Supplement to Augustsson et al. (2011)---LA-ICP-MS zircon U-Pb dating method and data
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1 Supplement to Augustsson et al. (2011)---LA-ICP-MS zircon U-Pb dating method and data Method After sieving, the heavy minerals of the < 250 µm fraction were separated with a sodium polytungstate liquid with a density of ca. 3 g/cm 3. Magnetic heavy minerals were removed with a Frantz magnetic separator (only SRT1). A random selection of the total zircon population was mounted in epoxy and polished to expose the centers of the grains. Zircon regions suitable for analysis were identified from CL and back-scatter electron imaging. Zircon U-Pb geochronology in Sydney was performed using the method described by Adams et al. (2007). Spot size was 30 µm. Total ablation time was 60 s preceded by 60 s background measurement. Wash-out times were set to s. The reference zircons GJ-1, MT-1 (Mud Tank), and were used as standards (Wiedenbeck et al., 1995; Jackson et al., 2004). The U and Pb isotope data were processed offline using the in-house GLITTER software (Jackson et al., 2004). In Münster, the method outlined in Kooijman (2009) was used. The spot size was µm. Total ablation time was 55 s, which included 20 s with the shutter closed to measure the background. Wash-out times were set to 90 s for AP20, AP27 and Chm3. For all analyzes in AP25, measurements to in AP20 and 82.1 to in AP27, each spot was preablated with three laser shots using a 45 µm beam to remove surface common Pb. For these zircons, wash-out times were reduced to 45 s. External standardisation was done using the GJ-1 reference zircon (Jackson et al., 2004). Measurement of the standard zircon (Wiedenbeck et al. 1995) as unknown indicated a reproducibility of 2.5 % for 238 U and 3.0 % for 206 Pb. The U and Pb isotope data were processed offline using an in-house Excel spreadsheet (Kooijman, 2009). Common-Pb correction generally was applied to zircons having 204 Pb < 5,000 using the Pb evolution model of Stacey and Kramers (1975). For zircons older than 1000 Ma, 206 Pb ages were used for age calculation and 238 U ages were used for younger zircons. Isoplot/Ex 2.49 (Ludwig, 2001) was used for age calculations (assuming λ( 238 U) = 1.551*10-10 a -1 and λ( 235 U) = 9.849*10-10 a -1 ; Jaffey et al. 1971) and statistical treatment of U-Pb data from zircons of all analyzed samples. Probability curves were calculated using AgeDisplay/Ex (Sircombe, 2004). U-Pb data of the Santa Rosa de Tastil batholith (SRT1)* Isotope ratios Ages (Ma) Grain 208 Pb/ 208 Pb/.spot 232 Th 2σ 232 Th 2σ *Values in italics were not used for intrusion age calculation U-Pb data of the Mesón Group Grain #/~ 1 Round- Grain Grain Isotope ratios: Ages (Ma): Concordance 204 Pb 3 (%) 5 AP20 (Lizoite Fm.) 01.1 # sa-sr elongated ~ sa-sr round # euhedral oval * (93) 04.1 mix * (97) 05.1 # sa-sr round
2 Concordance 204 Pb 3 (%) * * # sa-sr round ~c sa-sr elongated * # sa-sr round * (101) * # sa-sr oval * # sa-sr round * # sa-sr elongated * ~ sa-sr elongated * # sa-sr elongated * # sa-sr oval * * # sa-sr elongated (103) 24.1 # sa-sr round n. d ~ sa-sr round (97) 26.1 mix ~ sa-sr oval # sa-sr elongated * # euhedral oval n. d # sa-sr oval * ~ sa-sr oval * # sa-sr elongated # sa-sr elongated # sa-sr round * # sa-sr round * (95) 38.1 # euhedral elongated * (93) 39.1 # sa-sr elongated * # sa-sr round * * # sa-sr elongated * (106) 44.1 # sa-sr round (105) 45.1 # sa-sr elongated # sa-sr round # sa-sr elongated * # sa-sr round * # euhedral oval * # sa-sr elongated * * # sa-sr round * # sa-sr round # sa-sr round * # sa-sr oval ~ sa-sr round * # sa-sr elongated # euhedral round * # sa-sr round * # sa-sr elongated * # sa-sr round * # sa-sr round * (104) 63.1 # sa-sr round * (109) 64.1 # sa-sr round # sa-sr round * # sa-sr round * (101) 70.1 # sa-sr elongated * * ~ sa-sr oval # sa-sr oval # euhedral elongated * ~ euhedral round # euhedral oval # sa-sr elongated (102) 79.1 # sa-sr round
