Jet Fuel Analysis Laboratory Instruments for quality control, analysis and calibration of aviation fuels

Transcription

1 Laboratory Instruments for quality control, analysis and calibration of aviation fuels Jet A-1 Jet A Jet B JP-8 FT-SPK HEFA-SPK

2 Avcount2 Laser Based Particle Counter (SA1000-2) IP 565; ASTM D7619; Defence Standard (DEF STAN) & ASTM D975; ASTM D6786, ASTM D7647, ISO 4406 (1991 & 1999), GOST 17216, NAS 1638, SAE AS4059E, SAE A6D, SAE 749D, GB 5930, GJB , GJB 420-A-1996, GJB 420B-2006 Particle size ISO 11171: 4μm(c) to >70μm(c); ISO 4402: 2μm to >100μm; GOST : 2μm to >200μm Cumulative & distributive particle counts Cleanliness code reporting Uses Straight from the Bottle samples Precise and reliable results Rugged case suitable for laboratory or portable use Typical test time of less than 6 minutes 16 fixed measuring channels (calibration in compliance with ISO MTD for measuring oil An upper and lower limit value can be set for each of the first 6 counting channels Data storage for up to 2300 measurements across 64 memories Internal Double Pump System downstream of measurement cell Optional in-line high pressure testing up to 315 Bar Dual calibration tables:- NIST SRM 2806b and NIST SRM 2806a APPLICATIONS Aviation turbine fuel Aviation turbine oils Hydraulic and lubricating oils Skydrol hydraulic fluid (SA version) Biofuels and biofuel blends Heating oil Gas oil Diesel - automotive and marine Gasoline and kerosene AvCount2 (SA1000-2) AvCount2 is a laser based particle analyser used for determining the particle concentration in liquid fuels and oils. It can be used throughout distribution networks and in the laboratory, in fact anywhere that requires accurate determination of particle distribution in a liquid sample. Whether checking the quality of fuel, efficacy of filter systems or condition of in-service lubricants, AvCount2 provides fast and precise results. AvCount uses the light emitted by a laser to illuminate a cell through which the sample is passed. Each particle present in the sample casts a shadow onto the sensor within the cell, and as the shadow passes across the sensor the voltage output of the sensor drops. The voltage drop of the cell is proportional to the particle size and AvCount2 calculates the size of the particle based on this principle. Results are displayed in real time and are simultaneously printed out on the integral printer. The test methods embedded in AvCount2 cover a range of fuels, lubricating oils and hydraulic fluids and can be edited to create custom test profiles. Versatile connectivity and memory management allow results to be accessed, printed out or downloaded to a USB stick. AvCount2 supports dual calibration tables, allowing users to select tests using an ISO calibration traceable to NIST SRM 2806b or to a secondary working standard traceable to the last certified values of NIST SRM 2806a. View a demo video online: Sample Preparation AvCount Bottle Tumbler (SA1010-0) Fitted with 250ml syrup bottle holder. Provides a consistent gentle end-over-end tumble action to maintain a homogeneous suspension. IATA Tumbler (5 Litre) (SA1020-0) Suitable cans: UN LACQ 1A1/X/550 Cans (W 210mm x H 220mm). UN LA1A1/X1.6/600 Cans (W 180mm x H 260mm). Verification AvCount Verification Material (SA1006-0) The material is a suspension of a NIST medium test dust in a super-clean clear, mineral based, technical oil, traceable to NIST 2806 cx) AvCount Verification Material is manufactured in accordance with ISO 11171:2016 Annex F, with the exception of the use of a clear technical oil as diluent. The certified values are statistically derived from the results of a significant number of tests conforming to IP 565, using AvCount instruments calibrated in accordance with ISO 11171:2016, using materials traceable to NIST SRM 2806b, under ISO 9001 conditions. The certificate also gives values for instruments calibrated with materials traceable to NIST SRM 2806a. The homogeneity and variability of the AvCount Verification Fluid is checked in accordance with ISO Guide 35 and the essentials of ISO Guide 34. NOTE: Supplied in 250ml bottle with Certificate of Measurement. Ultrasonic Bath to ISO11171 ( ) Required for preparation of calibration and verification materials. 2

