PRODUCT GUIDE AUTOMOTIVE, COMMERCIAL & INDUSTRIAL

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1 ENGINE OILS AUTOMOTIVE GEAR OILS TRANSMISSION/POWER FLUIDS GREASES INDUSTRIAL FLUIDS INDUSTRIAL GEAR OILS METALWORKING FLUIDS INDUSTRIAL GAS ENGINE OILS RAILROAD LUBRICANTS FUNCTIONAL PRODUCTS COMPRESSOR LUBRICANTS PROCESS OILS SMALL ENGINE OILS AUTOMOTIVE, COMMERCIAL & INDUSTRIAL PRODUCT GUIDE 2018 FC1

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3 2018 Edition This CITGO Lubricants product guide is your directory to CITGO fluids, greases and their applications Edition (Vol. 1) Products are not available at all source points. Please check product availability and container sizes for your normal source point(s). This CITGO Lubricants product guide is your directory to CITGO fluids, greases, and their applications. Technical information and assistance: Properties shown Product are Answer based Line on typical values for the product only and do not constitute a specification. The information contained herein is subject to change without notice. Pre-shipment Products inquiries: are not available at all source points. Please check product availability Order Management and container sizes for your normal source point(s) , option 1 Pricing, availability, post-shipment inquiries: For additional technical information on products, contact: Customer Service , Product option Answer 2 Line Properties shown are based on typical values for the product only and do not constitute a specification. The information contained herein is subject to change without notice. The information in this book is provided with no express or implied warranty but with good faith on the basis of the most accurate information available; CITGO accepts no liability for content errors or omissions, or for damages as a result of relying on information contained within. Consult your owner s manual for proper lubricant selection CITGO Petroleum Corporation. All rights reserved. Please visit for the most up-to-date Please information visit on products or for Safety for the Data most Sheets. Consult up-to-date your information owner s manual on products for proper or for lubricant Safety Data selection. Sheets. i

4 Lubricants Business Unit Quality Statement CITGO Lubricants is committed to providing our customers with the highest quality products and services. This will be accomplished by: Satisfying mutually agreed upon expectations and customer requirements. Focusing on quality, employee involvement and continuous improvement of our processes. Establishing and maintaining an effective quality management system in compliance with ISO Certifications Achieved and Maintained ISO 9001 CITGO Lubricant Plants ISO 9001 LubeAlert Oil Analysis Program ii

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6 TABLE OF CONTENTS ENGINE OILS PCMO CITGO SUPERGARD European Formula Motor Oils... 1 CITGO SUPERGARD Motor Oils CITGO SUPERGARD UltraLife Motor Oils CITGO SUPERGARD Synthetic INTL Motor Oils CITGO SUPERGARD Synthetic Blend Motor Oils CITGO SUPERGARD Full Synthetic Motor Oils CITGO SUPERGARD Full Synthetic 0W-16 Motor Oils HDEO CITGO CITGARD 500 Engine Oil CITGO CITGARD 500 HSN Engine Oils Monogrades. 13 CITGO CITGARD 500 HSN Engine Oil SAE 15W CITGO CITGARD 500 HSN Engine Oil SAE 20W CITGO CITGARD HD Engine Oil CITGO CITGARD 600 Engine Oils Multi-Viscosity CITGO CITGARD 600 Engine Oils Monogrades CITGO CITGARD 700 Synthetic Blend Engine Oils CITGO CITGARD 700 MFE Synthetic Blend Engine Oil CITGO CITGARD SynDurance PLUS Synthetic Heavy Duty Engine Oils CITGO CITGARD CNG/LNG Engine Oill Small Engine Oils CITGO Multi-Purpose Air-Cooled 2-Cycle Engine Oil CITGO SUPERGARD Air-Cooled 2-Cycle Engine Oil CITGO SUPERGARD Marine Plus 2-Cycle Engine Oil CITGO SUPERGARD Sea & Snow 2-Cycle Engine Oil AUTOMOTIVE GEAR OILS CITGO CITGEAR HD Synthetic Gear Lubricants CITGO Synthetic Gear Lubricants CITGO Syndurance Synthetic MTF CITGO Premium (LS) Gear Oil CITGO Premium Gear Oils (MP) CITGO Regular Gear Oil CITGO SUPERGARD Marine Plus Lower Unit Gear Lubricant TRANSMISSION/POWER FLUIDS CITGO Final Drive Oil CITGO Power Steering Fluid with Stop Leak CITGO QuatraSyn Synthetic Transmission Fluid Emgard 2805 ATF CITGO TRANSGARD ATF, MECRON V CITGO TRANSGARD ATF, Type F CITGO TRANSGARD ATF CITGO TRANSGARD CVT Fluid CITGO TRANSGARD DEXRON -VI ATF CITGO TRANSGARD Heavy Duty Transmission Fluids CITGO SynDurance Synthetic All Seasons Heavy-Duty Transmission Fluid CITGO TRANSGARD Multi-Purpose ATF CITGO TRANSGARD Synthetic Multi-Vehicle High Viscosity ATF CITGO TRANSGARD Synthetic Multi Vehicle Low Viscosity ATF CITGO TRANSGARD Tractor Hydraulic Fluids GREASES CITGO Aluminum Complex PL Grease CITGO Calsuplex MP Grease CITGO Cotton Picker Spindle Grease CITGO Jet Lubricant TM CITGO Lithoplex CM & HM Greases CITGO Lithoplex MP Greases CITGO Lithoplex PM Grease CITGO Lithoplex Red MP Grease CITGO Lithoplex RT Greases CITGO Lithoplex ST Greases CITGO Lithoplex PL Greases CITGO Lithoplex PTG Grease CITGO Lithoplex PTG WPM No CITGO OverDrive HD Grease CITGO Premium Coupling Grease CITGO Premium Lithium EP Greases CITGO Railroad Curve Greases CITGO Supergard Marine Plus Grease CITGO SynDurance Premium Synthetic 460 Grease #00 Red CITGO SynDurance Premium Synthetic 460 Greases CITGO SynDurance ST Synthetic Greases CITGO UltraLife CSEP 5M Grease INDUSTRIAL FLUIDS CITGO Amplex Oils CITGO Sentry Oils CITGO Pacemaker Oils CITGO Pacemaker T Oils CITGO Pacemaker ST Continued iii

7 TABLE OF CONTENTS (Cont d.) CITGO HyDurance AW Fluids CITGO HyDurance AW AII Temp Fluids CITGO HyDurance AW CP Fluids CITGO HyDurance AW NZ Fluids CITGO HyDurance AW Super NZ Fluid CITGO HyDurance AW Synthetic Fluids CITGO HyDurance AW/AL HVI CITGO AW Hydraulic Oils CITGO AW Hydraulic Oils Super MV CITGO AW 68 Mining Hydraulic Oil CITGO ELO CITGO FR WG-40XD Hydraulic Fluid CITGO Glycol FR-5046HP CITGO Cylinder Oils INDUSTRIAL GEAR OILS CITGO EP Compounds CITGO CITGEAR Synthetic EP Lubricants CITGO CITGEAR Synthetic HT Lubricants CITGO CITGEAR Synthetic PAG Gear Fluids CITGO EP Gear Semi Synthetic CITGO CITGEAR WT CITGO CITGEAR XCO Oils CITGO Pacemaker SD Oils CITGO CITGEAR MGW-OGL METALWORKING FLUIDS CITGO Autokut AS Series CITGO Autokut IS Series CITGO Autokut Extrusion Oil CITGO Autokut Tri-Purpose CITGO Trukut GP CITGO Trukut HD CITGO CITCOOL SS-HD CITGO CITCOOL CITGO RUST-O-LENE LT CITGO RUST-O-LENE ST CITGO AR Slushing Oil CITGO Quenchol CITGO Sliderite Oils CITGO Tul-Kut Oil Base Cutting Oil Concentrate INDUSTRIAL GAS ENGINE OILS CITGO Pacemaker Gas Engine Oil 15SL CITGO Pacemaker Gas Engine Oil 700 Series CITGO Pacemaker Gas Engine Oil 800 Series CITGO Pacemaker Gas Engine Oil 1000 Series CITGO Pacemaker Gas Engine Oil 1200 Series CITGO Pacemaker Gas Engine Oil 1600 Series CITGO Pacemaker Gas Engine Oil 1700 Series CITGO Pacemaker Gas Engine Oil 1900 XL Series CITGO Pacemaker Gas Engine Oil LFG LA RAILROAD LUBRICANTS CITGO Railroad Car Journal Oil No CITGO RD-969 and RD-1069 Diesel Engine Oils CITGO RD-2069 LE Diesel Engine Oil FUNCTIONAL PRODUCTS CITGO Diamond Oils CITGO Hydraulic/Press Oil CITGO Press Oil CITGO Hytherm Oil CITGO Ice Machine Oil CITGO North Star Refrigeration Oils CITGO North Star Refrigeration Oil CITGO Bar and Chain Oil CITGO Concrete Form Oil CITGO SATISOL Concrete Form Release CITGO Rock Drill Oils CITGO Wireline Lubricants COMPRESSOR LUBRICANTS CITGO CompKleen Synthetic Cleaner CITGO Compressor Oil 35LP and 45LP CITGO Compressor Oil CITGO CompressorGard DE CITGO CompressorGard GE CITGO CompressorGard H Series CITGO CompressorGard IPG CITGO CompressorGard PAG CITGO CompressorGard PAO CITGO CompressorGard PS 68 Fluid CITGO CompressorGard SS CITGO CompressorGard XA CITGO Gascom R Oil CITGO Pacemaker HV Oils PROCESS OILS CITGO Procoil Oils REFERENCE INFORMATION API guide to certification marks, service symbols & categories (CJ-4 & prior) HDEO Cross Reference Chart SAE J300 viscosity grades for engine oil SAE J306 automotive gear viscosity classification iv

8 CITGO Grease Characteristics Chart NLGI Grease Classifications ASTM D 4950 Classification & Specifications for Automotive Service Greases Grease Thickener Compatibility Guide to synthetic industrial lubricants Compatibility of common elastomers with CITGO products chart Compressor OEM fluid cross reference Understanding ISO cleanliness Particle counting accuracy Use of fire resistant hydraulic fluids Water glycols compatibility Comparative viscosity classifications, ISO & AGMA Viscosity blending chart Metalworking Product Application Guide - Water Miscible Products Metal removing Product Application Guide - Straight Oils Metal removal product offering Metallurgy and machinability Stationary natural gas engine oil cross reference Stationary natural gas compressor lubricant chart Stationary natural gas compressor application chart Pacemaker GEO application chart EPA amendments to RICE NESHAP CITGO sensitive products list GHS label compliance Lubricant storage How to take a sample Glossary of common terms & acronyms Products by 40C Viscosity Approximate Equivalence of Viscosity Grading Systems TABLE OF CONTENTS (Cont d.) PRODUCT INDEX v

9 CITGO SUPERGARD EUROPEAN FORMULA MOTOR OILS Date 04/18 DESCRIPTION: CITGO SUPERGARD European Formula Motor Oils are premium quality, high performance full synthetic oils formulated for use in certain European vehicles. These specially crafted formulations contain well-balanced combinations of today s highest quality synthetic base stocks and advanced additive systems specifically designed to provide superior performance and protection under the most demanding driving conditions. PCMO Engine Oils QUALITIES: APPLICATIONS: Excellent low-temperature starting and pumpability characteristics High-temperature/high-shear properties well above conventional oils Extended drain interval capabilities Lower volatility when compared to conventional oils Excellent thermal and oxidation stability Enhanced protection against varnish buildup and sludge formation in critical engine parts for top performance and long engine life Extended engine life due to control of wear and deposit formation For use in certain Audi, BMW, Mercedes Benz, Porche, Volkswagen and other European vehicles SAE 5W-40 approved under VW Standard and VW Standard Consult owner s manual for proper fluid specifications. TYPICAL PROPERTIES: CITGO SUPERGARD EUROPEAN FORMULA MOTOR OILS SAE Grade 5W-30 5W-40 Material Code Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, ASTM D92, F ( C), COC 442 (228) 450 (232) Low Temperature Cranking, ASTM D5293 Temperature, F ( C) -22 (-30) -22 (-30) Viscosity, cp 6,030 5,935 Viscosity ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -49 (-45) -51 (-46) Color, ASTM D1500 L2.5 L3.0 API SN Yes Yes OEM Approvals: VW , Yes VW , Pending BMW Longlife-01 Pending BMW Longlife-04 Pending Mercedes Benz Pending Mercedes Benz Pending CITGO and SUPERGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