3 Concordance 204 Pb 3 (%) * # sa-sr oval # sa-sr oval # euhedral oval * * # sa-sr oval * # sa-sr oval # sa-sr elongated (100) 91.1 # sa-sr elongated mix * # sa-sr elongated n. d # sa-sr elongated # sa-sr round * # sa-sr round # sa-sr oval * (94) 99.1 # euhedral round # sa-sr round # sa-sr round # sa-sr elongated * # sa-sr oval n. d # sa-sr elongated * # sa-sr round # sa-sr round # sa-sr oval # sa-sr oval (99) ~ sa-sr round * # sa-sr oval # sa-sr elongated * # rounded round * (94) * * # euhedral oval * # sa-sr elongated # sa-sr round * # sa-sr elongated n. d * # sa-sr oval (104) # sa-sr elongated * (97) # sa-sr round * # sa-sr round ~ sa-sr elongated (107) # euhedral oval * (94) # euhedral elongated # sa-sr elongated # sa-sr round # euhedral round # euhedral elongated * # sa-sr oval n. d # sa-sr elongated # euhedral elongated n. d # sa-sr oval n. d # sa-sr elongated
4 Concordance U 2σ U 2σ Pb 2σ Pb 3 U 2σ Pb 2σ (%) # euhedral elongated * # sa-sr elongated # euhedral oval # euhedral elongated mix # euhedral elongated # euhedral oval # euhedral elongated # euhedral elongated ~ sa-sr oval # euhedral elongated n. d # sa-sr oval n. d # euhedral elongated n. d ~ sa-sr elongated n. d * # sa-sr round n. d # euhedral elongated (92) ~ sa-sr round # sa-sr round * # sa-sr oval n. d mix n. d ~ sa-sr round # sa-sr elongated ~ sa-sr oval mix * # sa-sr elongated n. d # sa-sr round (93) mix * (106) * # sa-sr round * * ~ sa-sr oval # euhedral elongated * # sa-sr oval AP25 (Campanario Fm.) 02.1 # sa-sr oval # sa-sr elongated * # sa-sr elongated * # sa-sr round # sa-sr oval * # sa-sr oval # sa-sr elongated * # rounded round n. d # sa-sr elongated * ~ sa-sr elongated n. d (93) 23.1 # sa-sr round * # sa-sr oval * # sa-sr oval *
5 Concordance 204 Pb 3 (%) # rounded round # rounded round n. d * * # sa-sr oval n. d # sa-sr oval n. d.* n. d * * # sa-sr round # sa-sr elongated # rounded elongated mix ~ rounded oval ~ rounded round n. d # sa-sr elongated * # sa-sr oval # sa-sr elongated * ~ sa-sr oval ~ sa-sr oval * * # sa-sr elongated * * mix n. d # sa-sr round * (98) 79.1 # sa-sr round * # rounded elongated # euhedral round mix * # sa-sr oval * * # sa-sr round # sa-sr elongated * ~ sa-sr round * ~ rounded oval * # sa-sr elongated # sa-sr oval n. d #c sa-sr oval * * # rounded oval # sa-sr round n. d # euhedral elongated # sa-sr round n. d ~ sa-sr elongated # sa-sr oval * # sa-sr oval # euhedral oval # sa-sr oval
6 Concordance 204 Pb 3 (%) # sa-sr elongated * (103) # rounded elongated n. d # sa-sr oval # rounded elongated * (101) mix n. d # euhedral elongated ~ sa-sr round # rounded round mix * (94) # sa-sr oval (91) * * # sa-sr elongated * * # euhedral elongated * * ~ rounded oval * # euhedral oval * # sa-sr elongated n. d.* # sa-sr elongated * # sa-sr elongated * # euhedral elongated # rounded elongated * ~ sa-sr elongated * ~ sa-sr elongated ~ sa-sr round * # sa-sr round n. d # sa-sr round * # sa-sr elongated # sa-sr elongated * # sa-sr round * # rounded oval # sa-sr elongated * # sa-sr round # sa-sr elongated n. d ~ rounded elongated # sa-sr round * n. d mix n. d # sa-sr elongated # sa-sr oval # sa-sr oval * # sa-sr round # sa-sr oval # euhedral oval # sa-sr elongated n. d # rounded elongated mix * * ~ rounded round # rounded oval * # euhedral round * # sa-sr round n. d # sa-sr round *
