Certificate of Analysis / Certificat d analyse

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1 Date: (YYYY-MM-DD / AAAA-MM-JJ) Certificate of Analysis / Certificat d analyse Product code / Code du produit: Batch No. / No. de lot: Trade name / Nom commercial: Botanical name / Nom botanique: INCI name / Nom INCI: Use of product / Utilisation: Country of origin / Pays d origine: Certification: VHE056B MP Essential Oil of Cinnamosma Fragrans / Huile essentielle de Cinnamosma Fragrans (Saro ou Mandravasarotra) Cinnamosma Fragrans CINNAMOSMA FRAGRANS OIL Fragrant and/or flavour substance Substance odorante et/ou aromatique Madagascar Ecocert Canada Organic / Biologique Ecocert Canada 1. Method of production / Méthode d obtention Essential Oil obtained by steam distillation of the leaf of Cinnamosma Fragrans. / Huile essentielle obtenue par distillation à la vapeur d'eau de la feuille de Cinnamosma Fragrans. 2. Certificate of Purity and Origin / Certificat de pureté et d origine - 100% pure and natural without any additive/ 100% pur et naturel sans aucun additif. - Certified Madagascar origin / Origine Madagascar certifiée. 3. Organoleptic and Physical Properties / Caractéristiques organoleptiques et physiques Requirements / Spécifications Results /Résultats Physical appearance / Aspect physique: Clear mobile liquid liquid / Liquide mobile limpide Compliant /Conforme Colour / Couleur: Colorless to dark yellow / Incolore à jaune foncé Compliant /Conforme Odor / Odeur: Fresh, pleasant and rising Compliant /Conforme / Fraîche, agréable et montante Specific Gravity at 68ºF (20ºC) / Densité à 20ºC: 0,890 to/à 0,900 0,894 Refractive Index at 68ºF (20ºC) / Indice de réfraction à 20ºC: 1,465 to/à 1,475 1,4720 Optical Rotation at 68ºF (20ºC) / Pouvoir rotatoire à 20ºC: -10 to/à ,2 info@union-nature.com - 1/5

2 4. Analysis Properties / Caractéristiques d analyse 4.1 Operating Conditions / Conditions opératoires Gas Chromatography / Chromatographie à phase gaseuse (CPG-FID): Hewlett Packard Column / Colonne polaire: HP INNOWAX-WAX Temperature Programming/ Programmation de température: 6 mn at/à 50 C 2 C/mn 250 C-10mn at/à 250 C Injected Volume / Volume injecté: 0,2 μl Carrier Gas: He / Gaz vecteur: He: 22psis 4.2 Chromatographic Profile / Profil chromatographique info@union-nature.com - 2/5

3 4.3 Chromatographic Profile Interpretation / Interprétation du profil chromatographique Peaks / Main Components Results Table 1 / Tableau 1 de résultats des principaux constituants 2 6,5 2-METHYLBUTANAL 0,01 3 6,6 ISOVALERALDEHYDE 0, ,0 α-pinene 4, ,1 α-thuyene 0, ,3 PRENOL 0, ,6 α-fenchene 0, ,0 CAMPHENE 0, ,2 β-pinene 6, ,9 SABINENE 7, ,1 PINADIENE 0, ,4 THUYADIENE 0, ,2 β-myrcene 2, ,4 α-phellandrene 0, ,7 ψ-limonene 0, ,4 α-terpinene 1, ,1 2,3-DEHYDRO-1,8-CINEOLE 0, ,7 LIMONENE 8, ,7 1,8-CINEOLE 41, ,7 Cis-β-OCIMENE 1, ,7 γ-terpinene 1, ,9 Trans-β-OCIMENE 0, ,3 p-cymene 0, ,1 TERPINOLENE 0, ,8 ISOAMYL ISOVALERATE / ISOVALERATE D ISOAMYLE 0, ,9 6-METHYL-5-HEPTEN-2-ONE / 6-METHYLE-5-HEPTENE-2-ONE 0, ,3 ALLO-OCIMENE ISOMERE 0, ,7 3-HEXEN-1-OL / 3-HEXENE-1-OL 0, ,2 AROMATIC COMPOUND Mw=150 0,01 / COMPOSÉ AROMATIQUE Mw= ,8 α,p-dimethylstyrene 0, ,1 LINALOOL CIS-OXIDE / Cis-OXYDE DE LINALOL 0, ,2 α-cubebene 0, ,5 trans-thuyanol 0, ,0 δ-elemene 0, ,8 CITRONELLAL 0, ,1 YLANGENE 0, ,7 α-copaene 0, ,6 β-bourbonene 0, ,7 CAMPHOR / CAMPHRE 0, ,0 BENZALDEHYDE 0, ,8 LINALOOL / LINALOL 7, ,0 β1-cubebene 0, ,2 Cis-THUYANOL 0, ,5 LINALYL ACETATE / ACETATE DE LINALYLE 0,04 info@union-nature.com - 3/5