10 PCMO Engine Oils CITGO SUPERGARD MOTOR OILS Date 04/18 DESCRIPTION: CITGO SUPERGARD Motor Oils are premium quality engine oils designed to provide optimum performance in high-output gasoline (including turbocharged and supercharged) engines in passenger cars, vans, sport utility vehicles, and light trucks. The new technology incorporated in this latestgeneration lubricant enables it to exceed manufacturers performance requirements. These engine oils demonstrate improved performance in today s advanced engine designs. CITGO SUPERGARD is available in both single and multigrades. The SAE 5W-20 and SAE 5W-30 are classified as synthetic blends. QUALITIES: SERVICE CATEGORIES: APPLICATIONS: Exceed latest SAE low-temperature pumping viscosity requirements. Provide improved performance in foaming control. Provide significantly greater engine cleanliness, wear protection and resistance to oil thickening. Protect against varnish buildup and sludge formation on critical engine parts. Control high-temperature deposits in critical ring belt area. Provide maximum protection against rust and corrosion. Meet SAE standards for high-temperature/high-shear rate viscosity. Extend engine life by controlling wear and deposit formation. All viscosity grades are licensed for API SN and are backward compatible with prior API Service Categories (SM, SL, SJ and SH). SAE 5W-20 and SAE 5W-30 are synthetic blends with API SN, Resource Conserving and ILSAC GF-5. SAE 10W-30 API SN, Resource Conserving and ILSAC GF-5. SAE 5W-20 and 5W-30 Meet the performance requirements of Ford WSS-M2C 930-A and M2C929-A respectively. SAE 5W-20 Meets the performance requirements of Honda SAE 5W-20 specification. SAE 5W-30, 5W-20 Meets the performance requirements of General Motors GM6094M. Military CID: A-A (Commercial Item Description, supercedes MIL-L-46152). CITGO SUPERGARD Motor Oils are recommended for passenger cars, sport utility vehicles, and light trucks operating on gasoline. CITGO SUPERGARD Motor Oils are also recommended for use in gasoline engines which have been converted to operate on compressed natural gas (CNG), liquified natural gas (LNG), and liquified petroleum gas (LPG which includes propane and butane). Consult the vehicle owner s manual for proper engine lubricant selection. CITGO SUPERGARD SAE 5W-20 and 5W-30 are synthetic blends incorporating a high percentage of synthetic components and meet the performance requirements for latest gasoline-fueled engine service and display the API Certification Mark. SAE 5W-20, 5W-30, and 10W-30 have also demonstrated benefits in industry accepted fuel economy tests. Note: CITGO SUPERGARD Motor Oils are not recommended for use in diesel engines. CITGO CITGARD Motor Oils are recommended for diesel applications. (Continued) C

11 CITGO SUPERGARD MOTOR OILS Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: PCMO Engine Oils CITGO SUPERGARD MOTOR OILS SAE Grade 5W-20 5W-30 10W-30 10W-40 20W Material Code Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, ASTM D92, COC, F ( C) 439 (226) 442 (228) 450 (232) 453 (234) 473 (245) 489 (254) 500 (260) Low Temperature Cranking, ASTM D5293 Temperature, F ( C) -22 (-30) -22 (-30) -13 (-25) -13 (-25) 5 (-15) Viscosity, cp 5,970 5,200 5,770 6,000 6,120 Viscosity: ASTM D445, cst at 40 C ASTM D 445,cSt at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -33 (-36) -38 (-39) -33 (-36) -33 (-36) -27 (-33) -22 (-30) 0 (-18) Color, ASTM D 1500 L3.5 L3.5 L3.5 L3.5 L3.5 L3.5 L4.0 API Service Category SN SN SN SN SN SN SN API Certification Mark Yes Yes Yes No No No No Resource Conserving Yes Yes Yes No No No No CITGO and SUPERGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

12 PCMO Engine Oils CITGO SUPERGARD ULTRALIFE MOTOR OILS Date 03/18 DESCRIPTION: CITGO SUPERGARD UltraLife Motor Oils are premium quality engine oils designed to improve the life of older, higher-mileage engines. They will provide optimum performance in higher mileage gasoline engines including turbocharged and supercharged engines found in passenger cars, vans, sport utility vehicles, and light trucks. These oils are formulated with highly refined base oils and additive systems that will handle those problems associated with older, higher-mileage engines that have exceeded their warranty. BENEFITS: APPLICATIONS: CITGO SUPERGARD UltraLife Motor Oils benefits your engine in the following ways: Provides extra wear protection Provides improved seal conditioning to help reduce oil leakage and valve deposits Offers excellent resistance to oil burn-off Provides extra cleaning to critical engine parts Helps improve overall engine performance Offers excellent oxidation and thermal stability to help maintain engine cleanliness and deposit formation Consult the owner s manual for proper lubricant selection. CITGO SUPERGARD UltraLife Motor Oils are recommended for the older higher mileage, rebuilt, and new passenger cars, sport utility vehicles and light trucks operating on gasoline. CITGO SUPERGARD UltraLife Motor Oils are available in SAE 5W-20, 5W-30, 10W-30, and 10W-40 grades, are licensed for API SN, and are backward compatible with prior API Service Categories (SM, SL and SJ). Additionally, the SAE 5W-20, 5W-30 and SAE 10W-30 grades are licensed ILSAC GF-5 Resource Conserving. TYPICAL PROPERTIES: CITGO SUPERGARD ULTRALIFE MOTOR OILS SAE Grade 5W-20 5W-30 10W-30 10W-40 Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash point, COC, ASTM D92, F ( C) 450 (232) 450 (232) 450 (232) 453 (234) Viscosity ASTM D445, cst at 40 C cst at 100 C Viscosity Index Pour Point, ASTM D97, F ( C) -42 (-41) -38 (-39) -44 (-42) -38 (-39) Low Temperature Cranking at -22 F (-30 C), ASTM D5293, cp 6,280 6,250 Low Temperature Cranking at -13 F (-25 C), ASTM D5293, cp 6,180 6,080 Low Temperature Pumping at -31 F (-35 C), ASTM D4684, cp 21,200 29,300 Low Temperature Pumping at -22 F (-30 C), ASTM D4684, cp 23,200 31,500 Yield Stress, Pa <35 <35 <35 <35 CITGO, SUPERGARD and UltraLife are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

13 DESCRIPTION: P R O D U C T I N F O R M A T I O N CITGO SUPERGARD SYNTHETIC INTL MOTOR OILS Date 04/18 CITGO SUPERGARD Synthetic Motor Oils are well-balanced combinations of today s highest quality synthetic base stocks and contain an advanced additive system that meets stringent automotive specifications. They are designed to provide excellent protection in today s high performance gasoline (including turbocharged and supercharged) engines in passenger cars, vans, sport utility vehicles, and light trucks. These synthetic engine oils demonstrate improved performance in today s advanced engine designs, and are available in SAE 0W-20, 5W-20 and 5W-30 viscosity grades. PCMO Engine Oils QUALITIES: APPLICATIONS: Excellent low-temperature starting and pumpability characteristics High-temperature/high-shear properties well above conventional oils Lower volatility when compared to conventional oils Excellent thermal and oxidation stability Enhanced protection against varnish buildup and sludge formation in critical engine parts for top performance and long engine life Extended engine life due to control of wear and deposit formation Compatible with conventional and synthetic motor oils CITGO SUPERGARD Synthetic Motor Oils are recommended for passenger cars, sport utility vehicles and light trucks operating on gasoline. They are also recommended for use in gasoline engines which have been converted to operate on compressed natural gas (CNG), liquified natural gas (LNG), and liquified petroleum gas (LPG-which includes propane and butane). Consult the vehicle owner s manual for proper engine lubricant selection. CITGO SUPERGARD Synthetic Motor Oils meet the performance requirements for the latest gasoline-fueled engine service ILSAC GF-5/Resource Conserving and API SN and display the API Certification Mark and API Service Symbol. They have also demonstrated benefits in industry accepted fuel economy tests. NOTE: CITGO SUPERGARD Synthetic Motor Oils are not recommended for use in diesel engines in passenger cars, vans or light trucks. CITGO CITGARD Motor Oils are recommended for these applications. (Continued) (Continued) CITGO Petroleum Corporation 800/ Houston, Texas Manufactured in in USA USA C

14 PCMO Engine Oils CITGO SUPERGARD SYNTHETIC INTL MOTOR OILS Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO SUPERGARD SYNTHETIC INTL MOTOR OILS SAE GRADE 0W-20 5W-20 5W-30 Material Code Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, ASTM D92, F ( C), COC 428 (220) 442 (228) 450 (232) Low Temperature Cranking, ASTM D5293 Temperature, F ( C) -31 (-35) -22 (-30) -22 (-30) Viscosity, cp 5,190 5,300 4,080 Viscosity, ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -33 (-36) -33 (-36) -27 (-33) Color, ASTM D1500 L3.5 L3.5 L3.5 ILSAC GF-5 Yes Yes Yes API SN Yes Yes Yes Resource Conserving Yes Yes Yes dexos1 Licensed No No No CITGO and SUPERGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. CITGO Petroleum Corporation 800/ Houston, Texas Manufactured in in USA USA C

15 CITGO SUPERGARD SYNTHETIC BLEND SAE 10W-30 and 10W-40 MOTOR OIL Date 04/18 DESCRIPTION: CITGO SUPERGARD Synthetic Blend Motor Oils (SAE 10W-30 and 10W-40) are premium engine oils designed to provide optimum performance in high-output gasoline (including turbocharged and supercharged) engines in passenger cars, vans, sport utility vehicles, and light trucks. The new technology incorporated in these latest-generation lubricants enable them to exceed manufacturers performance requirements. These engine oils demonstrate improved performance in today s advanced engine designs. PCMO Engine Oils QUALITIES: APPLICATIONS: Licensed for API SN. Exceeds latest SAE low-temperature pumping viscosity requirements. Provides improved performance in foaming control. Provides significantly greater engine cleanliness, wear protection and resistance to oil thickening. Protects against varnish buildup and sludge formation on critical engine parts. Controls high-temperature deposits in critical ring belt area. Provides maximum protection against rust and corrosion. Meets SAE standards for high-temperature/high-shear rate viscosity. Extends engine life by controlling wear and deposit formation. CITGO SUPERGARD Synthetic Blend Motor Oils (SAE 10W-30 and 10W-40) are recommended for passenger cars, sport utility vehicles, and light trucks operating on gasoline. Consult the vehicle owner s manual for proper engine lubricant selection. Note: This motor oil is not recommended for use in diesel engines. TYPICAL PROPERTIES: CITGO SUPERGARD SYNTHETIC BLEND MOTOR OILS SAE Grade 10W-30 10W-40 Material Code Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, ASTM D92, COC, F ( C) 450 (232) 453 (234) Low Temperature Cranking, ASTM D5293 Temperature, F ( C) -13 (-25) -13 (-25) Viscosity, cp 5,450 5,700 Viscosity: ASTM D445, cst at 40 C ASTM D 445,cSt at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -44 (-42) -27 (-33) Color, ASTM D1500 L3.0 L3.5 API Service Category SN/ILSAC GF-5 SN CITGO and SUPERGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

16 PCMO Engine Oils CITGO SUPERGARD FULL SYNTHETIC MOTOR OILS Date 03/18 DESCRIPTION: CITGO SUPERGARD Full Synthetic Motor Oils are well-balanced combinations of today s highest quality synthetic base stocks and contain an advanced additive system that meets stringent automotive specifications. They are designed to provide excellent protection in today s high performance gasoline (including turbocharged and supercharged) engines in passenger cars, vans, sport utility vehicles, and light trucks. These synthetic engine oils demonstrate improved performance in today s advanced engine designs, and are available in SAE 0W-16, 0W-20, 5W-20, 5W-30 and 10W -30 viscosity grades. QUALITIES: APPLICATIONS: Excellent low-temperature starting and pumpability characteristics High-temperature/high-shear properties well above conventional oils Lower volatility when compared to conventional oils Excellent thermal and oxidation stability Enhanced protection against varnish buildup and sludge formation in critical engine parts for top performance and long engine life Extended engine life due to control of wear and deposit formation Compatible with conventional and synthetic motor oils Protect engines from Low Speed Pre-ignition (LSPI) occurring CITGO SUPERGARD Full Synthetic Motor Oils are recommended for passenger cars, sport utility vehicles and light trucks operating on gasoline. They are also recommended for use in gasoline engines which have been converted to operate on compressed natural gas (CNG), liquified natural gas (LNG), and liquified petroleum gas (LPG-which includes propane and butane). Consult the vehicle owner s manual for proper engine lubricant selection. CITGO SUPERGARD Full Synthetic Motor Oils meet the performance requirements for the latest gasoline-fueled engine service ILSAC GF-5/Resource Conserving (excludes SAE 0W-16) and API SN and display the API Certification Mark and API Service Symbol. They have also demonstrated benefits in industry accepted fuel economy tests. CITGO SUPERGARD Full Synthetic SAE 0W-16 Motor Oil is an ultra-low viscosity engine oil and is recommended for Original Equipment Manufacturers (OEM) such as Toyota and Honda where a SAE 0W-16 is specified. CITGO SUPERGARD Full Synthetic SAE 0W-20 is recommended for Original Equipment Manufacturers (OEM) such as Toyota and Honda where a SAE 0W-20 is specified. CITGO SUPERGARD Full Synthetic SAE 0W-20, under material code , is Approved GM dexos1 Gen2 License D10393HF121. CITGO SUPERGARD Full Synthetic SAE 5W-20 is Approved GM dexos1 Gen2 License D10745HL121 and provides excellent performance where Ford WSS-M2C945-A is referenced. CITGO SUPERGARD Full Synthetic SAE 5W-30 is Approved GM dexos1 Gen2 License D10373HF121and provides excellent performance where Ford WSS-M2C946-A is referenced. CITGO SUPERGARD Full Synthetic SAE 10W-30 provides excellent performance where a SAE 10W-30 engine oil is specified. NOTE: CITGO SUPERGARD Full Synthetic Motor Oils are not recommended for use in diesel engines. CITGO CITGARD Motor Oils are recommended for these applications. Consult your owner s manual for proper lubricant selection. (Continued) C

