Accurate to 0.1 NIST Traceable Advanced PID Algorighm USB Port Free datalogging/control software. Controllers I N S C O N TA G N

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1 Accurate to 0.1 NIST Traceable Advanced PID Algorighm USB Port Free datalogging/control software Controllers P 2010 C O N TA R I C I I N S G N Serving the laboratory glassware industry for over 70 years

Economy Controllers State-of-the-Art and Vacuum Controllers Ace Glass now offers the most advanced laboratory temperature controllers for virtually every application in your lab.

Units are available in four different thermocouple types and temperature ranges.

2 Economy Controllers State-of-the-Art and Vacuum Controllers Ace Glass now offers the most advanced laboratory temperature controllers for virtually every application in your lab. From a simple temperature monitor to a full research-grade Quad unit with four full independent channels, ACE can provide the answer and the best value for your application. Units are available in four different thermocouple types and temperature ranges. Controllers may be purchased with or without thermocouples, and the probe receptacles on each unit are color coded to match the thermocouple types they accept: blue = T ; yellow = K ; Black = J ; and white = RTD. All controllers have free control software that provides 0.1º C regulation of any lab device or piece of equipment. Included in this brochure is a portion of our wide offering of thermocouple probes, and our latest models for vacuum and pressure control, which feature free control software that can also provide data-logging capabilities Ultra Compact Economy Controller with J thermocouple input; output power 120 volt/60 Hz, 15 amp maximum. Bench or bar mountable. 120 volt/60 Hz input. Single-loop time proportional output: 10 seconds cycle rate. Solid state relay control contact. Range is 0 to +800 C, 0.1 C resolution. Accuracy over range: 0.25% (max 2 C). Set-point control accuracy: ± 0.1 C. Microprocessor-based 1/32 DIN module, dual process and set-point value display. Auto tuned PID with fuzzy logic. Programmable: ramp and soak (16 segment). Size: 2"x 5¼"x 5¼" (HxWxD); 120vac, 15 amps, Weight: 2 lbs, 2 oz. With Sensor Cord No 0 to 800 J Model 150, J-Kem An ideal controller for applications that don t require the precise regulation of 200 Series controllers. This compact unit features 1200 watts of power, sufficient for heating 5 L mantles, many ovens, and other devices. Ramp-to-Set Point feature standard. USB port and data logging and control software optional. 2.5" x 3.75" x 5.25" (HxWxD) / 120vac, 10 amps, 1200 watts With Sensor Cord 150-T No 200 to 250 T J No 0 to 800 J K No 50 to 1200 K T-S Yes 200 to 250 T J-S Yes 0 to 800 J K-S Yes 50 to 1200 K Model 150/Timer, J-Kem Same power and versatility as the Model 150, but with a 100-hour digital timer to turn heating ON or OFF at a user-specified time. 2.5" x 4.75" x 5.5" (HxWxD) / 120vac, 10 amps, 1200 watts With Sensor Cord 150/Timer-T No 200 to 250 T /Timer-J No 0 to 800 J /Timer-K No 50 to 1200 K /Timer-T-S Yes 200 to 250 T /Timer-J-S Yes 0 to 800 J /Timer-K-S Yes 50 to 1200 K

Single-Channel Controllers 12325 Model 210, J-Kem The Model 210 is our most compact research grade controller, yet packed with 1200 watts of power.

Power control computer provides 0.1 C regulation of anything. A 230VAC, CE-approved model is also available via special order. 3.25" x 5.25" x 7.

80 210-Pt No 200 to 400 RTD 12325-08 782.00 210-T-S Yes 200 to 250 T 12325-22 851.00 210-J-S Yes 0 to 800 J 12325-24 851.00 210-K-S Yes 50 to 1200 K 12325-26 851.

