy fuel) Low Detection (LD) Diesel Detects quality and contamination of petrochemicals from crude through the final blended light fuels. Conforms to ASTM D It includes both light and heavy fuel calibration programs. Special calibration for #2 Diesel with low limits of detection for alkali metals and vanadium. Specifically, the LOD of V is down to 0.1ppm, critical to meet turbine OEM specifications for diesel fuel quality control CS Base Oil CS-GT ppm for light fuel CS-GT ppm for heavy fuel CS-HP-100 High purity base oil CS-GT ppm, 15 elements CS-GT ppm, 15 elements ppm for Li, Na, K, V Coolant/Glycol Process water JOAP Airforce Analyzes in service coolants (water glycol mix) for additives and contamination Measures contamination in a variety of applications like power plant cooling water and turbine wash-down water JOAP Airforce calibration with 15 elements. Results correlate to SpectrOil M/N-W JOAP Army JOAP Army calibration with 20 elements. Results correlate to SpectrOil M/N-W ppm for V JDIW SIGLYCOLSTD-500 STE006 KIT DI water D19-0 Base Oil Diluted glycol standard DI water and 5ppm standard D elements, 100ppm D3-100 Zn, Mo, B, 100ppm D19-0 Base Oil D elements, 100ppm D3-100 Zn, Mo, B, 100ppm CS G SMA G 24 elements, 10ppm 5 elements, 900ppm Consumables used by calibration programs To ensure accurate and stable measurement results, different consumables are used for different calibration programs. Only Spectro Scientific certified consumables are qualified to meet performance specifications. CALIBRATION PROGRAMS DISC ROD SAMPLE HOLDER (CUP) Lubricant, coolant, water M97008 M97009 P high temperature sample cup (black) Light, heavy fuel, LD fuel M97008 M97009 P high temperature sample cup (black) M90204 sample cover for low flash point fuels JOAP Airforce and Army M97200 M97201 M90909 Aluminum boat sample holder Transit Case A transit case was designed for military personnel to transport the SpectrOil M where it is needed. A hydraulic lifting system is carefully balanced to the right of the SpectrOil so it is easily raised without effort. Four lifting rods are supplied with the SpectrOil M; they can be mounted on the unit so two people can quickly transfer the SpectrOil M from the transit case to a table top, and vice versa. OIL ANALYSIS LABORATORY INSTRUMENTS Product Catalog 67

68 SpectrOil M Series Product Information PRODUCT INFORMATION Part Numbers Spectro-M/C-W, Spectro-M/F-W Spectro-M/F-W, Spectro-M/C/R-W Spectro-M/N/R-W Applications new and in service lubricant, hydraulic, light or heavy fuel, water/glycol mix, water Output ASTM Calibration mg/kg (ppm) D6595 (Oil), D6728 (Fuel) Factory set, no re-calibration needed HARDWARE SPECIFICATIONS Excitation Source Oscillatory arc discharge Optical System Rowland Circle polychromator Optic. Temperature controlled at 40 C +/- 1C Spectral Range 203 nm to 810 nm Detectors CCD array OPERATIONAL SPECIFICATIONS Sample Volume 2 ml of fluid Ambient Operating 0 to 40 C (32F to 104F) Temperature Relative Humidity 0 to 90%, non-condensing USER INTERFACE SPECIFICATIONS Operating System Windows 7 Pro; Software SpectrOil V8 PC and Display Industrial touch panel PC, 12 diplay Data Storage Internal PC, USB, CD-RW POWER REQUIREMENTS Voltage Input AC 120/240V, 50/60Hz Power Consumption 1000 Watts at test MECHANICAL SPECIFICATIONS Dimensions 80 cm (L) x 63.5 cm (W) x 70 cm (H) (31.5 in x 25 in x 27 in) M/C, M/N, M/F Weights Shipping Dimensions Shipping Weights 114 kg (250 lbs) M/C, M/N, M/F 132 kg (290 lbs) M/C/R, M/N/R 102 cm (L) x 91 cm (W) x 94 cm (H) (40 in x 36 in x 37 in ) for M/C, M/N, M/F 152 cm (L) x 91 cm (W) x 94 cm (H) (60 in x 36 in x 37 in ) for M/C/R, M/N/R 261 kg (575 lbs) M/C, M/N, M/F 295 kg (650 lbs) M/C/R, M/N/R Element Lubricant Lubricant Extended Light Fuel Heavy Fuel Fuel Low Detection Glycol/ Coolant Ag Al As B ,000 Ba 0-6,000 Bi Ca 0-6, Cd Ce Co Cr Cu Fe In K ,000 Li Mg 0-6, , Mn Mo Na 0-6, ,000 Ni P 0-6, ,500 Pb Sb Si Sn Ti V W Zn 0-6, Zr Robotics Option The Double Disc Rapid Robot (D2R2) autosampler is a factory configured option for the SpectrOil M/C or SpectrOil M/N spectrometers that provides automatic operation of used oil sample analysis. The SpectrOil D2R2 does not use the traditional rod electrode used in manual systems. A specially designed rotrode disc is used, allowing for unattended operation. Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 68 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. SpectrOil M Series_DSv3_

69 SpectrOil 100 Series MARKET-LEADING RDE-OES SPECTROMETER FOR ELEMENTAL ANALYSIS SpectrOil Advantage SpectrOil RDE technology is a proven means of precisely determining elemental composition in engine oil, coolant, fuels, grease, process water, and a wide variety of critical operating fluids. For decades this robust technology has been used as both a quality control tool and machine health monitor. MACHINE HEALTH Oil is the lifeblood of equipment and thus oil analysis provides unique insights into machinery health. As a result, wear metals analysis with SpectrOil 100 is the backbone of used oil analysis programs and enables effective condition based maintenance programs. FLUID QUALITY CONTROL The precision of RDE spectrometry enables reliable, low concentration measurement of additive packages or harmful contaminants in virgin fuels, blended oil, coolants and wash down water. The precision of SpectrOil 100 makes it an essential fluids analysis tool in QC labs, and its simplicity and ease of use brings these reliable measurements to on-site predictive maintenance teams. The SpectrOil 100 is a Rotating Disk Electrode, Optical Emission Spectrometer (RDE-OES) built upon decades of technology development in support of the U.S. Military s Joint Oil Analysis Program (JOAP). This robust technology enables measurements to be made quickly and accurately on a variety of fluid types for condition monitoring and QC. Provides precise and reliable results Simultaneous multi-element analysis Repeatable and sensitive fluid characterization Conforms to ASTM-D6595 (oil), and ASTM-D6728 (fuel) Fast and easy to operate No sample preparation required No solvents or gasses required Quick 30 second analysis time Minimal training/background required to operate Immediate results on-site Analysis at your facility Bench-top, transportable system Low cost per sample SpectrOil 110 Basic Engine Wear package (15 essential elements) SpectrOil 120 Standard (24 elements) & Extended Range packages (31+ elements); options include Wear Metals, Coolants, Fuels and custom application packages MODEL 110E 120C 120F 120M Number of Elements OIL ANALYSIS LABORATORY INSTRUMENTS Default Calibration Lubricating Oils Lubricating Oils Light/Heavy Fuel JOAP Optional Calibrations No Yes Yes Yes Product Catalog 69

70 SpectrOil 100 Series Laboratory Precision At the core of the SpectrOil 100 is a precision Rotating Disk Electrode, Optical Emission Spectrometer (RDE-OES). Measure sub-ppm elemental concentrations with high-purity carbon electrodes. Detect elements in solution or particles as large as 10μm with RDE s precision pulsed-power, high-temperature plasma. Accurately identify elements in a wide variety of substances without sample preparation or dilution. HOW IT WORKS The RDE-OES technology utilizes a high-purity carbon electrode to transmit high-voltage electricity across a small gap to a nearby carbon disk. The rotating disk is partially submerged in a miniature cup of fluid sample and continuously carries the sample into the electrical discharge gap between electrodes. When the electricity arcs across the gap containing the sample, it forms a hightemperature plasma which emits a unique, sample-dependent spectrum of light from the ultraviolet, through the visible, and into the infrared wavelengths. The emitted light is collected and fiber-optically coupled to the SpectrOil 100 s sensitive optics which includes a diffraction grating to sort the light by wavelength and focus it onto an array of highly sensitive CCD Grating cameras. Sophisticated spectral Exit Slits analysis software processes the CCDs spectra to precisely determine concentration of CCDs dozens of elements with Fixed Electrode sub-ppm precision. AC Arc Entrance Slit Optics & diffraction grating produce a spectrum Rotating Electrode Fiber Optic Cable Sample Cup Schematic of how a SpectrOil analyzes a fluid sample to determine sub-ppm elemental content. 70 Product Catalog

