Viscometers, Monitor and control - Analytical consumables

Transcription

1 ROTARY VISCOMETERS GLASS THERMOMETERS FLOW CUPS REACTORS GLASS VISCOMETERS MONITOR AND CONTROL ANALYTICAL CONSUMABLES Rotary viscometers pages 80 to 8-85 Flow cups for measuring liquid viscosity pages 83 to 8 Viscometer precision bath page 8 Glass viscometers page 85 Monitor and control apparatus pages 86 to 88 Glass thermometers pages 89 to 90 Laboratory reactors pages 91 to 9 Analytical consumables page 93 to 99 Medical devices for disposable IN VITRO Viscometers, Monitor and control - Analytical consumables True knowledge is rigorous and hard on itself. At the same time is amiable and tolerant. Plutarco

2 Rotary Viscometers Rotary viscosimeters ST-00 INTRODUCTION Rheology is the study of the effects experimented in a substance when a mechanical force is applied on a it (flow and deformation) under different external conditions. It is used to describe the consistency of different products and is normally defined by the components: viscosity and elasticity. Measuring viscosity is determined by the tangible force required to displace the materials particles with a specific deformation-flow i.e. velocity. The relationship between the tangible force and the deformation flow obtains the viscosity result. Ambient conditions such as temperature and pressure also have an effect on viscosity. The measurement of viscosity is not just limited to the research laboratory, it has progressively entered the field of industrial quality control. PRINCIPLES OF VISCOSITY These instruments operate by means of a cylinder or disk (spindle) that is submerged into the material to be analysed and by measuring the resistance of the substance at a selected known speed. This resistance results is the measurement of the viscosity according to the flow characteristics of the reference spindle; the instrument calculates the result and directly displays the viscosity that is reported in cp (CGS) or mpa-s (SI). A wide range of viscosity can be measured using viscometers that are equipped with different types of spindles and speed ranges. The design of the spindles and the principals of measurement principles are regulated by ISO 555 and ISO 165 standards. All spindles are made of AISI 316 stainless steel. Each spindle can be identified by a letter and a number. SELECTION TABLE Standard measuring range of the viscometers, without additional accessories Part no Model ST-00 L ST-00 R Units centipoise (cp) centipoise (cp) Standard spindle L1 to L R to R7 Speed range r.p.m. 1 to 60 0,1 to 100 Measuring range 0 to cp 0 to cp Temperature range C 0,0 a 100,0 0,0 a 100,0 Power requirement 115/30V to 1VDC 1.A 115/30V to 1VDC 1.A Power 15 W 15 W Weight 5 Kg 5 Kg L.C.D. display of parameters and results: - Selected speed r.p.m. - Selected spindle s.p. - Viscosity result cp (mpa-s) or cst. - Base scale percentage %. - Sample temperature: C or F. Auto alarm in the case of any fault being detected. Off scale detection and indication by an audible and visual signal. Step controlled speed to prevent spindle vibrations. Velocity from 0,1 to 100 r.p.m. Mains power surge protection. TECHNICAL DATA Direct results in cp(mpa-s) or cst.: models ST- 010 L & R. Direct results in Poise (Pa-s) or St.: model ST-010 H. Precision: ±1% base scale. Measuring range: See table Repeatability: 0.%. Supplied complete with: - Anti shock carry case. - Main unit. - Support base. - Spindle protector. RS 3 unidirectional interface, download to a computer. DIGITAL THERMOMETER SPECIFICATIONS Temperature range:- from 0.0 C to C (+ 3.0 F to F). - Resolution: 0.1 C (0.17 F). - Precision: ± 0.1 C. ACCESSORIES Spindle R1 suitable for low viscosity samples. Fits model R. Part No Spindle R1 - Spindle support. - Set of spindles (model dependant) - Temperature prove Rack of standard spindles L1, L, L3,L : Suitable for models L. Small sample volume adapters. Suitable for models ST-00L and ST-00R. Suitable for sample volumes from 10 to 0 ml. With water jacket. If constant temperature is required, this adapter has a water jacket that can be connected to an external re-circulation equipment suitable for temperatures from 0 C to +100 C. Part No Small sample adapter with water jacket.(special spindles included). Low viscosity adapters. Required to improve low viscosity measurements. Newtonians and no Newtonians. Reproducible results and measurements of viscosity from 1 cp. Suitable for models L and R for viscometers ST-00. Sample volume: 5 to 30 ml. Includes special spindle. Without water jacket. Part No Adapter without water jacket. Model ST00L Rack of standard spindles R, R3, R, R5, R6 and R7: Suitable for model R. Part No Part No NEW DESIGN 80 Viscometer