17 CITGO SUPERGARD FULL SYNTHETIC MOTOR OILS Date 03/18 - (Continued) TYPICAL PROPERTIES: PCMO Engine Oils CITGO SUPERGARD FULL SYNTHETIC MOTOR OILS SAE Grade 0W-16 0W-20 0W-20 5W-20 5W-30 10W-30 (dexos1 ) (dexos1 ) (dexos1 ) Gen2) Gen2) Gen2) Material Code Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, ASTM D92, 442 (228) 435 (220) 428 (220) 442 (228) 450 (232) 450 (232) F ( C), COC Low Temperature Cranking, ASTM D5293 Temperature, F ( C) -31 (-35) -31 (-35) -31 (-35) -22 (-30) -22 (-30) -13 (-25) Viscosity, cp 5,770 5,330 5,190 3,500 4,320 4,000 Viscosity, ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -38 (-39) -49 (-45) -33 (-36) -44 (-42) -27 (-33) -27 (-33) Color, ASTM D1500 L3.5 L3.5 L3.5 L3.5 L3.5 L3.5 ILSAC GF-5 Yes Yes Yes Yes Yes API SN Yes Yes Yes Yes Yes Yes Licensed GM dexos1 Gen2 N/A Yes Yes Yes N/A CITGO and SUPERGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

18 PCMO Engine Oils CITGO SUPERGARD FULL SYNTHETIC SAE 0W-16 MOTOR OIL Date 04/18 DESCRIPTION: CITGO SUPERGARD Full Synthetic 0W-16 Motor Oil is an ultra-low viscosity engine oil made with a well-balanced combination of today s highest quality synthetic base stocks and advanced additives. The lubricant is formulated to achieve minimal friction, wear and fuel consumption while providing excellent cold start pumpability. The excellent cold start performance ensures optimum lubrication reliability in extreme cold. Improved fuel economy is achieved thanks to the smooth-running properties of the new SAE category 0W-16. QUALITIES: Excellent low-temperature starting and pumpability characteristics High-temperature/high-shear properties much improved over conventional oils Lower volatility when compared to conventional oils Excellent thermal and oxidation stability Enhanced protection against varnish buildup and sludge formation in critical engine parts for top performance and long engine life Extended engine life due to control of wear and deposit formation Compatible with conventional and synthetic motor oils APPLICATIONS: CITGO SUPERGARD Full Synthetic 0W-16 Motor Oil is designed to provide excellent protection in, and are recommended for, today s high performance gasoline (including turbocharged and supercharged) engines in passenger cars, vans, sport utility vehicles, and light trucks. Consult the vehicle owner s manual for proper engine lubricant selection. NOTE: CITGO SUPERGARD Full Synthetic Motor Oils are not recommended for use in diesel engines. CITGO CITGARD Motor Oils are recommended for these applications. (Continued) CITGO Petroleum Corporation 800/ Houston, Texas Manufactured in in USA USA C

19 CITGO SUPERGARD FULL SYNTHETIC SAE 0W-16 MOTOR OIL Date 04/18 - (Continued) TYPICAL PROPERTIES: PCMO Engine Oils CITGO SUPERGARD FULL SYNTHETIC 0W-16 MOTOR OIL SAE Grade 0W-16 Material Code Gravity, ASTM D4052, API 32.3 Pounds Per Gallon Flash Point, ASTM D92, F ( C), COC 442 (228) Low Temperature Cranking, ASTM D5293 Temperature, F ( C) -31 (-35) Viscosity, cp 5,770 Viscosity, ASTM D445 cst at 40 C 37.0 cst at 100 C 7.2 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -38 (-39) Color, ASTM D1500 L3.5 API SN Yes CITGO and SUPERGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. CITGO Petroleum Corporation 800/ Houston, Texas Manufactured in in USA USA C

20 HDEO Engine Oils CITGO CITGARD 500 ENGINE OIL Date 04/18 DESCRIPTION: CITGO CITGARD 500 Engine Oil SAE 25W-60 is specially formulated and engineered for diesel engines operating in severe conditions requiring extra protection to maintain engine cleanliness and wear protection. CITGO CITGARD 500 Engine Oil SAE 25W-60 is also excellent for higher mileage or older diesel engines by providing improved engine cylinder liner oil film retention that improves piston ring and liner sealing resulting in reduced oil consumption and improved engine efficiency. QUALITIES: APPLICATIONS: CITGO CITGARD 500 Engine Oil SAE 25W-60 is formulated with a balanced base oil and additive combination to deliver balanced protection. The formulation provides added corrosive wear protection to neutralize the harmful effects of fuel sulfur acid. The SAE 25W-60 multi-grade maintains a stable viscosity and protective oil film when operating at higher loads and temperatures. The performance benefits include overall engine cleanliness, reduced oil consumption and higher sulfur fuel neutralization. CITGO CITGARD 500 Engine Oil SAE 25W-60 is recommended for diesel engines operating in a variety of severe conditions and an excellent choice for such transit bus applications and other fleet operations that can benefit from a high performance diesel engine oil. TYPICAL PROPERTIES: CITGO CITGARD 500 ENGINE OIL SAE 25W-60 SAE Grade 25W-60 Material Code Gravity, ASTM D4052, API 27.7 Density, lbs/gal at 60 F 7.40 Flash Point, ASTM D92 (COC), F ( C) 500 (260) Viscosity ASTM D445, cst at 40 C 248 cst at 100 C 23.9 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -17 (-27) Sulfated Ash, ASTM D874, m% 1.15 Total Base Number, ASTM D2896, mg KOH/g 10 CITGO and CITGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

21 CITGO CITGARD 500 HSN ENGINE OILS MONOGRADES Date 04/18 DESCRIPTION: CITGO CITGARD 500 HSN Engine Oils SAE 40 and SAE 50 are specially formulated and engineered for diesel engines operating in severe conditions requiring extra protection to maintain engine cleanliness and wear protection. CITGO CITGARD 500 HSN Engine Oils SAE 40 and SAE 50 are also excellent choices for higher mileage or older diesel engines operating in warmer climates. The additive technology provides improved engine cylinder liner oil film retention that improves piston ring and liner sealing resulting in reduced oil consumption and improved engine efficiency. HDEO Engine Oils QUALITIES: APPLICATIONS: CITGO CITGARD 500 HSN Engine Oils SAE 40 and SAE 50 are formulated with a balanced base oil and additive combination to deliver balanced protection. The higher TBN (Total Base Number) formulation provides added corrosive wear protection to neutralize the harmful effects of fuel sulfur acid. The performance benefits include overall engine cleanliness, reduced oil consumption and higher sulfur fuel neutralization. CITGO CITGARD 500 HSN Engine Oils SAE 40 and SAE 50 are recommended for diesel engines operating in a variety of severe conditions and an excellent choice for transit bus applications and other fleet operations that can benefit from a high performance diesel engine oil. TYPICAL PROPERTIES: CITGO CITGARD 500 HSN ENGINE OILS MONOGRADES SAE Grade Material Code Gravity, ASTM D4052, API Density, lbs/gal at 60 F Flash Point, ASTM D92 (COC), F ( C) 486 (252) 482 (250) Viscosity ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -22 (-30) -27 (-33) Sulfated Ash, ASTM D874, m% Total Base Number, ASTM D2896, mg KOH/g CITGO and CITGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

22 HDEO Engine Oils CITGO CITGARD 500 HSN ENGINE OIL SAE 15W-40 Date 04/18 DESCRIPTION: CITGO CITGARD 500 HSN Engine Oil SAE 15W-40 is specially formulated for turbo charged diesel engines operating in severe conditions and using higher sulfur fuel. CITGO CITGARD 500 HSN Engine Oil SAE 15W-40 is designed to provide improved performance for older engines and newer engines that are not equipped with diesel particulate filters. QUALITIES: PERFORMANCE CAPABILITIES: APPLICATIONS: CITGO CITGARD 500 HSN Engine Oil SAE 15W-40 is formulated with a balanced base oil and additive combination to deliver optimum performance.in the critical areas of lubrication. The higher TBN (Total Base Number) formulation provides added corrosive wear protection to neutralize the harmful effects of fuel sulfur acid. The SAE 15W-40 multi-grade maintains a stable viscosity and protective oil film when operating at higher loads and temperatures. The performance benefits include overall engine cleanliness, reduced oil consumption and improved engine cold cranking start up protection. Equipment requiring API CI-4/SL Cummins CES Caterpillar ECF-2 CITGO CITGARD 500 HSN Engine Oil SAE 15W-40 is recommended for turbocharged and naturally aspirated diesel engines operating with higher sulfur fuel. TYPICAL PROPERTIES: CITGO CITGARD 500 HSN ENGINE OIL SAE 15W-40 SAE Grade 15W-40 API Service Category CI-4/SL Material Code Gravity, ASTM D4052, API 30.0 Density, lbs/gal at 60 F 7.30 Flash Point, ASTM D92 (COC), F ( C) 450 (232) Viscosity ASTM D445, cst at 40 C 120 cst at 100 C 15.8 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -38 (-39) Sulfated Ash, ASTM D874, m% 1.3 Total Base Number, ASTM D2896, mg KOH/g 11.3 CITGO and CITGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

23 CITGO CITGARD 500 HSN ENGINE OIL SAE 20W-50 Date 04/18 DESCRIPTION: CITGO CITGARD 500 HSN Engine Oil SAE 20W-50 is specially formulated and engineered for diesel engines operating in severe conditions requiring extra protection to maintain engine cleanliness and wear protection. CITGO CITGARD 500 HSN Engine Oil SAE 20W-50 is also an excellent choice for higher mileage or older diesel engines. It provides improved engine cylinder liner oil film retention that improves piston ring and liner sealing resulting in reduced oil consumption and improved engine efficiency. HDEO Engine Oils QUALITIES: APPLICATIONS: CITGO CITGARD 500 HSN Engine Oil SAE 20W-50 is formulated with a balanced base oil and additive combination to deliver balanced protection. The higher TBN (Total Base Number) formulation provides added corrosive wear protection to neutralize the harmful effects of fuel sulfur acid. The SAE 20W-50 multi-grade maintains a stable viscosity and protective oil film when operating at higher loads and temperatures. The performance benefits include overall engine cleanliness, reduced oil consumption and higher sulfur fuel neutralization. CITGO CITGARD 500 HSN Engine Oil SAE 20W-50 is recommended for diesel engines operating in a variety of severe conditions and an excellent choice for transit bus applications and other fleet operations that can benefit from a high performance diesel engine oil. TYPICAL PROPERTIES: CITGO CITGARD 500 HSN ENGINE OIL SAE 20W-50 SAE Grade 20W-50 Material Code Gravity, ASTM D4052, API 28.7 Density, lbs/gal at 60 F 7.36 Flash Point, ASTM D92 (COC), F ( C) 471 (244) Viscosity ASTM D445, cst at 40 C 164 cst at 100 C 18.6 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -44 (-42) Sulfated Ash, ASTM D874, m% 1.3 Total Base Number, ASTM D2896, mg KOH/g 11 CITGO and CITGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

