GC Method Compliance and Large Valve Oven Application
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1 GC Method Compliance and Large Valve Oven Application Solution Focused Kelly Beard June 20, 2016
2 Compliant Methods
3 Compliant Methods What are our options? Analyzers and Analyzer Kits High Volume Well Known Analysis Many Options Application Notes Lower Volume Usually Requires a Consultant Possible Future Analyzer, Given Acceptable Sales Quantiles Channel Partner Solutions Requires Third Party Software or Requires Third Party Hardware 3 June 27, 2016
4 Analyzers and Application Kits Updated HPI Solution Guide Searchable, 139 pages PN: EN Links to Analyzer Chapter 4 Analyzer Overview January 2013
5 Analyzers and Application Kits 5 Analyzer Overview January 2013
6 Analyzers and Application Kits 6 Analyzer Overview January 2013
7 Analyzers and Application Kits 7 Analyzer Overview January 2013
8 Analyzers and Application Kits 8 Analyzer Overview January 2013
9 Application Notes Example: D5769 Determination of Benzene, Toluene, Total Aromatics in Finished Gasolines by Gas Chromatography/Mass Spectrometry Fred Feyerherm developed application, via ASTM method Very successful Custom Calculations Consultant is Requited for Application Very popular lately Sales Quantities have Increased Analyzer Kit In Developed as a Result 9 Analyzer Overview January 2013
10 Channel Partner ASTM D6730 Standard Test Method for Determination of Individual Components in Spark Ignition Engine Fuels by 100-meter Capillary (with PreColumn) High Resolution Gas Chromatography Detailed Hydrocarbon Analysis Difficult Analysis with 100 s of Compounds Requires Custom Software Software is Difficult to Support via Agilent Field Resources Many Software and Third Party Providers 10 Analyzer Overview January 2013
11 Channel Partner ASTM D5599 Standard Test Method for Determination of Oxygenates in Gasoline by Gas Chromatography and Oxygen Selective Flame Ionization Detection O-FID Analysis Requires a Custom Platinum Catalyst Requires Custom Reporting Hardware can not be Supplied by Agilent Wasson-ECE is our Partner of Choice for this Analysis with Many Years of Experience on the Application. 11 Analyzer Overview January 2013
12 Channel Partner ASTM D8003 Standard Test Method for Determination of Light Hydrocarbons and Cut Point Interals in Live Crude Oils and Condensates by Gas Chromatography New Live Crude Oil Analysis Requires HPLIS Third Party Injection Source Intended for the introduction of pressurized liquid samples containing very polar, high boiling or high carbon number analytes Requires Custom Reporting Hardware can not be Supplied or Supported by Agilent 12 Analyzer Overview January 2013
13 Channel Partner Reformulyzer - Hydrocarbon Group Type Analysis PAC Provided Solution Test Methods: ASTM D5443, ASTM D6839, IP 566, EN ISO 22854, SH/T 0741, GB/T , GOST R EN ISO Intended for the introduction of pressurized liquid samples containing Extensive Hardware Addition 13 Analyzer Overview January 2013
14 Questions 14 Analyzer Overview January 2013
15 Introducing the 7890B Large Valve Oven Isothermal Zone for Valves and Columns Temperature control: - Independent control of LVO and GC oven zones Temperature Limit: - Max 330 C (valve and column dependent) Valve configurations: - Accommodates 4/6/10/14 port valves including Hastelloy valves Column Compatibility: - Large Mandrel: Accommodates 15 feet of 1/8 inch OD metal column - Small Mandrel: Accommodates 7 Ft of 1/8 OD metal column 15 LVO Analyzer Training June 27, 2016
16 Introducing the 7890B Large Valve Oven Isothermal Zone for Valves and Columns Column Mandrel Valve or Mandrel Position 6 Internal Positions: Valves or Columns Variable Restrictor - Up to six (6) heated valve positions - Four (4) needle valve positions - Uses 1 heated zone 6-port Valve 12-port Valves 16 LVO Analyzer Training June 27, 2016