71 On-site Simplicity The simplicity and ease of using the SpectrOil 100 enables RDE technology to be brought to on-site inspection and condition based maintenance sites. The disposable electrodes & sample cup facilitate rapid sample changes and ensure contamination free measurements. Without the purge gas or sample dilution required by other technologies, the simple RDE-OES steps are: Pour your fluid, close the door, and press START. The sophisticated analytics are automated, so no highly skilled or trained users are required. Just follow the simple steps and read the elemental results. APPLICATIONS Oil & Grease Condition Monitoring Detecting and quantifying elemental wear in lubricants enables a rapid, non-invasive determination of machine condition, while monitoring for additive depletion ensures that lubricating fluids continue to protect critical assets according to ASTM-D6595. WEAR: Quantify elemental composition of wear debris to determine the location and severity of component wear. CONTAMINATION: Detect unexpected elements to indicate fouled air filters, coolant leaks, sea water ingress, or dirt ingestion. CHEMISTRY: Measure additive package depletion to ensure expected oil protection. Fuel & Lubricant Quality Control SpectrOil is used to ensure composition and quality of petrochemicals from crude through the final blended product to ensure that processing is acceptable and to protect finished fuel against trace contamination through handling, storage, and to the user in accordance with ASTM D Coolant Condition Measurements Analyzing in-service coolant is a quick and accurate means of ensuring that it continues to provide the required corrosion protection and heat transfer. OIL ANALYSIS LABORATORY INSTRUMENTS Process Water Condition Analysis Measuring contamination in a variety of applications like power plant cooling water and turbine wash water provides unique system condition insights and ensures compliant disposal or reuse. *Trivector is a trademark of Emerson Process Systems *Trivector is a trademark of Emerson Product Catalog Process Systems 71

72 SpectrOil 100 Product Information PRODUCT INFORMATION Part # Applications Output Methodology Standard Analytical Range Calibration Excitation Source OPTICAL SYSTEM Optical System Spectral Range Spectro-[Model]-[Hz]-[Volts] Mineral and synthetic lubricants, distilled fuel, heavy fuel oil (HFO), crude, glycol coolants and turbine washdown water Concentration mg/kg (ppm) ASTM D6595; D6728 Up to 31 elements from Li to Pb Typically ppm (varies by application) Factory set, no maintenance required Oscillatory arc discharge, JOAP characteristic Pashen-Runge polychromatar optic (Rowland Circle Alignment) 203 nm to 810 nm Temperature Control Thermally Stabilized; 40 C ± 1 C Detectors OPERATIONAL SPECIFICATIONS Sample Volume Solvents/Reagents Ambient Operating Temperature Relative Humidity CCD proprietary design for frequency range of interest 2 ml of fluid None 0 to 40 C (32 F to 104 F) 0 to 90%, non-condensing USER INTERFACE SPECIFICATIONS Software/Operating System Display Data Storage Data Transfer Data Entry POWER REQUIREMENTS Windows 10 Pro or Windows 7 Pro, 32 or 64 bit, US English version External Monitor External PC USB External Keyboard and Mouse SpectrOil Models and Calibration Ranges in ppm APPLICATION 110E 120C 120F BASIC ENGINE STANDARD LUBRICANTS EXTENDED OPTION COOLANT FUELS Ag Al As B ,000 Ba 0-6,000 Bi Ca 0-3, , Cd Ce Co Cr Cu Fe In K , Li Mg 0-6, ,500 Mn Mo Na 0-3, , , Ni P 0-3, , ,500 Pb S Sb Si Sn Ti V W Zn 0-3, , Zr Total# Voltage Input Power Consumption Fusing AC 120/240V, 50/60 Hz 500 Watts at test 10 amps Consumables & Standards MECHANICAL SPECIFICATIONS Dimensions 70.6 cm (H) x 38.4 cm (W) x 66 cm (L) (27.8 in x 15.1 in x 26 in) Weight 70 kg (154 lbs) Shipping Package Dimensions Shipping Package Weight COMPLIANCE CE Mark: EMC Directive (2004/108/EC); RoHS cm (H) x 63.5 cm (W) x cm (L); (48 in x 25 in x 43 in) 150 kg (330 lbs) KITS M97007 M97016 M97017 M97018 M97019 M97020 M96380 Consumables Kit for 500 measurements (rod & disk electrodes, sample cups, pipettes, wipes, cleaning solution, swabs, gloves) Oil Standards Fuel Standards Fuel Standards, Low Detection Water Standards Coolant Standards Routine Maintenance Kit Use Spectro Scientific certified consumables and standards to ensure the accuracy and repeatability of your measurements. Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 72 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. SpectrOil100_DSv3_

73 Ferrous content Wear particle shape Particle count and codes LaserNet 200 Series PARTICLE COUNTER, WEAR CLASSIFIER, FERROUS MONITOR The LaserNet 200 Series is much more than a particle analyzer. It also calculates free water in ppm, and differentiates contaminants (silica) from machine wear (metal). In addition, this instrument provides particle counts and codes, abnormal wear classification and ferrous wear measurement. Widest range up to 10 million particles/ml Automatic wear particle shape classification and ferrous particle analysis Imaging of dark fluids containing up to 2% soot Error correction for water and air bubbles LaserNet Comparison Total particle count & codes Non-metallic particles (sand/dirt) Free water measurement Air bubble/water droplet correction Wear particle classification Total ferrous concentration Ferrous particle count & size distribution Large ferrous concentration Autosampler option The LaserNet 200 Series is the world s best particle analyzer for lubrication and hydraulic oil testing. In commercial laboratories, power generation plants and industrial facilities, the LaserNet 200 Series offers unrivaled functionality for contamination control and condition-based maintenance programs. FEATURES INCLUDE: Particle count, size distribution and codes (ISO 4406, NAS 1638, NAVAIR 01-1A-17, SAE AS 4059, GOST, ASTM D6786, HAL and user-defined bins). Differentiation of contaminants (silica and fibers from machine wear metal) Classification of wear particles, image storage and reporting of particle count and size for Cutting, Sliding, Fatigue, Fibers and Non-metallics wear types Ferrous content measurement in the sample with ferrous particle count and size distribution Differentiation of large ferrous particles >25 micron from total ferrous particles. Reporting percentage of large ferrous particles and ferrous wear severity index for easy trending and interpretation of the ferrous measurements. Multiple configurations and options cover the needs of commercial laboratories and industrial plants for contamination control and predictive maintenance. OPTIONS INCLUDE: Ferrous Monitor to measure ferrous content enables measurement of both ferrous content and total particle count on the same sample, eliminating the need to measure ferrous content on another instrument Classification of wear particle shape directly images wear particle silhouettes and counts and classifies wear particles over 20 microns Autosampler for high throughput sample processing provides automated, unattended processing of up to 24 used oil or hydraulic fluid samples OIL ANALYSIS LABORATORY INSTRUMENTS Product Catalog 73

74 Particle Counter, Wear Classifier, and Ferrous Monitor The LaserNet 200 Series provides particle counts and codes, large wear particle classification and ferrous wear monitoring. Options include an autosampler for high throughput sample processing as well as configurations without the ferrous monitor and wear classification. CUTTING WEAR FATIGUE WEAR SLIDING WEAR NONMETALLIC Establishing alarm limits and condemnation levels for large machinery wear particles is often challenging. Unlike parameters such as ISO code, water, elemental concentration and TAN, there are no pre-defined limits set by the equipment supplier. In each piece of equipment, machinery wear particles of different sizes reach their own dynamic equilibrium condition. The LaserNet 200 software calculates recommended wear particle limits for categories of cutting wear, severe sliding wear and fatigue wear by analyzing a series of six or more samples. Wear images are stored and analyzed directly on the LaserNet 200 software. They can be sorted by wear class. OilView TM software also reports on particle count and size distribution by wear category. Ferrous Particle Count & Size FILTER SCREEN FLOW CELL x4 Lens CCD CAMERA 640 x 480 resolution 100 frames/s Actual Pixel Resoluion SMALL COIL SET Particle size distribution ISO 4406 cleanliness codes Particle shape classification CUTTING SLIDING FATIGUE NON METALLIC WATER LARGE COIL SET Ferrous PPM PUMP WASTE Schematic of LaserNet 230 Series 74 Product Catalog