24 HDEO Engine Oils CITGO CITGARD HD ENGINE OIL Date 04/18 DESCRIPTION: QUALITIES: CITGO CITGARD HD Engine Oil is a heavy duty engine oil designed for both older and newer diesel engines equipped with low emission technology. CITGARD HD Engine Oil is recommended for equipment owners operating within normal duty cycles and maintaining engine manufacturer recommended oil change intervals. This product meets the API CK-4 and earlier API Categories. Clean engine Detergent Additive System Soot Control Protection Wear reduction additive technology Protects against viscosity breakdown Corrosive Wear Protection Improved oxidation protection compared to API CJ-4 engine oils. APPLICATIONS: Caterpillar ECF-3 Mack EOS-4.5 Volvo VDS-4.5 Cummins CES Detroit Diesel DFS 93K222 API Service - API CK-4, CJ-4, CI-4 Plus, CI-4, CH-4/SN TYPICAL PROPERTIES: CITGO CITGARD HD ENGINE OIL SAE Grade 15W-40 Material Code Gravity, ASTM D4052, API 29.7 Density, lbs/gal 7.31 Flash Point, ASTM D92 (COC), F ( C) 442 (228) Viscosity ASTM D445, cst at 40 C 117 cst at 100 C 15.6 Viscosity Index, ASTM D HTHS Rate Viscosity at 150 C, ASTM D4683, cp 4.2 CCS Viscosity at -20 C, ASTM D5293, cp 5800 MRV Pumpability at -25 C, ASTM D4684, cp MRV Yield Stress at -25 C, ASTM D4684 <35 Pour Point, ASTM D97, F ( C) -33 (-36) Color, ASTM D1500 L4.5 Sulfated Ash, ASTM D874, m% 1.0 CITGO and CITGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

25 CITGO CITGARD 600 ENGINE OILS Date 04/18 DESCRIPTION: CITGO CITGARD 600 Engine Oils use superior technology to protect low-emissions engines equipped with exhaust after-treatment systems and other new design features. These products meet the API CJ-4 heavy duty requirements as well as existing API CI-4 PLUS and earlier categories. HDEO Engine Oils PERFORMANCE BENEFITS: PERFORMANCE CAPABILITIES: APPLICATIONS: Formulated specifically for low emission engines equipped with EGR, DOC and SCR Provides advanced soot control utilizing SootArrest, soot dispersant chemistry Offers advantages for heavy duty commercial trucks and other diesel-fueled applications, including off-road equipment State-of-the-art wear control technology for reduced wear Exceptional oxidation and thermal protection for operating at extreme temperatures Extends diesel particulate filter (DPF) life SAE 10W-30 improves fuel economy and cold cranking lubrication Equipment requiring API CJ-4, CI-4 PLUS, CI-4, CH-4/SN Detroit Diesel 93K218 Caterpillar ECF-3 Mack EO-O Premium Plus Cummins CES Volvo VDS-4 Mercedes Recommended for use in heavy-duty service in commercial trucks, agricultural equipment, construction equipment, stationary engines, and other diesel-fueled engine applications. TYPICAL PROPERTIES: CITGO CITGARD 600 ENGINE OILS SAE Grade 15W-40 10W-30 Material Code Gravity, ASTM D4052, API Density, lbs/gal Flash Point, ASTM D92 (COC), F ( C) 450 (232) 450 (232) Viscosity, ASTM D445, cst at 140 C Viscosity, ASTM D 445,cSt at 100 C Viscosity Index, ASTM D HTHS Rate Viscosity at 150 C, ASTM D4683, cp CCS Viscosity, ASTM D5293, cp 5,850 at -20 C 6,250 at -25 C MRV Pumpability, ASTM D4684, cp 16,100 at -25 C 23,000 at -30 C MRV Yield Stress, ASTM D4684 <35 at -25 C <35 at -30 C Pour Point, ASTM D97, F ( C) -22 (-30) -37 (-39) Color, ASTM D1500 L3.5 L3.0 Sulfated Ash, ASTM D874, m% Total Base Number, ASTM D2896, mg KOH/g CITGO and CITGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C10005B 17

26 HDEO Engine Oils CITGO CITGARD 600 ENGINE OILS MONOGRADES Date 04/18 DESCRIPTION: CITGO CITGARD 600 Engine Oils Monogrades are high quality, heavy-duty crankcase oils. This product line is manufactured with the latest additive technologies to provide excellent performance. SAE 30, 40, and 50 viscosity grades are designed with low sulfated ash to give optimal performance in Detroit Diesel Two Stroke Cycle diesel engines calling for obsolete service category CF-2. These mono-grade products also meet the performance requirements of obsolete service category CF. SAE 10W and SAE 30 viscosity grades have also passed the requirements of the Allison C-4 specification. These lower viscosity grade fluids are excellent for hydraulic applications calling for Allison C-4 and / or Caterpillar TO-2 performance with engine oil type technology additive systems. PERFORMANCE BENEFITS: Excellent detergency control of exhaust port deposits in Detroit Diesel Two-stroke cycle diesel engines. Excellent dispersancy and oxidation resistance protect against excessive viscosity increase. Superior wear protection in hydraulic pumps and Detroit Diesel Two-stroke cycle diesel engines. Good TBN properties protect against corrosive wear. Proven oil consumption control in heavy duty service. Shear stability of mono-grades assures stay-in-grade performance. Meets Detroit Diesel recommendations of 1.0% maximum sulfated ash for Two-stroke cycle diesel engines. PERFORMANCE CAPABILITIES*: APPLICATIONS:: Caterpillar TO-2 Detroit Diesel Two-stroke Cycle diesel engines Allison C-4 US CID A-A *Some performance capabilities are applicable to specific viscosity grade(s). CITGO CITGARD 600 Engine Oils Monogrades are intended for use in heavy-duty service in commercial trucks, agricultural equipment, construction equipment, and other diesel fueled engine, hydraulic, and transmission applications. Specific viscosity grades are approved for use in powershift, manual, and hydrostatic transmissions, final drives, and hydraulic systems where the equipment manufacturer designates the use of a heavy-duty, detergent-type engine oil. See CITGARD 600 Multi-Grade Product Information Sheet for more options. Check Owners Manuals for specific viscosity grade and API Service Category recommendations. (Continued) (Continued) C10005A 18

27 CITGO CITGARD 600 ENGINE OILS MONOGRADES (Continued) Date 04/18 - (Continued) TYPICAL PROPERTIES: HDEO Engine Oils CITGO CITGARD 600 ENGINE OILS MONOGRADES SAE Grade 10W Material Code Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, ASTM D92 (COC), F ( C) 439 (226) 489 (254) 486 (252) 482 (250) Viscosity, ASTM D445, cst at 100 C ASTM D 445,cSt at 40 C Viscosity Index, ASTM D HTHS Rate Vis at 150 C & 10 6 sec -1, cp CCS Vis, ASTM D5293, cp at C 4,000 at -25 NR* NR* NR* MRV Vis, ASTM D4684, cp at C 10,000 at -30 NR* NR* NR* MRV Yield Stress, ASTM D4684, Pa at C <35 at -30 NR* NR* NR* Pour Point, ASTM D97, F ( C) -38 (-39) -11 (-24) +10 (-12) +10 (-12) Sulfated Ash, ASTM D874, %m TBN (Total Base No.), ASTM D Color, ASTM D1500 (may vary by location) L3.0 L3.0 L4.0 L4.0 KEY PERFORMANCE CLAIMS AND APPLICATIONS: Obsolete Service Categories CF-2 CF Approvals or performances that are Viscosity Grade specific: Allison C-4 US CID A-A *NR = No Requirement CITGO and CITGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C10005A 19

28 HDEO Engine Oils CITGO CITGARD 700 SYNTHETIC BLEND ENGINE OILS Date 04/18 DESCRIPTION: PERFORMANCE BENEFITS: RECOMMENDED FOR: CITGO CITGARD 700 Synthetic Blend Engine Oils deliver the performance needed for newer engine designs while improving performance in older engines. Engineered with a proprietary additive technology that protects engines running at higher operating temperatures and fuel injection pressures, while meeting tighter wear limits and lower emission requirements. SAE 10W-30 viscosity grade assists in attaining the new Phase II fuel efficiency standards by improving fuel economy, increasing cold start up lubrication, and providing superior engine durability. SAE 10W-30 offers up to 3% fuel economy advantage over conventional SAE 15W-40 viscosity grade oils Maintains viscosity over extended service drain intervals Up to 100% increase in oxidation protection compared to conventional CJ-4 engine oils Always follow OEM recommendations when extending oil drain intervals Advanced wear protection in older and newer engines Reduced air entrainment in high pressure hydraulic fuel injection systems Equipment requiring: API CK-4, CJ-4, CI-4 PLUS, CI-4, CH-4/SN (SN applies to 15W-40 only) Caterpillar ECF-3 Cummins CES Detroit Diesel DFS 93K222 Mercedes Paccar Volvo/Mack/Renault - VDS-4.5/EOS-4.5/RLD-4 Ford WSS-M2C171-F1 Note: Use of diesel engine oils in automotive gasoline engines can shorten the life of catalytic converters. APPLICATIONS: CITGO CITGARD 700 Synthetic Blend Engine Oils provide superior performance for commercial trucks, agricultural equipment, construction equipment, stationary engines, and other diesel-fueled engine applications. Consult owner s manual for proper lubricant selection. API Comparison Chart Category CITGARD 700 API CJ-4 CITGARD 700 API CK-4 Back serviceable YES YES Viscosity grades 15W-40/10W-30 15W-40/10W-30 Fleet million mile engine test rating Better Best 100% improved oxidation stability NO YES Greater shear stability vs. conventional API CJ-4 YES YES Aeration control vs. conventional API CJ-4 Better Best SAE 10W-30 sustains improved fuel economy through Better Best 50,000 miles Compatible with conventional API CJ-4 oils YES YES Best Overall Performance and Backward compatibility Better Best (Continued) (Continued) C

29 CITGO CITGARD 700 SYNTHETIC BLEND ENGINE OILS (Continued) Date 04/18 - (Continued) Volvo T-13 Oxidation Stability Test vs API CK-4 CITGARD 700 API CK-4 Reduces oil oxidation by 100% HDEO Engine Oils CITGARD 700 CK-4 TYPICAL PROPERTIES: CITGO CITGARD 700 SYNTHETIC BLEND ENGINE OILS SAE Grade 10W-30 15W-40 Material Code Gravity, ASTM D4052, API at 60 F Pounds/Gallon at 60 F Specific Gravity at 60 F Viscosity at 40 C, cst Viscosity at 100 C, cst Viscosity Index CCS Viscosity, Temperature -25 C -20 C MRV Viscosity, Temperature -30 C -25 C MRV Yield Stress, Temperature <35 <35 Pour Point, F ( C) -38 (-39) -33 (-36) Flash Point, COC, F ( C) 435 (224) 439 (226) Noack Evaporative, ASTM D5800, % Loss Color, ASTM D1500 L3.0 L3.5 Total Base Number, ASTM D Sulfated Ash, ASTM D874, % wt CITGO and CITGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

30 Small Engine Oils CITGO CITGARD 700 MFE SYNTHETIC BLEND ENGINE OIL Date 04/18 DESCRIPTION: CITGO CITGARD 700 MFE Synthetic Blend Engine Oil SAE 10W-30 is engineered for maximum fuel efficiency and API FA-4 compliant engines. Formulated with proprietary additive technology that protects engines running at higher operating temperatures and higher fuel injection pressures, while meeting tighter wear limits and lower emission requirements. Provides additional fuel economy compared to API CK-4 or API CJ-4 SAE 10W-30 engine oils. CITGO CITGARD 700 MFE Synthetic Blend SAE 10W-30 Engine Oil is a new generation engine oil that supports the Phase II fuel efficiency standards which are driving the need for even more fuel efficient heavy duty engine oils combined with excellent wear protection and engine durability. PERFORMANCE BENEFITS: RECOMMENDED FOR: APPLICATIONS: Up to 4% fuel economy advantage over conventional SAE 15W-40 viscosity grade oils Maintains viscosity over extended service intervals Up to 100% increase in oxidation protection compared to conventional CJ-4 engine oils. Always follow OEM recommendations when extending oil drain intervals Advanced wear protection for newer FA-4 compliant engines Reduced air entrainment in high pressure hydraulic fuel injection systems API FA-4 Compliant Engines Cummins CES Detroit Diesel DFS 93K223 CITGO CITGARD 700 MFE Synthetic Blend SAE 10W-30 Engine Oil is engineered for API FA-4 compliant engines. Consult owner s manual for proper lubricant selection. CITGARD 700 MFE Synthetic Blend Engine Oil vs API CK-4 or CJ-4. (Continued) (Continued) C

31 CITGO CITGARD 700 MFE SYNTHETIC BLEND ENGINE OIL (Continued) Date 04/18 - (Continued) Volvo-T-13 Oxidation Stability HDEO Engine Oils CITGARD 700 MFE 10W-30 CITGARD 700 MFE 10W-30 TYPICAL PROPERTIES: CITGO CITGARD 700 MFE SYNTHETIC BLEND ENGINE OIL SAE 10W-30 SAE Grade 10W-30 Material Code Gravity, ASTM D4052, API at 60 F 31.5 Pounds/Gallon at 60 F 7.25 Specific Gravity at 60 F 0.87 Viscosity at 40 C, cst 66 Viscosity at 100 C, cst 10.0 Viscosity Index 136 CCS Viscosity, Temperature -25 C MRV Viscosity, Temperature -30 C MRV Yield Stress, Temperature <35 Pour Point, F ( C) -33 (-36) Flash Point, COC, F ( C) 446 (230) Noack Evaporative, ASTM D5800, % Loss 12.7 Color, ASTM D1500 L3.5 Total Base Number, ASTM D Sulfated Ash, ASTM D874, % wt 1.0 CITGO and CITGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

