22-25 LA VALVOTECNICA CIT

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1 Table of contents SAMPLING VALVES 1. Dead Volume Free Sampling Valve : Type 125 A Dead Volume Free Sampling Valve : Type 125 AUT Compact Sampling Valve : Type 120 B Dead Volume Free Sampling Valve for High Temperature : Type 135 A Contamination-Free Sampling Valve : Type 125 ST Dead Volume Free Sampling Valve, Easy Clean : Type 125 TC 22-25

2 DEAD VOLUME FREE SAMPLING VALVE TYPE 125 A APPLICATION Sampling of chemicals (liquids, powders, pasteous) out of reactors, dryers, and pipes, under process conditions. Pressure up to 145psi (10bar) or vacuum, temperature up to 180 C (360 F) ADVANTAGES - Compact dimensions - Full safety for user and environment. - No dead volumes

3 TYPE 125 A patented 1. Technical description Sampling Valve Type 125 A Sampling of chemicals out of reactors and pipes under vacuum or pressure. (up to 10 bar and 180 C) Body: Piston: O-Rings: With : Stainless Steel (316l), Hastelloy, Titanium,etc. PTFE, reinforced with glassfibers (FDA) Chemraz white, Viton/PTFE encapsulated, Viton, Silicone, EPDM (FDA) - Bottle 150ml, glass pyrex covered in stainless steel and quick coupling - Purging valve 1/4'' 2. Sampling free of dead volumes Tightness with patented piston In closed position tightness is made directly by the piston on the inside walls of the valve, without O-Rings, packing or seats allowing a perfect tightness without dead volumes. Several options and flexibility Valve and flange dimensions can be adapted to your requirements. Materials for body, piston, and O-Rings can be adapted to the product. Options : - Sampling of sterile and toxic mediums - Automatic sampling - Sampling with mechanical or pneumatic safety device - Special sampling bottles and accessories - Crust breaking piston Short deliveries. All spare parts on stock,

4 4. Functioning TYPE 125 A patented Fig. 1 Fig. 2 Normally closed position : - The piston (9) closes the connection of the reactor or pipe without dead volume (Fig. 1). The perfect tightness is ensured directly by the piston (9) on the body. Sampling : - The piston (9) is wheeled down to the opened position. The product flows down into the sampling bottle (2) (Fig. 2). - The operator checks the desired quantity of product through the sight glass. - The piston (9) is wheeled up, and ensures a perfect tightness when in closed position (Fig. 1). - The pressure (or vacuum) in chamber (25) is equilibrated by opening valve (V). - The sampling bottle (2) can now be removed by the quick-coupling connection (5).

5 5. Mounting TYPE 125 A patented In standard configuration the valve is delivered as shown below (Fig.3) Fig. 3 A B C Nb D E F*** FAMAT (DIN)* 61 mm 125 mm 100 mm 4 13 mm 35 mm 18 mm DIN PN10 DN50 61 mm 165 mm 125 mm 4 18 mm 35 mm 21 mm FAMAT (ANSI)** 61 mm 125 mm 98.4 mm mm 35 mm 18 mm ANSI 2" 150 lbs 61.9 mm mm mm 4 19 mm 35 mm 18 mm OTHER * Special compact flange (circle hole DIN PN10 DN40) ** Special compact flange (circle hole ANSI 1 ½" 150 lbs) *** Only for stainless steel, other material: F = 12 On request: The valve and flange dimensions can be Adapted to your requirements (if possible join drawing with your enquiry).

6 DEAD VOLUME FREE SAMPLING VALVE TYPE 125 AUT Patented APPLICATION Sampling of chemicals (liquids, powders, pasteous) out of reactors, dryers, and pipes, under process conditions. Pressure up to 145psi (10bar) or vacuum, temperature up to 180 C (360 F) ADVANTAGES - Compact dimensions - Full safety for user and environment. - No dead volumes