75 Sample preparation Sample preparation is efficient with the LaserNet 200 Series viscosities up to 320cSt can be processed without dilution due to the wide dynamic range. And, unlike conventional light blockage particle counters, there are no flow control valve adjustments needed when testing different sample viscosities. With an intuitive, configurable graphical user interface and no calibration required, the LaserNet 200 Series is fast, accurate and easy to use. Data Management The LaserNet 200 Series has a data export capability to laboratory LIMS systems as well as comma or tab delimited text file formats. The wear images can be exported as.jpeg or.bmp files. Spectro Scientific s MiniLab Series software, when integrated with the OilView LIMS module, can transfer data to the AMS Machinery Health Manager LIMS module. SpectroTrack is a browser-based Laboratory Information Management System (LIMS). It provides a single view of a sample lifecycle from scheduling the sample to report generation and includes a customizable asset management database for trend analysis. ASP Autosampler The ASP autosampler is a low cost solution for automatic and unattended processing of a batch of up to 24 samples. The ASP may be added to existing LaserNet 200 installations with minimal setup. Features include: Automatic reversing stirrer Two-stage wash system using focused spray jets Quick disconnect/shutoff for solvent supply and drainline SpectroTrack LIMS sample lifecycle report LaserNet 200 Series integrates with the AMS Machinery Health OilView TM LIMS OIL ANALYSIS LABORATORY INSTRUMENTS Product Catalog 75

76 LaserNet 200 Series Product Information PART NUMBER LaserNet 210 particle counter. Requires SA1023 or SA1024 accessory kit and a PC LaserNet 215 particle counter with ferrous monitor. Requires SA1025 or SA1026 accessory kit and a PC LaserNet 220 particle counter with wear particle shape classifier. Requires SA1023 or SA1024 accessory kit and a PC LaserNet 230 particle counter, wear particle classifier, and ferrous monitor. Requires SA1025 or SA1026 accessory kit and a PC. SA1023 SA1024 SA1025 SA1026 LaserNet 210/220 standard accessories with ultrasonic cleaner, 115V LaserNet 210/220 standard accessories with ultrasonic cleaner, 220V LaserNet 215/230 standard accessories with ultrasonic cleaner, 115V LaserNet 215/230 standard accessories with ultrasonic cleaner, 220V ACCESSORIES AND CONSUMABLES LNF-909 LaserNet 200 Series routine maintenance kit LNF-910 LaserNet 200 Series with Skydrol configuration routine maintenance kit LNF-509 LNF-545 Calibration check fluid 2806, 400 ml Ferrous validation standard, 400 ml LNF-902 Skydrol kit (phosphate ester fluids) for LaserNet 210 and LaserNet 220 only (factory installation) LNF-905 Skydrol kit (phosphate ester fluids) for LaserNet 215 and LaserNet 230 only (factory installation) M99919 ASP sample bottles, 120 ml (4 oz), package of Spectro certified sample bottle, PET, 120 ml (4 oz), package of 50 ASP Autosampler for LaserNet 200 Series, 115/230V M90035 SpectroTrack LIMS software For other configuration options see SpectroTrack datasheet PRODUCT INFORMATION Applications Mineral and synthetic lubricants including gear, engine, hydraulic, turbine and distillate fuels Output Methodology Particle count: ISO 4406, NAS 1638, NAVAIR 01-1A-17, SAE AS 4059, GOST, ASTM D6786, HAL and user defined Total ferrous, ppm Large ferrous, ppm Ferrous particle count and distribution Percentage large ferrous particles, % Ferrous wear severity index Free water, ppm; Soot wt. %; Particle shape per LaserNet 200 Series method ASTM D7596 Standard Analytical Range Calibration Particles 4 μm μm Not required. Validation standards supplied with instrument. OPERATIONAL SPECIFICATIONS Sample Volume 5-30 ml, varies with viscosity Solvents/Reagents Recommended solvents when processing mineral based oils: Electron-22 Environmentally Safe Solvent Alternative solvent for dry oils Lamp Oil/Kerosene Diesel or Jet Fuel Notes: 1. Lamp oil/kerosene, diesel, or jet fuel not effective for flushing after samples with high water content. 2. Higher flammability solvents (Isopropyl Alcohol (IPA), Hexane, Heptane, Naptha, Mineral Spirits, Toluene, Petrol) may be used with appropriate caution in the LaserNet, however; these may NOT be used with an ASP. 3. Solvent options when processing Skydrol: IPA (Isopropyl Alcohol) or Acetone only Environmental Operating Requirements USER INTERFACE SPECIFICATIONS Software/Operating System 5C to 40C ambient temperature, 10-80% relative humidity, non-condensing, 2000 m maximum altitude Windows 7, Windows 10 Pro, 32 or 64 bit, US English version POWER REQUIREMENTS Power LaserNet 200 Series: AC 110/240 V, 50/60 Hz, 10 Watts ASP: AC 115/230 V. 50/60 Hz, 2.5A/1.6A MECHANICAL SPECIFICATIONS Dimensions H x W x D Weight Shipping Package Dimensions H x W x L Shipping Package Weight LaserNet 200 Series: 22.9 cm x 17.8 cm x 43.2 cm (9 in x 7 in x 17 in) ASP: 55 cm x 62 cm x 52 cm (21.5 in x 24.5 in x 20.5 in) LaserNet 200 Series: 7.7 kg (17 lbs) ASP: 35 kg (76 lb) LaserNet 200 Series: 35.6 cm x 36.8 cm x 78.7 cm (14 in x 14.5 in x 31 in) ASP: 82 cm x 76 cm x 71 cm (32 in x 30 in x 28 in) LaserNet 200 Series: 12.2 kg (27 lbs) ASP: 60 kg (130 lbs) COMPLIANCE CE Mark: EMC Directive (2004/108/EC); RoHS, UL, CSA, ETL SUPPORT CONTRACTS SVC025 Service Contract LaserNet 210/LaserNet 220 SVC026 Service Contract LaserNet 215/LaserNet 230 Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 76 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. LaserNet 200 Series_DSv4_

77 T2FM 500 FERROGRAPHY LABORATORY Predictive maintenance by wear particle analysis In today s modern power generation, manufacturing, refining, transportation, mining and military operations, the cost of equipment maintenance, service, and lubricants are ever increasing. Parts, labor, equipment downtime, lubricant prices and disposal costs are a primary concern in a well run maintenance management program. Machine condition monitoring based on oil analysis has become a prerequisite in comprehensive maintenance programs. The Ferrography Laboratory plays a key role in such programs. It separates and concentrates wear and contaminant particles for microscopic examination. Particle size, surface characteristics and composition are then used to determine wear modes inside a machine so that maintenance recommendations can be made. Particles and contaminants indicate the wear mode inside a machine. A Ferrography Laboratory for fast efficient, low cost separation and interpretation of wear and contaminant particles from used lubrication oils, hydraulic fluids, greases, coolants and fuels. The Thistle Tube Concept T2FM stands for Thistle Tube Ferrogram Maker. The heart of the T2FM is the glass thistle tube. The name comes from its unique shape resembling the thistle plant. The glass thistle tube provides a constant and efficient flow of sample into the substrate. The sample, after dilution, is poured directly into the top of the thistle tube. In seconds, the sample begins flowing across the ferrogram. The diameter and length of the capillary section of the thistle tube controls the flow rate onto the ferrogram. A rinse cycle is initiated as soon as the last of the sample has left the thistle tube. Solvent is dripped onto the lip of the thistle tube as it is slowly rotated, thoroughly rinsing the walls and cleaning it for the next sample. Innovation, Quality and Support The T2FM 500 prepares a ferrogram more quickly than ever before. There is no delay time as sample is pumped through plastic tubing before reaching the ferrogram surface. Furthermore, the rinse may begin as soon as the sample leaves the thistle tube. The T2FM delivers the entire sample and all the particles contained therein onto the ferrogram surface. There is also no distortion of particles since the thistle tube concept eliminates the need for a pump. A crystal clear rinse is obtained without fail for every ferrogram. There are no last minute drips of oil sample onto the ferrogram leaving distracting halos around the particles when viewed under the microscope. Bichromatic Microscope A bichromatic microscope is used to view and examine ferrograms made with the T2FM 500. The bichromatic microscope is equipped with both reflected and transmitted light sources so that the ferrogram may be illuminated from both above and below the microscope stage. A green filter is used in the transmitted light path and a red filter is used in the reflected light path, this is referred to as bichromatic illumination in the practice of ferrography. With bichromatic illumination, metal particles which reflect light appear bright red, whereas nonmetallic particles appear green because light transmits through them. Product Catalog 77 OIL ANALYSIS LABORATORY INSTRUMENTS