32 HDEO Engine Oils CITGO CITGARD SYNDURANCE PLUS SYNTHETIC HEAVY DUTY ENGINE OILS Date 04/18 DESCRIPTION: CITGO CITGARD SynDurance PLUS Synthetic Heavy Duty Engine Oil s Advanced Fuel Efficiency formula delivers maximum fuel economy, extreme cold temperature performance and superior engine durability. These engine oils contain a careful balance of synthetic base oil components with a shear stable viscosity modifier, which insures heavily loaded engine parts have protective oil films. CITGO CITGARD SynDurance PLUS Synthetic Heavy Duty Engine Oils meet the performance requirements of newer engines operating at higher temperatures, with lower RPM, higher torque and advanced combustion design. CITGO CITGARD SynDurance PLUS Synthetic Heavy Duty Engine Oils have been field tested for over a million miles with engine teardown inspections compared to premium SAE 15W-40 viscosity grade oils. The results indicate superior wear protection and oil consumption control. BENEFITS: Up to 4% fuel economy advantage over conventional SAE 15W-40 viscosity grade oils Longer starter/battery life with reduced dependency on block heaters resulting in lower energy costs Up to 100% increase in oxidation protection compared to conventional CJ-4 engine oils. Always follow OEM recommendations when extending oil drain intervals Reduced air entrainment in high pressure fuel injection systems Addresses the environmental challenge of reducing greenhouse gases and carbon foot print APPLICATIONS: RECOMMENDED FOR: API CK-4, CJ-4, CI-4 PLUS, CI-4, CH-4 Caterpillar ECF-3 Cummins CES Detroit Diesel DFS 93K222 Volvo/Mack/Renault VDS-4.5/EOS-4.5/RLD-4 Mercedes Paccar Navistar Ford WSS-M2C171-F1 (5W-40 Only) C

33 CITGO CITGARD SYNDURANCE PLUS SYNTHETIC HEAVY DUTY ENGINE OILS Date 04/18 - (Continued) TYPICAL PROPERTIES: Small Engine Oils CITGO CITGARD SYNDURANCE PLUS SYNTHETIC HEAVY DUTY ENGINE OILS 5W-30 5W-40 Material Code Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, COC, ASTM D92, F ( C) 428 (220) 453 (234) Viscosity, ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D CCS Vis, ASTM D5293, cp at C -30 C 6,350 at -30 C MRV Vis, ASTM D4684, cp at C 21,970 at -35 C 30,060 at -35 C MRV Yield Stress, ASTM D4684, Pa at C <35 <35 Pour Point, ASTM D97, F ( C) -38 F (-39 C) -44 F (-42 C) TBN (Total Base No.), ASTM D Color, ASTM D1500 L5.5 L5.5 NOACK Volatility, ASTM 05800, % Loss Low Temperature Pumpability Comparison How much wear occurs waiting on 15W-40? Savings Category Fuel Savings Advantage Conventional 15W-40 CITGARD SynDurance PLUS 5W-30 Savings* C10234 SynDurancePlus 5W-40 Conventional SAE 15W-40 SynDurancePlus 5W-40 Conventional SAE 15W-40 3 seconds 7 seconds Cold box testing at -22 F (-30 C) of used oil demonstrates the superior flow characteristics of SynDurance Plus Synthetic 5W-40 Number of Units Annual Miles/Unit 100, ,000 MPG Fuel Savings % Increase None 3.00 Fuel Cost Annual Unit Fuel Gallons 15,384 14, Annual Unit Fuel Cost $30,768 $29,940 $828 Fleet Anual Fuel Gallons 1,538,400 1,497,000 41,400 Total Savings Including Cost of Oil $82,800 *Savings is example only Individual fleet result will vary CITGO, CITGARD and SynDurance are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. 25

34 Small Engine Oils CITGO CITGARD CNG/LNG ENGINE OIL Date 04/18 DESCRIPTION: QUALITIES: BENEFITS APPLICATIONS: CITGO CITGARD CNG/LNG Engine Oil is a specially formulated synthetic blend for compressed natural gas (CNG) engines in transit operation. It is available as a SAE 15W-40 viscosity grade. Building on CITGO s long heritage of outstanding gas engine oils for stationary applications, CITGO CITGARD CNG/LNG Engine Oil provides the protection needed in today s demanding mobile CNG applications. CITGO CITGARD CNG/LNG Engine Oil is formulated with base stocks specially selected for compressed natural gas operation, proven additives and a shear stable VI improver. This unique combination provides protection against deposits in the higher temperature natural gas combustion chamber. Liner and tappet wear protection far exceed original equipment manufacturer s requirements. CITGO s combination of components provides excellent cold pumpability, foam protection, exceptional oxidation and nitration control, overall engine cleanliness, and reduced oil consumption. Extensively field tested under severe mobile operating conditions Meets major mobile-on highway gas engine requirements Longer engine oil service life capability in a variety of mobile engine applications. Always follow OEM recommendations when extending oil drain intervals Excellent TBN and TAN retention Resists viscosity breakdown and maintains excellent oil films under high engine loads over engine oil service intervals Reserve protection against oxidation and nitration resulting from higher CNG LNG operating temperatures CITGO CITGARD CNG/LNG Engine Oil is conforming to Cummins CES and to Detroit Diesel Corporation (DDC) Power Guard Oil specification 93K216, and is recommended for use in Series 60G, 50G and 30G natural gas engines. Mack Trucks and John Deere also call for this quality of oil in their natural gas fueled engines. CITGO CITGARD CNG/LNG Engine Oil is also suitable for use with other gaseous fuels such as LPG. Always consult your owner s manual for correct oil recommendations. (Continued) C

35 CITGO CITGARD CNG/LNG ENGINE OIL Date 04/18 - (Continued) APPLICATIONS: (Cont d.) TYPICAL PROPERTIES: CITGO CITGARD CNG/LNG ENGINE OIL Small Engine Oils SAE Grade 15W-40 Material Code Gravity, ASTM D4052, API 29.7 Pounds Per Gallon 7.31 Flash Point, ASTM D92, F ( C) 437 (225) Viscosity ASTM D445, cst at 40 C 128 cst at 100 C 15.9 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -33 (-36) Sulfated Ash, ASTM D872, % 0.91 Total Base Number, ASTM D CITGO and CITGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

36 Small Engine Oils CITGO MULTI-PURPOSE AIR-COOLED 2-CYCLE ENGINE OIL Date 04/18 DESCRIPTION: CITGO Multi-Purpose Air-Cooled 2-Cycle Engine Oil is designed for use in air-cooled two-stroke engines. QUALITIES: CITGO Multi-Purpose Air-Cooled 2-Cycle Engine Oil is engineered for lower smoke and protection against exhaust port blocking, combustion chamber and piston deposits, ring sticking and scuffing, and wear in today s high RPM air-cooled 2-cycle engines. APPLICATIONS: CITGO Multi-Purpose Air-Cooled 2-Cycle Engine Oil can be used in motorcycles, generators, lawnmowers, and hand held power equipment such as leaf blowers, trimmers, and chainsaws operating in hot, dirty, dusty environments and high loads for extended periods. Do not use in engines requiring an NMMA TC-W3 product. Consult owners manual for Fluid Specification. TYPICAL PROPERTIES: CITGO MULTI-PURPOSE AIR-COOLED 2-CYCLE ENGINE OIL Material Code Gravity, ASTM D4052, API 31.5 Density, lb/gal, at 60 F 7.23 Flash Point, PMCC, ASTM D93, F ( C) 201 (94) COC, ASTM D92, F ( C) 221 (105) Viscosity, ASTM D445, cst at 40 C 61 cst at 100 C 8.6 ASTM D2161, SUS at 100 F 295 SUS at 210 F 55 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -42 (-36) Appearance, Color Purple Sulfated Ash, ASTM D874, % 0.11 Total Base Number, ASTM D2896, mg KOH/g 1.6 CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

37 CITGO SUPERGARD AIR-COOLED 2-CYCLE ENGINE OIL Date 03/18 DESCRIPTION: CITGO SUPERGARD Air-Cooled 2-Cycle Engine Oil is a premium performance synthetic blend lubricant designed for use in high performance air-cooled two-stroke engines. Small Engine Oils QUALITIES: APPLICATIONS: SUPERGARD Air-Cooled 2-Cycle Engine Oil is engineered for lower smoke and advanced protection for air-cooled 2-cycle engines. This synthetic blend formula meets or exceeds the rigorous requirements of the API TC, JASO FD and ISO-L-EGD classifications for 2-cycle air-cooled engine oils and also exceeds the performance requirements for JASO FC, FB; ISO-L-EGC and -EGB. This advanced oil helps to protect today s high RPM air-cooled 2-cycle engines against exhaust port blocking, combustion chamber and piston deposits, ring sticking and scuffing, and wear. The JASO FD Certification number for this lubricant is 001 CGO 545. SUPERGARD Air-Cooled 2-Cycle Engine Oil is formulated with premium base oils and a low ash additive package that provides excellent lubricity and detergency performance which surpasses the standard for preventing piston and combustion chamber deposits. In addition, SUPERGARD Air-Cooled 2-Cycle Engine Oil is a synthetic blend which reduces exhaust smoke and prevents piston seizure and cylinder scuffing. SUPERGARD Air-Cooled 2-Cycle Engine Oil mixes readily with fuel for pre-mix type, even at low temperatures. Consult owners manual for Fluid Specification. CITGO SUPERGARD Air-Cooled 2-Cycle Engine Oil is recommended for use in air-cooled, 2-cycle applications where an API TC, JASO FD or ISO-L-EGD product is preferred. This oil supercedes previous JASO and ISO specifications. It can be used in either premix or oil injection systems up to 50:1 fuel to oil ratios. Do not use in engines requiring an NMMA TC-W3 product. SUPERGARD Air-Cooled 2-Cycle Engine Oil can be used in motorcycles, generators, lawnmowers, and hand held power equipment such as leaf blowers, trimmers, and chainsaws operating in hot, dirty, dusty environments and high loads for extended periods. SUPERGARD Air-Cooled 2-Cycle Engine Oil provides the necessary protection to keep your air-cooled 2-stroke cycle engine running cleaner, longer and with less smoke. TYPICAL PROPERTIES: CITGO SUPERGARD AIR-COOLED 2-CYCLE ENGINE OIL Material Code Gravity, ASTM D4052, API 32.0 Density, lb/gal, at 60 F 7.21 Flash Point, PMCC, ASTM D93, F ( C) 185 (85) Flash Point, COC, ASTM D92, F ( C) 203 (95) Viscosity, ASTM D445, cst at 40 C 55 cst at 100 C 8.5 ASTM D2161, SUS at 100 F 281 SUS at 210 F 54.8 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -49 (-45) Appearance, Color Purple Sulfated Ash, ASTM D874, % 0.1 Total Base Number, ASTM D2896, mg KOH/g 2.2 CITGO and SUPERGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

38 Small Engine Oils CITGO SUPERGARD MARINE PLUS 2-CYCLE ENGINE OIL Date 04/18 DESCRIPTION: CITGO SUPERGARD Marine Plus 2-Cycle Engine Oil is a licensed NMMA TC-W3 oil that effectively combats wear, scuffing, deposit build-up, and enhances lubricity to provide longer engine life. BENEFITS: APPLICATIONS: Reduces carbon and deposit build-up on engine parts Helps prevent piston ring sticking High film strength for improved lubricity which provides: Increased engine efficiency Excellent scuffing protection of rings and cylinder and reduced bearing wear Cleaner, better-running engines producing less smoke Guaranteed to protect OEM engine warranties CITGO SUPERGARD Marine Plus 2-Cycle Engine Oil is recommended for all water-cooled or liquidcooled 2-cycle engines requiring an NMMA TC-W3, TC-WII or TC-W type oil. It may also be used in many air-cooled 2-cycle engine applications requiring API Service Category TC. Recommended for both direct injected and pre-mix systems. CITGO SUPERGARD Marine Plus 2-Cycle Engine Oil will provide protection for gasoline fueled 2-cycle engines when used at the primary dilution recommended by the original equipment manufacturer. Consult owners manual for Fluid Specification. TYPICAL PROPERTIES: CITGO SUPERGARD MARINE PLUS 2-CYCLE ENGINE OIL Material Code Gravity, ASTM D4052, API 31.5 Density, lb/gal at 60 F 7.23 Flash Point, PMCC, ASTM D93, F ( C) 178 (81) (1) Flash Point, COC, ASTM D92, F ( C) 197 (92) Viscosity, ASTM D445, cst at 40 C 32.0 cst at 100 C 5.9 ASTM D2161, SUS at 100 F 163 SUS at 210 F 46 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -38 (-39) Appearance, Color Blue/Green Sulfated Ash, ASTM D874, % <0.004 Total Base Number, ASTM D2896, mgkoh/g 8.6 NOTE (1) Combustible liquid CITGO and SUPERGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