3 Wide range rotary viscosimeters STS-011 MODEL WITH TEMPERATURE READOUT AND SHEAR RATE MEASUREMENT. 10 different options of language. L.C.D. display of parameters and results. Parameters display: - Selected speed r.p.m. - Selected spindle - Viscosity result cp (mpa-s) or cst. - Base scale percentage %. - Sample temperature: C or F. - Deformation ratio (with special spindle) - Torsion force (with special spindles) - Density (input by the user) g/cm 3. This instrument determines both relative and absolute viscosity. Data can be changed between S.I. and C.G.S. Automatically checks for correct operation point by scanning at different speeds. Auto alarm in the case of any fault being detected. Off scale detection and indication by an audible and visual signal. Step controlled speed to prevent spindle vibrations. Calibration by the user himself. 18 preselected speeds from 0.3 a 100 r.p.m. The operator can select any speed within this range. USB port. Mains power surge protection. 10 memoirs of working programs. TECHNICAL DATA Temperature range:- from 0.0 C to C (+ 3.0 F to F). - Resolution C: 0.1 C (0.17 F). - Precision C: ± 0.1 C. - Probe type: Pt 100. Direct results in cp(mpa-s) or cst.: models STS-011 L & R. Direct results in Poise (Pa-s) or St.: model STS-011 H. Precision: ±1% base scale. Supplied complete with: - Anti shock carry case. - Main unit. - Support base. - Spindle protector. - Spindle support. - Set of spindles (model dependant) (see table). NEW USB MODELS Part No. Measuring Standard Power Power Weight range spindles requirement W Kg STS-011 L to cp L1, L, L3, L V 50/60 Hz 15 5 STS-011 R to cp R, R3, R, R5, R6, R V 50/60 Hz 15 5 STS-011 H to cp R, R3, R, R5, R6, R V 50/60 Hz 15 5 ACCESSORIES Spindle R 1 suitable for low viscosity samples. Fits models R and H. Part No Small sample volume adapters (APM). Suitable for sample volumes from 8 to 13 ml. Requires the TL or TR set of spindles. Unit suitable for temperatures from 0 C to +100 C. Part No Small sample adapter APM with water jacket. Part No Temperature sensor suitable for APM. Special Spindles Part No set of spindles TL5 TL6- TL7 for models L. Part No set of spindles TR8 - TR9 - TR10 - TR11 for models R and H. Spindle R1. Part No Low viscosity adapters. (LCP). Required if low viscosity measurements are necessary. Reproducible results and measurements of viscosity from 1 cp. Suitable for models L and R. Sample volume: 16 to 18 ml. Includes special spindle LCP. Part No Adapter LCP with water jacket. Part No Temperature sensor suitable for LCP. Displacement spiral helix adapter. Required for low fluidity samples. Part No Part No Part No Part No Viscometer 81

4 Temperature control equipment for viscosity measurements for viscometers ST-00 and STS-011 The influence of temperature while measuring viscosity is considerable, lower temperatures increase viscosity. Therefore it is indispensable to control temperature when precise viscosity measurements are required. The control of temperature by using a thermostatically controlled bath is the most efficient, because of the recirculation of liquid produces a rapid and stable temperature. We recommend our range of immersion thermostats for this application. TEMPERATURE CONTROL AND CONFIGURATION FOR VISCOSITY MEASUREMENTS: FRIGITERM-10 Part No , FRIGTERM-30 Part No or DIGIT COOL Part No , suitable for below ambient working environments (see page 97 to 99 for specifications). For temperatures above ambient see the DIGITERM-100 Part No , or DIGITEM-00 Part No complete with 1 litre tank Part No , (see pages 96 and 97 for specifications). Frigiterm thermostat bath with adapter kit Part No , fitted with a rotary viscometer. Support base Spindle An adapter kit for the thermostat bath is required Part no This kit adjusts the bath measuring height to enable samples to be placed inside. Part No , Adapter for thermostat bath comprising of an extension spindle and leg adjusters for the bath. (Kit can be fitted by the user.) Part No Support for 500 ml beakers, to be placed inside the bath. Part No Support base for the DIGITERMimmersion thermostats. This accessory is recommended to close the bath and maintain a constant temperature. CONSTANT TEMPERATURE CONTROL ACCESSORY FOR SMALL SAMPLE VOLUME ADAPTERS. USE WITH THE RE-CIRCULATING JACKET ACCES- SORIES. PART NO To work below ambient temperatures, we recommend the use of the FRIGITERM-10 Part No , or FRIGITERM-30 Part No (see page 97 for specifications.) It is necessary to configure the immersion thermostats for external re-circulation. The Bath adapter kit is not required. Support for beakers Digiterm thermostat bath with support base Part No litre bath Part No and adapter kit Part No To be used with a rotary viscometer and beaker support Part No For temperatures above ambient see the DIGITERM-100 Part No , or DIGITERM-00 Part No complete with 1 litre tank Part No , (see pages 96 and 97 for specifications). OIL STANDARDS Certified known viscosity standards, suitable for calibrating rotary viscometers. Comes complete with official certificate. Immersion thermostat Digiterm controlling temperature of viscometer. Rotary Viscometer NDJ-1 APPLICATIONS The instrument operates by rotating a disk or cylinder, (spindle), that is submerged in the liquid or fluid to be analysed. A pre-selected speed is set, the unit measures the absolute resistance from viscosity of the fluid being analysed. Suitable for samples such as: foods, cosmetics, fats and oils, pharmaceutical products, paints and plastics, etc. The asynchronous motor is connected to a graduated disk with different speeds that propel the spindle via a spiral and die. Supplied complete with a set of spindles in a box, numbered 1 to with spindle stand. The viscometer includes a level and adjustable screw feet support base and protective case. MODEL Part No. Measuring Tolerance Spindle Speed Power Weight range r.p.m. for 1 to W Kg NDJ mpas ±5% Liquid Newtons Viscometer

5 Flow cups for measuring liquid viscosity CUP Nº STANDARD DIN CUPS STANDARD ISO 31. CUP FORD STANDARD ASTM D-100. Suitable for measuring kinematic viscosities from 5 to 700 cst, model dependent. Metallic cups, chrome finished and calibrated. Flow cups with handle. Models DIN 5311 Nº and Ford ASTM D-100. Flow cups. Standard models. ACCESSORY Support stand with adjustable level. Part No Heated cups with threaded base, can be connected to a water bath or to a temperature regulator Electemp. ACCESSORIES Water bath with heater and screw on disk, with level. Part No Temperature controller Electemp. Part No Pt 100 sensor probe for the Electemp and water bath. Part No (See page 86). MODELS Part No. Standard Bore Format Range Admisable Ø mm cst fall times DIN 5311 Standard 90 to to DIN 5311 Heated 90 to to DIN 5311 With handle 90 to to ISO 31 3 Standard 5 to 30 to ISO 31 3 Heated 5 to 30 to ISO 31 Standard 35 to to ISO 31 Heated 35 to to ISO 31 5 Standard 100 to to ISO 31 5 Heated 100 to to ISO 31 6 Standard 190 to to ISO 31 6 Heated 190 to to to 10 0 to ASTM D Standard 0 to 0 0 to to to to 10 0 to ASTM D Heated 0 to 0 0 to to to to 10 0 to ASTM D With handle 0 to 0 0 to to to 100 Comes with a calibration certificate with results traceable to know standards and equipment Viscometer 83