3 Laboratory instruments for quality control, analysis and calibration AvCount Lite Laser Based Particle Counter (SA1800-0) IP 565; ASTM D7619; ASTM D975; Defence Standard & Particle size ISO 11171: 4μm(c) to >100μm(c) Cumulative particles/ml Bottle samples or on-line Simple operation High visibility screen Suitable for laboratory or portable use Integral battery option (max 3 hours, 60+ tests) Stand-alone or PC controlled Programmable via PC Volume or time based Data storage for up to 600 results Typical test time of less than 4 minutes AvCount Lite provides fast and reliable results for determining the particle concentration in liquid fuels and oils. A combination of innovative features and rapid measurement technologies make the AvCount Lite highly flexible, whilst its portable design allows use in the field and the laboratory, without ease of use or accuracy of results being affected. AvCount Lite is fitted with a precision dual piston pump. When measuring samples from a bottle, the pump draws an aliqot of sample through the measurement cell at a consistent flow rate. When connected to a pressurised line, the pump provides accurate metering and control. A pressure reduction system is available for applications above 10 bar. Custom test methods can be created on a PC or laptop before being uploaded to the AvCount Lite s memory. Test progress and results for up to 6 size bands are displayed as cumulative particles/ml and ISO 4406 cleanliness codes. Results are then stored within the AvCount Lite s internal memory which has space for up to 600 sets of results. If required, the results can be downloaded via USB port for further analysis and printing from a computer. AvCount Lite is supplied with ASTM D7619, IP 565 and ISO 4406 pre-installed. APPLICATIONS Aviation turbine fuel Aviation turbine oils Hydraulic fluids Skydrol hydraulic fluid (SA version) Biofuels and biofuel blends Gas oil Diesel - automotive and marine Gasoline and kerosene AvCount Lite (SA1800-0) AvCount Software Three Windows based programmes are available and compatible with the AvCount Lite. Protrend - Allows an operator to control an AvCount Lite from a personal computer or laptop. It allows the operator to create local custom test methods, run tests and download data. Protrend supports multiple AvCount Lite units, synchronising the sampling and measurement to allow trend analysis. Partikel - Used to create and upload test methods into the memory of the AvCount Lite. Intended for supervisors, it allows the AvCount to be configured with up to 3 test methods. Once uploaded, AvCount Lite can be used as a standalone instrument, Partikel software is supplied. Calibration - Supplied with the instrument for the calibration of AvCount Lite, calibration curves can be created and uploaded. These can be based on a number of different standards including Seta SA1018-0, a secondary working standard traceable to NIST SRM 2806b. 3

4 FIJI FAME in Jet Instrument (SA5000-2) ASTM D1655; Defence Standard IP 583; ASTM D7797 Determination of the fatty acid methyl esters (FAME) content of aviation turbine fuel (AVTUR) by Fourier Transform Infrared Spectroscopy - Rapid screening method All FAME types from C8 to C22 including Coconut, Mustard, Palm, Rapeseed, Sunflower oil, Soya, Jatropha Analysis time 20 minutes Certified range mg/kg FAME in AVTUR Measuring range mg/kg in AVTUR Certified range 20ppm to 20% in Middle Distillates Laboratory and field instrument Fully automatic Suitable for untrained operators No cleaning solvents required No pre-sample preparation required 50 ml sample volume FIJI (SA5000-2) The patented Fame In Jet Instrument (FIJI) has been developed to offer the industry a rapid and easy check on Parts Per Million (ppm or mg/kg) levels of FAME in Aviation fuel using test method IP 583 and ASTM D7797. FIJI uniquely utilises state of the art FTIR (Fourier Transform Infra-Red Spectroscopy) technology and a patented sample preparation system which allows FAME detection accuracy down to the 10mg/kg level. FIJI can be used as a field or lab based screening tool to give a quick indication of possible FAME contamination that may then necessitate further investigations. The instrument can be used to prevent expensive testing and avoid costly delays of fuel release. The FIJI instrument is robust, extremely simple to use and is fully automatic so no specialist operator training is involved. Tests require less than 50ml of sample and typically take under 20 minutes. Results are presented in mg/kg units together with an optional traffic light system for flagging FAME contamination levels of the fuel. By comparison current analytical tests can take many hours, require complex equipment and demand high skill levels. Using a unique sample preparation module the sample is pumped at a controlled flow rate though a proprietary disposable cartridge. The sample components are spectrally analysed by the FTIR and a result is displayed in mg/kg and a graphical spectrum is also shown. The system is self-cleaning so no solvents are required. After each test the cartridge is simply and easily replaced and the instrument is immediately ready for the next sample. Visit: View a demo video online: Test OK at < 50ppm Test Fail at >50ppm Operator Sequence Place Sample Cartridge Load Cartridge Press GO Test Completed 4