39 CITGO SUPERGARD SEA & SNOW 2-CYCLE ENGINE OIL Date 04/18 DESCRIPTION: CITGO SUPERGARD Sea & Snow 2-Cycle Engine Oil is a synthetic blend, low smoke oil designed for use in high performance air- or liquid-cooled two-stroke engines of Personal Water Craft (PWC) and Snowmobiles. Small Engine Oils QUALITIES: APPLICATIONS: SUPERGARD Sea & Snow 2-Cycle Engine Oil is engineered for lower smoke and advanced protection for air-cooled 2-cycle engines. The synthetic blend formula meets or exceeds the rigorous requirements of the API TC, JASO FD and ISO-L-EGD classifications for 2-cycle air-cooled engine oils. This advanced oil helps protect today s high performance air-cooled 2-cycle engines against exhaust port blocking, combustion chamber and piston deposits, ring sticking and scuffing, and wear. The JASO FD Certification number for this lubricant is 001 CGO 555. SUPERGARD Sea & Snow is formulated with premium base oils and a new synthetic low ash additive package that provides excellent lubricity and detergency performance that surpasses standards for preventing piston and combustion chamber deposits. In addition, SUPERGARD Sea & Snow is a synthetic blend which reduces exhaust smoke and prevents piston seizure and cylinder scuffing. SUPERGARD Sea & Snow mixes readily with fuel for pre-mix type, even at low temperatures. CITGO SUPERGARD Sea & Snow 2-Cycle Engine Oil is recommended for use in air-cooled, 2-cycle applications where an API TC, JASO FD or ISO-L-EGD product is preferred. This oil supercedes previous JASO and ISO specifications. It can be used in either premix or oil injection systems up to 50:1 fuel ratios. It may also be used in certain motorcycle engines which are liquid cooled. Do not use in engines requiring an NMMA TC-W3, TC-WII, or TC-W product. SUPERGARD Sea & Snow is formulated primarily for use in snowmobiles and personal watercraft. It can be used in motorcycles, generators, lawnmowers, and hand held power equipment such as leaf blowers, trimmers, and chainsaws. SUPERGARD Sea & Snow provides the necessary protection to keep your snowmobile or PWC running cleaner, longer, and with less smoke. Consult owners manual for Fluid Specification. TYPICAL PROPERTIES: CITGO SUPERGARD SEA & SNOW 2-CYCLE ENGINE OIL Material Code Gravity, ASTM D4052, API 32.0 Density, lb/gal at 60 F 7.21 Flash Point, PMCC, ASTM D93, F ( C) 185 (85) COC, ASTM D92, F ( C) 203 (95) Viscosity, ASTM D445, cst at 40 C 55 cst at 100 C 8.5 ASTM D2161, SUS at 100 F 281 SUS at 210 F 54.8 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -49 (-45) Appearance, Color Purple Sulfated Ash, ASTM D874, % 0.0 Total Base Number, ASTM D2896, mg KOH/g 2.2 CITGO, SUPERGARD and Sea & Snow are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

40 CITGO CITGEAR HD SYNTHETIC GEAR LUBRICANTS Date 04/18 Automotive Gear Oils DESCRIPTION: QUALITIES: CITGO CITGEAR HD Synthetic Gear Lubricants are state-of-the-art heavy duty, synthetic gear and bearing lubricants designed for use in manual transmission, transfer cases and differentials of passenger cars, trucks, farm tractors, construction equipment and over-the-road trucks. CITGO CITGEAR HD Synthetic Gear Lubricants are formulated using a proprietary combination of synthetic base stocks and additives. This unique combination of components offers the maximum protection for gears and bearings over a wide range of operating temperatures. Superior oxidation resistance for extended drain intervals. Excellent load carrying properties (SAE 75W-90, 75W-140 and 80W-140) for maximum protection. High viscosity index and low pour point synthetic base stocks provide reduced friction resulting in fuel economy potential during low temperature startups or operation conditions. Excellent demulsibility Shear resistant Hydrolytically stable Non-foaming APPLICATIONS: CITGO CITGEAR HD Synthetic Gear Lubricants (SAE 75W-90, 75W-140 and 80W-140) are recommended for differentials (including limited slip units), manual transmission for which hypoidtype lubricants are required and transfer cases for heavy equipment found in trucks, tractors, industrial gear drives, automobiles and farm machinery. These products meet or exceed the following performance requirements: API Service Classification GL-5 and MT-1 CITGO CITGEAR HD Synthetic Gear Lubricant SAE 50 is recommended for heavy-duty service in manual transmissions for which the manufacturer normally recommends either engine oils or GL-1 to GL-4 lubricants. This product contains antiwear, rust, oxidation, foam and corrosion inhibitors to protect bearings and synchronizers and to promote longer transmission life. As in the other products in this series, CITGO CITGEAR HD Synthetic Gear Lubricant SAE 50 provides improved start-up, easier shifting and less gear wear in low temperature environments. Less friction, less drag and improved oxidation resistance combine to provide fuel economy benefits and longer drain intervals. This product is recommended in applications calling for the following specifications: API GL-4, MT-1 (Continued) (Continued) C

41 CITGO CITGEAR HD SYNTHETIC GEAR LUBRICANTS Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO CITGEAR HD SYNTHETIC GEAR LUBRICANTS SAE Grade 75W-90 75W W Material Code Specific Gravity Density, lb/gal Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445, cst at 100 C Viscosity Index, ASTM D Brookfield Viscosity, ASTM D2983, cp at -26 C 72,300 28,800 cp at -40 C 114, ,500 Pour Point, ASTM D97, F ( C) -65 (-54) -60 (-51) -49 (-45) -60 (-51) Flash Point, ASTM D92, F ( C) 378 (192) 370 (188) 381 (194) 507 (264) Foam Test, ASTM D892 Pass Pass Pass Pass Copper Corrosion, ASTM D130 1A 1A 1A 1A FZG, Failure Stage >12 >12 >12 NA Automotive Gear Oils NA = Not Applicable CITGO and CITGEAR are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

42 CITGO SYNTHETIC GEAR LUBRICANTS Date 04/18 Automotive Gear Oils DESCRIPTION: PROPERTIES: CITGO Synthetic Gear Lubricants are heavy-duty, synthetic gear and bearing lubricants designed for use in manual transmissions, transfer cases and differential axles of trucks, farm tractors, construction, passenger cars and miscellaneous industrial equipment. Blended from very high viscosity index, low pour point synthetic base stocks, these oils provide maximum protection to gears and bearings operating over a wide range of temperatures, speeds and loads. Their superb resistance to oxidation provides the benefit of extended drain intervals. Available in three viscosity grades: SAE 75W-90, 80W-140 and 50. Superior oxidation resistance for extended drain intervals Excellent load carrying properties (SAE 75W-90 and 80W-140) for maximum protection against component wear High viscosity index and low pour point synthetic base stocks provide reduced fluid friction with resultant fuel savings potential during low temperature start-up or operating conditions Excellent demulsibility separates water readily Shear resistant Provides full protection to system parts against rust and corrosion Non-foaming APPLICATIONS: CITGO Synthetic Gear Lubricants (SAE 75W-90 and 80W-140) are recommended for differentials, manual transmissions for which hypoid-type lubricants are required and transfer cases for heavy equipment trucks, tractors, industrial gear drives, automobiles, farm machinery, etc. These products meet or exceed the following performance requirements: API Service Classification GL-5 and MT-1 SAE J2360; former U.S. Military Specification MIL-L-2105D and MIL-PRF-2105E Scania STO 1:0 Eaton Roadranger E500 DANA SHAES 256, Rev. C (75W-90) DANA SHAES 256, Rev. A (80W-140) Mack GO-J Plus (75W-90) Mack GO-J (80W-140) ArvinMeritor O-76N International TMS-6816 CITGO Synthetic Gear Lubricant SAE 50 is recommended for heavy-duty service in manual transmission for which the manufacturer normally recommends either engine oils or GL-1 to GL-4/MT-1 lubricants. This product contains antiwear, rust, oxidation, foam and corrosion inhibitors to protect bearings and synchronizers and to promote longer transmission life. As in the other products in this series, CITGO Synthetic Gear Lubricant SAE 50 provides improved start-up, easier shifting and less gear wear in low temperature environments. Less friction, less drag and improved oxidation resistance combine to provide fuel economy benefits and longer drain intervals. (Continued) C

43 CITGO SYNTHETIC GEAR LUBRICANTS Date 04/18 - (Continued) APPLICATIONS: CITGO Synthetic Gear Lubricant SAE 50 (Continued) This product meets or exceeds the following performance requirements: MT-1 Eaton Roadranger Extended Drain (E500) PS-164 Rev. 7 Mack TO-A PLUS 500,000 Mile Extended Drain ZF Freedom Line ZF TE-ML-04D International TMS 6816 TYPICAL PROPERTIES: CITGO SYNTHETIC GEAR LUBRICANTS SAE Grade 75W-90 80W Material Code API Classification GL-5 GL-5 GL-4 AGMA Grade Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, ASTM D92, F ( C) 405 (204) 410 (210) 435 (224) Pour Point, ASTM D97, F ( C) -65 (-54) -54 (-48) -49 (-45) Color, ASTM D Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445,cSt at 100 C Viscosity Index Brookfield Viscosity, ASTM D2270 cp at -18 C 5,715 22,700 6,835 cp at -26 C 60,950 cp at -40 C 93,050 <120,000 Foam Test, ASTM D892 Pass Pass Pass Copper Corrosion, ASTM D130 1A 1A 1A Rust Protection, ASTM D A/B Pass Pass Pass Automotive Gear Oils CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

44 CITGO SYNDURANCE SYNTHETIC MTF Date 04/18 Automotive Gear Oils DESCRIPTION: FEATURES AND BENEFITS CITGO SynDurance Synthetic MTF transmission fluid is a specially formulated synthentic lubricant designed for fuel efficiency, extended drain intervals and severe service in heavy duty commercial vehicle transmissions which require a non-ep transmission lubricant. It is specially formulated to protect higher torque transmissions coupled with increased horsepower engines. It is approved for use in Eaton transmissions such as Ultrashift Plus, Fuller Advantage, FR and RT Series transmissions. Replaces SAE 50 transmission fluid and is for use where SAE 50 weight was recommended. SynDurance Synthetic MTF provides the following Features, Benefits and Advantages: Uniquely formulated to provide up to 1.5% fuel economy improvement while maintaining excellent shear stability. Provides high performance and extended drain capabilites in transmissions. Has excellent thermal and oxidation stability which resists deposit and sludge formation. The advanced additive system in SynDurance Synthetic MTF provides excellent protection from corrosion, foaming, rust, and wear. The use of high viscosity index sythetic base fluids allows SynDurance Synthetic MTF to provide superior high and low temperature performance. Provides friction retention, friction durability, and excellent shear stability to ensure and maintain smooth transmission operations throughout the extended drain interval. Formulated to reduce sump operating temperatures. APPLICATIONS: SynDurance Synthetic MTF (transmission fluid) is recommended where low temperatures, wear or heat present major problems and a non-ep lubricant is required. Typical usage includes transmissions, transfer cases, and wheel end hubs. Recommended commercial vehicle applications include line haul, vocational, off-road, pick up and delivery, and buses. CITGO SynDurance Synthetic MTF is approved for these OEM specifications: Eaton PS-386 (supersedes PS-164 Rev7) Mack TO-A Plus Navistar MPAPS B-6816 Type II API MT-1 Also recommended for: Eaton Fuller Transmissions, Volvo ishift Transmissions, Mack mdrive Transmissions, ZF Freedomline (AS-Tronic) Transmissions, Meritor Transmissions (O-81), Meritor Transfer Cases and Con Met Wheel Ends. (Continued) (Continued) C

45 CITGO SYNDURANCE SYNTHETIC MTF Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO SYNDURANCE SYNTHETIC MTF Material Code SAE Viscosity Grade 75W-90 Gravity, ASTM D4052, API 34.9 Specific Gravity at 60 F.085 Density, lb/gal at 60 F 7.09 Viscosities: at -40 C, cp 51,900 at 40 C, cst at 100 C, cst Viscosity Index 163 Pour Point, ASTM D97, F ( C) -44 (-42) Flash Point, ASTM D92, F ( C) 460 (238) Automotive Gear Oils CITGO and SYNDURANCE are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