6 Ford cup thermostat for viscosity measurement TV-15 CUP MODELS THAT CONFORM TO THE FOLLOWING STANDARDS: DIN 5311, ISO 31 AND ASTM 100. ELECTRONIC DIGITAL CONTROL FROM 10ºC TO 110ºC. APPLICATIONS Thermostat Ford cups for viscosity measurement need to be maintained at a precise temperature of 10 and 60 C. Made up of an independent Peltier thermostat control system that heats and cools. Made from AISI 30 stainless steel, with adjustable levelling feet supports, and central orifice for locating the cup. CONTROL PANEL Illuminate ON/OFF switch Digital temperature display Key pad to select readout and temperature. Heating and cooling by Peltier effect MODEL Part No. Temperature Stability Homogeneity Read Resolution Height / Width / Depth Power Weight C C C error cm W Kg to 60 C ±0.1 ±0. ± See the different standards, models and cups (see page 83.) Viscometer Precision Bath VB-13 FOR CONTROLLABLE TEMPERATURES FROM AMB.+5 C TO 100 C. STABILITY ±0.05 C. HOMOGENEITY ±0.05 C. READING ERROR ±0.09 C. RESOLUTION 0.1 C. SAFETY: STANDARD DIN CONTROLLABLE SAFETY THERMOSTAT WITH MANUAL RESET. Temperature sensor Pt100 thermo-resistor, stainless steel AISI 30 lid with three viscometer locations ports, three independent lids and an additional location port for the control thermometer. The main body of the bath is made of a 0 litre borosilicate glass tank. A white plate is located at the back to help optimise and read the viscometers. Used for measurements with glass viscometers Made for the calibration of viscometers according to the following standards UNE 00313, ISO 3105, ASTMD 5 and 515 CONTROL PANEL 1. Mains power iluminated switch.. Temperature regulator: 3. Real time temperature display.. Push button to increase value. 5. Push button to decrease value. 6. Push button to configure operation. 7. Safety thermostat safety lamp MODEL Part No. Control range Capacity Height / Ø Height / Ø Power Weight C litres (tank) cm (total) cm W Kg amb.+5 up to ACCESSORIES Universal viscometer support made from PTFE with stainless steel AISI 30 support. Suitable for the following viscometers : - Cannon-Fenske for transparent liquids. - Cannon-Fenske for opaque liquids. - Ubbelohde. - Ostwald. - BS U Tube. -Cannon-Manning semi-micro. - Ubbelohde type BS/IP/SL, BS/IP/SL(S) & type BS/IP/MSL. - DIN Ubbelohde. Part No Calibration Chronometers (see page 88). Thermometers for viscometer baths. Part No Thermometer ASTM 10C at 38.6 to 1. C divisions 0.05 C Thermometer ASTM 11C at 98.6 to 101. C divisions 0.05 C Thermometer ASTM 91C at 0.0 to 50.0 C divisions 0.1 C Thermometer ASTM 9C at 0.0 to 70.0 C divisions 0.1 C Thermometer ASTM 93C at 60.0 to 90.0 C divisions 0.1 C Thermometer ASTM 9C at 80.0 to C divisions 0.1 C. 8 Viscometer

7 Glass Viscometers VISCOMETER UBBELOHDE ASTM D5 - ASTM D6 - ISO ISO Suitable for transparent liquids. Complete with calibration certificate. Total length 83 mm. Permanent amber markings. ACCESSORY Viscometers support rack. Part No Capacity: 6 viscometers. Part No. Type Nominal constant Viscosity range in cst to C to B to to C to B to to C to B to to C to B to to C to Ubbelohde VISCOMETERS CANNON-FENSKE TRANSPARENT ASTM D5 - ASTM D6 - ISO ISO IP 71. Suitable for transparent liquids. Complete with calibration certificate. Constant at 0 C to 100 C. Total length 50 mm. Permanent amber markings. Part No. Serie Nominal constant Viscosity range in cst ,00 0, a 1, ,00 0,8 a 3, ,008 1,6 a 6, ,015 3 a ,035 7 a ,1 0 a ,5 50 a ,5 100 a , 0 a ,5 500 a a a 0000 Transparent VISCOMETERS CANNON-FENSKE OPAQUE ASTM D5 - ASTM D6 - ISO ISO Suitable for opaque and transparent liquids. Complete with calibration certificate. Constant at 0 C and 100 C. Total length 95 mm. Permanent amber markings. Part No. Serie Nominal constant Viscosity range in cst ,00 0, a 1, ,00 0,8 a 3, ,008 1,6 a 6, ,015 3 a ,035 7 a ,1 0 a ,5 50 a ,5 100 a , 0 a ,5 500 a a a 0000 Opaque Viscometer 85