7 TYPE 125 AUT patented 1. Technical description Sampling Valve Type 125 AUT Sampling of chemicals out of reactors and pipes under vacuum or pressure. (up to 10 bar and 180 C) Body: Piston: O-Rings: With : Stainless Steel (316l), Hastelloy, Titanium,etc. PTFE, reinforced with glassfibers (FDA) Chemraz white, Viton/PTFE encapsulated, Viton, Silicone, EPDM (FDA) - Bottle 150ml, glass pyrex covered in stainless steel and quick coupling - Purging valve 1/4'' 2. Sampling free of dead volumes Tightness with patented piston In closed position tightness is made directly by the piston on the inside walls of the valve, without O-Rings, packing or seats allowing a perfect tightness without dead volumes. Several options and flexibility Valve and flange dimensions can be adapted to your requirements. Materials for body, piston, and O-Rings can be adapted to the product. Options : - Sampling of sterile and toxic mediums - Sampling with mechanical or pneumatic safety device - Special sampling bottles and accessories - Crust breaking piston Short deliveries. All spare parts on stock,

8 4. Functioning TYPE 125 AUT patented Figure 5 9. Piston 25 Venting valve 72 Actuator 1 Sampling bottle 1 Check that the sampling bottle 1 is fixed, and the venting valve 25 closed (Fig. 5). 2 Open progressively the piston and: 3 Observe the flow of the product in the sampling bottle. Caution! Do not overfill! This could result in flow of product when removing the sampling bottle! 4 Close the sampling valve. 5 Open the venting valve Remove the sampling bottle 1. 7 Refix the empty sampling bottle 1. 8 Close the venting valve 25.

9 5. Mounting TYPE 125 A patented In standard configuration the valve is delivered as shown below (Fig.3) Fig. 3 A B C Nb D E F*** FAMAT (DIN)* 61 mm 125 mm 100 mm 4 13 mm 35 mm 18 mm DIN PN10 DN50 61 mm 165 mm 125 mm 4 18 mm 35 mm 21 mm FAMAT (ANSI)** 61 mm 125 mm 98.4 mm mm 35 mm 18 mm ANSI 2" 150 lbs 61.9 mm mm mm 4 19 mm 35 mm 18 mm OTHER * Special compact flange (circle hole DIN PN10 DN40) ** Special compact flange (circle hole ANSI 1 ½" 150 lbs) *** Only for stainless steel, other material: F = 12 On request: The valve and flange dimensions can be Adapted to your requirements (if possible join drawing with your enquiry).

10 COMPACT SAMPLING VALVE TYPE 120 B dead volume free / patented APPLICATION Sampling of chemicals (liquid, powders, pasteous) out of reactors, dryers, and pipes, under pressure up to 145 Psi (10 bar) or vacuum, temperature up to 180 C (360 F). - Compact Dimensions - No dead volumes ADVANTAGES

11 TYPE 120 B dead volume free / patented 1. Technical Description Sampling valve type 120 B PN10 DN25 Sampling of chemicals (powders, liquids), out of reactors and pipes under pressure (up to 10 bar) or vacuum. Body: Stainless Steel (316l), Hastelloy C22, Alloy 59, , Titan, etc. Piston: PTFE, reinforced with glassfibers (FDA) O-Rings: Chemraz white (FDA) With : - Bottle 150 ml, glass Pyrex covered in stainless steel - Purging valve 1/4 2. Sampling free of dead volumes Tightness by patented piston In closed position tightness is made directly by the piston on the inside walls of the valve. No O-Rings, packing or seat required, allowing a perfect tightness without dead volumes. Advantages of Sampling System Type 120 B - Compact construction - Simple and safe service

12 TYPE 120 B dead volume free / patented 4. Functioning Fig 1 Normally closed position (fig. 1): - The piston (9) closes the connection of the reactor or pipe without dead volume. The perfect tightness is insured directly by the piston (9) in the valve body. Sampling (fig 2): Fig. 1 Fig. 2 - The Piston (9) is wheeled down to the opened position. The product flows down into the sampling bottle(2). - The Piston is wheeled up, and ensures a perfect tightness when in closed position (Fig.2). - The pressure (or vacuum) is equilibrated by opening the purging valve (25). - The sampling bottle 2 can be removed.

13 TYPE 120 B dead volume free / patented 5. Mounting In standard configuration the valve is delivered as shown below (fig. 3): A B C Qty D E F DIN DN25 PN16 32 mm 115 mm 85 mm 4 14 mm 35 mm 16 mm ANSI 1" 150 lbs 32 mm 108 mm 79.4 mm mm 35 mm 14.3 mm Other On request Onrequest Onrequest On request On request: The valve and flange dimension can be adapted to your requirements (if possible join drawing with enquiry).