3 Single-Channel Controllers Model 210, J-Kem The Model 210 is our most compact research grade controller, yet packed with 1200 watts of power. Sufficient for heating mantles up to 5 L in size, and most laboratory ovens, hot plates, reaction blocks and other heaters. Comes complete with USB port and data logging and control software. Power control computer provides 0.1 C regulation of anything. A 230VAC, CE-approved model is also available via special order. 3.25" x 5.25" x 7.25" (HxWxD) / 120vac, 10 amps, 1200 watts J-Kem Model 210-T No 200 to 250 T J No 0 to 800 J K No 50 to 1200 K Pt No 200 to 400 RTD T-S Yes 200 to 250 T J-S Yes 0 to 800 J K-S Yes 50 to 1200 K Pt-S Yes 200 to 400 RTD Model 210/Timer, J-Kem Same power and versatility as the Model 210, above, but also contains a 100-hour digital timer to turn heating OFF or ON at a user-specified time. A new safety feature automatically disconnects power from the heater following recovery from a power failure. Comes complete with USB port and data logging and control software. Power control computer provides 0.1 C regulation of anything. A 230VAC, CE-approved model is also available via special order. 3.5" x 6.75" x 6" (HxWxD) / 120vac, 10 amps, 1200 watts 210/Timer-T No 200 to 250 T /Timer-J No 0 to 800 J /Timer-K No 50 to 1200 K /Timer-Pt No 200 to 400 RTD /Timer-T-S Yes 200 to 250 T /Timer-J-S Yes 0 to 800 J /Timer-K-S Yes 50 to 1200 K /Timer-Pt-S Yes 200 to 400 RTD , Model 250, J-Kem The Model 250 has both heating and cooling outlets for maximum versatility. Two heating outlets supply 1800 watts of power for large equipment and heating mantles up to 22 L. The third outlet, also 1800 watts and normally used for cooling, is programmable to provide power above, below, or at the set point. Comes complete with USB port and data logging and control software. Power control computer provides 0.1 C regulation of anything. 3.5" x 7.75" x 9.25" (HxWxD) / 120vac, 15 amps, 1800 watts J-Kem Model With Sensor Cord 250-T No 200 to 250 T J No 0 to 800 J K No 50 to 1200 K Pt No 200 to 400 RTD T-S Yes 200 to 250 T J-S Yes 0 to 800 J K-S Yes 50 to 1200 K Pt-S Yes 200 to 400 RTD ,

12318 Model 260/Timer, J-Kem The Model 260/Timer disconnects output power if the process temp exceeds the setpoint by a user specified amount or following a recovery from a power failure.

NIST traceable, USB port and free data logging and control software. 3.5" x 7.75" x 9.25" (HxWxD) / 120vac, 15 amps, 1800 watts With Sensor Cord 260/Timer-J No 0 to 800 J 12318-01 1,081.

80 260/Timer-K-S Yes 50 to 1200 K 12318-23 1,163.80 260/Timer-T-S Yes 200 to 250 T 12318-25 1,163.80 260/Timer-Pt-S Yes 200 to 400 RTD 12318-27 1,228.

4 12318 Model 260/Timer, J-Kem The Model 260/Timer disconnects output power if the process temp exceeds the setpoint by a user specified amount or following a recovery from a power failure. Overtemp is signaled by both a lamp an an audible alarm. Features a 100 hour timer, 2 power outlets and 0.1 deg C regulation of anything. NIST traceable, USB port and free data logging and control software. 3.5" x 7.75" x 9.25" (HxWxD) / 120vac, 15 amps, 1800 watts With Sensor Cord 260/Timer-J No 0 to 800 J , /Timer-K No 50 to 1200 K , /Timer-T No 200 to 250 T , /Timer-Pt No 200 to 400 RTD , /Timer-J-S Yes 0 to 800 J , /Timer-K-S Yes 50 to 1200 K , /Timer-T-S Yes 200 to 250 T , /Timer-Pt-S Yes 200 to 400 RTD , High Safety Controller Monitor Model 270, J-Kem Designed for processes requiring uncompromising safety. The only temperature controller available with a built-in, independent backup controller to guard against heating accidents resulting from equipment failure. The desired temperature is entered into the main temperature controller, which regulates heating, and then a hightemperature cut-off is entered into the backup limit controller. If the reaction reaches the high-temperature limit, or if a thermocouple should break, power is turned off to the heater until the controller is manually reset. Both meters independently monitor the reaction temperature. In the event that one meter fails, the other takes over to prevent a heating accident. Provides 100% redundant control. 3.75" x 7.75" x 9.25" (HxWxD) / 120vac, 15 amps, 1800 watts total 1200 watts maximum per channel 270-T No 200 to 250 T , J No 0 to 800 J , K No 50 to 1200 K , T-S Two of each 200 to 250 T , J-S Two of each 0 to 800 J , K-S Two of each 50 to 1200 K , The Model 270 Series units noted above each come with two thermocouple sensors, two cords and two adapters Digital Monitor Monitors and displays the temperature of an attached piece of equipment on a bright LED display. Built-in USB port and free data logging software allows remote temperature monitoring, and provides a GMP, GLP compliant temperature history. Audible digital alarm available as an option. A 230VAC, CE-approved model is also available via special order. 2.5" x 4.75" x 5.5" (HxWxD) / 120vac, 50 watts, USB 2.0 DM120-T 200 to 250 T DM120-J 0 to 800 J DM120-K 50 to 1200 K

