Phillips 66 Pipeline LLC. Blue Pipeline Natural Gas Liquids Specifications

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1 Current Publication Date: 5//208 Previous Publication Date: //208 Revision Notes: Increased Propane RVP maximum from 204 psig to 208 psig. Published 4/0/208

2 Product Index Product Name Destination(s) NGL Products, Propane NP NGL Products, Butane, Normal Butane NNB NGL Products, Butane, Refinery Grade (RGB) NCC NGL Products, Iso-Butane NIB Published 4/0/208

3 NP NGL Products, Propane Property Test Method Units Min Max Specific Note# Comp., Butane & heavier D263 lv% Composition, Propane D263 lv% Composition, Propylene D263 lv% 5.00 Copper Strip Corrosion D838 Rating Fluorides ASTM D7359 ppmw Hydrogen Sulfide D2420 Most Current Version See Note 2 Other Deleterious Substances Inspection see note 3 Residual Matter, GC D7756 ppmw Residual Matter, Oil Stain D258 Pass 5 Residual Matter, Residue D258 ml Specific 60/60F D Report Specifications See Note 6 Sulfide, Carbonyl D5623 ppmw 20 7 Sulfur D2784 or D6667 ppmw 23 8 Vapor 00F D267, D2598, or D6897 psig Volatile Res., 95% Evap D837 deg F Test Methods See Note Neg 0.05 Published 4/0/208 Specification Ref. # 8750

4 NP NGL Products, Propane Notes:. One of the following specifications must be met: the maximum propylene or the 95% evaporated maximum temperature (ASTM D835 Table ). 2. The most current version of this specification can be found on the Phillips 66 Midstream website, 3. This specification defines only a basic purity for this product. This product is to be free of any contamination or impurities that might render the product unusable for its commonly used applications. Specific contaminants include (but are not limited to) dirt, rust, scale, and other types of solid contaminants, gum, gum-producing substances, oil, caustics, chlorides, heavy metals, glycol, oxygenates, inorganic gases, masking agents, or any compound added to enhance the ability to meet these specifications that has not been approved by Phiillips Test Method D7756 may be used in place of Test Method D258. In case of dispute, Test Method D258 shall be the referee test method. See ASTM D835 for information about residues in LPG and for information about gas chromatographic test for residues in LPG. 5. An acceptable product shall not yield a persistent oil ring when 0.3 ml of solvent residue mix is added to a filter paper in 0. ml increments and examined in daylight after 2 minutes as described in Test Method D These specifications are intended to meet the latest version of ASTM D835 as well as all downstream customer/pipeline requirements. In case of conflict, the most restrictive specification shall apply. 7. Carbonyl sulfide above 3.0 ppmw can react in the downstream cavern to form hydrogen sulfide, which can result in a copper strip corrosion failure. 8. The total sulfur limits in this specification DO include the sulfur compounds used for stenching purposes. In case of dispute, Test Method D6667 shall be the referee method. (ASTM D835) 9. The referee method shall be ASTM D One of the following specifications must be met: the maximum propylene or the 95% evaporated maximum temperature (ASTM D835 Table ).. Test methods designated with the letter D are ASTM test methods. The most recent year revision shall be used. Published Specification Ref. # 8750

5 NNB NGL Products, Butane, Normal Butane Property Test Method Units Min Max Specific Note# Comp.- Butadiene D263 lv% Comp.- Hexanes & Heavier D263 lv% Comp.- Iso-butane D263 lv% Comp.- Normal Butane D263 lv% Comp.- Olefins D263 lv% Comp.- Pentanes & Heavier D263 lv% Comp.- Propylene, Propane & Lighter D263 lv% Copper Strip Corrosion D838 Fluorides UOP 69, ASTM D7359 ppmw Hydrogen Sulfide Moisture Content- Free Water D2420 Visual Pass None A or B is pass Most Current Version See Note Other Deleterious Substances Inspection see note 2 Oxygenates, IPA & Heavier Alcohols ASTM D7423, UOP-845 ppmw Oxygenates, Methanol ASTM D7423, UOP-845 ppmw Oxygenates, MTBE & other Ethers ASTM D7423, UOP-845 ppmw Oxygenates, Other Oxygenates ASTM D7423, UOP-845 ppmw Oxygenates, Total ASTM D7423, UOP-845 ppmw Specifications See Note 3 Sulfur D2784 or D6667 ppmw 93 4 Vapor 00 F D267, D2598, or D6897 psig 50 5 Test Methods See Note Published 4/0/208 Specification Ref. # 8752