5 Laboratory instruments for quality control, analysis and calibration WSI Water Separation Instrument (SA9000-0) ASTM D8073 Substantial cost saving per test Fully automated sample handling Measures 50 to 100 WSI 250ml sample volume Simple operation for non-chemists Patented Ultra Sonic Mixer 10 minute test duration Sonic mixing sequences providing consistent water droplet size and stable emulsion Featuring an API/EI th edition filter material High resolution optical water detector measuring to <1ppm water concentration USB data output The WSI is used in the aviation sector to provide an indication of the presence of surfactants in aviation fuel. Surfactants, or surface active agents, are not normally present in aviation fuel, but can be picked up during transportation in pipelines, ships or storage, or through misadditization. Surfactants in the fuel affect the ability of filters in the distribution network to remove entrained water through coalescence. The WSI is a small fully automated laboratory instrument which reduces the chance of error in this critical aviation fuel test. Simple touch screen operation enables tests to be started quickly and easily. Using a disposable filter cartridge, and a patented specific dye detector, the WSI dynamically measures the sample under test for its ability to separate water. Sample preparation is automatic and uses patented sonic mixing technology to emulsify the sample, which enables a uniform water/fuel mixture every time. Results are calculated from the detector reading and displayed on screen as the Water Separation Index (WSI). A high WSI, such as 100, indicates the sample coalesces easily and is relatively free of surfactants. WSI Filter cartridges use API/EI th edition filter material which is less sensitive to weak surfactants and is less affected by SDA, eliminating uncertainty over static dissipater additives, but is responsive to the presence of ester based additives. WSI (SA9000-0) The instrument features fully automated sample handling and therefore requires minimal operator time with just 3 simple steps to start a test. To operate the instrument, a sample is first poured into the test beaker and a filter cartridge fitted. Next, using the user friendly touch screen the sample information is entered before pressing start to commence the test. Once the test is underway the sample is purged through the instrument, then a specific amount of dyed water is added via the accurate microliter pump. The ultrasonic mixer emulsifies the fuel/water mixture according to a defined routine to make an emulsified sample. The emulsified sample is passed to the detector, the water content is checked, and then passed through the filter cartridge to the detection system. If the water in the emulsion is successfully removed (good water separation) by the filter cartridge then the aviation fuel is deemed to be free from surfactants and a high value is reported (WSI 97 to 100). If water passes through the filter (poor separation), it is measured by the detector, and a lower WSI number is reported, indicating a fuel which may contain surfactants. View a demo video online: Evochrom Aromatics HPLC System - Diesel & Jet Fuel (SA2400-3) ASTM D6379; IP 436 Complete HPLC system allows plug and go for the busy lab Precision engineered HPLC hardware with proven technology Chromatography assured with optimised column technology meeting the latest ASTM D6379 and IP 436 Method requirements Quality separations provide accurate and precise results every time Fully compatible to meet and measure Aromatics as referenced in DEF STAN and ASTM D1655 High performance liquid chromatography (HPLC) measuring mono and di-aromatic hydrocarbon content in aviation kerosenes and petroleum distillates. Evochrom (SA

6 Setaflash Series 3 ( ) Setaflash Series 3 Flash Point Tester ( & ) ASTM D3828; ASTM D7236; IP523; ISO3679 Rapid equilibrium (flash / no flash) 1 or 2 minutes test time 2ml sample Ambient to 300 C Ramp mode Compact, portable and rugged design Automated flash detection USB port and results storage SPECIFICATIONS Seta Part No Methods: ASTM D3828; IP523; ISO3679 ASTM D3828; ASTM D7236; IP523; ISO3679 Cup: Closed Closed Material: Aluminium Aluminium Temperature Range: Test Duration Rapid Equilibrium Mode Temperature Ramp Mode: Ambient to 300 C Ambient to 300 C 1 minute 1 minute Automatic or custom settings (ramp rate: up to 6 C/min and beep rate: up to 5 C/B intervals). Extended test range, 100 C from The Setaflash Series 3 provides fast start temperature and reliable results for determining the Temperature C or F C or F flammability of Avtur. The versatility of the Series 3 makes it ideal for mobile testing Selection: User Interface: Colour LCD display - touch screen Colour LCD display - touch screen sensitive sensitive whilst also suitable for product checks Navigation: Control knob (rotational and Control knob (rotational and in-house. push-down) push-down) A simple user interface and colour digital Data Storage & 1GB internal memory and 1GB internal memory and display guides the user through the straightforward testing process, minimising the need for operator skill or expertise. Ramp mode allows standard testing in Download: Fuel Supply: Sample Size: Pressure integrated USB port Integrated gas tank (removable) 2ml or 4ml Automatic barometric correction integrated USB port Integrated gas tank (removable) 2ml or 4ml Automatic barometric correction Correction: accordance with ASTM D7236. Tests require only a 2ml sample and take no more than 1 minute to complete, enabling laboratories to maximise operability whilst reduce cost and waste per test. Setaflash Series 3 Activecool ( ) ASTM D3828; ASTM D7236; IP 523; ISO 3679 Rapid equilibrium (flash / no flash) Ramp mode Sub-Ambient Tests and Rapid Cool Down Temperature range 10 to 130 C Corrosion Resistant option 2/4ml Sample Size Electronic heating and cooling View a demo video online: Setaflash Series 3 Activecool ( ) Setaflash Series 8 Activecool Closed Cup Tester ( ) ASTM D3828; IP 523; ISO 3679 Rapid equilibrium (flash / no flash) Ramp mode Temperature range of -20 to 130 C Small sample size, 2 or 4ml Corrosion Resistant cup option Electric ignitor (with gas option) Automatic dipping and flash detection ActiveCool electronic Peltier cooling 64 Test memory & RS232 interface C or F temperature display Barometric pressure correction Setaflash Series 8 ( ) The Setaflash Series 8 ActiveCool is an automated closed cup flash point tester with a temperature range of 10 to 130 C (50 to 266 F) with no external cooling required. When connected to a suitable chilled water supply, the range is extended down to -20 C (-4 F). There are two modes of operation; flash/no flash and ramp. The ramp mode increases the sample temperature at a rate of 2 C/min and automatically dips the ignitor every 1 C up to 100 C (every 2 C above 100 C), until either a flash is detected or the end of test temperature is reached. View a demo video online: 6