78 Video Camera and Software A video camera connected to a computer displays, prints, stores and retrieves ferrographic images. Comparison of old ferrograms with ferrograms from recent lubricating oil samples allows determination of evolving wear modes inside a machine or engine. Main Components of the Ferrography Laboratory Model T2FM Analytical Ferrograph Bichromatic microscope Video camera Video capture card Image capture software Optional industrial standard PC Key Features of the T2FM 500 Efficient separation of wear and contaminant particles from fluid samples Rapid preparation of ferrogram No deformation of particles Separates particles up to 800 μm in size Lower cost per sample Uses fewer consumables Achieves cleaner rinses Easy to operate ASTM D7690 compliant Combination of analytical ferrography and total ferrous content analyzer improves speed and provides more comprehensive wear particle analysis. Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 78 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. T2FM 500_DSv2_

79 Application Specific Instruments

80 Application Specific Instruments In addition to the oil analysis systems and instruments used for wide range of industry and applications, Spectro Scientific provides applications specific instruments to help customer solve unique problems in their industry. InfraCal 2 ATR-B are ATR-E are biodiesel and ethanol blend analyzer using filter-based infrared absorption technology to provide simple and accurate biofuel blend measurement for biofuel production and distribution. InfraCal 2 Trans-SP and ATR-SP are oil in water/soil analyzer using filter-based infrared absorption technology to test water quality for Oil and Gas and industrial discharge water applications. SpectrOil MNW is a rugged elemental spectrometer specifically designed for US DOD Joint Oil Analysis Program (JOAP) to support fix-wing air planes, helicopters, ground support vehicles and marine vessels worldwide. SpectrOil MFW Elemental Spectrometer based on Option Emission Spectroscopy (OES) is for quality inspection and treatment of diesel, light and heavy fuel for gas turbines and diesel engines in power plants worldwide. Fluidscan 1210 InfraRed BN Analyzer is to measure Base Number (BN) for cylinder oil in large 2 stroke engines used in Marine vessels and power generation plants based on Infrared absorption spectroscopy. CoolCheck2 is a UV-VIS and NIR dual spectrometer testing Coolant and DEF (Diesel Exhausted Fluid) for on and off road transportation fleet maintenance 80 Product Catalog

81 Infracal 2 Biofuel Analyzers MEASURING PERCENT BIODIESEL IN DIESEL OR ETHANOL IN GASOLINE As more mandates for a minimum of ethanol in gasoline and biodiesel in diesel come into effect, a large number of major oil companies are blending higher percentages of biofuels at their terminals. Although manufacturers of in-line blending systems claim indisputable accuracy, a quick analytical measurement method to assess the blend ratio gives real data to a claimed assumption In less than a minute, the user gets a direct readout in percent biodiesel or ethanol on-site at a terminal, distribution center or laboratory. This can be a valuable asset for: Terminal managers Fuel distributors Engine manufacturers Fleet operators Regulatory agencies InfraCal 2 Biofuel Analyzers are: Rugged and compact Portable and easy to use Designed for non-technical personnel The InfraCal 2 Biofuel Analyzer is a low-cost, single wavelength analyzer with filters preset for a particular measurement either biodiesel in diesel or ethanol in gasoline. Biodiesel has a characteristic infrared absorption band at 5.73 μm (1745 cm -1 ). Ethanol s infrared absorbance is at 9.6 μm (1045 cm -1 ). As the biodiesel or ethanol percentage increases, the infrared absorbance increases. An internal calibration table in the InfraCal 2 Biofuel Analyzer converts infrared absorbance to a digital readout in percent. A fuel sample is placed directly on the exposed ATR sample window and after 10 seconds the percent biodiesel or percent ethanol is displayed. The fuel is easily cleaned off the window using a solvent and a wipe and the analyzer is ready for the next sample. The InfraCal 2 Biofuel Analyzers are ideal where a single, repetitive analysis is needed. InfraCal 2 ATR-B for measuring percent biodiesel has a measurement range of 0-100% biodiesel in diesel and an accuracy of +/- 0.2, the InfraCal 2 is based on proven IR technology developed by Wilks and used by regulatory agencies and fuel terminals worldwide. The compact, easy-to-use InfraCal 2 ATR-B measurement results are comparable to both ASTM D7371 and EN Biodiesel in diesel % +/ /- 0.2 Biodiesel in diesel % +/- 1% of concentration The InfraCal 2 ATR-E is the latest introduction to our easy to use analyzers for measuring ethanol in petrol. The InfraCal 2 ATR-E is a stand-alone fixed filter infrared instrument that gives results that are comparable to gas chromatographic methods and correlates with ASTM Ethanol in gasoline 0-20% +/- 0.2 Ethanol in gasoline 70-98% +/- 1% of concentration Principle of Operation Samples are applied to a zinc selenide (ZnSe) attenuated total reflectance (ATR) sample plate. Infrared light from a source bounces multiple times between the top and bottom surfaces of ZnSe crystal as it travels horizontally from one side to the other. It is then filtered and measured by the detector. The loss of the light at a specific wavelength is due to the absorption by the fuel sample on the top plate and it is then calculated to percentage of biodiesel or ethanol based on calibration APPLICATION SPECIFIC INSTRUMENTS Product Catalog 81

82 InfraCal 2 Biofuel Analyzers Product Information PART NUMBERS Model ATR-B calibrated: 0-100% biodiesel in diesel using standards prepared by a certified laboratory. Includes internal battery, auto adapter and universal power supply Model ATR-E calibrated: 0-20% & % ethanol in gasoline using standards prepared by a certified laboratory. Includes internal battery, auto adapter and universal power supply. SPECIFICATIONS InfraCal 2 ATR-B InfraCal 2 ATR-E Applications Biodiesel in diesel Ethanol in gasoline Analytical Wavelength/ Wave Number Outputs 5.7 mm, 1745 cm mm, 1045 cm -1 % (by weight) biodiesel in diesel % (by weight) ethanol in gasoline Analytical Range 0-100% 0-20 & 70-98% Analysis Time Less than 30 seconds Less than 30 seconds Instrument Repeatability USER INTERFACE SPECIFICATIONS User Interface Data input 0-30% ± 0.2%, % ±1% of biodiesel (FAME) concentration 6 color display Touch screen Communication Port USB, RS 232 POWER REQUIREMENTS Battery Power Source External Power Requirements Power Adaptor Input Battery Run Time 18 volt NiCad battery 18 volts DC, 3.3 amps Universal AC/DC 4-6 hours 0-20% ± 0.2%, 20-98% ± 1% of ethanol in petrol concentration MECHANICAL SPECIFICATIONS Weight Dimensions Shipping Weight Shipping Dimensions COMPLIANCE CE, FCC Class B, NEMA 2, IP lbs (3.2 kg) 6.7 x 7.8 x 5.2 (170 x 198 x 132 mm) 8.0 lbs (3.6 kg) 10 x 10 x 14 (254 x 254 x 355 mm) INFRACAL 2 ATR-B CALIBRATION STANDARD SETS % Biodiesel in Diesel Calibration Standards The set includes eight standards; 0, 2, 5, 10, 15, 20, 25, and 30% biodiesel in High Cetane diesel fuel prepared by a certified laboratory. Each vial contains 20 ml of standard, good for a minimum of 15 tests % Biodiesel in Diesel Calibration Standards The set includes twelve standards; 0, 2, 5, 10, 15, 20, 25, 30, 50, 75, 95, 100 biodiesel in High Cetane diesel fuel prepared by a certified laboratory. Each vial contains 20 ml of standard, good for a minimum of 15 tests. INFRACAL 2 ATR-E CALIBRATION STANDARD SETS Point Ethanol Low Concentration Calibration Standard Set Standard concentrations are 0, 5, 10, 15, and 20% ethanol in gasoline. Standards are prepared by a certified laboratory. Each vial contains 20 ml of standard, good for a minimum of 15 tests Point Ethanol High Concentration Calibration Standard Set Standard concentrations are 70, 80, 90, 95, and 100% ethanol in gasoline. Standards are prepared by a certified laboratory. Each vial contains 20 ml of standard, good for a minimum of 15 tests. ACCESSORIES Carrying case for InfraCal Analyzers with pre-diced pluck foam x 14.6 x 8 ; 10 lbs Dust cover OPERATING SPECIFICATIONS Sample Volume Solvent/Reagent Operating Temperature Relative Humidity Altitude < 1 ml None 5 C - 40 C 0-90%, non-condensing Up to 5000 meters Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 82 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. InfraCal 2 ATR-B & ATR-E_DSv1_