6 NNB NGL Products, Butane, Normal Butane Notes:. The most current version of this specification can be found on the Phillips 66 Midstream website, 2. This specification defines only a basic purity for this product. This product is to be free of any contamination or impurities that might render the product unusable for its commonly used applications. Specific contaminants include (but are not limited to) dirt, rust, scale, and other types of solid contaminants, gum, gum-producing substances, oil, caustics, chlorides, heavy metals, glycol, oxygenates, inorganic gases, masking agents, or any compound added to enhance the ability to meet these specifications that has not been approved by Phiillips These specifications are intended to meet all applicable industry standards and downstream customer/pipeline requirements. In case of conflict, the most restrictive specification shall apply. 4. The total sulfur limits in this specification DO include the sulfur compounds used for stenching purposes. In case of dispute, Test Method D6667 shall be the referee method. (ASTM D835) 5. The referee method shall be ASTM D Test methods designated with the letter D are ASTM test methods. The most recent year revision shall be used. Published Specification Ref. # 8752

7 NCC NGL Products, Butane, Refinery Grade (RGB) Property Test Method Units Min Max Specific Note# Color (See Note) D258 See Note Comp.- Normal Butane D263 lv% Comp.- Propane D263 lv% Comp.- Total Olefins D263 ppm Copper Strip Corrosion D838 Fluorides ASTM D7359 ppmw Hydrogen Sulfide Moisture Content- Free Water D2420 Visual 65.0 Pass Report None A or B is pass Most Current Version See Note 2 Other Deleterious Substances Inspection see note 3 Specifications See Note 4 Sulfur D2784 or D6667 ppmw Vapor 00 F D267, D2598, or D6897 psig Volatile Res., 95% Evap D837 or D263 deg F Test Methods See Note 7 60 Notes:. OneOK requires that the solvent/residue mixture obtained by ASTM D258 be free of any visible color. 2. The most current version of this specification can be found on the Phillips 66 Midstream website, 3. This specification defines only a basic purity for this product. This product is to be free of any contamination or impurities that might render the product unusable for its commonly used applications. Specific contaminants include (but are not limited to) dirt, rust, scale, and other types of solid contaminants, gum, gum-producing substances, oil, caustics, chlorides, heavy metals, glycol, oxygenates, inorganic gases, masking agents, or any compound added to enhance the ability to meet these specifications that has not been approved by Phiillips These specifications are intended to meet all applicable industry standards and downstream customer/pipeline requirements. In case of conflict, the most restrictive specification shall apply. 5. The referee method shall be ASTM D ASTM D263 may be used, but the ASTM D837 value shall prevail in the event of a dispute. 7. Test methods designated with the letter D are ASTM test methods. The most recent year revision shall be used. Published 4/0/208 Specification Ref. # 8753

8 NIB NGL Products, Iso-Butane Property Test Method Units Min Max Specific Note# Comp.- Iso-butane D263 lv% Comp.- Normal Butane & Heavier D263 lv% Comp.- Propane & Lighter D263 lv% Copper Strip Corrosion D838 Fluorides ASTM D7359 ppmw Hydrogen Sulfide Moisture Content- Free Water D2420 Visual Pass Report None A or B is pass Most Current Version See Note Other Deleterious Substances Inspection see note 2 Specifications See Note 3 Sulfur D2784 or D5623 ppmw Vapor 00 F D267, D2598, or D6897 psig Volatile Res., 95% Evap D837 deg F +6 Test Methods See Note 5 93 Notes:. The most current version of this specification can be found on the Phillips 66 Midstream website, 2. This specification defines only a basic purity for this product. This product is to be free of any contamination or impurities that might render the product unusable for its commonly used applications. Specific contaminants include (but are not limited to) dirt, rust, scale, and other types of solid contaminants, gum, gum-producing substances, oil, caustics, chlorides, heavy metals, glycol, oxygenates, inorganic gases, masking agents, or any compound added to enhance the ability to meet these specifications that has not been approved by Phiillips These specifications are intended to meet all applicable industry standards and downstream customer/pipeline requirements. In case of conflict, the most restrictive specification shall apply. 4. The referee method shall be ASTM D Test methods designated with the letter D are ASTM test methods. The most recent year revision shall be used. Published Specification Ref. # 8754

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