7 Laboratory instruments for quality control, analysis and calibration PM-93 Pensky-Martens Closed Cup Flash Point Tester ( ) ASTM D93 Procedures A, B and C IP 34 Procedures A, B and C ISO 2719 Procedures A, B and C Strict conformance to international test methods Temperature range ambient +5 to 400 C Easy 3-step to test operation involving minimal operator intervention Unique SafeFlash fire extinguishing system Large touch screen Single action lifting pod Small, compact footprint Seta Ignite - robust and long lasting ignitor 30 programmable test profiles, test methods & sample names Rapid fan assisted cooling Optional barcode reader available The Seta PM-93 is a fully automated Pensky-Martens Closed Cup Flash Point Tester which combines strict method conformance with state of the art control technology and safety systems to provide the next generation of automated precision flash point instruments. Seta PM-93 provides rapid sample testing using integral heating and forced air sample cooling systems. An intuitive user menu and 8.4 (215mm) SVGA colour touch screen operation provide unrivalled ease of use with real time display of test progress. Large capacity memory allows storage of test profiles, operator names, test methods and in excess of 2000 results. Unique test profiles enable the test to be set up and repeated quickly without re-entering the same information. For example, if numerous jet samples with similar expected flash points are being tested then a test profile can be set up and stored to memory so the user can select this option without the need to program the test parameters. Operation is simple, just a single raising or lowering action when loading or removing the test cup. The lid and shutter are integral to a hinged pod and fitted with a fire detection probe, fire extinguishing manifold, ignitor, flash detector and temperature probe. The stirrer drive, shutter actuator and ignitor dipping mechanism are also self contained within the pod module. A unique alignment design ensures that the lid and cup locate perfectly every time. The ignition source is a purpose-designed extended life hot wire, a gas ignition option is also included. The sample temperature probe is a class A PRT and flash detection is by a thermocouple. An optional, unique SafeFlash fire extinguishing system ( ) is available which automatically and immediately activates an extinguisher in the event of excess flame or fire around the test cup. If discharged the screen prompts the user to re-activate the extinguisher by simply replacing the integral inert gas canister. Canisters remain sealed inside the instrument until pierced by the actuator mechanism. Additional safety features include PRT checks, safety dip before starting, overtemperature cut out, gas flame relight and gas shut off. Rapid turnaround between tests is achieved using a high capacity cooling fan and optimised air flow. A password protected calibration mode quickly allows verification of instrument performance (a suitable range of traceable verification and calibration materials are available from Seta). Cleaning & maintenance procedures are simple. The instrument s lid and shutter can be cleaned in-situ to minimise down time between tests and a quick release mechanism allows easy access to the lid and shutter for maintenance. Visit: View a demo video online: PM-93 ( ) 7

8 Jet Fuel Analysis Seta Multiflash Tag & Abel Flash Point Module ( , & ) ABEL IP 170; TAG ASTM D56 Highly automated low cost Modular System with in-built safety Strict conformity to test methods Gas or Electric Ignition Temperature in C or F The Seta Multiflash Universal Base can be used with either an Abel or Tag module to conform precisely to reference test methods. Multiflash comprises a water/air bath, sample cup and lid, temperature probes, flash detector, and a DIPS pod (Dipping, Ignition, Pilot, Stirrer) containing the ignitor dipping mechanism with co-axial gas/electric ignitor, and a stirrer (Abel). Interchanging the test module is straightforward and completed in just a few minutes, the base unit recognises that the Abel or Tag module is connected and configures standard test parameters. View Multiflash ABEL: View Multiflash TAG: Multiflash ( & ) Seta Semi-Automatic Tag Flash Point Tester ( ) ASTM D56 Ambient to 93 C Variable temperature rise rate 500ml bath The Seta Tag Flash Point tester is equipped with an electrically heated cup. The controller has the facility to allow the user to vary the rise rate of the temperature. The test flame can operated from either mains gas or the optional portable gas tank ( ). The stainless steel case has an integral drip tray and bath overflow. Visit: Tag Tester ( ) Seta Pensky-Martens Closed Cup Flash Point Tester ( ) ASTM D93 Ambient to 370 C Variable ramp rate Two speed stirrer Forced air cooling facility The Pensky-Martens closed cup flash point tester has an electrically heated cup, adjustable temperature ramp rate and two speed stirrer (for ASTM D93-IP34 Methods A & B). Visit: Pensky-Martens Closed Cup Tester ( ) 88