83 InfraCal 2 Analyzers MEASURING OIL IN WATER & SOIL APPLICATIONS Testing produced water on offshore or onshore oil rigs Monitoring refinery or industrial plant wastewater effluents Measuring FOG discharge levels Checking oil/water separation systems Measuring oil in drilling mud/cuttings Testing for residual oil on pre-cleaned metal components Determining the purity level of reclaimed solvents Onsite testing of soil at remediation sites FEATURES Results in less than 15 minutes Sub-ppm measurements Rugged, portable, easy-to-use Internal data logging Export via USB Multiple calibrations InfraCal 2 ATR-SP InfraCal 2 TRANS-SP MDL Water 0.3 ppm 0.1 ppm MDL Soil 3 ppm 1 ppm Solvent Method Complies Method Compares Hexane, pentane, cyclohexane, Vertrel MCA EPA 1664 ISO Perchloroethylene, S-316, Freon-113 ASTM D7066 EPA & EPA EPA 1664 ISO Over 4,000 oil in water/soil analyzers in world-wide use today The InfraCal 2 Oil in Water Analyzers quickly and accurately measure TOG (total oil & grease), FOG (fats, oil and grease) and TPH (total petroleum hydrocarbons) in produced water, industrial wastewater and soil. InfraCal 2 analyzers have become the petrochemical industry standard ensuring oil content levels in produced water, drill cuttings or soil are below the regulated limit. The InfraCal 2 ATR-SP is recommended for measuring oil in water, TPH in soil or FOG in wastewater concentration levels when using hexane, pentane or Vertrel MCA as the extracting solvent. Measurement data obtained with this analyzer will correlate to EPA Method 1664 as both procedures are based on evaporation techniques and measuring the residual oil and grease. The analyzer is equipped with a built-in cubic zirconia horizontal attenuated total reflection (HATR) stainless steel sample stage. The InfraCal 2 TRANS-SP is recommended for measuring oil in water, TPH in soil or FOG in wastewater concentration levels using the traditional EPA methods and or ASTM method D and Freon-113, hydrocarbon-free grade of perchloroethylene, AK-225, S-316 or other spectroscopic infrared transparent solvent as the extracting solvent. Since the extract is deposited into a 10 mm quartz cuvette cell with Teflon stopper, light end volatile components are retained for measurement. Accurate down to 0.1 ppm. ATR-SP TRANS-SP Principle of Operation The InfraCal 2 Analyzers for measuring total oil and grease and total petroleum hydrocarbons in water and soil makes use of the fact that hydrocarbons such as oil and grease can be extracted from water or soil through the use of an appropriate solvent and extraction procedure. The extracted hydrocarbons absorb infrared energy at a specific wavelength and the amount of energy absorbed is proportional to the concentration of oil and grease in the solvent. The analyzer can be calibrated to read out directly in the desired units. APPLICATION SPECIFIC INSTRUMENTS Product Catalog 83

