B/R Vacuum Distillation ASTM D1160. Fully Automatic Vacuum Distillation According to D1160

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Kerry Fitzgerald
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1 B/R Vacuum Distillation ASTM D1160 Fully Automatic Vacuum Distillation According to D1160

B/R Fully Automatic ASTM D1160 Vacuum Distillation Turn Key System: This system includes everything needed to automatically perform a vacuum distillation according ASTM D1160.

All you need is space for the unit and a standard electrical outlet and you are ready to run a sample. Fully Automatic: This system performs the D1160 test automatically.

2 B/R Fully Automatic ASTM D1160 Vacuum Distillation Turn Key System: This system includes everything needed to automatically perform a vacuum distillation according ASTM D1160. All glassware, a complete vacuum system, circulating bath, PC and other items needed to perform the test are mounted in an ergonomic safety cabinet. All you need is space for the unit and a standard electrical outlet and you are ready to run a sample. Fully Automatic: This system performs the D1160 test automatically. Just put sample in the boiling flask and start the test. Everything else is done automatically including: n Vacuum control n Distillation rate control n Condenser and receiver temperature control n Recording of distillation data, first drop (IBP) and final boiling point (FBP) n Detection of cracking and boiling flask over-temperature n Ending of distillation, cool down and generation of the final report Easy to Use: PC control automates the D1160 test from beginning to end. New and experienced operators will find this system simple to use. The software steps you through the testing process from start up to printing of results. Easy to understand software and easy access to all the distillation components makes performing the test as simple as possible.

Fully Automatic D1160 Features Features Specifications Operation Results Boiling Flask/Heating Mantle Distillation Column First Drop Detector Receiver/Volume Measurement Circulating Bath Vacuum

3 Fully Automatic D1160 Features Features Specifications Operation Results Boiling Flask/Heating Mantle Distillation Column First Drop Detector Receiver/Volume Measurement Circulating Bath Vacuum Operation Vacuum Components Cold Trap Optional Foam Sensor PC/Monitor Automatic Control of Distillation including: Distillation rate Vacuum level Degassing Receiver/condenser temperatures Printing of results Automatic Detection and Recording of: First drop detection (IBP) Distillation rate Vapor and liquid temperatures, vacuum level Receiver volume Final boiling point (FBP) Calculation of vapor AET Sample cracking 500 ml Borosilicate or quartz High wattage heating mantle Insulating top Automatic cool down fan According ASTM specifications Vertical viewing window for easy viewing Highly reflective vacuum jacket Adjustable vapor temperature probe Automatically detects and records the first drop (IBP) Precision diameter (±0.01 mm) Automatic precision volume measurement (±0.1 ml) Programmable chamber temperature IR level follower eye Automatic control Programmable C Standard Optional -10 to 100 C Low liquid cut off Over temperature cut off Automatic control Programmable Automatic degassing mmhg range standard (MKS) Optional mmhg range (MKS) Optional mmhg range (MKS) Automatic control valve (MKS) Vacuum pump (Edwards) Cooling by dry ice Optional automatic cooler Graduated Easy access Easy to see contents Easy to remove contents Automatically detects foam formation Included with distillation unit Keyboard and monitor integrated into distillation system Dimensions 91.5 cm x 94 cm x 53 cm (H x W x D) Power (Distillation Unit Only) 10 amps 220 VAC

Condenser and Side Arm Condenses vapor Prevents crystallization and wax formation Circulating bath controlled by distillation program Vacuum System Vacuum system lowers the boiling point of high

4 Condenser and Side Arm Condenses vapor Prevents crystallization and wax formation Circulating bath controlled by distillation program Vacuum System Vacuum system lowers the boiling point of high temperature samples Automatically regulates to programmable vacuum level Cold trap in front of unit for easy viewing and access Distillation Column According to ASTM specifications Vertical window for easy viewing Vapor temperature probe with adjustable position Receiver/Chamber Automatic volume measurement (±0.1 ml) Programmable Chamber Temperature IR Level Follower Eye Boiling Flask/Heating Mantle Borosilicate or quartz High temperature heating mantle Automatic control of distillation rate Automatic Control Automatic control of distillation process Automatic report of distillation data PC, monitor, mouse and keyboard included Thermowell