9 Laboratory instruments for quality control, analysis and calibration Handheld Conductivity Meter ( ) ASTM D2624; IP 274; DEF STAN , ASTM D1655 High Accuracy AC Measurement (± 1.5% of reading) Conductivity and temperature output capability Measure in any sample container No need to relax fuel Calibration kit available Stores up to 8 Data Locations USB interface for ease of data transfer Fully Temperature Compensated Measurement The Seta D2 Hand Held Conductivity Meter (D2 JF-1A-HH model) meets the requirements of ASTM D2624. It provides an accurate and rapid conductivity measurement of distillate fuels; and is specifically designed for testing low conductivity fluids such as such as aviation kerosene, ULSD, home heating fuel, Naphtha, and printing ink. The Meter can measure fuel electrical conductivities between 0 and 2000 picosiemens/meter (ps/m), although it is optimised and normally used in the 0 to 500 ps/m range. Visit: Conductivity Meter ( ) Conductivity Calibration & Verification Tool ( ) The Calibration & Verification tool fits easily onto the tip of the Handheld Conductivity Meter for quick and easy calibration or verification of the instrument. It has one switch to easily alter the range from low value (200 ps/m) to high value (500 ps/m). This allows the user to verify or calibrate conductivity in the field thus eliminating the costly requirement of returning the instrument to the factory. The tool is optimised for AC conductivity measurement with active components ensuring long term stability and accuracy. Visit: Calibration Tool ( ) In-Line Conductivity Analysis ( ) ASTM D2624 High-Accuracy AC measurement technology Allows precise control & measurement of SDA Additive Injection Can be linked to automatic dosing system Local display available Connect to standard 4 to 20 ma current loop Stainless Steel construction Easily fitted and retracted from the pipeline via a retractable mount Can be fitted to pipes of various diameters ATEX, FM, FMc Certified for Zone 1, Hazardous Areas 16 Bar pressure or 100 Bar with the High Pressure Unit. The In-Line Analyser provides a continuous 24/7 highly accurate record of product conductivity levels inside the distribution lines. In-Line conductivity measurement provides significant benefit to operators by offering the ability to measure conductivity in real time thereby continuous compliance with conductivity level requirements. It also eliminates the requirement for manual sampling and record keeping. Process connection types: ANSI, DIN, NPT or BSP. Visit: In-line Conductivity ( ) 9

10 Jet Fuel Analysis Seta Existent Gum Solid Bath ( ) ASTM D381-IP 131; IP 540; ISO Test stations Suitable for air operation Digital temperature control 140 to 260 C temperature range Flow gauge calibrated for air A Solid Block Bath designed to carry out up to five simultaneous tests for determining existent gum content in fuels by the Jet Evaporation method. The unit comprises a solid block bath with removable taper-fit conical air jet adaptors with copper screens, and an air flow control valve and gauge. The bath has five test wells and a thermometer well. Outlets can be individually checked for uniform flow of air. The bath has a temperature range of 140 to 260 C, and is controlled by a digital temperature controller which displays both the set temperature and the actual bath temperature measured by a probe. The flow of air is adjusted by an inlet control valve and monitored on a calibrated Bourdon gauge. An air and steam unit is also available ( ) Visit: Existent Gum Bath ( ) SSAFlab Filtration Kit ( ) ASTM D5452, IP 423 The Seta SSAFlab Filtration Kit is used to determine particulate contamination in aviation fuels in accordance with ASTM D5425 and IP 423. The kit comprises 0.45 micron filter, matched weight pair of 0.8 micron filters, stainless steel filter holder with stainless steel screen, filter forceps, 25mm solvent filtering dispenser, vacuum filtering flask, petrislide and earth bonding/grounding as specified in the method. Visit: Filtration Kit ( ) Seta Hydro-Light Water Pad Tester ( ) ASTM D3240 Fully automatic reader, simple to use Reads standard 25mm test pads 0-50ppm measurement range No maintenance required, longlife LED lightsource Highest precision of any instrument available for test method ASTM D3240 Supplied with calibration standard The Hydro-Light was adopted into ASTM D3240 in 2009 and provides the most precise measurement of the 25mm water pads. The instrument is exceptionally easy to use and provides a result within 30 seconds. The instrument is small and ideally suited for either portable or lab use, an optional battery pack allows 24 hours of continuous use between charging cycles. Each instrument is provided with a factory calibrated standard that enables instant confirmation that the Hydro-Light is working correctly, the same standard can also be used to calibrate the instrument in the field. Visit: Hydro-Light ( ) 10 10

11 Laboratory instruments for quality control, analysis and calibration KV-2 Viscometer Bath ( ) ASTM D445-IP 71; ISO 3104 Temperature range -40 to +20 C High stability ±0.015 at -20 C, ±0.01 at -40 C Accommodates up to 2 standard viscometer tubes Illuminated bath Insulated and heated viewing window Heated top plate The Seta KV-2 is a two place low temperature viscosity bath designed to achieve ultra-high stability in the temperature range of +20 to -40 C. The instrument has a small footprint and is ideally suited for busy labs. Stability is better than ±0.015 at -20 C and ±0.01 at -40 C. The bath is fully self contained and requires no external chillers or connections. A heated top plate and viewing window prevent condensation and ice formation, this, combined with high intensity long life ultra-bright LED lighting ensures clear bath visibility at all times. Data logging via the external RS-232 port is also possible when connected to a PC and suitable software. Each bath is provided with a factory calibration certificate, traceable to UKAS including temperature traces. Customers can request specific temperature calibrations and traces if required, ensuring that the product meets their exact requirements. Visit: KV-4 Low Temperature Viscosity Bath is also available ( ) Visit: KV-2 Viscometer Bath ( ) ASTM stability limits ASTM stability limits ASTM stability limits ASTM stability limits Stability trace at -20 C. Solid red line shows ASTM stability limits (±0.05 C) Stability trace at -40 C. Solid red line shows ASTM stability limits (±0.05 C) Kerosene Viscosity Standards ASTM D445; ISO 3104 Certified according to ISO / ISO Guide 34 under UKAS accreditation Supplied in 500mL bottle Fully traceable to international standards Ensures full compliance to ASTM & IP test method protocol 2 Year shelf life Seta Part No. Temperature Kinematic Viscosity mm²/s (cst) (nominal value) JF1-20 C (-4 F) JF2-40 C (-40 F) Kerosene Density CRM ( ) ASTM D1480; ASTM D4052; ISO 365; ISO Viscosity Standards Certified to ASTM D1480 for 15.0 C Supplied in 250mL bottle Dual certified in accordance with ISO and ISO Guide 34 under UKAS accreditation All data generated exclusively by UKAS ISO accredited laboratories Fully traceable to international standards 11