Multi-Channel Controllers 12310 Gemini Series, J-Kem The Gemini Series features two temperature controllers in a single cabinet to regulate two independent reactions.

Features include: over-temperature protection circuit with audible alarms; dual temperature displays; selectable operating modes; twin circuit breakers; and 100% solid-state design. 3.75" x 7.75" x 9.

80 Gemini-K No 50 to 1200 K 12310-08 1,265.00 Gemini-Pt No 200 to 400 RTD 12310-10 1,265.00 Gemini-T-S Two of each 200 to 250 T 12310-25 1,416.80 Gemini-J-S Two of each 0 to 800 J 12310-27 1,416.

5 Multi-Channel Controllers Gemini Series, J-Kem The Gemini Series features two temperature controllers in a single cabinet to regulate two independent reactions. This versatile controller has high-power outlets and a 100-hour digital timer (on Channel One) to turn heating on or off at a user-entered time. Features include: over-temperature protection circuit with audible alarms; dual temperature displays; selectable operating modes; twin circuit breakers; and 100% solid-state design. 3.75" x 7.75" x 9.25" (HxWxD) / 120vac, 15 amps, 1800 watts total 1200 watts maximum per channel Gemini-T No 200 to 250 T , Gemini-J No 0 to 800 J , Gemini-K No 50 to 1200 K , Gemini-Pt No 200 to 400 RTD , Gemini-T-S Two of each 200 to 250 T , Gemini-J-S Two of each 0 to 800 J , Gemini-K-S Two of each 50 to 1200 K , Gemini-Pt-S Two of each 200 to 400 RTD , Apollo Series, J-Kem Has all the features of the Gemini series, above, but also has an independent 100- hour digital timer on each controller channel. 4" x 8" x 9" (HxWxD) / 120vac, 15 amps, 1800 watts total 1200 watts maximum per channel Apollo-T No 200 to 250 T , Apollo-J No 0 to 800 J , Apollo-K No 50 to 1200 K , Apollo-Pt No 200 to 400 RTD , Apollo-T-S Two of each 200 to 250 T , Apollo-J-S Two of each 0 to 800 J , Apollo-K-S Two of each 50 to 1200 K , Apollo-Pt-S Two of each 200 to 400 RTD , The Apollo and Gemini Series units noted above each come with two thermocouple sensors, two cords and two adapters Quad Series, J-Kem The Quad is your solution when bench space is at a premium the Quad packs four independent temperature controllers into a single unit! Each of the four controller channels has 1200 watts of power, an independent display, and an over-temperature protection circuit. 5.25" x 7" x 7.5" (HxWxD) / 120vac, 15 amps, 1800 watts total 1200 watts maximum per channel Quad-T No 200 to 250 T , Quad-J No 0 to 800 J , Quad-K No 50 to 1200 K , Quad-Pt No 200 to 400 RTD , Quad-T-S Four of each 200 to 250 T , Quad-J-S Four of each 0 to 800 J , Quad-K-S Four of each 50 to 1200 K , Quad-Pt-S Four of each 200 to 400 RTD , The Quad Series units noted above each come with four thermocouple sensors, four cords and four adapters. 5

High Power Controller Instatherm Controller Sample Instatherm Configuration 12317 Model HCC, J-Kem The HCC line of controllers are designed to power large-scale equipment with volumes up to 100

Built with the same commitment to safety as our 12316 controller, the HCC Series features a built-in, independent backup controller to guard against heating accidents resulting from equipment failure.

If the reaction reaches the high-temperature limit, or if a thermocouple should break, power is turned off to the heater until the controller is manually reset.