8 Monitor and Control Apparatus Electronic controller Electemp Digital temperature controller with a user configurable microprocessor. For AUTOTUNNING and automatic adjustment to the material being measured. (solid, liquid, air). Temperature range: -150 C to 1300 C. (Temperature probe dependent.). Precision ±0.1 C. Resolution ±0.1 C with Pt 100 probe. ±1 C with a K type probe. Functions: ON/OFF P.I.D. control. CONTROL PANEL Main On/Off switch. On Indicator lamp. Indicator lamp of external device connected. Real time digital temperature display. Set temperature display. Push button to increase value. Push button to decrease value. Push button to P.I.D hysteresis. Push button control in C or F, temperature limits. BACK PANEL Power output (SCHUKO plug) 3100 W at 30 V. Protection fuse. Pt100 probe connection. K type probe connection. Data output. APPLICATIONS Digital thermometer. To control and display temperature in any equipment with temperature control system, that uses a contact thermometer, such as: Baths, Immersion thermostats, Hotplates and Hotplate stirrers, Mantles, etc. Can also be used by a immersion thermostat controlling a heater element. (maximum power 3100 W). As a regulator or temperature reader in equipment that are labelled with. Electronic contact thermometer Sensoterm ll DIGITAL DISPLAY, PT 1000 PROBE, AISI 30 STAINLESS STEEL. STABILITY ±1 C, ±1 DIGIT. RESOLUTION ±1 C. MODEL Part No. Height / Width / Depth Max. power Weight cm (exterior) W (at 30 V) Kg ACCESSORIES Pt 100 probe. Immersion dimensions: mm Ø, 130 mm length. Cable: 150 cm length. Part No Type K probe. Immersion dimensions: mm Ø, 150 mm length. Cable: 150 cm length. Part No NEW ONLY SUITABLE FOR INSTRUMENTS THAT CAN USE AN ELECTRICAL CONTACT THERMOMETER. Advantages include a separate temperature probe that maintain the main body away from steam and other vapours. Safer than a glass contact thermometer, eliminating the risk of broken it and a mercury spillage. Main body made of ABS plastic. TECHNICAL DATA Temperature range: from -50 C to 300 C. Temperature probe: 3.5 mm Ø x 50 mm immersion. Temperature Display: 8 mm high LCD display. Ambient working range: 0 to 60 C and a relative humidity of 80 %. MODEL Part No. Height / Width / Depth Weight cm (exterior) Kg Instruments labelled with that can use the electronic controller Electemp and the electronic contact thermometer Sensoterm. Sand Bath Combiplac-Sand Parts No and Hotplate - Rectangular Combiplac Parts No and Hotplate - Circular Combiplac Parts No and NOTE: Any equipment that can be connected to an electrical contact thermometer can also be used with an Electemp or Sensoterm unit. Magnetic Stirrers Agimatic Parts No , 70031, 70006, , , and Monitor and control

9 Electronic energy controller Enertron Regulates the power to the heating element by pulsing electronic circuit, free of noise and interferences CONTROL PANEL Main ON/OFF switch. Mains ON indicator lamp. ON indicator power out. Controllable from % to 100 %. APPLICATIONS Regulates the power of a heating element in ovens baths, radiators, hotplates, etc. MODEL Part No. Height / Width / Depth Max. power Weight cm (exterior) W (at 30 V) Kg BACK OF CONTROLLER Output of power (Schuko plug system). Protection fuse. Connection for a contact thermometer. Enertron application to a hotplate, showing the unit connected with an electronic contact thermometer. Digital thermometer TC-96-A Main body made of PVC with anti-slide for better stability. Temperature range from -00 C to 1370 C (-38 to 98 F). Reads C or F, reading within 1 second. Memorizes the last 10 temperature readings. Displays the reading for 3 seconds. It is posibles to hold the reading on the screen. Switches off automatically after 1 hour (if it is in a continuous mode). LCD with back light illumination. Low battery power indicator. Powered by 3 x 1.5V "AAA" batteries. Compatible with most Type K sensors. Operating conditions: from 10 to 50 C. Dimensions: (height x width x depth): 17 x 7 x 3 cm. Weight 150g. MODEL Part No. Temp. range C Resolution C Precision C from -00 to -50: ± CT-96-A to from -50 to 70: ±1 from 70 to 1370: ± The precision figures supplied are based on a measurement range from 18 to 8 C (does not include the sensor error). Supplied complete with a Type K sensor and cable of 1.0 mm Ø x 100 cm long. ACCESSORY Sensor type K of 8 mm Ø x 30 cm length. Part No Digital Humidity meter with Thermometer RH-600 Temperature range from 0 C to 60 C. Humidity range from 10% to 95% RH. Digital Display C or in F Fast response: 0.. Power: battery 9 V. Dimensions: (height x width x depth): 3. x 7 x 15.5 cm. Weight: 370 g. Part No Supplied complete with humidity / temperature sensor, protective cover and carry case. MODEL Part No. Temp. range Resolution Precision Humidity Humidity Humidity C C C range % resolution % precision % RH from 0 to ±0.8 from 10 to > 70%: ±3% +1% < 70%: ±3% Monitor and control 87

10 Ink Printer Microprinter APPLICATIONS Small ribbon printer (not thermal) with paper roll 1/" (56 mm) wide. Interface connection: RS3. Applications: Measuring equipment, ph meters, conductivity meters, spectrophotometers, etc. Includes interface cable and power transformer 5V - 3A and cable. MODEL Part No. Height / Width / Depth Power Weight cm supply Kg DC 5V 3A 1 Automatic programmer Promat H Connects and disconnects electrical power by a pre-programmed timer switch. Adjustable timer: Cycles up to hours, with controllable connection disconnection up to every 15 minutes. Manual interrupt setting to disconnect the program, luminous indicator shows when power is being applied. Maximum current: 16 Amp. Part No Timer alarm Relavis Audible sound when the program time has lapsed. Time setting from 0 to 60 minutes in 1 minute intervals. Part No Digital alarm timer Count Down-Up Maximum count time 99 min. 59 sec. Timer: count-down and count-up. Portable: table top with magnetic holder or clip if used on a pocket or overall. Audible alarm fitted. Part No Digital Chronometer Diamond Maximum timer: 3 hr 59 min 59 sec. Division 1/100 seconds. Control: LAP/SPLIT (timer: split time and accumulative time). Date incorporated. Audible Alarm (duration 60 seconds). Audible Alarm "snooze" function (once pressed the stop alarm goes off every 5 minutes until it is completely shut off). Part No Thermometer reader Micro-Temp SUITABLE FOR MEASURING TEMPERATURE FROM -50 C TO +300 C OR FROM -58 F TO +57 F. Applications: process control, laboratories, pharmacies, food processes and agriculture in general. Digital screen readout in C or F. Stainless steel penetration probe of 3.5 mm Ø x 10 mm long. Retention memory of minimum and maximum data readout. Disconnects automatically after 1 hour. Powered by a 5V - 3A battery. MODEL Part No. Precision Resolution ±1 C / 1 F 0.1 C / 0.1 F Comes complete with protective cover and support clip. 88 Monitor and Control