84 InfraCal 2 ATR-SP and TRANS-SP Product Information SPECIFICATIONS Analytical Wavelength/ Wave Number Power Requirements Power Supply Weight Dimensions Suggested Operating Range Measurement Range For Water Measurement Range For Soil Analysis Time 3.4 µm, 2930 cm volts DC, 3.3 amps, internal battery Universal AC/DC provided 5.8 lb (2.6 kg), with battery lbs (3.2 kg) 6.7 (17cm) x 7.8 (19.8 cm) x 5.2 (13.2 cm) 40 F (5 C) 110 F (40 C) ATR-SP: ppm TRANS-SP: ppm ATR-SP: ppm TRANS-SP: ppm minutes, including extraction process Instrument Repeatability ATR-SP: ±0.2 ppm TRANS-SP: ±0.1 ppm Communication Port USB, RS 232 INFRACAL 2 ATR-SP FACTORY CALIBRATED ANALYZERS Includes a factory calibration using Hexane TOG/TPH High Range Calibration Standards for samples containing primarily petroleum hydrocarbons. Water: 10, 25, 50, 100, 150, and 200 mg/l Includes a factory calibration using Hexane TOG/TPH Low & High Range Calibration Standards for samples containing primarily petroleum hydrocarbons. Water: 0.5, 1, 2.5, 5.0, and 7.5 mg/l & 10, 25, 50, 100, 150, and 200 mg/l Includes a factory calibration using Hexane TOG/FOG Calibration Standards for wastewater that contains animal and/or plant oils. Water: 10, 25, 50, 100, 150, and 200mg/L INFRACAL 2 ATR-SP CALIBRATION STANDARDS SETS Low Range Hexane TOG/TPH Five Point Calibration Standard Set: Light Mineral Oil in hexane prepared by a certified laboratory. The set contains 6 standards from 0.5mg/L to 7.5 mg/l (ppm) for water and 5 mg/kg to 75 mg/kg for soil, includes solvent blanks. Recommended for customers in the petroleum industry who are primarily measuring low levels of petroleum hydrocarbons in water or soil Hexane TOG/TPH Six point Calibration Standard Set: Light Mineral Oil in N-Hexane prepared by a certified laboratory for TOG/TPH Analysis. Nominal concentration values are 100 mg/kg (ppm), 250 mg/kg, 500 mg/kg, 1000 mg/ kg, 1500 mg/kg and 2000 mg/kg for soil assuming a 1:1 extraction ratio; and 10 mg/l (ppm), 25 mg/l, 50 mg/l, 100 mg/l, 150 mg/l and 200 mg/l for water assuming a 10:1 extraction ratio. The set contains 6 standards along with a solvent blank in 2 ml flame sealed ampoules. Recommended for customers in the petroleum industry who are primarily measuring petroleum hydrocarbons in water or soil Hexane TOG/FOG Six Point Calibration Standard Set: 50:50 Soybean Oil/Hexadecane in N-Hexane prepared by a certified laboratory. Nominal concentration values are 10 mg/l (ppm), 25 mg/l, 50 mg/l,100 mg/l, 150 mg/l and 200 mg/l for water assuming a 10:1 extraction ratio. The set contains 6 standards along with a solvent blank in 2 ml flame sealed ampoules. Recommended for customers measuring non-polar (petroleum) and polar (animal and vegetable fats) hydrocarbons for TOG or FOG measurements such as municipal wastewater or industrial wastewater that includes animal and vegetable fats. INFRACAL 2 TRANS-SP FACTORY CALIBRATED ANALYZERS TRANS-SP Includes a factory calibration using S-316 standards for samples containing primarily petroleum hydrocarbons with minimal animal/plant oils. Water: 10, 25, 50, 100, 150, and 200 mg/l TRANS-SP Includes a factory calibration using S-316 standards for samples containing primarily petroleum hydrocarbons with minimal animal/plant oils. Water: 0.5, 1, 2.5, 5.0, and 7.5 mg/l & 10, 25, 50, 100, 150, and 200 mg/l TRANS-SP Includes a factory calibration using S-316 standards for samples containing primarily animal and/or plant oils. Water: 10, 25, 50, 100, 150, and 200 mg/l TRANS-SP Includes a factory calibration using Tetracloroethylene standards for samples containing primarily petroleum hydrocarbons with minimal animal/plant oils. Water: 10, 25, 50, 100, 150, and 200 mg/l TRANS-SP Includes a factory calibration using Tetracloroethylene standards for samples containing primarily petroleum hydrocarbons with minimal animal/plant oils. Water: 0.5, 1, 2.5, 5.0, and 7.5 mg/l & 10, 25, 50, 100, 150, and 200 mg/l INFRACAL 2 TRANS-SP CALIBRATION STANDARDS SETS TOG/TPH Low Range S-316 TOG/TPH Five Point Calibration Standard Set: Light Mineral Oil in S-316 prepared by a certified laboratory. The set contains 6 standards from 0.5mg/L to 7.5 mg/l (ppm) for water and 5 mg/kg to 75 mg/kg for soil, includes solvent blanks. Recommended for customers in the petroleum industry who are primarily measuring low levels of petroleum hydrocarbons in water or soil TOG/TPH High Range S-316 Six Point Calibration Standard Set: Light Mineral Oil in S-316 prepared by a certified laboratory for TOG/TPH Analysis. Nominal concentration values are 100 mg/kg (ppm), 250 mg/kg, 500 mg/kg, 1000 mg/kg, 1500 mg/kg and 2000 mg/kg for soil assuming a 1:1 extraction ratio; and 10 mg/l (ppm), 25 mg/l, 50 mg/l, 100 mg/l, 150 mg/l and 200 mg/l for water assuming a 10:1 extraction ratio. The set contains 6 standards along with a solvent blank in 4 ml flame sealed ampoules. Recommended for customers in the petroleum industry who are primarily measuring petroleum hydrocarbons in water or soil FOG/TOG High Range S-316 TOG/FOG Six Point Calibration Standard Set: 50:50 Isooctane/Octanoic Acid in S-316 as per ASTM Method D prepared by a certified laboratory. Nominal concentration values are 10 mg/l (ppm), 25 mg/l, 50 mg/l, 100 mg/l, 150 mg/l and 200 mg/l for water assuming a 10:1 extraction ratio. The set contains 6 standards along with a solvent blank in 4 ml flame sealed ampoules. Recommended for customers measuring non-polar (petroleum) and polar (animal and vegetable fats) hydrocarbons for TOG or FOG measurements such as municipal wastewater or industrial wastewater that includes animal and vegetable fats TOG/TPH Low Range Tetrachloroethylene TOG/TPH Five Point Calibration Standard Set: Light Mineral Oil in Tetrachloroethylene prepared by a certified laboratory. The set contains 6 standards from 0.5mg/L to 7.5 mg/l (ppm) for water and 5 mg/kg to 75 mg/kg for soil, includes solvent blanks. Recommended for customers in the petroleum industry who are primarily measuring low levels of petroleum hydrocarbons in water or soil TOG/TPH High Range Tetrachloroethylene TOG/TPH Six Point Calibration Standard Set: Light Mineral Oil in Tetrachloroethylene prepared by a certified laboratory for TOG/TPH Analysis. Nominal concentration values are 100 mg/ kg (ppm), 250 mg/kg, 500 mg/kg, 1000 mg/kg, 1500 mg/kg and 2000 mg/kg for soil assuming a 1:1 extraction ratio; and 10 mg/l (ppm), 25 mg/l, 50 mg/l, 100 mg/l, 150 mg/l and 200 mg/l for water assuming a 10:1 extraction ratio. The set contains 6 standards along with a solvent blank in 4 ml flame sealed ampoules. Recommended for customers in the petroleum industry who are primarily measuring petroleum hydrocarbons in water or soil. ACCESSORIES Set of 4 10 mm quartz cuvette cells for use with TRANS-SP Carrying case with pre-diced pluck foam x 14.6 x 8 ; 10 lbs Dust cover Field sampling kit for TOG/TPH in water for use with the ATR-SP Field sampling kit for TOG/TPH in water for use with the TRANS-SP Field sampling kit for TOG/TPH in soil for use with both the ATR-SP and TRANS-SP Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 84 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. InfraCal 2 OIW_DS_

85 SpectrOil M/N-W MILITARY OIL ANALYSIS SPECTROMETER JOAP standard for spectrometric oil analysis Originally designed for military applications in the mid 1990s and enhanced over the last two decades, the SpectrOil M/N-W is the only approved in service oil analysis spectrometer in the US Department of Defense (DoD) Joint Oil Analysis Program. It has been the industry standard for rapid, deployable and reliable spectrometers for the Air Force, Navy, Army and Marines. The SpectrOil M/N-W performs the rapid analysis of in service oils so the military s high value assets are ready to deploy when needed. The SpectrOil M/N-W is the military version of the SpectrOil M family of oil and fuel analysis spectrometers. It is a compact, rugged, transportable and easy to use spectrometer designed for the analysis of wear metals, contaminants and additives in lubricants, hydraulic fluids and coolants. The SpectrOil M/N-W uses the time-tested and reliable rotating disc electrode (RDE) technique to measure quantities of dissolved and suspended fine particles in natural or synthetic petroleum based products and coolants. It was tested and selected by the U.S. Department of Defense (DoD) Joint Oil Analysis Program (JOAP) as its solely approved oil analysis spectrometer. SpectrOil M/N-W Key Features Rugged frame and optics system that meets military shock and vibration and environmental test standards (JOAP CID-0191) Designed for remote locations and frequent transportation No sample preparation 30 second analysis time Analyzes up to 31 elements simultaneously Self-sustained with built-in industrial touch panel PC Simple to operate; does not require special training No special utilities or gases required, only AC power Optional transit case for easy transportation Placement of the accessory and consumables tray on the transit case APPLICATION SPECIFIC INSTRUMENTS Product Catalog 85

86 SpectrOil M/N-W Product Information PRODUCT INFORMATION Part Numbers Spectro-M/N-W Spectro-M/N/R-W Applications new and in-service lubricant, hydraulic Output mg/kg (ppm) MIL Spec JOAP CID 0191 (1999) Calibration Factory set, no re-calibration needed HARDWARE SPECIFICATIONS Excitation Source Oscillatory arc discharge Optical system Spectral Range Detectors Rowland Circle polychromator Optic. Temperature controlled at 40C +/- 1C 203 nm to 810 nm CCD array OPERATIONAL SPECIFICATIONS Sample Volume 2 ml of fluid Ambient Operating Temperature C ( F) per MIL-STD Relative Humidity 0 to 90%, MIL-STD-810E, Method Vibration MIL-STD-810E, Method 514.4, Category I; MIL-STD-167 Type I Shock MIL-STD Procedure I & VI EMF MIL-STD 461 C & MIL-STD 462 High Altitude Transport MIL-STD-810E Method Proc I USER INTERFACE SPECIFICATIONS Operating system Windows 7 Pro; Software SpectrOil V8 PC and display Data Storage Industrial touch panel PC, 12 display Internal PC, USB, CD-RW POWER REQUIREMENTS Voltage Input AC 120/240V, 50/60Hz Power Consumption 1000 Watts at test MECHANICAL SPECIFICATIONS Dimensions 80 cm (L) x 63.5 cm (W) x 70 cm (H) (31.5 in x 25 in x 27 in) Weights Shipping Dimensions Shipping Weights 114 kg (250 lbs) M/N 132 kg (290 lbs) M/N/R 102 cm (L) x 91 cm (W) x 94 cm (H) (40 in x 36 in x 37 in ) for M/N 152 cm (L) x 91 cm (W) x 94 cm (H) (60 in x 36 in x 37 in ) for M/N/R 261 kg (575 lbs) M/N 295 kg (650 lbs) M/N/R National Stock Numbers and Configurations NSN PART NUMBER M97200 M97201 M90909 Optional Accessories DESCRIPTION D19-0 Base oil Graphite discs, 500, JOAP only Graphite rod, 50, JOAP only Reusable sample holder D elements, 100 ppm D3-100 Zn, Mo, B, 100 ppm CS G SMA G CONFIGURATION elements elements with transit case elements elements with transit case Consumables SpectrOil M/N-W uses special JOAP approved consumables and standards that differ from other SpectrOil models to ensure data correlation to all historical and current JOAP data. 24 elements, 100 ppm, JOAP 20 elements calibration only 5 elements, 900 ppm, JOAP 20 elements calibration only Automation: The Double Disc Rapid Robot (D2R2) automates the operation of the SpectrOil M/N-W. It is an innovative design that consists of two parts, a robot to exchange consumables and an automatic sample changer. Up to 80 used oil samples can be analyzed per hour (factory option only). Transit Case: The SpectrOil transit case features a shock mounted cradle designed for the SpectrOil and its accessories and consumables. A gas cylinder mechanism is used to raise the spectrometer to a comfortable operating height (variable). Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 86 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. M/N-W_DSv4_