17 Large Valve Oven Features/Benefits Feature 6 position isothermal valve oven for actuated valves, microgasifiers, needle valves, and columns (including 1/8 in packed columns) with access to valves connections without removing actuators Benefit Open configuration that allows for easy maintenance; maximizing up-time. Also allows for multiple configurations for method development as well as set SP1 and configured Feature Use only one 7890B heated zone Benefit Current multi-valve configurations may quickly consume 6 heated zones, LVO uses 5 leaving 1 for future applications Feature Dual thermal zones allow for thermal isolation between column oven and LVO Benefit Ability to configure analyses that require multiple thermal zones. Can run isothermal temperatures in the LVO while temperature ramping the GC oven 7890B with Large Valve Oven 17 LVO Analyzer Training June 27, 2016
18 Fast Refinery Gas Analysis with Micropacked Columns Simultaneous O 2 and H 2 S determination 7890 GC System, LVO, Column, Sample Option 112 S/SL Inlet G3445B Option #532 Option 210 FID with EPC Option 220 TCD with EPC Option 221 Left Mount TCD Option 002 or 003 Fast Oven Option 311 and 312 Cryo 18 LVO Analyzer Training June 27, 2016
19 Performance Features LVO RGA Analyzers Fast RGA Analyzer Total run time is 8 minutes - LVO at 70 C Hydrocarbons to C 5 (C 6+ backflush) Permanent Gases O 2 and H 2 S Compounds Limit Hydrocarbons 0.01 Mol% Hydrogen Sulfide 500 ppm Carbonyl Sulfide 300 ppm Hydrogen 0.01 Mol% O2, N2, CO, CO Mol% June 27,
20 Fast RGA with Micropacked Columns GC/FID/TCD/TCD Micropack LVO Plumbing Micropack System Flow Diagram 20 LVO Analyzer Training June 27, 2016
21 Fast RGA with Micropacked Columns Helium Carrier Selected Method Parameters Split/Splitless inlet: 120 ºC, 100:1 split FID (front): 250 ºC TCD (rear): 260 ºC He carrier Ref. 30 ml/min Makeup 2 ml/min TCD (side): 250 ºC N2 carrier Ref. 45 ml/min Makeup 2 ml/min, neg. polarity Main Oven Program: 60 ºC ( 1 min) to ºC/min to ºC/min Large Valve Oven: Isothermal, 65 ºC and 70 ºC 21 LVO Analyzer Training June 27, 2016
22 Fast RGA with Micropacked Columns Analytical Performance Hydrocarbon Channel (FID), LVO at 70 C 22 LVO Analyzer Training June 27, 2016
23 Fast RGA with Micropacked Columns Analytical Performance Permanent Gas Channel (TCD), LVO at 70 C LVO Analyzer Training June 27, 2016
24 Fast RGA with Micropacked Columns Analytical Performance Oxygen Stability 70 C 75 C Stability of Oxygen Isothermal Oven at 70 C Stability of Oxygen Isothermal Oven at 75 C 24 LVO Analyzer Training June 27, 2016
25 Fast RGA with Micropacked Columns Helium Carrier Application Note Fast Refinery Gas Analysis System Based on the Agilent 7890B GC System and G3507A Large Valve Oven Using Micropacked Columns 25 LVO Analyzer Training June 27, 2016
26 Simultaneous analysis of hydrogen hydrocarbons and permanent gases Fast RGA LVO Analyzer Value Overview Analyzer, G3445B #532 Large Valve Oven External Thermal Zone Isothermal Operation Up to 6 valves or columns Expands capability of 7890 Micropacked Columns Built for speed Rapid 8 minute cycle time Isothermal Zone Protect temperature sensitive columns Simultaneous analysis of hydrogen disulfide (H 2 S) and oxygen (O 2 ) Stable response for oxygen (O 2 ) Three Channel Analytical Method Simultaneous analysis of O 2 and H 2 S <8 Minutes GC/FID/MS Blood Alcohol Analyzer February
27 LVO Based Fast RGA with Hydrogen Carrier Analytical Performance (G3445B, #533 Available on July 1, 2014 CPL) FID Channel C6+ 27 LVO Analyzer Training June 27, 2016
28 Fast Refinery Gas Analysis with Micropacked Columns Simultaneous O 2 and H 2 S determination using Hydrogen Carrier Gas 7890 GC System, LVO, Column, Sample Option 112 S/SL Inlet G3445B Option #533 Option 210 FID with EPC Option 220 TCD with EPC Option 221 Left Mount TCD Option 002 or 003 Fast Oven Option 311 and 312 Cryo 28 LVO Analyzer Training June 27, 2016
29 Overview - GC Platforms & Positioning 7820 GC Entry Level LTM /7890 GC Fast heating/ cooling Price/Performance 490 Micro GC Fast Gas Analysis Compact Size 7890 GC Highest flexibility Industry leader Technologies 6850 GC Small footprint Page 29 Gas Chromatograph Agilent Restricted
30 Thank You. Page 30 HPI Solution overview Agilent Restricted Neophyte training Shanghai,Sep, 2007
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