7 Concordance 204 Pb 3 (%) # sa-sr elongated * # sa-sr elongated * ~ sa-sr round #c rounded oval * AP27 (Chalhualmayoc Fm.) # rounded round * # rounded elongated * #c sa-sr oval * # sa-sr round * * ~ rounded round * * * # sa-sr elongated * (93) 15.1 # sa-sr round * (109) 16.1 #c sa-sr oval * # rounded elongated # sa-sr elongated * * ~ sa-sr round n. d # sa-sr elongated # sa-sr round * (90) 24.1 # sa-sr oval * # sa-sr round (98) * # sa-sr oval # rounded elongated # sa-sr oval * # rounded elongated # sa-sr elongated * # sa-sr oval * # sa-sr round (104) 42.1 # sa-sr elongated ~ rounded round # sa-sr elongated # sa-sr elongated # rounded round # sa-sr elongated # sa-sr elongated # sa-sr round # sa-sr oval n. d.* # sa-sr round # sa-sr elongated n. d.* # rounded round # sa-sr round # rounded elongated (94) 63.1 # sa-sr elongated (99) 64.1 # sa-sr elongated (93) 66.1 # sa-sr oval (93) 67.1 ~ sa-sr round (99) - 7 -
8 Concordance 204 Pb 3 (%) # sa-sr oval # rounded round (91) # sa-sr oval # sa-sr round # rounded round n. d.* # sa-sr elongated # sa-sr elongated # sa-sr oval ~c sa-sr oval # sa-sr oval # sa-sr round n. d ~ rounded elongated n. d # sa-sr elongated ~ sa-sr round # sa-sr oval # rounded oval n. d # rounded elongated # rounded round n. d # sa-sr round * ~ sa-sr elongated n. d (93) 99.1 ~c rounded elongated # sa-sr round * * mix # sa-sr elongated n. d # sa-sr round * (110) # sa-sr round n. d # rounded oval # rounded round n. d # sa-sr round * # euhedral oval ~ sa-sr elongated n. d # rounded oval # sa-sr elongated # rounded elongated # sa-sr elongated n. d # sa-sr elongated n. d # sa-sr elongated * # sa-sr oval (93) ~ sa-sr elongated n. d # rounded elongated n. d # rounded round # rounded round * # sa-sr oval ~ sa-sr elongated * * # euhedral elongated # rounded elongated * # sa-sr round # sa-sr oval ~ sa-sr oval ~ rounded elongated n. d ~ sa-sr round
9 Concordance 204 Pb 3 (%) # sa-sr round ~ sa-sr round Chm3 (Chalhualmayoc Fm.) 01.1 ~ rounded elongated # sa-sr oval (95) 03.1 mix # sa-sr oval * # rounded round # sa-sr elongated n. d ~ sa-sr round #c rounded round n. d # sa-sr elongated # sa-sr elongated * # rounded round # rounded round # sa-sr elongated * ~ sa-sr round * ~ rounded elongated n. d # rounded elongated ~ rounded oval * # sa-sr oval # rounded oval n. d ~ rounded oval ~ sa-sr oval # sa-sr oval * ~ sa-sr oval ~ sa-sr elongated # sa-sr elongated # sa-sr round # rounded elongated n. d # sa-sr elongated * # sa-sr elongated * # sa-sr elongated ~ rounded elongated (95) 34.1 # sa-sr elongated # rounded oval ~c rounded oval ~ sa-sr oval * # sa-sr elongated n. d # rounded elongated mix ~ rounded elongated # rounded oval # sa-sr elongated # euhedral oval # rounded oval n. d # euhedral round ~ rounded oval # rounded elongated * # sa-sr elongated * # sa-sr oval * ~ rounded oval # rounded round n. d # sa-sr oval
10 Concordance 204 Pb 3 (%) # sa-sr round (101) 66.1 # sa-sr oval n. d # rounded round ~ rounded oval ~ sa-sr round (97) 70.1 mix * # sa-sr elongated (100) 73.1 # sa-sr oval (100) 74.1 # euhedral elongated # sa-sr elongated * # sa-sr oval ~ sa-sr oval ~ sa-sr elongated # sa-sr oval # rounded oval # sa-sr elongated # sa-sr elongated * # rounded oval # rounded oval (104) 86.1 ~ rounded elongated ~ sa-sr round * (94) 89.1 ~c sa-sr elongated # sa-sr oval # sa-sr oval * # sa-sr elongated ~ sa-sr oval * ~ sa-sr round (92) 97.1 # sa-sr elongated (102) 98.1 # euhedral round * (94) 99.1 # sa-sr oval # sa-sr round ~ sa-sr elongated * (92) ~ sa-sr elongated * ~ rounded oval * ~ rounded elongated (94) ~ sa-sr oval * (97) #c sa-sr round (95) # sa-sr oval # rounded oval (92) ~ sa-sr oval n. d.* ~ sa-sr round (96) mix # euhedral oval ~ rounded round * # euhedral round * * * # sa-sr elongated n. d # sa-sr elongated # rounded round n. d mix *
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