87 TBN FluidScan 1210 HANDHELD INFRARED BN ANALYZER Base number test for marine cylinder lube oils Marine engine suppliers recommend daily monitoring of the Base Number (BN) to optimize cylinder lubrication feed rate and determine the residual BN of the piston underside oil. Recent changes in vessel operation are driving innovation in engine monitoring including: Shift to slow steaming and the resulting cold corrosion affecting every vessel in operation. Increases in early failure due to cylinder scuffing & scaling from improper lubrication in constantly changing conditions. New sulfur emissions requirements impacting some vessels. Running with multiple fuel types means major changes in lubrication BN to compensate for high fluctuations in acidic conditions in the cylinders. According to Wärtsilä Services Technical Bulletin RT-161, daily control of the cylinder oil BN is the most effective way to prevent cold corrosion. The FluidScan 1210 meets this challenge with a handheld BN analyzer. The FluidScan 1210 provides direct quantitative BN measurement of cylinder lube oil for two-stroke engines in less than a minute. Reduce lubrication oil costs Optimize feed rate to the cylinders, eliminating wasteful over-lubrication. Allows ship engineers to quickly comply with manufacturer recommendations for BN in new and residual cylinder oils. Increase component lifetime Reduce cold corrosion due to the effects of slow steaming. Reduce cylinder scuffing due to insufficient lubrication. Prevent scaling which results from over-lubrication. The FluidScan brings innovation to ship-board BN tests Fast and easy to use needs just one drop of oil and one minute to test, plus color-coded alarm limits for easy results interpretation. Reduced testing costs fewer consumables and solvent-free. Eliminates need for hazardous chemicals onboard. More accurate avoids the operator error of traditional onboard tests and correlates with lab methods (ASTM D2896) BN mg KOH/g) BN Analyzer vs Onshore Lab R² = BN by Laboratory Titration, mg KOH/g (ASTM D2896) Cylinder oil and inlet oil BN measurement APPLICATION SPECIFIC INSTRUMENTS Correlation of 1210 BN analyzer to laboratory titration Product Catalog 87

88 FluidScan 1210 Product Information The FluidScan 1210 includes the FluidScan device, battery charger, USB cable, USB flash drive, and the Fluid Manager Suite, which contains the Fluid Manager desktop application, user manuals, and a backup copy of the FluidScan device software. The FluidScan standard accessories kit includes cleaning pads and pipettes for 100 samples and the IR check fluid. The FluidScan 1210 enables ship managers to keep optimal residual BN values to avoid cold corrosion and scuffing without wasting cylinder oil to over lubrication. PART NUMBER FluidScan-Q1210 SA marine cylinder lubrication oil BN analyzer. Requires SA1001 accessory kit. FluidScan standard accessory kit PRODUCT INFORMATION Application Marine cylinder oil (MCL) BN (Base Number) Unit mg KOH/g Methodology ASTM D7889, ASTM E1655 Range BN Accuracy ± 5% of measured value, typical Repeatability ± 5% of measured value, typical Calibration Factory calibrated to wet chemistry methods ASTM D2896 for TBN. Use Check Fluid for instrument validation. OPERATIONAL SPECIFICATIONS Sample Volume 100 μl (about 1 drop) Solvents/Reagents None Ambient Operating 10 C to 50 C (14 F to 122 F) Temperature Relative Humidity Ambient Altitude USER INTERFACE SPECFICATIONS Software/Operating System Display Data Storage Data Transfer Data Entry 0 to 100%, non-condensing up to 5,000 meters (16,404 feet) Device: Microsoft Windows CE PC System: Windows 7 Pro, 32/64 bit, English US version (for Fluid Manager software) 320 x 320 transflective color screen Up to 5,000 analyses USB for data updates and synchronization Directional pad and soft buttons POWER REQUIREMENTS Battery Power Source Built in rechargeable lithium ion battery Power AC 110/240 V, 50/60 Hz, 10 Watts Typical Runtime 6-8 hours Recharge Time 6.5 hours MECHANICAL SPECIFICATIONS Dimensions 240 mm (H) x 140 mm (W) x 70 mm (D) (9.5 in x 5.5 in x 2.75 in) Weight 1.4 kg (3 lbs) Shipping package dimensions Shipping package weight 45.7 cm (H) x 40.6 cm (W) x 35.6 cm (L) (18 in x 16 in x 14 in) 8.1 kg (18 lbs) COMPLIANCE CE Mark: EMC Directive (2004/108/EC); RoHS ACCESSORIES & CONSUMABLES FL310 IR Check Fluid 5 ml PV1011 Disposable non-abrasive cleaning pads; package of 500 P µl disposable pipettes, package of 500 PV µl disposable pipettes & non-abrasive cleaning pad kit; pkg. of 100 each Note: System includes data logging on device and export capability to spreadsheet. System is upgradeable with additional lubricant library and parameters for other shipboard equipment. FluidScan 1210 and FerroCheck 2000 combination kit provides BN and total ferrous content for marine engine oil analysis. Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 88 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. FluidScan 1210_

89 CoolCheck 2 AUTOMATED COOLANT AND DIESEL EXHAUST FLUIDS ANALYSIS SYSTEM Accurate, on-location testing in seconds Cooling systems play a vital role in preserving overall engine heat balance and in protecting engine components. Testing your coolant and maintaining your system at optimum levels will help prevent: Corrosion, pitting, rust build-up Damaged seal/coolant leaking into oil Overheating, boil-over, engine seize-up Engine damage from freezing As an added benefit, CoolCheck 2 tests for correct DEF levels. An incorrect DEF mixture can also be harmful: Reduces engine efficiency Negates emission reduction efforts CoolCheck 2 provides measurement and profiling of coolant condition and diesel exhaust fluid (DEF) integrity. Designed for use by the non-expert Executes 9 different tests in less than 45 seconds Measured results are also graded as: > NORMAL > ABNORMAL > SEVERE Provides corrective advice to avoid potential failures before they happen Replaces hazardous chemicals, time-consuming titration methods and inaccurate test strips used in manual testing CoolCheck 2 helps prevent the most common problems with cooling systems Mixed fluid types Depletion of key performance additives System contamination COOLANT TESTS Coolant type Clarity Color Contamination Glycol content (%) Boil point Freeze point Nitrites (ppm) DEF TESTS % Urea % DEF NIR UV-VIS Patented Near IR/UV-VIS Dual Spectrometer Principle of Operation The core of CoolCheck 2 coolant and DEF analyzer is the patented near IR (NIR) and UV/Visible dual spectrometer that measures the absorption spectrum at these two wavelengths simultaneously using a unique sample vial. Physical parameters are extrapolated from the obtained spectrum with special calibrations (done in the factory). Alarm limits stored in the device provide a traffic light style report for immediate decision making. The entire test takes less than a minute. APPLICATION SPECIFIC INSTRUMENTS Product Catalog 89