11 GLASS THERMOMETERS COMMON All thermometers are made of glass rod or with an opal scale, with a reinforced bulb. A wide selection of scales and temperature ranges is available. Scales etched in acid and graduated with indelible ink. Resistant to most chemical agents. All thermometers are supplied with a protective plastic cover. Solid stem Themometers Yellow backed, mercury filled. Part No. Range Division scale Total length C C cm / / / / / * * White back. Enclosed scale thermometers White back, with red liquid content. Suitable for measuring samples where mercury is not permitted. E.g. food products, drinks, etc. Part No. Range Division scale Total length C C cm /1 30 Yellow backed with suspension ring, mercury filled. Part No. Range Division Immersion Total C scale C length cm length cm / / With prismatic capillary, with easy to read scale. Contains mercury. Part No. Range Division scale Immersion length Total length C C cm cm / / / / / / / / / / Monitor and Control 89

12 Precision thermometers Mercury thermometers. Complete with calibration certificate PROTON registration control no. 0-C.37 and 0-V.06 (Meteorological control). Traceable certificate indicating the proof of continued quality of workmanship against different temperatures, with method and conditions of measurement against known traceable standards. Part No. Range Division scale Type Total length C C cm /1 solid stem /1 solid stem solid stem solid stem solid stem /1 enclosed scale /1 enclosed scale enclosed scale enclosed scale enclosed scale 5 Case with 7 glass rod mercury thermometers, white back, scale in 0.1 C. Range C* Total length cm cm cm cm cm cm cm *One thermometer per range. Part No with calibration certificate PROTON without calibration certificate. Electric contact thermometers Adjustable temperature setting with the use of a dial on the top of the thermometer. To provide better mercury flow, the capillary interior is filled with an inert gas. Supplied complete with a 100 cm cable with the appropriate connection on the end. Part No. Range Division scale Immersion length Total length C C cm cm / / / / / / Monitor and Control

13 Universal reactor for laboratory RV-1 ADAPTABLE TO ALL THE STANDARDIZED GLASS ELEMENTS WITH A MOUTH OF 100 MM Ø. REACTOR CAPACITY: 1 LITRES. APPLICATIONS Universal reactor suitable for all laboratory and pilot plant s operations. NEW Standard mouth for connection to DN100 glass reactor s covers. Reactor in stainless steel AISI 316, with a capacity of 1 litres and with a drain tap. STANDARD EQUIPMENT 1. Standard support. Part No Clamp with support ring for the reactor. Part No Reactor in stainless steel AISI 316, capacity 1 litres with drain tap. External sizes: Height 38 cm. x 5 cm. Ø. Weight:,5 Kg Part No Glass cover for reactor COMPLEMENTS 13. Clasp for fastening normalized flat gaskets for reactor RV-1 or any glass reactor with normalized mouth of 100 mm. Ø. Part No Stirrer RZR-1 with adjustable speed. Part No Double bosshead MAXIM. Part No Flexible shaft holder for 8 mm. Ø stirring shaft. Part No Half-moon shape stirring shaft, 8 mm. Ø stainless steel AISI 30 (length 90 x shovel width 1 cm). Part No Helix shape stirring shaft, 8 mm. Ø stainless steel AISI 30 and PTFE shovel (length 90 x shovel width cm). Part No Electronic controller ELECTEMP. Part No with connector for inner temperature control, if the heating mantle is used. 11. Support plate with bosshead for Electemp regulator. Part No Pt100 probe Part No mm length x mm. Ø, with connection cable to Electemp regulator. 13. Ring holder with double bosshead for heating mantle. Part No Heating mantle with doble heating elements for temperatures up to 00 C. Power consumption 100W. Part No OPTIONAL Note: It is supplied without glass elements. Aisi 316 stainless steel device, with standard double mouth and coll for liquid heating or refrigeration inside the reactor. This device can be connected to the universal reactor part no or to glass reactors with a 10 l. capacity and with DN-100 standard mouth. Coil measurement: A: 1 cm. B: 15 cm. C: 10 cm. Part No For reactors higher than 0 cm., it must be manufactured according to drawing. Note: Several tests have been made in the laboratory with the silicone oil 7V50 and with the Ultraterm-00 thermostat. Part No (See page 96), reaching temperatures up to 170 ºC in 35 inside the reactor properly isolated with durablanket10. With methanol fluid transmitter liquid and with Frigiterm-30 thermostat. Part No (see page 97), reaching temperatures up to -1 ºC in 57 inside the reactor properly isolated with durablanket10. B C A Reactor 91

14 Reactor for pilot plant R-60 CAPACITY UP TO 0 LITRES ACCESORIES NEW Drip inlet valve External feed inlet Drip bottle feeding inlet Cooling cycle water inlet Flask for drip liquid medium Drip control valve Vacuum gauge Digital thermometer TC-96-A Temperature range: -00 ºC. to 1370 ºC. Part No: Drip inlet valve Air release valve Reflux control valve Cooling and heating circulation liquid inlet Liquid collection flask PTFE faucet and bellows for liquids/solids suspensions evacuation. Part No: Double layer glass flask Outlet valve Drainage devide Anchor blade for stirring Cooling and heating circulation liquid outlet Over elevation support base about 65 cm. height for bottles filling up to 0L capacity. Part No: APPLICATIONS This equipment is designed for reflux and distillation operations with a stirring element, for all laboratory s pilot plant operations and small productions. Reactor module built-in, made of glazed steel in epoxy, composed of an engine group stirring and a reaction borosilicate glass GGA container, graduated for a volume from to 0 litres and with double layer for tempering. Stirring anchor blade and elements in contact with the liquid or reaction steam, composed of borosilicate glass and PTFE. CONTROL PANEL Main switch ON / OFF. Regulator knob for stirring speed from 0 to 800 rpm, and with digital reading. MODELS Part no. Total dimensions Reactor Operating Power Weight Height / Width / Depth capacity temperature W Kg ºC to 00 ºC Recirculation thermostat Ultraterm-00. Recirculation cryothermostat Frigiterm-30. For adjustable temperatures from ambient +5 ºC. to 00 ºC. Part no (See pag: 96). For adjustable temperatures from -30 ºC. to 100 ºC. Part no (See pag: 97). 9 Reactor