12 Jet Fuel Analysis Copper Corrosion ASTM D130-IP 154; ISO 2160 Solid or Liquid baths 2, 4 and 9 place options Suitable for copper and silver corrosion tests Seta offer a range of baths suitable for Copper and Silver Corrosion tests. The model is a compact two place liquid bath which is suitable for both copper and silver corrosion tests. The bath has a temperature range of ambient +5 to 120 C, ±0.1 C and comes complete with lids and hooks to suspend the test vessels during the test. The model is a compact 4 place solid block bath suitable for both copper and silver corrosion tests. The solid bath has a temperature range of 50 to 150 C with stability better than 0.1 C. The bath is supplied with lids and hooks to suspend the test vessels during the test. Seta Copper-Silver Corrosion Bath ( ) Visit: Seta Copper-Silver Block Bath ( ) Visit: Copper-Silver Block Bath ( ) Shown with optional test vessel, test tube holder & temperature probe Copper-Silver Corrosion Bath ( ) Setastill Distillation ( ) ASTM D86; IP 123; ISO 3405 Ambient to 400 C distillation range Adjustable height heater/flask platform Toughened glass window Cooling fan The distillation unit, mounted to the left, comprises a flask support mechanism, heater elements, and the heater controller. The flask is supported by a drop-in ceramic-glass support board mounted to a platform that is adjustable for height. The quartz enclosed heating elements are also attached to the platform, and are powered by a solid-state energy regulator and calibrated control. A cooling fan is installed in the rear of the distillation unit to reduce cooling time between distillations. The condenser unit is attached to the distillation unit, and may be used with either a static fill of coolant or a laboratory cooling supply. Visit: Seta Smoke Point Apparatus ( ) ASTM D1322; IP 57; IP 598; ISO 3014 Tripod stand, lamp body and chimney Viewing window Robust construction Setastill Distillation ( ) The Seta Smoke Point Apparatus determines the smoke point of kerosine and aviation turbine fuel by measuring the maximum flame height prior to smoke formation and comparing the results with those of known standards. Smoke point gives an indication of aromatic content and radiant heat transfer characteristics and has good correlation with IP 598 and ASTM D1740 (Luminometer number). Comprises a tripod stand, lamp body, and chimney. The measuring scale is viewed through a curved glass window on the front of the instrument. A mirror ( ) can be attached to the chimney to aid smoke detection. Visit: Smoke Point Apparatus ( ) and Mirror ( ) Seta Freezing Point Apparatus ( ) ASTM D2386; IP 16 Freezing Point Apparatus ( ) Detects solid hydrocarbon crystals Reference method Comprises sample tube, paddle, unsilvered flask, cork stopper/thermometer support, and an insulated metal case with a viewing slot. Visit:

13 Laboratory instruments for quality control, analysis and calibration Seta Mobile Test Kits Seta offer Aviation Fuel Test Kits for rapid detection of contamination in jet aviation fuel. The kits are designed for use on the apron and at fuel storage facilities allowing users to carry out tests that can quickly provide a go/no-go decision on aviation fuel quality. The kits can be easily transported to test sites which have limited or difficult access and are ideally suited for shipboard use providing both rapid and easy verification of product integrity prior to off-loading. SSAFPAK Test Kit ( ) Visit: Fuel Integrity Test Kit ( ) Visit: SPECIFICATIONS: Mobile Test Kits Seta Part No. SSAFPAK Test Kit ( ) Fuel Integrity Test Kit ( ) Test Methods: Density - ASTM D7777 Flashpoint - ASTM D3828 Contamination Conductivity - ASTM D2624 Flashpoint - ASTM D3828 Density - ASTM D7777 Conductivity - ASTM D2624 Water Content - Shell Capsule Water Content - Shell Capsule Microbial Activity - ASTM D8070 Case Style: Rugged fitted case Rucksack Size (HxWxD): 35 x 90 x 80cm 30 x 30 x 30cm Weight: 12kg 6.5kg SSAFCON Sampler ( ) SSAFPAK Test Kit ( ) ASTM D2276; IP 216 Filter tests for particle contamination and colour rating of Aviation Fuels Eliminates the exposure of fuel during testing In-line test - no fuel disposal/waste requirement Improves operator safety SSAFCON is a unique monitoring system for portable line sampling of aviation turbine fuel to determine particulate contamination and colour ratings. The system was originally developed in collaboration with a leading aviation fuel producer and is now used by companies responsible for distributing and uploading aviation fuel on a worldwide basis. Visit: SSAFCON ( ) Seta Multi-Colour Automatic Colorimeter ( ) ASTM D156; ASTM D6045 Automatic operation Multiple colour scales including ASTM and Saybolt Rapid measurement < 25 seconds Objective colour measurement RS232 interface Integrated remote calibration An automated spectrometric colorimeter designed for rapid colour analysis of petrochemical products. Visit: Multi Test Verification Material Colorimeter ( ) Test Name: Method: Seta Kerosene MTVM ( ) Distillation IBP Distillation 10% D86-IP123 D86-IP123 D86-IP 123; EN ISO 3405; IP 170; EN ISO 13736; D2386-IP 16; D1319-IP 156; D1322-IP 57; ISO 1322; D445-IP 71; EN ISO 3104; D3242-IP 354; D3227-IP 342; ISO 3012 Distillation 50% Distillation 90% Distillation FBP D86-IP123 D86-IP123 D86-IP123 Multi Test Verification Materials (MTVM) allow routine verification of instrument performance and compliance to test methods. The Seta MTVM range is unique in that unlike most other certified reference materials that are only suitable for validating a specific parameters the MTVM s enable the user to validate a range of different tests and instrumentation using the same sample material. Distillation Residue Distillation Loss Flash Point Freezing Point D86-IP123 D86-IP123 IP170 D2386-IP16 The MTVM material is blended and manufactured in conformance to ISO9001 and EN ISO/ IEC 17025:2005 (ISO Guide 25 and EN 45001). The certified values are the mean results obtained by a statistically significant number of participating laboratories. Each MTVM is 500ml and has a shelf life of 18 months. Visit: Aromatics FIA Smoke Point Kin Vis -20C Acid Number Mercaptans Density at 15 C D1319-IP156 D1322 IP71 IP354 IP342/D3227 IP365 Kerosene MTVM ( ) 13