6 High Power Controller Instatherm Controller Sample Instatherm Configuration Model HCC, J-Kem The HCC line of controllers are designed to power large-scale equipment with volumes up to 100 liters. Built with the same commitment to safety as our controller, the HCC Series features a built-in, independent backup controller to guard against heating accidents resulting from equipment failure. The desired temperature is entered into the main temperature controller, which regulates heating, and then a high-temperature cut-off is entered into the backup limit controller. If the reaction reaches the high-temperature limit, or if a thermocouple should break, power is turned off to the heater until the controller is manually reset. Both meters independently monitor the reaction temperature. In the event that one meter fails, the other takes over to prevent a heating accident. Provides 100% redundant control. These highpower controllers also incorporate a 100-hour timer to turn heating ON or OFF at a user-specified time. Comes complete with USB port and data logging and control software. Power control computer provides 0.1 C regulation of anything. Requires sensor (not included) for operation. 5.5" x 12" x 12.5" (HxWxD) / vac, 30 amps, 3600 watts HCC-130-T No 200 to 250 T , HCC-130-J No 0 to 800 J , HCC-130-K No 50 to 1200 K , Model 410, J-Kem The Model 410 is designed for heaters that cannot be operated at 120VAC. This makes the unit perfect for use with many of our Ace Instatherm oil baths. Maximum output voltage of the Model 410 is selected using the power output knob on the front of the controller. Selectable output voltage limit provides precise power and temperature control while protecting low voltage heaters. Comes complete with USB port and data logging and control software. Power control computer provides 0.1 C regulation of anything. 3.25" x 5.25" x 7.25" (HxWxD) / 10, 20, 40, 60, 120 vac, 10 amps, 1200 watts 410-T No 200 to 250 T J No 0 to 800 J K No 50 to 1200 K Pt No 200 to 400 RTD T-S Yes 200 to 250 T J-S Yes 0 to 800 J K-S Yes 50 to 1200 K Pt-S Yes 200 to 400 RTD

7 / Sensors For J-Kem Controllers T- Sensors T thermocouple temperature sensors for use with all J-Kem T model temperature controllers. Either 1/4- or 1/8-inch O.D. Available in 304 stainless steel or PTFE coated stainless steel sheaths of various lengths. O.D. PTFE Coated? 1/8 6 No /8 12 No /8 18 No /8 24 No /8 36 No /8 6 Yes /8 12 Yes /8 18 Yes /8 24 Yes /8 36 Yes /4 6 No /4 12 No /4 18 No /4 24 No /4 36 No /4 6 Yes /4 12 Yes /4 18 Yes /4 24 Yes /4 36 Yes J- Sensors J thermocouple temperature sensors for use with all J-Kem J model temperature controllers. Either 1/4- or 1/8-inch O.D. Available in 304 stainless steel or PTFE coated stainless steel sheaths of various lengths. O.D. PTFE Coated? 1/8 6 No /8 12 No /8 18 No /8 24 No /8 6 Yes /8 12 Yes /8 18 Yes /8 24 Yes /8 36 Yes /4 6 No /4 12 No /4 18 No /4 24 No /4 36 No /4 6 Yes /4 12 Yes /4 18 Yes /4 24 Yes /4 36 Yes K- Sensors K thermocouple temperature sensors for use with all J-Kem K model temperature controllers. Either 1/4- or 1/8-inch O.D. Available in 304 stainless steel or PTFE coated stainless steel sheaths of various lengths. O.D. PTFE Coated? 1/8 6 No /8 12 No /8 18 No /8 24 No /8 36 No /8 6 Yes /8 12 Yes /8 18 Yes /8 24 Yes /8 36 Yes /4 6 No /4 12 No /4 18 No /4 24 No /4 36 No /4 6 Yes /4 12 Yes /4 18 Yes /4 24 Yes /4 36 Yes RTD Sensors RTD (Pt/100) type thermocouple temperature sensors for use with J-Kem model RTD temperature controllers. Either 1/4- or 1/8-inch O.D. All PTFE coated stainless steel sheaths of various lengths. Uncoated available via special order. O.D. PTFE Coated? 1/8 6 Yes /8 12 Yes /8 18 Yes /8 24 Yes /8 36 Yes /4 6 Yes /4 12 Yes /4 18 Yes /4 24 Yes /4 36 Yes For extension cords, see Ace straight and coiled cords, on the following page. 7

Sensor extension cords for use with all J-Kem thermocouple probes. Cords match color of probe type, blue, black, yellow or white. Available in either 10- or 20-foot coiled or straight styles.