15 AQUISEL MEDICAL DEVICES PRODUCTOS SANITARIOS MEDICAL DEVICES MANUFACTURER FOR DISPOSABLE IN VITRO DIAGNOSTIC. FABRICANTE DE PRODUCTOS SANITARIOS PARA DIAGNÓSTICO IN VITRO. UN SOLO USO. SELECTA GROUP Eliminate unnecessary risks with the AQUISEL Valve-Stopper system. Evite riesgos innecesarios con el sistema Tapón-Válvula AQUISEL. Container with AQUISEL Valve-Stopper. Contenedor con Tapón-Válvula AQUISEL. ICO /0-009 Pipettes for E.S.R. with zero levelling and automatic closure system for conventional tubes or AQUISEL Valve- Stopper. Pipetas VSG de enrase a cero. Con émbolo de presión para tubos convencionales o con Tapón-Válvula AQUISEL. EN-ISO-9001 QUALITY MANAGEMENT SYSTEMS / EN-ISO-1385 MEDICAL DEVICES EN-ISO-9001 SISTEMAS DE GESTIÓN DE LA CALIDAD / EN-ISO-1385 PRODUCTOS SANITARIOS

16 AQUISEL VALVE-STOPPER System available for sample manipulation without the need of uncorking the tube, maintaining it hermetically sealed and avoiding the risk of contamination. TAPÓN- VÁLVULA AQUISEL Sistema que permite su manipulación sin necesidad de destaponar, permaneciendo hermético y evitando el riesgo de contaminación. The AQUISEL system consist of a tube, valve-stopper and an appropriate reagent for specific use. The AQUISEL tube is made of a high resistance transparent polypropylene. The valvestopper is a very elastic material and has a special cross-cut design which allows an automatic recover to its initial closed position, after insertion or extraction of the sample. The tube s reagent contents is offered through different possibilities identified by colours in accordance with International Standards. It can be used by most of the current analytical procedures, even if they are manual, semi-automatic or automatic procedures. It allows inter-hospital road and postal transport thanks to its hermetic seal and high resistance to uncorking due to vibrations, hits, cold, heat, etc. USE AND APPLICATIONS 1. Inserting (blood) samples with syringe (without needle).. Extraction and dosage with semi-automatic pipette. 3. Capillary blood extraction.. Capillary filling for microhematocrite. 5. Automatic sampling for haematology in primary tubes. 6. Sample road transport. 7. Centrifuge heads adaptable. 1 El sistema AQUISEL se compone de tubo, tapón-válvula y del reactivo apropiado para su uso específico. El tubo del sistema AQUISEL está fabricado en polipropileno de alta resistencia y de gran transparencia. El tapón-válvula es de material muy elástico y posee unos cortes que por su diseño especial recuperan automáticamente su hermeticidad, después de la introducción o extracción de la muestra. Su contenido en reactivo ofrece diferentes posibilidades que se distinguen por su color según Normas Internacionales. Puede ser utilizado con la mayoría de los procedimientos analíticos actuales, ya sean manuales, semiautomáticos o automáticos. Permite el transporte neumático intrahospitalario e incluso por correo por su hermeticidad y gran resistencia a destaponarse con movimientos, golpes, frío, calor, etc USO Y APLICACIONES 1. Introducción de muestra con jeringuilla (sin aguja).. Extracción y dosificación con pipeta semiautomática. 3. Recogida de sangre capilar.. Llenado de capilar para microhematocrito. 5. Toma de muestras automática para hematología en tubos primarios. 6. Transporte neumático de muestras. 7. Adaptable a cabezales de centrífuga o Analitical consumables

17 Tubes with AQUISEL Valve-Stopper Tubos con Tapón-Válvula AQUISEL There are different size and volume tubes with additives: anticoagulant, antiglicolytics, clotting accelerators or empty tubes. Diferentes formatos y volúmenes de tubos con aditivos: anticoagulantes, antiglicólicos, aceleradores de la coagulación o vacíos. Tubes for small blood volume, size 55x1 Tubos para pequeños volúmenes de sangre de 55x1. Suitable for paediatrics or small sample volumes. Indicados para pediatría, o para pequeños volúmenes de muestra. Product presentation Presentación del producto The tubes are presented in polystyrene racks of 100 units. Every 50 units are covered with a transparent lid for protection. Los tubos van colocados en gradillas de poliestireno de 100 unidades. Cada 50 unidades se cubren con una tapa transparente de protección. Accesory: CAP-GALET Accesorio: CAP-GALET Funnel adapter which can be used together with the primary AQUISEL tubes and allows sample blood transfer to secondary tubes, useful for capillary blood extractions in paediatrics, for low blood volumes, can be used in all auto-analysers for primary tube sampling, etc. All these procedures could be completed without uncorking the primary AQUISEL tubes. Once the CAP-GALET is removed, the tube remains sealed again for conservation or disposal. Adaptador en forma de embudo que juntamente con los tubos primarios AQUISEL permite trasvasar las muestras a tubos secundarios, realizar extracciones de sangre capilar en pediatría, útil para bajos volúmenes de sangre, ser utilizado en todos los autoanalizadores con toma-muestra de tubo primario, etc.todos los procesos se realizan sin necesidad de destaponar los tubos primarios AQUISEL. Una vez extraído el CAP-GALET, el tubo permanece de nuevo cerrado para su conservación o desecho. Analitical consumables 95