14 Seta Twin Column Adsorption Apparatus ( ) ASTM D1319-IP 156; BIS IS 1448 Part 23; BS 2000 Part 156; FTM ; ISO 3837 Determines volume % of saturates, olefins and aromatics in petroleum fractions Analyses 2 samples simultaneously Measuring Fluorescent Indicator Adsorption in Liquid Petroleum Products, the Seta Twin Column Adsorption Apparatus is a wall mounted system that comprises a control box, measuring scales with slide markers, mounting clips for two columns and a 365mm UV light mounted vertically to optimise fluorescence when viewing boundaries and saturates zones. Separate pressure gauges and valves provide individual pressure control to each column. Adsorption Columns and component parts Twin Column Adsorption Apparatus ( ) Multi-Level Sampler ( ) Suitable for true spot samples 1 litre Stainless Steel Snatch cord opening Valve latches open Top Hat prevents sample contamination Opened at the required depth by a top opening snatch valve which is fitted with a top hat to prevent contamination by higher level samples streaming into the container during retrieval. Multi Level Sampler ( ) Winder with Depth Counter ( ) A mechanically driven depth counter shows the operator the depth of the sampler at all times. The design also includes a reduction gear drive between the winding handle and the reel to assist the lifting and lowering of samples. Contamination that can occur with ropes and chains is avoided with the stainless steel cable and the special hook minimises the risk of a sample becoming detached from the winder. The hook and cable, together with the winder s earthing strap, ensure electrical continuity and prevent the build up of static electricity. Equipped with an automatic reel lock for added safety. Winder with Depth Counter ( ) Portable Density Measurement Kit ( ) IP 559; ASTM D to 3g/cm3 range Single hand operation Density and SG measurements Explosion proof - Ex II 2 G EEx ib llc T4 Automatic temperature compensation Density standards included in the kit Via a spring loaded plunger action pump, the oscillating U tube type density meter draws sample into the measurement chamber. Alternatively, a sample can be introduced by syringe through the supplied Luer adaptor. The internal seals are manufactured from Kalrez and are resistant to attack from petrol and similar organic solvents. Portable Density Measurement Kit ( ) Hydrometer Jar (Pack of 5) ( ) Glass hydrometer reading jar with foot, measuring 47 (h) x 6.3 (dia) cm and supplied in packs of 5. Hydrometer Jar ( ) Jet Fuel Hydrometer ( ) ASTM D1298; ASTM D1665; DEF STAN 91-91; IP 160 A BS718 M50SP hydrometer specifically calibrated for a range of 0.775g/ml to 15 C for measuring the density of jet turbine fuels such as Jet A, Jet A1 and JP-8. Jet Fuel Hydrometer ( ) 14 14