46 PREMIUM (LS) Gear Oil Date 04/18 Automotive Gear Oils DESCRIPTION: QUALITIES: CITGO Premium (LS) Gear Oil is a multipurpose, limited slip automotive gear lubricant. Selected additives impart extreme pressure properties which protect automotive gears operated under the most severe service conditions encountered in passenger cars, trucks, farm tractors, earthmoving, construction and other heavy-duty equipment. These additives impart the antiweld, antiscuff and antiwear properties which are necessary in heavy-duty applications. The friction modifier meets the requirements of positive traction or limited slip type differentials. CITGO Premium (LS) Gear Oil is blended to meet the multigrade viscosity requirements described in SAE Standard J306. This gear lubricant is formulated with high VI, refined base oils and thus does not require viscosity improver to meet multigrade viscometric properties. Because this lubricant does not contain VI improver, it will maintain its viscometric properties throughout its useful life and will not lose viscosity through shear. Equipment manufacturers recommendations should be followed when the gear lubricant is subject to high ambient temperatures. While some gearsets are designed for year-round operation using an SAE 80W-90, others may require SAE 85W-140 for high ambient temperature operations. CITGO Premium (LS) Gear Oil is designated for the highest severity of gear service, API Service Classification GL-5. CITGO Premium (LS) Gear Oil is on Mack Truck s list of approved GO-H lubricants. APPLICATIONS: CITGO Premium (LS) Gear Oil is recommended for use where multipurpose gear oil or one suitable for API Service GL-5 is required. Premium (LS) is for use in differentials of passenger cars and light trucks. Premium (LS) is also for use in limited slip differentials known as Sure-grip, Posi-trac, Trac-lock, etc., for complete fill or for top-off. Premium (LS) is also for service in transmissions, differentials, final drives and other gearcases of trucks, buses and farm tractors where extreme pressure, hypoid or multipurpose gear oils are specified by the equipment manufacturer, including differentials. (Continued) (Continued) C

47 PREMIUM (LS) Gear Oil Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO PREMIUM (LS) GEAR OIL SAE Grade 80W-90 Material Code SAE Grade 80W-90 Gravity, ASTM D4052, API 27.4 Specific Gravity 0.89 Density, lb/gal at 60 F 7.4 Flash Point, COC, ASTM D92, F ( C) 430 (221) Viscosity, ASTM D445, cst at 40 C 142 cst at 100 C 14.2 ASTM D2161, SUS at 100 F 721 SUS at 210 F 76 ASTM D2983, cp at -26 C 125,000 Viscosity Index, ASTM D Pour Point, ASTM D97 (1), F ( C) -27 (-33) Channel Point, F ( C), Max. -31 (-35) Foam Test, ASTM D892 Pass Automotive Gear Oils Notes: (1) Method 3456 of Federal Test Method Standard No. 791 CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

48 CITGO PREMIUM GEAR OILS (MP) Date 04/18 Automotive Gear Oils DESCRIPTION: QUALITIES: CITGO Premium Gear Oils (MP) are multipurpose gear lubricants whose high performance level is obtained by using a sulfur-phosphorus additive system. The selected additives impart extreme pressure properties to protect automotive gears which may be operated under the most severe service conditions encountered in passenger cars, trucks, farm tractors, earth moving, construction and other heavy-duty equipment. These additives specifically impart antiweld, antiscuff and antiwear properties necessary in heavy-duty service gear lubricants. API Service Classification: GL-5 and MT-1; SAE J2360 pending CITGO Premium Gear Oils (MP) are blended to meet the multigrade viscosity requirements described in SAE J306 viscosity recommended practice. These gear lubricants are formulated with naturally high VI, highly refined base oils and do not require viscosity index improvers to meet multigrade viscometric properties. These lubricants maintain their viscometric properties throughout their useful life and will not lose viscosity through shear. Viscosity Grades Available: SAE 80W-90 grade for use at ambient temperatures down to -15 F. SAE 85W-140 grade for use at ambient temperatures down to +10 F. Equipment manufacturers recommendations should be followed when the gear lubricant is subject to high ambient temperatures. While some gear sets are designed for year-round operation using an SAE 80W-90, others may require SAE 85W-140 for high ambient temperature operations during the hot weather months. CITGO Premium Gear Oils (MP) exceed the severe gear performance requirements of Military Specifications SAE J2360, as well as former MIL-PRF-2105E and MIL-L-2105D. They are designated for API Service Classification GL-5 and MT-1. CITGO Premium Gear Oils (MP) meet Mack Trucks GO-J Specification. APPLICATIONS: CITGO Premium Gear Oils (MP) are recommended for the following applications: Where a multipurpose gear oil or one meeting the requirements of SAE J2360, API Service GL-5 and/or MT-1 is required. In transmissions, differentials, final drives and other gear cases of trucks, buses and farm equipment where extreme pressure (EP), hypoid or multipurpose gear oils are specified by the manufacturer. (Continued) C

49 CITGO PREMIUM GEAR OILS (MP) Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO PREMIUM GEAR OILS (MP) SAE Grade 80W-90 85W-140 Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash Point, ASTM D92, F ( C) 448 (231) 478 (248) Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 602, cst at 100 C Viscosity, ASTM D2161, SUS at 100 F Viscosity, ASTM D 2161,SUS at 210 F Brookfield Viscosity, ASTM D2983 cp at C 120,000 cp at -12 C 65,000 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -27 (-33) 0 (-18) Channel Point, F ( C), Max. -31 (-35) -4 (-20) Foam Test, ASTM D892 Pass Pass Copper Corrosion, ASTM D130 Pass Pass Automotive Gear Oils CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

50 CITGO REGULAR GEAR OIL Date 04/18 DESCRIPTION: This lubricant is designed for some manually operated transmissions and spiral-bevel axles operating under mild conditions. CITGO Regular Gear Oil is made from high quality mineral oil and selected inhibitors. Available in SAE 90 grade. API Service Classification GL-1.* Automotive Gear Oils QUALITIES: APPLICATIONS: CITGO Regular Gear Oil utilizes high quality, refined base oils. Additives are incorporated to provide oxidation, corrosion and foam inhibition not normally achieved with straight mineral oil. Friction modifiers and extreme pressure agents are not employed in GL-1 oils. CITGO Regular Gear Oil is recommended for use in certain transmissions, final drives and miscellaneous applications in bearing and gear lubrication of mobile equipment where GL-1 or straight mineral oil is specified by the manufacturer. *CITGO Premium Gear Oil (MP) is recommended for hypoid axles and other automotive applications requiring an extreme pressure lubricant for GL-5 service. TYPICAL PROPERTIES: CITGO REGULAR GEAR OIL SAE Grade 90 Material Code Gravity, ASTM D4052, API 27.5 Density, lb/gal at 60 F 7.41 Flash Point, COC, ASTM D92, F ( C) 420 (215) Viscosity, ASTM D445, cst at 40 C, 200 Viscosity, cst at 100 C 17 ASTM D2161, SUS at 100 F 1050 Viscosity, SUS at 210 F 91 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) 0 (-18) CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. (Continued) C

51 CITGO SUPERGARD MARINE PLUS LOWER UNIT GEAR LUBRICANT Date 03/18 DESCRIPTION: CITGO SUPERGARD Marine Plus Lower Unit Gear Lubricant is formulated specifically for the marine industry. It contains the latest generation of proprietary EP additives, designed to provide maximum protection against wear, rust, corrosion and deposits. It is also guaranteed to protect OEM lower unit warranties. QUALITIES: APPLICATIONS: This improved gear lubricant, specifically designed for boating applications, offers unmatched protection, surpassing other marine gear lubricants using GL-4 and GL-5 80W-90 technology: Superior EP lubrication and corrosion protection in the presence of moisture (fresh and sea water). Improved gear protection for shock load conditions encountered with harsh startup engagement, power reversal, and propeller entanglement. Recommended for use in all outboard and stern drive gear units specifying SAE 90, 80W-90 or 85W-90, including OMC Type C. Includes MerCruiser, OMC Cobra, Volvo stern drives and Mercury, Evinrude, Johnson, Mariner, Yamaha, Suzuki, and Force outboards. Consult owner s manual for Fluid Specifications. Automotive Gear Oils TYPICAL PROPERTIES: CITGO SUPERGARD MARINE PLUS LOWER UNIT GEAR LUBRICANT SAE Grade 85W-90 Material Code Gravity, ASTM D4052, API 26.3 Density, lb/gal at 60 F 7.5 Flash Point, ASTM D92, COC, F ( C) 420 (216) Viscosity, cst at 100 C 16.0 Brookfield Viscosity, -23 C, cp 102,000 Pour Point, ASTM D97, F ( C) -15 (-26) Channel Point, F ( C), Max -31 (-35) Color, Visual Blue Foam Test, ASTM D892 Pass Copper Corrosion, 3 hrs at 250 F Pass CITGO and SUPERGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

52 CITGO FINAL DRIVE OIL Date 04/18 DESCRIPTION: CITGO Final Drive Oil is a new generation lubricant that meets the Caterpillar FD-1 specification and is designed for heavy-duty construction equipment final drives and axles operating under severe loads and temperatures. Compared to TO-4 lubricants, CITGO Final Drive Oil will deliver greater protection against gear and bearing fatigue resulting from the higher loads and operating conditions frequently encountered in track type equipment and large off road haul truck final drives. CITGO Final Drive Oil is compatible with TO-4 lubricants in the event of lubricant mixing with the understanding the product mixing does result in decreased level of performance. CITGO Final Drive Oil should not be used in diesel engines and should not be used in compartments that contain friction materials unless recommended by the equipment manufacturer. Available Viscosity Grades: SAE 60. Transmission/Power Fluids QUALITIES: APPLICATIONS: CITGO Final Drive Oil is designed with the following qualities: Performance engineered formula meeting Caterpillar FD-1 specification and has passed the Cat FD-1 test requirements Superior protection against rust, corrosion and lubricant foaming Minimizes lubricant oxidation resulting from higher operating temperatures and loads Protects against gear and bearing fatigue resulting from operating temperatures and loads Formulated to meet the performance requirements of: Caterpillar FD-1 SAE 60 grade Caterpillar Final Drives and Axles where recommended by Caterpillar Up to two times the lubricant service life compared to TO-4 type lubricants. (Refer to chart below for Performance Criteria.) Superior wear protection in highly loaded bearings and gears optimizes component life CITGO LubeAlert HD Oil Analysis is included to provide optimum lubricant service and component life and reduce overall maintenance costs. Longer component life cycles results in improved equipment productivity and reduced equipment rebuild costs and downtime Improved overall profitability especially in high production construction, mining and aggregate operations PERFORMANCE CRITERIA TO-4 60 CITGO FINAL DRIVE OIL Lubricant Service Life 2000 Hours 4000 Hours* Cat FD-1 Approval No Yes Passing FD-1 Testing No Yes LubeAlert HD Oil Analysis Availability Varies Yes Optimum Gear & Bearing Life No Yes * Lubricant Service Life is dependent on the following: Operating conditions, vehicle condition and maintenance practices. Inspect fluid levels regularly and add as needed with CITGO Final Drive Oil Use CITGO LubeAlert HD Oil Analysis program to support maximum component life (Continued) C

53 CITGO FINAL DRIVE OIL Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO FINAL DRIVE OIL SAE Grade 60 Material Code Gravity, ASTM D4052, API 27.7 Density, Pounds Per Gallon 7.40 Flash Point, COC, ASTM D92, F ( C) 265 (129) Viscosity, ASTM D445, cst at 40 C 334 Viscosity, ASTM D 445,cSt at 100 C 25.7 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -47 (-44) Color, ASTM D1500 L4.0 Total Base Number, mgkoh/g D Foam Test, Seq. I, Tendency, ml D Foam Test, Seq. II, Tendency, ml D Foam Test, Seq. III, Tendency, ml D Appearance C&B Moisture, Hot Plate Pass CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Transmission/Power Fluids C

54 CITGO POWER STEERING FLUID WITH STOP LEAK Date 04/18 DESCRIPTION: CITGO Power Steering Fluid with Stop Leak is formulated with high-quality base stocks and additives designed to ensure smooth system operation and revitalize dried, shrunken, and hardened seals. This product helps stop or reduce fluid loss caused by leaky seals and, when used as a preventative maintenance fluid, helps avoid future leaks. QUALITIES: Superior cold temperature performance Excellent friction and wear protection Anti-wear agents to protect pump components Antioxidants to prevent sludge formation Anti-foam agents to prevent pump cavitation and steering loss Corrosion inhibitors to protect metal components Wide range of seal compatibility Transmission/Power Fluids APPLICATIONS: For use where the following fluids are specified: GM , Chrysler 5931, and Ford M2C33-F. For a complete list of equipment specs, visit Consult the owner s manual for proper fluid selection. TYPICAL PROPERTIES: CITGO CITGO POWER STEERING FLUID WITH STOP LEAK Material Code Gravity, ASTM D4052, API 32.9 Pounds Per Gallon 7.15 Flash Point, COC, ASTM D92, F ( C) 424 (218) Pour Point, ASTM D97, F ( C) -54 (-48) Viscosity, ASTM D445, cst at 40 C 34.3 cst at 100 C 6.95 ASTM D2983, cp at -20 C 1,020 cp at -40 C 15,100 Viscosity Index, ASTM D Color Light Amber CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