18 Product table - Cuadro de productos AQUISEL TUBES WITH VALVE-STOPPERS - TUBOS AQUISEL CON TAPÓN-VÁLVULA TUBES QUANTITY IN THE SHIPPING BOX (100 UNITS RACKS) Nº DE TUBOS EN LAS CAJAS DE EXPEDICIÓN (GRADILLAS DE 100 UNIDADES) K3E K3E NC 9 NC LH LH LH Nominal size of the tube: length x diameter in mm. Tamaño nominal del tubo: long x diámetro en mm. CONTENT / REAGENTS CONTENIDO / REACTIVO EDTA 3K EDTA 3K CITRATE 3 Na - CITRATO 3 Na 0,106 M~3,8% 1: VSG / ESR CITRATE 3 Na - CITRATO 3 Na 0,106 M~3,8% 1:9 CLOTTING FACTORS FACTORES DE COAGULACION Li HEPARIN - HEPARINA Li LI HEPARIN WITH SEPARATOR GEL HEPARINA Li CON GEL SEPARADOR Li HEPARIN + MONOIODO ACETATE Li HEPARINA Li + MONOIODO ACETATO Li DOSAGE TYPE TIPO DE DOSIFICACION LIQUID LIQUIDO LIQUID LIQUIDO LIQUID LIQUIDO LIQUID LIQUIDO LIQUID LIQUIDO LIQUID AND GEL LIQUIDO Y GEL LIQUID LIQUIDO STOPPER COLOUR COLOR DEL TAPON MAUVE MALVA MAUVE MALVA BLACK NEGRO LIGHT BLUE AZUL CLARO GREEN VERDE GREEN VERDE GREEN VERDE 100 x16 75 x16 Code Código ml blood sangre 10 Code Código ml blood sangre 55 x16 FLAT BOTTOM CON FALDON Code Código ml blood sangre * * 80 x13 70 x1 Code Código ml blood sangre,5 *,5* 1,6 1 Code Código ml blood sangre 3 1, 55 x1 CAP Code Código ml blood sangre 1 0,5 0,5 1 0,3 1 0, FX Z Z Z Z Z Z Z MONOIODO ACETATE Li + CLOTTING GRANULES MONOIODO ACETATO Li + GRANULOS ACTIVADOR FLUORIDE Na + OXALATE K FLUORURO Na + OXALATO K EMPTY AND UNLABELLED VACIO SIN ETIQUETA EMPTY WITH BLANKLABEL FOR SERUM VACIOS CON ETIQUETA EN BLANCO PARA SUERO SEPARATOR GEL FOR SERUM GEL SEPARADOR PARA SUERO PS GRANULES FOR SERUM GRANULOS PS PARA SUERO CLOTTING ACCELERATOR ACTIVADOR DE LA COAGULACION CLOTTING ACCELERATOR SEPARATOR GEL ACTIVADOR DE LA COAGULACION Y GEL SEPARADOR CLOTTING ACCELERATOR PS GRANULES FOR SERUM ACTIVADOR DE LA COAGULACION Y GRANULOS PS PARA SUERO GRANULES GRANULOS LIQUID LIQUIDO POWDER PULVERIZADO GEL GRANULES GRANULOS LIQUID LIQUIDO LIQUID AND GEL LIQUIDO Y GEL GRANULES GRANULOS LIGHT GREY GRIS CLARO DARK GREY GRIS OSCURO WHITE BLANCO WHITE BLANCO WHITE BLANCO WHITE BLANCO RED ROJO RED ROJO RED ROJO Long Largo *Special for Haematology Shipping (cm) automatic machines boxe size Width Ancho (cm) (special cut 5 mm) Medidas High Alto *Especial para máquinas Caja (cm) automáticas de hematología Weight Peso Expedición,3,3,0 3,5 3 (corte especial del tapón 5 mm) (Kg) 75x13 size tube for AQUISEL P- pipette. Special tube for AQUISEL P-3 pipette. Special tube for AQUISEL P- MICRO pipette. Tubo 75x13 para pipeta AQUISEL P-. Tubo especial para pipeta AQUISEL P-3. Tubo especial para pipeta AQUISEL P- MICRO ,5 1 1,5 1,5 1,5 1,5 96 ACCESORY: CAP-GALET - ACCESORIO: CAP-GALET Code Supplied in bags of 500 units. Código Se suministra en bolsas de 500 unidades. AQUISEL TUBES WITH NON-CUT STOPPER - TUBOS AQUISEL CON TAPÓN SIN CORTES CONTENT/REAGENTS CONTENIDO/REACTIVO K3E EDTA 3K Analitical consumables DOSAGE TYPE TIPO DOSIFICACION LIQUID LIQUIDO STOPPER COLOUR COLOR TAPON MAUVE MALVA Nº TUBES PER BOX Nº TUBOS POR CAJA 800 Code Código ml blood ml sangre LENGTH x Ø Tube mm LONG. x Ø Tube mm. Width / Depth / Height Box cm Ancho / Fondo / Alto Caja cm Weight Peso Kg x