15 Laboratory instruments for quality control, analysis and calibration Aviation Fuel Test Methods, Product Guidance Test Method Test description IInstrument Seta Reference ASTM D56 Flash Point by Tag Closed Cup Method Automatic Multiflash, Manual , IP 170 ISO Flash Point by Abel Closed Cup Method Automatic Multiflash, Manual , ASTM D86 IP 123 ISO 3405 Distillation of Petroleum Products at Atmospheric Pressure Manual Distillation ASTM D93 IP 34 ISO 2719 Flash Point by Pensky-Martens Closed Cup Method Automatic PM-93, Multiflash, Manual ASTM D130 IP 154 ISO 2160 Corrosiveness to Copper from Petroleum Products by Copper Strip Test ASTM D156 Saybolt Color of Petroleum Products (Saybolt Chromometer Method) Copper Corrosion Liquid Baths Copper Corrosion Solid block baths , , , Automatic Multi-Colour , ASTM D381 IP 540 ISO 6246 Gum Content in Fuels by Jet Evaporation Existent Gum Bath ASTM D445 IP 71 ISO 3104 Kinematic Viscosity of Transparent and Opaque Liquids KV-2 Low Temperature Viscometer Bath ASTM D1298 IP 160 Density and Relative Density (Specific Gravity) of Liquids Hydrometers Please contact Seta ASTM D1319 IP 156 Hydrocarbon Types in Liquid Petroleum Products by FIA Seta FIA Apparatus ASTM D1322 IP 57, IP 598 ISO 3014 Smoke Point of Kerosene Smoke Point Apparatus ASTM D2276 IP 216 Particulate Contaminant in Aviation Fuel by Line Sampling SSAFCON Sampler ASTM D2386 IP 16 Freezing Point of Aviation Fuels Freeze Point Apparatus (reference method) ASTM D2624 IP 274 Electrical Conductivity of Aviation and Distillate Fuels Conductivity Meter: Handheld Conductivity: In-line ASTM D3240 Undissolved Water In Aviation Turbine Fuels Hydro-Light Water Pad Tester ASTM D3828 IP 523 ISO 3679 Flash Point by Small Scale Closed Cup Method Series 3 & Series 8 ActiveCool , , , ASTM D5452 IP 423 Particulate contaminant in aviation turbine fuels by laboratory filtration ASTM D6045 Color of Petroleum Products by the Automatic Tristimulus Method ASTM D6379 IP 436 Determination of Aromatic Hydrocarbon Types in Aviation Fuels and Petroleum Distillates by HPLC ASTM D7777 Density, Relative Density, or API Gravity of Liquid Petroleum products ASTM D7797 IP 583 FAME Content of Aviation Turbine Fuel - Rapid Screening Method ASTM D8073 IP 565 Cleanliness of aviation turbine fuel by Portable automatic particle counter Water separation characteristics of Aviation Turbine Fuel by Small Scale Water Separation Tester SSAFLab Filtration Kit Automatic Multi-Colour, Saybolt Chromometer EvoChrom SA Portable Density Meter FIJI AvCount, AvCount Lite WSI SA SA1000-2, SA SA

16 Aviation Fuel Specifications, Check List Jet A-1, and Guidance Material DEF STAN ASTM D1655 AFQRJOS IATA ASTM D7566 (Synthesized Hydrocarbons) Aromatics ASTM D1319; 6379; IP 156; 436 ASTM D1319; D6379; IP 436; 156 ASTM D1319; ASTM D6379; IP 156; 436 ASTM D1319; ASTM D6379; IP 156; 436 ASTM D1319; ASTM D6379; IP 156; 436 Colour ASTM D156, D6045 ASTM D156, D6045 ASTM D156, D6045 Corrosion ASTM D130; IP 154 ASTM D130; IP 154 ASTM D130; IP 154 ASTM D130; IP 154 ASTM D130; IP 154 Conductivity ASTM D2624; IP 274 ASTM D2624 ASTM D2624; IP 274 ASTM D2624; IP 274 ASTM D2624; IP 274 Density ASTM D1298; IP 160 ASTM D1298; IP 160 ASTM D1298; IP 160 ASTM D1298; IP 160 ASTM D1298; IP 160 Distillation ASTM D86; IP 123 ASTM D86 ASTM D86; IP 123 ASTM D86; IP 123 ASTM D86; IP 123 Existent Gum ASTM D381; IP 540 ASTM D381; IP 540 ASTM D381; IP 540 ASTM D381; IP 540 ASTM D381; IP 540 FAME ASTM D7797; IP 583 ASTM D7797; IP 583 ASTM D7797; IP 583 ASTM D7797; IP 583 ASTM D7797; IP 583 Flash Point ASTM D3828, D56; IP 170; IP 523 ASTM D3828, D56; D93; IP 170; 523 ASTM D3828, D56; IP 170; IP 523 ASTM D3828, D56; IP 170; IP 523 ASTM D3828, D56; IP 170; IP 523 Freezing Point ASTM D2386; IP 16 ASTM D2386; IP 16 ASTM D2386; IP 16 ASTM D2386; IP 16 ASTM D2386; IP 16 Sulfur ASTM D1266; IP 107 ASTM D1266 ASTM D1266 ASTM D1266; IP 107 ASTM D1266 Smoke Point ASTM D1322; IP 598; 57 ASTM D1322; IP 57 ASTM D1322; IP 598 ASTM D1322; IP 57 ASTM D1322; IP 57 Particulates (Counts) IP 565 IP 565 Particulates mg/l (manufacture) ASTM D5452; IP 423 ASTM D5452; IP 423 ASTM D5452; IP 423 ASTM D5452; IP 423 Particulates mg/l (delivery) ASTM D2276; IP 216 ASTM D2276; IP 216 ASTM D2276; IP 216 Viscosity ASTM D445; IP 71 ASTM D445; IP 71 ASTM D445; IP 71 ASTM D445; IP 71 ASTM D445; IP 71 * Referee test methods are indicated in bold 16 Issue 2