14 DEAD VOLUME FREE SAMPLING VALVE FOR HIGH TEMPERATURE TYPE 135 A Patented APPLICATION Sampling of chemicals (liquids, powders, pasteous)out of reactors, dryers, and pipes, under process conditions. Pressure up to 10bar (145psi) or vacuum, temperatures up to 300 C (572 F) ADVANTAGES - Adaptation to customer's requirements. - Full safety for user and environment.

15 1.Technical description TYPE 135 A patented Sampling Valve Type 135 A Sampling of chemicals out of reactors and pipes under pressure conditions (up to 10bars and 300 C) Body: Piston: O-Rings: With : Stainless Steel (316l), Hastelloy, Titanium etc. Stainless Steel (316I), Hastelloy etc. Chemraz white (FDA) - Bottle 150ml, made of stainless steel with sighting glass pyrex and quick-coupling - Purging Valve 1/4" 2. Sampling free of dead volumes Tightness by patented piston The stainless steel piston closes on its metallic seat, and a supplementary tightness is ensured by a high temperature gasket. 3. Advantages of Sampling System Type 135 A Several options and flexibility Valve and flange dimensions can be adapted to your requirements. Materials for body, piston, and O-Rings can be adapted to the product. Options : - Sampling for sterile and toxic mediums - Automatic sampling - Sampling with mechanical or pneumatic safety device - Special Sampling bottles and accessories Short deliveries. All spare parts on stock.

16 4. Functioning TYPE 135 A patented Fig. 1 Fig. 2 Normally closed position : - The piston (9) closes the connection of the reactor or pipe without dead volume (Fig.1). The perfect tightness is ensured by a contact metal-on-metal on the seat, and in supplement by a high timperature gasket (91). Sampling : - The piston (9) is wheeled down to the opened position. The product flows down into the sampling bottle (Fig.2). - The operator checks the desired quantity of product through the sight glass (3). - The piston (9) is wheeled up, and ensures a perfect tightness when in closed position. - The pressure (or vacuum) in chamber (V) is equilibrated by opening valve (25). - The sampling bottle (2) can now be removed by the quick-coupling connection (5).

17 TYPE 135 A patented 5. Mounting In standard configuration the valve is delivered as shown below (Fig. 4) A B C Nb D E F*** FAMAT (DIN)* 61 mm 125 mm 100 mm 4 13 mm 35 mm 18 mm DIN PN10 DN50 61 mm 165 mm 125 mm 4 18 mm 35 mm 21 mm FAMAT (ANSI)** 61 mm 125 mm 98.4 mm mm 35 mm 18 mm ANSI 2" 150 lbs 61.9 mm mm mm 4 19 mm 35 mm 18 mm OTHER * Special compact flange (circle hole DIN PN10 DN40) ** Special compact flange (circle hole ANSI 1 ½" 150 lbs) *** Only for stainless steel, other material: F = 12 On request : The valve and flange dimension can be adapted to your requirements (if possible join drawing with your enquiry).

18 CONTAMINATION-FREE SAMPLING VALVE TYPE 125 ST without dead volume / patented APPLICATION Sampling of chemicals (liquids, powders, pasteous) out of reactors, dryers and pipes, under process conditions. Pressure up to 145 psi (10 bars) or vacuum, max. temperature 180 C (360 F) ADVANTAGES - No dead volumes - Safety device to prevent any contact between process and atmosphere - No contamination of product and environnement - Compact dimensions

19 TYPE 125 ST without dead volume / patented 1. Features - No dead volumes - Safety device to prevent any contact between process and atmosphere - Sampling bottle with sighting glass and quick coupling 2. Specification Body: Piston: Gaskets: With : Stainless steel (316l), Hastelloy,Titanium PTFE reinforced with glassfiber (FDA) Chemraz white (FDA) - Sampling bottle, 150 ml made of stainless steel with sighting glass pyrex. - Butterfly valve in stainless steel 316, with gasket Viton, EPDM, HNBR, Silicone (FDA) - Purging valves 1/4'' in st. steel Security The mechanical locking device secures the sampling procedure. - The valve can only be opened if the sampling bottle is coupled on the valve and the purging valve closed. - The sampling bottle can only be removed if the valve is completely closed and the purging valve opened.