4 Peaks / Main Components Results Table 2 / Tableau 2 de résultats des principaux constituants 46 44,1 Trans-p-MENTH-2-EN-1-OL 0, ,3 e-cadinene + FENCHOL 0, ,5 BORNYL ACETATE / ACETATE DE BORNYLE 0, ,6 a,trans-bergamotene 0, ,0 ß-ELEMENE 0, ,4 ß-CUBEBENE 0, ,7 TERPINENE-4-OL 3, ,9 ß-CARYOPHYLLENE 1, ,6 AROMADENDRENE 0, ,2 Cis-p-MENTH-2-EN-1-OL 0, ,3 CITRONELLYL FORMATE / FORMIATE DE CITRONELLYLE 0, ,9 CADINA-3,5-DIENE 0, ,8 D-TERPENYL ACETATE / ACETATE DE d-terpenyle 0, ,0 ALLO-AROMADENDRENE 0, ,2 CITRONELLYL ACETATE / ACETATE DE CITRONELLYLE 0, ,4 E-ß-FARNESENE 0, ,6 ZONARENE 0, ,0 d-terpineol 0, ,3 a-humulene 0, ,7 CRYPTONE 0, ,9 NERAL 0, ,3 γ-muurolene 0, ,6 α-terpineol 2, ,7 TERPINENYL ACETATE / ACETATE DE TERPENYLE 1, ,9 BORNEOL 0, ,8 GERMACRENE D 0, ,0 CUBENENE 0, ,2 NERYL ACETATE / ACETATE DE NERYLE 0, ,5 ß-BISABOLENE 0, ,6 α-muurolene 0, ,9 ACETATE D éxo-2-hydroxycineole + GERANIAL 0, ,2 CARVYL ACETATE / ACETATE DE CARVYLE 0, ,4 BICYCLOGERMACRENE 0, ,5 trans-piperitol 0, ,0 GERANYL ACETATE / ACETATE DE GERANYLE 0, ,2 CITRONELLOL 0, ,4 d-cadinene 0, ,7 γ-cadinene 0, ,1 SESQUITERPENE 0, ,1 CADINA-1,4-DIENE 0, ,4 NEROL 0, ,0 ALIPHATIC ESTER / ESTER ALIPHATIQUE 0, ,5 Trans-CARVEOL 0, ,0 GERANIOL 0, ,1 CALAMENENE 0,13 info@union-nature.com - 4/5

5 Peaks / Main Components Results Table 3 / Tableau 3 de résultats des principaux constituants 91 61,3 p-cymene-8-ol 0, ,8 BENZYL ALCOHOL / ALCOOL BENZYLIQUE 0, ,1 Epi-CUBEBOL 0, ,8 CALACORENE 0, ,9 CUBEBOL 0, ,9 CARYOPHYLLENE OXIDE / OXYDE DE CARYOPHYLLENE 0, ,6 NEROLIDOL 0, ,9 Epoxy-6,7-HUMULENE 0, ,4 Epi-CUBENOL 0, ,8 CUBENOL 0, ,2 ELEMOL 0, ,3 SESQUITERPENOL 0, ,4 HYDROKETONIC COMPOUND / COMPOSÉ HYDROXYCETONIQUE 0, ,8 γ-eudesmol 0, ,7 SESQUITERPENOL 0, ,6 α-eudesmol 0, ,1 β-eudesmol 0, ,1 GERANIC ACID / ACIDE GERANIQUE 0,47 TOTAL 99,96 Note: The allergens are identified in bold / Les allergènes sont identifiés en caractères gras. Analysis Date / Date de l analyse: Tomas Seijas, Chemist/Chimiste, OCQ # info@union-nature.com - 5/5

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