Software automatically controls: Distillation rate Vacuum level Degassing Chamber/condenser temperatures End of distillation Cool down B/R Automatic D1160 Software Vacuum System You don t need to be

0 mmhg 60ºC Vacuum system lowers the boiling point of high temperature Software samples Automatically automatically regulates programmable records: vacuum level Cold trap in front of unit for easy

5 Software automatically controls: Distillation rate Vacuum level Degassing Chamber/condenser temperatures End of distillation Cool down B/R Automatic D1160 Software Vacuum System You don t need to be an expert to use the automatic D1160 software. The software is easy to use for new or experienced operators ºC 257.2ºC 60% 6.8 ml/min 5.0 mmhg 60ºC Vacuum system lowers the boiling point of high temperature Software samples Automatically automatically regulates programmable records: vacuum level Cold trap in front of unit for easy viewing First and access drop (IBP) Vapor and liquid temperatures AET vapor temperature Vacuum level Receiver volume Distillation Rate Chamber/condenser temperatures Final boiling point (FBP) Sample cracking Receiver/Chamber Distillation results are provided in both graph and table format. They can be printed or they can be exported to common electronic formats such as pdf for easy sharing. Or connect the PC to your network and access the flat files directly. Distillation Results Automatic volume measurement (+0.1 ml) Programmable Chamber Temperature IR Level Follower Eye Automatic Control Automatic control of distillation process Automatic report of distillation data PC, monitor, mouse and keyboard included

Other Petroleum Testing Products by B/R Instrument Other D1160 Products Model Typical Customer Applications Semi auto D1160 For laboratories with Testing of: smaller sample loads or Gas oil smaller

6 Other Petroleum Testing Products by B/R Instrument Other D1160 Products Model Typical Customer Applications Semi auto D1160 For laboratories with Testing of: smaller sample loads or Gas oil smaller budgets Fuel oil Diesel Biodiesel Residues Manually Operated For laboratories with Other petroleum D1160 limited samples loads or products requiring very limited budgets vacuum distillation ASTM Crude Oil Distillation Model Typical Customer Applications Fully Automatic For laboratories requiring Crude Oil and D2892 and D5236 highly automatic crude condensates for oil distillation. quality control or research and Semi-Automatic For laboratories with development D2892 and D5236 fewer samples or smaller budgets Manually Operated For laboratories with D2892 and D5236 limited sample loads or very limited budgets Other Crude Oil and Petroleum Fractional Distillation Model Typical Customer Applications Mini Crude Oil For laboratories with Fractional Distillation of: Distillation samples sizes in the 50 Crude oil to 1000ml range. Petroleum fractions Biodiesel Coal tar oil Micro Crude Oil For customers with Other petroleum Distillation samples in the products requiring 3-80 ml range fractional distillation

B/R Instrument Corporation B/R Instrument was founded in 1966 by Roger Roark, Sr. and Harry Brown, Jr. The name B/R comes from the first letter of each founder s last name, Brown and Roark BR.

7 B/R Instrument Corporation B/R Instrument was founded in 1966 by Roger Roark, Sr. and Harry Brown, Jr. The name B/R comes from the first letter of each founder s last name, Brown and Roark BR. Originally a manufacturer of general glassware, the company began to specialize in the manufacture of spinning band distillation systems in 1968 under a DuPont patent. Since then the company has grown steadily in the distillation and laboratory equipment markets and now distributes products to customers throughout the world. Located in Easton, Maryland on the beautiful Eastern Shore of the Chesapeake Bay, the B/R facility encompasses 14,700 square feet (1,370 square meters) and houses manufacturing, sales, engineering, service and administrative divisions. B/R INSTRUMENT B/R Instrument Corporation Easton, Maryland USA better.results@brinstrument.com www. brinstrument.com B/R Instrument Corporation

ADU 5. Automatic Distillation Unit

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