20 TYPE 125 ST without dead volume / patented OPERATION Normally closed position: The piston (9) closes the connection of the reactor without dead volume and a perfect tightness is insured directly by the piston. The venting valve (25) is closed. The sampling bottle (3) is connected. The butterfly valve (31) is closed. Purging valves (26, 27, 28, 29, 30) are closed. Sampling: The sampling is only possible with closed venting valve (25) and sampling bottle connected. The butterfly valve (31) is opened. The piston (9) is wheeled down to the open position. The product flows down into the sampling bottle (3). The operator checks the desired quantity of product through the sight glass. The piston is wheeled up, and ensures a perfect tightness when in closed position. Only when the piston is fully closed the venting valve (25) can be opened. Close the butterfly valve (31). Rince the volume between piston and butterfly valve through the venting valve (25) and the purging valve (26). The sampling bottle, with butterfly valve (31) closed, can now be removed through its quick-coupling (5). Cleaning : Connect sampling bottle,open butterfly valve (31) clean the volume between the piston and the sampling bottle using the venting valves (25) and (27). The volume under the piston is cleaned using the purging valves (29) and (30).

21 TYPE 125 ST without dead volume / patented Mounting Standard: If not specified otherwise, the sampling valve Type 125 ST is supplied according. (Fig.4) Fig. 4 A B C Nb D E F*** FAMAT (DIN)* 61 mm 125 mm 100 mm 4 13 mm 35 mm 18 mm DIN PN10 DN50 61 mm 165 mm 125 mm 4 18 mm 35 mm 21 mm FAMAT (ANSI)** 61 mm 125 mm 98.4 mm mm 35 mm 18 mm ANSI 2" 150 lbs 61.9 mm mm mm 4 19 mm 35 mm 18 mm OTHER * Special compact flange (circle hole DIN PN10 DN40) ** Special compact flange (circle hole ANSI 1 ½" 150 lbs) *** Only for stainless steel, other material: F = 12 The flange and valve dimensions can be adapted to any counter-flange (if possible join drawing with your enquiry). 6. Options - Special sampling bottles - Limit Switches

22 DEAD VOLUME FREE SAMPLING VALVE TYPE 125 TC EASY CLEAN APPLICATION Sampling of chemicals (liquids, powders, pasteous) out of reactors, dryers, and pipes, under process conditions. Pressure up to 145psi (10bar) or vacuum, temperature up to 150 C (302 F) ADVANTAGES - Quick dismantling (without tools) for cleaning - Compact dimensions - Full safety for user and environment. - No dead volumes

23 TYPE 125 TC patented 1.Technical description Sampling Valve Type 125 TC Sampling of chemicals out of reactors and pipes under vacuum or pressure (up to 10 bar and 150 C) Body: Piston: O-Rings: With : Stainless Steel (316l), Hastelloy, Titanium,etc. PTFE, reinforced with glassfibers (FDA) Chemraz white, PTFE/EPDM (FDA) - Bottle 150ml, glass pyrex covered in stainless steel and Tri clamp coupling - Purging valve 1/4'' 2. Sampling free of dead volumes Tightness by patented piston In closed position tightness is made directly by the piston on the inside walls of the valve, without O-Rings, packing or seats allowing a perfect tightness without dead volumes. Several options and flexibility Valve and Tri clamp dimensions can be adapted to your requirements. Materials for body, piston, and O-Rings can be adapted to the product. Options : - Automatic sampling - Sampling with mechanical or pneumatic safety device - Special sampling bottles and accessories - Crust breaking piston Short deliveries. All spare parts on stock,

24 4. Functioning TYPE 125 TC patented Fig. 1 Fig. 2 Normally closed position : - The piston (9) closes the connection of the reactor or pipe without dead volume (Fig. 1). The perfect tightness is ensured by the piston (9). Sampling : - The piston (9) is wheeled down to the opened position. The product flows down into the sampling bottle (2) (Fig. 2). - The operator checks the desired quantity of product through the sight glass. - The piston (9) is wheeled up, and when in closed position ensures a perfect tightness (Fig. 1). - The pressure (or vacuum) in chamber (V) is equilibrated by opening valve (25). - The sampling bottle (2) can now be removed by the Tri clamp connection (5).

25 5. Mounting TYPE 125 TC patented In standard configuration the valve is delivered as shown below (Fig.3) TRI-CLAMP A E STANDARD DIMENSIONS 61 mm 48 mm On request: The dimensions A and E can be adapted to your requirements (if possible join drawing with your enquiry).

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