19 AQUISEL PIPETTE PIPETTES FOR ERYTHROCYTE SEDIMENTATION READ E.S.R. WESTERGREN METHOD. Pipettes made in polystyrene with similar properties as glass ones. The ZERO-CLOSURE system allows the pipette filling, preventing that the blood exceeds the zero point and also avoiding total or partial loss. Automatic sealing makes it a disposable product. PIPETA AQUISEL PIPETAS PARA LA DETERMINACIÓN DE LA VELOCIDAD DE SEDIMENTACIÓN GLOBULAR V.S.G. MÉTODO WESTERGREN. Pipetas fabricadas en poliestireno con un comportamiento equivalente al vidrio. El sistema de CIERRE-CERO permite el llenado de la pipeta impidiendo que la sangre supere el punto cero y evitando el vaciado total o parcial. Al quedar automáticamente sellado se convierte en un artículo de un solo uso. AQUISEL Pipette A- without rubber. For any kind of tube use, even with AQUISEL or with a conventional stopper. Suitable for mechanical or manual aspiration. Pipeta AQUISEL A- sin émbolo. Para cualquier tipo de tubo, con tapon AQUISEL o convencional. Llenado por aspiración mecánica o manual. AQUISEL P- AQUISEL Pipette P- with rubber. For 75x13 tubes with AQUISEL or with a conventional stopper. Pipette filling by pressure till the bottom of the tube. Pipeta AQUISEL P- con émbolo. Para tubos de 75x13 con tapon AQUISEL o convencional. Llenado de la pipeta por presión hasta el fondo del tubo. AQUISEL Pipette P-3 and P- MICRO systems Set of AQUISEL pipettes and tubes. Tubes come with the valve-stopper which allows the pipette insertion without the need of uncorking. Pipette filling by pressure. Sistemas Pipeta AQUISEL P-3 y P- MICRO Conjuntos formados por pipetas y tubos AQUISEL. Los tubos llevan incorporado el TAPÓN-VALVULA lo que permite la introducción de la pipeta sin necesidad de destaponar. Llenado por presión. Analitical consumables 97

20 PRODUCT PRESENTATION - PRESENTACIÓN DEL PRODUCTO AQUISEL Pipettes A- Expanded polystyrene packaging of 500 units. Pipetas AQUISEL A- Envase de P.S. expandido. De 500 pipetas de capacidad. AQUISEL Pipettes P- 00 units cardboard package. Supplied in 800 units boxes. Pipetas AQUISEL P- Envase de cartón de 00 unidades. Se suministran en cajas de 800 unidades. Set P-3. AQUISEL Pipette and tube 00 units cardboard package and 100 tubes rack made of expanded polystyrene, supplied in 600 sets boxes. Conjunto P-3. Pipeta con tubo AQUISEL Envase de cartón de 00 pipetas y de P.S. expandido de 100 tubos. Se suministra en cajas de 600 conjuntos. Set P- Micro. AQUISEL Pipette and tube 100 pipettes cardboard package and 100 tubes rack made of expanded polystyrene, supplied in 00 sets box. Conjunto P- Micro. Pipeta con tubo AQUISEL Envase de cartón de 100 pipetas y de P.S. expandido de 100 tubos. Se suministra en cajas de 00 conjuntos. MODEL MODELO CODE CÓDIGO UNITS / BOX Nº UNIDADES CAJA BOX WEIGHT Kg PESO CAJA Kg BOX DIMENSIONS cm - MEDIDAS CAJA cm Width Ancho Depth Fondo Height Alto A , P Set P pipettes tubes Conjunto P pipetas tubos Set P- Micro Conjunto P- Micro pipettes + 00 tubes 00 pipetas + 00 tubos 3, COMPLEMENTS - COMPLEMENTOS Methacrylate rack 10 place rack. For P-3 / P- set. Code For tube Ø 13 mm - set P For tube Ø 1 mm - set P- Micro Gradilla en metacrilato 10 plazas numeradas. Para conjunto P-3 / P-. Código Para tubo Ø 13 mm - conjunto P Para tubo Ø 1 mm - conjunto P- Micro Metallic Westergren stand 10 place autoclavable stand. For any kind of AQUISEL pipettes with Ø 13 mm tubes and A- pipettes with Ø 16 mm tubes. Easy and functional system that allows the total set disposal. Code For Ø 13 mm tubes For Ø 16 mm tubes Loose tubes for pipettes: for AQUISEL P-3 (800 units/box) for AQUISEL P- Micro (1000 units/box) Soporte Westergren metálico 10 plazas numeradas. Autoclavable. Para todo tipo de pipetas AQUISEL con tubos de Ø 13 mm y para pipetas A- con tubos de Ø 16 mm. Sistema simple y funcional que permite el vertido total del conjunto. Código Para tubo Ø 13 mm Para tubo Ø 16 mm Tubos sueltos para pipetas: para AQUISEL P-3 (800 uds/caja) para AQUISEL P- Micro (1000 uds/caja) 98 Analitical consumables

21 AQUISEL URINE CONTAINER CONTAINER FOR URINE SAMPLES COLLECTION WITH AQUISEL VALVE- STOPPER. The AQUISEL VALVE-STOPPER allows the urine manipulation without uncorking, eliminating the contamination risks, samples loss, spillage, odours, etc. All the AQUISEL urine container presentations will be supplied with the GALLET accessory, which makes easy the sample dosage to a tube for sedimentation analysis, or the urine test strip insertion. CONTENEDOR PARA ORINA AQUISEL CONTENEDOR PARA LA RECOGIDA DE MUESTRAS DE ORINA CON TAPÓN- VÁLVULA AQUISEL. El TAPÓN-VÁLVULA AQUISEL permite la manipulación de la orina sin destaponar. Evita los riesgos de contaminación, pérdidas de muestra, derrames, malos olores, etc. Todas las presentaciones del contenedor de orina AQUISEL incorporan el accesorio GALET que facilita la dosificación de la muestra a un tubo para el análisis de sedimentación, o la introducción de la tira reactiva. Insertion of the GALET in the AQUISEL VALVE-STOPPER. Introducción del GALET en el TAPÓN- VÁLVULA AQUISEL. Urine sample extraction through the GALET. Extracción de la muestra de orina a través del GALET. Urine test strip insertion. Introducción de la tira reactiva. Dosage through automatic or conventional pipette. Dosificación por medio de pipeta automática o convencional. CODE CÓDIGO BAG BOLSA ASSAMBLED MONTADO UNITS BOX UDS. CAJA WEIGHT Kg PESO Kg DIMENSIONS cm - MEDIDAS cm Width Ancho Depth Fondo Height Alto NO NO NO NO NO NO YES SI YES SI YES SI Code GALET CONTAINER (1000 units package). Código GALET CONTENEDOR (paquetes de 1000 unidades). Analitical consumables 99