00 T 10 SMP 12190-03 29.00 RTD 10 SMP 12190-04 48.00 J 10 OST 12190-08 29.00 K 10 OST 12190-10 29.00 T 10 OST 12190-11 29.00 RTD 10 OST 12190-12 48.00 J 20 SMP 12190-20 47.00 K 20 SMP 12190-21 47.

8 Sensor extension cords for use with all J-Kem thermocouple probes. Cords match color of probe type, blue, black, yellow or white. Available in either 10- or 20-foot coiled or straight styles. Select length, type, and connector, SMP (flat plug) or OST (round plug). OST (Standard) SMP (Mini) Sensor Cords Coiled Probe Connector Style (ft.) J 10 SMP K 10 SMP T 10 SMP RTD 10 SMP J 10 OST K 10 OST T 10 OST RTD 10 OST J 20 SMP K 20 SMP T 20 SMP RTD 20 SMP J 20 OST K 20 OST T 20 OST RTD 20 OST Dual Sensor Cords Coiled Dual element extension cords for use with dual element sensors for J-Kem models HCC and 270 temperature controllers. Available in T, K, and J types in 10- or 25-ft. lengths. Probe Style (ft.) T J K T J K Sensor Cords Straight Probe Connector Style (ft.) J 10 SMP K 10 SMP T 10 SMP RTD 10 SMP J 10 OST K 10 OST T 10 OST RTD 10 OST J 20 SMP K 20 SMP T 20 SMP RTD 20 SMP J 20 OST K 20 OST T 20 OST RTD 20 OST Dual Sensors PTFE Coated Dual coupling temperature thermocouple sensors for use with Model HCC and 270 J-Kem temperature controllers. Available in J, T or J types. Probes are PTFE coated stainless steel in various lengths and O.D. Probes require extension cords. O.D. Sensor 1/8 12 T /4 12 T /4 24 T /4 36 T /8 12 J /4 12 J /4 24 J /4 36 J /8 12 K /4 12 K /4 24 K /4 36 K

Available in standard connections, and in 36- and 72-inch lengths. PTFE Coated? Sensor Yes 36 T 12185-01 94.20 Yes 36 K 12185-03 94.20 No 72 T 12185-04 32.00 No 72 K 12185-06 32.

9 12185 Wire Sensors Flexible 30-gauge thin wire thermocouple. Ideal for small volumes and hard-to-reach spots. Can be used with heating mantles, hotplates, inside of heating equipment and for small surface measurement. Can be inserted through rubber septum for an airtight seal. Available in standard connections, and in 36- and 72-inch lengths. PTFE Coated? Sensor Yes 36 T Yes 36 K No 72 T No 72 K No 72 J About J-KEM Needle-Tip Sensors Needle-tip, 17-gauge thermocouple sensor for measurement and control of very small volumes and in small systems. Sensors come coated and uncoated in 3.5- or 7-in. lengths. Actual temperature measure is at first 2mm of the probe and must have liquid contact for accurate readings. May be inserted through rubber septa 9107 or 9106 for airtight seal. Comes with 72-in. PTFE wire extension. Available in T, K, or J type connections. Sensor 3.5 T T K K J J T T K K T T Scientific Since its origin in 1987, J-KEM Scientific, Inc. has established itself as the leader in temperature and vacuum control equipment. The key to J-KEM s success is understanding the requirements of researchers and manufacturing products that surpass their needs. J-KEM s founder, Dr. Robert Elliott, worked for 14 years at a Fortune 500 research corporation as a group leader in the areas of process development, discovery synthesis and the automation of a combinatorial synthesis program. J-KEM is committed to responding to customers research needs, to excellent customer service, and to producing the best products in the market. 9

Vacuum Regulators 14063 Precision Vacuum Regulator, J-Kem Perfect for vacuum distillation, unit automatically compensates for leaks in the equipment under test and maintains precise pressure, even in

1 to 760 Torr (atm pressure) in test instruments with volumes as small as 1 ml. Standard features include 16-step programmable pressure ramp and serial communications for PC control and data logging.