90 CoolCheck 2 Product Information PRODUCT INFORMATION Part Number Accessories Applications Operating Mode OUTPUT Coolant Diesel Exhaust Fluids (DEF) DEVICE SPECIFICATIONS Spectral Range POS printer (included) LubeTrak data management software (optional) Cooling systems and Diesel Exhaust Fluid (DEF) Analysis Multi-parameter Tests Coolant Type, Clarity, Contamination, Color, Freeze Point, Glycol Content, Boil Point, Nitrites % Urea; DEF Amount nm Detectors Dual-Path multi-wave spectrometer UV/Vis ( nm) and NIR ( nm); Dual Xenon light source Calibration OPERATIONAL SPECIFICATIONS Sample Volume Required Sample Time Required Ambient Operating Temperature Operational Humidity 3 Standard fluids generate a polynomial 2nd / 3rd order fit. 0.5 oz. (15 ml) 45 seconds 0-40 C 5-95% (non-condensing) USER INTERFACE SPECIFICATIONS Display Panel touch screen Data Entry touchscreen / USB port for computer mouse Data Storage 16 GB internal Data Transfer LAN/wireless (FTP) to online reporting Communication Port 21 (online reporting through LubeTrak) POWER REQUIREMENTS Power 115/230V 50/60 Hz (single-phase) Power Consumption 20 Watts MECHANICAL SPECIFICATIONS Dimensions 10.5 (L) x 9 (W) x 4.5 (H) (28cm x 23cm x 11.5 cm) Weight 4.6 lbs. (2.1 kg) CONSUMABLES CoolCheck 2 sample vials, disposable single-use (200) Thermal Printer Paper Sample extractor pump Sample extractor tubing Coolant Control Sample, R Coolant Control Sample, DEF Coolant Control Sample, N Understanding Your CoolCheck 2 Report Info Sheet Ambient Altitude up to 11,500 feet (3000 meters) Optional LubeTrak Software allows managers to effectively maintain the health and efficient operation of equipment. Users can organize test data and maintenance recommendations from the CoolCheck 2 in a database with easy to use analysis and tracking capability. Stores analysis history Tracks equipment results Displays red flag problems Sends alerts to computer or smart phone Exportable data Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 90 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. CoolCheck 2_DSv3_

91 SpectrOil M/F-W FUEL ANALYSIS SPECTROMETER On site fuel analysis for gas turbines and diesel engines KEY APPLICATIONS Fuel quality analysis for liquid fired gas turbines and diesel engines of: - Electric power generation stations - Fuel treatment systems - Shipboard propulsion systems Qualification of fuel treatment system effectiveness Contaminant elements in turbine wash-down water can be checked with optional water calibration program The SpectrOil M/F-W and M/F-LD are widely used to check ash-forming contaminant in fuels for gas turbines and diesel engines in power plants worldwide. It measures concentrations of contaminant elements and the information is used for incoming inspection, transportation and treatment of the fuel to prevent or reduce corrosion of the turbines blades. Using the proven rotating disc electrode (RDE) Optical Emission Spectroscopy (OES) technology, it produces accurate and repeatable results quickly without extensive training. SpectrOil M/F-W and M/F-LD Key Features: Rugged frame and optics system designed for remote operations Easy to operation for non-skilled operators No sample preparation 30 second analysis time Self-sustained with built-in industrial touch panel PC No special utilities or gases required, only AC power Sub ppm LOD for most critical elements Compliant to ASTM D6728 Less than 100 ppb LOD for V and alkali metals for SpectrOil M/F-LD Typical Fuel Delivery Workflow Showing Common Sampling Points Fuel Delivery Ship, Road, Well or Pipeline Gas Turbine System = Fuel sampling & analysis points 7 Inhibitor Injection Secondary Start-up Fuel Fuel Heating, Filtration & Transfer 6 Fuel Treatment System Treated Fuel Storage Tank 5 When a fuel arrives on site, it has gone through production, storage, transport and storage. Few fuels are so clean after this cycle that that they can be used without treatment. Analysis requirements start with the delivery of the fuel, continue throughout fuel handling, and end only as the fuel is injected into the turbine. Preconditioning of the fuel before it reaches the gas turbine is a prerequisite for installation when contamination may be present. Spectrometric analysis determines the amount of treatment required and the efficiency of that treatment. In particular, sodium and potassium concentrations must be determined to well below one part per million in most fuels. In heavy fuels, the vanadium concentration is used to calculate the amount of magnesium treatment compound to be added to the fuel. APPLICATION SPECIFIC INSTRUMENTS Product Catalog 91

92 SpectrOil M/F-W and M/F-LD Product Information PRODUCT INFORMATION Part Numbers Spectro-M/F-W (light fuel, heavy fuel) Spectro-M/F-LD (low detection diesel) Output mg/kg (ppm) Calibration Factory set, no re-calibration needed HARDWARE SPECIFICATIONS Excitation Source Oscillatory arc discharge Optical system Rowland Circle polychromator Optic. Temperature controlled at 40C +/- 1C Spectral Range 203 nm to 810 nm Detectors CCD array OPERATIONAL SPECIFICATIONS Sample Volume 2 ml of fluid Ambient Operating 0 to 40C (32F to 104F) Temperature Relative Humidity 0 to 90%, non-condensing USER INTERFACE SPECIFICATIONS Operating System Windows 7 Pro PC and Display Industrial touch panel PC, 12 display Data Storage Internal PC, USB, CD-RW POWER REQUIREMENTS Voltage Input AC 120/240V, 50/60Hz Power Consumption 1000 Watts at test MECHANICAL SPECIFICATIONS Dimensions 80 cm (L) x 63.5 cm (W) x 70 cm (H) (31.5 in x 25 in x 27 in) Weights 114 kg (250 lbs) Shipping Dimensions 102 cm (L) x 91 cm (W) x 94 cm (H) (40 in x 36 in x 37 in ) Shipping Weights 261 kg (575 lbs) M/N Calibration Programs and Standards Light and heavy fuel (SpectrOil M/F-W) Low detection (LD) diesel (SpectrOil M/F-LD) CS CS-GT15-10 CS-GT CS-HP-100 CS-GT15-10 CS-GT Base Oil Calibration Program and Elemental Ranges Fuel Low Element Light Fuel Heavy Fuel Detection Al Water Ca Cr Cu Fe K Li Mg , Mn Na Ni Pb Si V Zn ppm for light fuel 100 ppm for heavy fuel High purity base oil 10 ppm, 15 elements 100 ppm, 15 elements ppm for Li, Na, K,V ppm for V Process water (optional) STE006 KIT DI water and 5 ppm standard Consumables Only use Spectro Scientific certified consumables for SpectrOil M/F-W and M/F-LD to ensure data integrity. M97008 Graphite disc D-2 AGKSP 500/Box M97009 Graphite rod.242x6 AGKSP Pkg/50 P High temperature sample cup (black) M90204 Sample cover for low flash point fuels Spectro Scientific One Executive Drive, Suite 101, Chelmsford, MA sales@spectrosci.com An ISO 9001:2008 company 92 Product Catalog Copyright 2017 Spectro Scientific. All rights reserved. While every effort is made to assure the information in this document is accurate, Spectro Scientific does not accept liability for any errors or mistakes that may arise. Specifications are subject to change without notice. M/F-W_DSv4_

93 Service and Support Spectro Scientific is committed to working with our customers and to support their instruments and maintenance requirements. We build some of the highest quality instruments for used oil and fuel analysis markets; however, even the best instruments can have a problem from time to time. Our dedicated service staff provides high quality service that ensures maximum performance from every instrument. Training service n Spectro provides scheduled user training classes for all of our products. For details about our training schedule, please visit our website services/training-courses/ n Spectro can provide onsite training classes based on request Remote support and diagnostics n For certain products, remote diagnostics and support can be provided based on annual service contract for speedy response Annual maintenance n Spectro recommend users to perform annual preventive maintenance (PM) on our products to reduce the chance of failure and improve the up time. Spectro provide on site and depot level PM services. Deport level calibration and repair n All Spectro products can be sent back to our certified depot repair centers for check-up, calibration, preventive maintenance and repair. A Return Good Authorization (RGA) number is required before sending the product back to depot. Extended warranty n Spectro provides extended part and/or labor warranty for our products. Extended warranty can be purchased along with annual maintenance contract International service coverage n Spectro has a network of certified service engineers around the world. Product Catalog 93