1% Proof Pressure: 200% Controller Regulation: Resolution: Vapor Path Materials: Ramp Rates: Serial Communications: 0.015% of range 0.1 Torr of 0.01 psi Stainless steel and PTFE 100 Torr/sec to 0.

10 Vacuum Regulators Precision Vacuum Regulator, J-Kem Perfect for vacuum distillation, unit automatically compensates for leaks in the equipment under test and maintains precise pressure, even in systems with a continuous gas purge. This computer (built-in) controlled vacuum regulator maintains pressure in the range of 0.1 to 760 Torr (atm pressure) in test instruments with volumes as small as 1 ml. Standard features include 16-step programmable pressure ramp and serial communications for PC control and data logging. DVR , Specifications: Transducer Diaphragm: Stainless Steel Accuracy: 0.1% Proof Pressure: 200% Controller Regulation: Resolution: Vapor Path Materials: Ramp Rates: Serial Communications: 0.015% of range 0.1 Torr of 0.01 psi Stainless steel and PTFE 100 Torr/sec to 0.1 Torr/hr. RS232 (RS485 or USB on request) Stainless Steel Proportioning Valves Select one for use with Digital Vacuum Regulator , above. For Reactor Volumes Cv Orifice Size PSV-2 1 ml to 2 L in PSV-3 25 ml to 4 L in PSV ml to 22 L in PSV-5 1 L to 50 L in PSV-6 Large Capacity in , PSV-7 Large Capacity in , PSV-8 Large Capacity in , PSV-9 Large Capacity in , DVR-PNV Stainless Steel Needle Valve, improves regulation

Ideally suited for large volume distillations, rotary evporators and vacuum chambers. Not recommended for small volume distillations or applications which involve a continuous purge with gas.

11 Connect to any vacuum pump or vacuum source, and then to any piece of equipment, to regulate pressure, in most cases to ±1 Torr. A standard pressure ramp feature evacuates equipment at a user-defined rate to eliminate bumping due to solvent degassing or over-evacuation. Ideally suited for large volume distillations, rotary evporators and vacuum chambers. Not recommended for small volume distillations or applications which involve a continuous purge with gas Vacuum Regulator No Mercury Designed for vacuum systems that run continuously, such as oil-filled vacuum pumps, aspirators, or with systems that are always on, like in-house vacuum systems. The unit regulates pressure by opening and closing a valve that separates the vacuum source from the system being evacuated. DVR , Vacuum Regulator No Mercury Designed for use with diaphragm vacuum pumps. In some systems, pressure is regulated by turning the vacuum pump itself on and off. This unit extends the life of diaphragm pumps by never forcing the pump to start against an established vacuum, which can increase pump life by 100%. DVR , Digital Vacuum Monitor Continuous, no regulation, 120V. Not pictured. DVM Ace Digital Pressure/Strain Gauge Gauge has a bright-red LED readout. Due to its compact size, it can easily be used on a bench or rack. The unit comes complete with an all stainless steel pressure sensor head. The head has a 3/8-inch NPT male thread fitting and a 10-foot cord. Pressure range: 9.9 to PSIG; ±0.5% accuracy full scale; Over pressure range to 215 PSIA; Electrical is switchable from 90 to 240V, 50/60Hz. Code Each Recovers >99% of solvent from rotary evaporators Solvent DVR Pressure (mm Hg) Solvent Volume Time To Dryness Percent Recovery Ether 475 Torr 340 ml 14.6 min. 99.6% CH 2 CI Torr 360 ml 21.9 min. 99.8% CH 2 CI Torr 255 ml 5.9 min. 99.5% EtOAc 90 Torr 316 ml 17.0 min. 99.9% Toluene 50 Torr 273 ml 15.7 Min. 99.4% 11

12 Controllers P.O. Box 688 Vineland, NJ Fax: TOLL-FREE: FAX: Prices and specifications are subject to change without notice

Accurate to 0.1 NIST Traceable Advanced PID Algorithm USB Port Free datalogging/control software

Accurate to 0.1 NIST Traceable Advanced PID Algorithm USB Port Free datalogging/control software CONTROLLERS Serving the laboratory glassware industry for over 75 years State-of-the-Art and Vacuum Controllers