55 CITGO QUATRASYN SYNTHETIC TRANSMISSION FLUID Date 04/18 DESCRIPTION: CITGO QuatraSyn Synthetic Transmission Fluid is a full synthetic, multipurpose heavy duty transmission fluid designed for use in a variety of automatic transmission applications and is engineered for severe duty service. CITGO QuatraSyn Synthetic Transmission Fluid improves maintenance efficiency by extending transmission life, resulting in reduced downtime and lower repair costs. QuatraSyn full synthetic technology also has the capability of extending the fluid service life compared to conventional transmission fluids. CITGO QuatraSyn Synthetic Transmission Fluid has a long history of proven performance by having been field tested in buses, refuse vehicles, construction material trucks, trailers and vehicles operating in stop and go conditions. CITGO Quatrasyn Synthetic Transmission Fluid is recommended for use in automatic transmission applications where TES-295 fluid is specified. CITGO QuatraSyn Synthetic Transmission Fluid is not an Allison approved fluid. QUALITIES: APPLICATIONS: CITGO QuatraSyn Synthetic Transmission Fluid is engineered with a proprietary combination of synthetic Group IV and Group V synthetic base oils and high performance additive technology. The unique synthetic formula offers performance benefits that can extend the life of key transmission components, compared with conventional fluids. CITGO QuatraSyn Synthetic Transmission Fluid is built without viscosity modifiers that can shear resulting in viscosity breakdown and loss of power transfer efficiency. CITGO QuatraSyn Synthetic Transmission Fluid provides excellent deposit control and reduces the tendency of fluid breakdown that leads to clutch plate glazing resulting in loss of clutch plate friction control. CITGO QuatraSyn Synthetic Transmission Fluid also provides wide temperature range performance and year around capability. CITGO QuatraSyn Synthetic Transmission Fluid provides: Extended drain and filter change intervals resulting in reduced oil disposal cost. Outstanding low temperature performance. Excellent thermal and oxidation stability resulting in better transmission performance through a reduction in sludge and deposit formation. Shear stability and viscosity retention since it contains NO viscosity modifiers. Optimized traction coefficients which can provide increased fuel economy. Fortified with seal conditioners to reduce the tendency for leakage after extended service. Transmission/Power Fluids CITGO QuatraSyn Synthetic Transmission Fluid is intended for use in the following universal powershift and automatic transmission applications: School Buses and Vans Refuse Fleets Commercial Trucks and Vehicles Motor Homes Emergency Vehicles On/Off-Highway Vehicles Inter/Intracity Buses Light Duty Pickup Trucks and Passenger Cars Recommended for use in automatic transmission applications where C-4 fluid is specified ZF Ecomat transmissions Voith DIWA Transmissions Always consult your owner s manual for proper fluid recommendations and warranty requirements. QuatraSyn is not an Allison approved fluid. (Continued) C

56 CITGO QUATRASYN SYNTHETIC TRANSMISSION FLUID (Continued) Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO QUATRASYN SYNTHETIC TRANSMISSION FLUID Material Code Transmission/Power Fluids Gravity, ASTM D237, API 37.1 Specific Gravity, D Density, lb/gal 6.99 Color Red Flash Point ASTM D92, F ( C) 402 (206) Viscosity ASTM D445, cst at 100 C 7.25 cst at 40 C 36.5 Viscosity Index 171 Brookfield Viscosity ASTM D2983 cp at -40 C 8,200 cp at -20 C 1,025 Pour Point ASTM D97, F ( C) <-87 (<-66) Total Acid Number, ASTM D664, mg KOH/gm Ball Wear, ASTM D kg, 1200 rpm, 1 hour, Cold Cranking Simulator, ASTM D5293, cp at -30 C 2260 CITGO and QuatraSyn are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. QuatraSyn Maintains Critical Viscosity Protection QuatraSyn resists viscosity breakdown during use Viscosity Many Conventional Automatic Transmission Fluids Miles or Hours C

57 Technical Information Fuel & Lubricant Solutions TI/EVO 0140 e April 2018 Page 1 of 3 Automotive Lubricants = registered trademark of BASF SE Emgard 2805 ATF General characterization Approvals Emgard 2805 ATF is a full synthetic, multi-functional fluid for automatic and power shift transmissions. Emgard 2805 ATF is composed of selected basestocks and an advanced additive system which provides excellent performance in General Motors and Allison heavy duty trans-missions. It has been approved for General Motors DEXRON-III, Allison TES-295 and Allison C-4. Allison TES-295 (AN ) Allison TES-468 Allison C-4 ( ) ZF TE-ML 14C Voith H DEXRON -IIIG (G-34746) Performance data Properties Emgard 2805 ATF Test method Transmission/Power Fluids SAE grade 20 SAE J-300 Viscosity, cst ASTM D C C 38.9 Viscosity index 168 ASTM D2270 Viscosity, 40 C, cp 8400 ASTM D2983 Cold cranking simulator viscosity, 2900 ASTM D5293 cp, 30 C Flash point, C ( F) 232 (448) ASTM D92 Fire point, C ( F) 274 (525) ASTM D92 Pour point, C ( F) 55 ( 67) ASTM (Continued) D5950 AP1 gravity, 15.6 C/60 F 35.0 ASTM D287 49

58 TI/EVO 0140 e April 2018 Page 2 of 3 Emgard 2805 ATF Specific gravity, 15.6 C/60 F 0.85 (7.08 lb/gal) ASTM D1298 NOACK evaporative loss, wt% 1 hr, 150 C Four-ball wear, mm scar 40 kg, 1200 rpm, 1 hr, 75 C 0.62 DIN ASTM D2266 Acid number [mg KOH/g] 1.5 ASTM D Application Use Emgard 2805 ATF is recommended for a variety of applications Inter/intra-city buses Vans, school buses Refuse fleets Emergency vehicles Commercial vehicles and trucks Motor homes On/off-highway vehicles Vocational vehicles Light duty pickup trucks and cars where DEXRON III is approved Transmission/Power Fluids Technical application data Advantages of Emgard 2805 ATF: Provides excellent performance due to the selected basestocks and advanced additive system, Emgard 2805 ATF provides high perfor mance and extended drain capabilities in transmissions. Excellent oxidation control Full synthetic Emgard 2805 ATF has excellent thermal and oxidation stability which resists deposit formation. It has extended drain and filter change intervals in Allison TES-295 approved equipment. Advanced wear control The additive system provides excellent protection from corrosion, foaming, rust, and wear. Use over wide temperature range Emgard 2805 ATF utilizes high viscosity index synthetic base fluids which provide superior high/low temperature performance. Emgard 2805 ATF provides friction retention, friction durability, and excellent shear stability to ensure and maintain smooth transmission operations with extended drain intervals. 50

59 TI/EVO 0140 e April 2018 Page 3 of 3 Emgard 2805 ATF Transportation, handling & storage Handling Shelf life Please refer to material safety data sheet for details. The product can stored for at least 3 years at ambient storage conditions and temperature without any deterioration. Note The data contained in this publication are based on our current knowledge and experience. In view of the many factors that may affect processing and application of our product, these data do not relieve processors from carrying out their own investigations and tests; neither do these data imply any guarantee of certain properties, nor the suitability of the product for a specific purpose. Any descriptions, drawings, photographs, data, proportions, weights etc. given herein may change without prior information and do not constitute the agreed contractual quality of the product. It is the responsibility of the recipient of our products to ensure that any proprietary rights and existing laws and legislation are observed. We support worldwide Responsible Care initiatives. We value the health and safety of our employees, customers, suppliers and neighbors, and the protection of the environment. Our commitment to Responsible Care is integral to conducting our business and operating our facilities in a safe and environmentally responsible fashion, supporting our customers and suppliers in ensuring the safe and environmentally sound handling of our products, and minimizing the impact of our operations on society and the environment during production, storage, transport, use and disposal of our products. April 2018 Transmission/Power Fluids North America: BASF Corporation 100 Park Avenue Florham Park NJ USA South America: BASF S/A Av. das Nacöes Unidas 14171, Morumbi Sao Paulo, SP Brazil Asia Pacific: BASF East Asia Regional Headquarters Ltd. 45/F, Jardin House, 1 Connaught Place, Central Hong Kong Europe: BASF SE Fuel and Lubricant Solutions Ludwigshafen Germany 51

60 CITGO TRANSGARD ATF, MERCON V Date 04/18 DESCRIPTION: CITGO TRANSGARD ATF, MERCON V is an advanced extended life automatic transmission fluid designed for Ford transmissions and transaxles. This product may also be used in automatic transmission units that require a fluid qualified against the Ford MERCON specification. QUALITIES: Compared with today s multipurpose ATFs, CITGO TRANSGARD ATF, MERCON V offers superior cold temperature performance, boosted oxidation resistance, extended seal compatibility and improved wear protection. The fluid is very shear resistant, allowing it to maintain its in-service viscosity much better than other ATFs. In addition, this product exhibits superior frictional durability and anti-shudder performance. Fortified against rust, corrosion and foaming. Dyed red for easy identification. Consult owners manual for Fluid Specification. Transmission/Power Fluids APPLICATIONS: CITGO TRANSGARD ATF, MERCON V is recommended for use in all applications requiring MERCON V, MERCON, DEXRON, ALLISON C-4 and JASO 1A. It is also formulated for use in most Toyota, Nissan, Honda and other imported vehicles. This product is an excellent choice for transmissions used in severe service, including passenger car and bus fleets as well as towing applications, and is designed to exhibit extended life compared with conventional multipurpose ATFs. TYPICAL PROPERTIES: CITGO TRANSGARD ATF, MERCON V Material Code Viscosity, cst at 40 C 35 Viscosity, cst at 100 C 7.6 Viscosity Index 189 Specific 60 F Pour Point, ASTM D97, F ( C) -60 (-51) Brookfield -40 C, cp 9600 Appearance Red CITGO and TRANSGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

61 CITGO TRANSGARD ATF, TYPE F Date 04/18 DESCRIPTION: QUALITIES: This product is a red-dyed automatic transmission fluid meeting all of the requirements of Ford Specification M2C33-F, Type F. CITGO TRANSGARD ATF, Type F has the following properties: Oxidation Resistance A high level of oxidation resistance to prevent sludge formation and poor transmission operation even after extended service at high temperatures. Temperature Stability Good low temperature shifting yet retaining the necessary viscosity for proper operation at temperatures in excess of 300 F. Antiwear Selected antiwear additives protect against the scuffing and wear of gears, pumps and other critical moving parts. Lubricity Has a high static coefficient of friction. It is designed specifically to provide proper and reliable operation of clutches requiring a fluid with these unique properties. APPLICATIONS: Seal Life Scientifically balanced formula provides the necessary seal swell properties and prevents the deterioration of rubber seals that otherwise can cause leakage. CITGO TRANSGARD ATF, Type F is recommended for use in all automatic transmissions for which a Type F fluid (Ford Specification M2C33-F) is specified. Always consult owner s manual for manufacturer s recommendation. (Note: Many Ford transmissions require MERCON or Ford Specification M2C138-CJ or M2C166-H. For these applications, CITGO TRANSGARD, Multi Purpose ATF is recommended.) CITGO TRANSGARD Type F is recommended for service fill of power steering units of many Ford passenger cars and light trucks, and can be used in various antiwear hydraulic fluid applications. Consult owner s manual for Fluid Specification. TYPICAL PROPERTIES: Transmission/Power Fluids CITGO TRANSGARD ATF, TYPE F Material Code Gravity, ASTM D4052, API 33.5 Pounds Per Gallon 7.14 Flash Point, COC, ASTM D92, F ( C) 405 (207) Viscosity, ASTM D445, cst at 100 C 7.57 Viscosity, ASTM D 2161, cst at 40 C 41.1 Viscosity, ASTM D 2161, cp at -18 C 1,040 Viscosity, ASTM D 2161, cp at -40 C 38,000 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -43 (-42) Color Red NOTES: (1) Ford Procedure BJ3-2; ASTM D2983, Brookfield Apparent Viscosity CITGO and TRANSGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks (Continued) or trademarks are the property of their respective owners. C

62 CITGO TRANSGARD ATF+4 Date 04/18 DESCRIPTION: CITGO TRANSGARD ATF+4 is a full synthetic automatic transmission fluid recommended for use in Chrysler vehicles. It has been extensively tested and approved by Chrysler under material specification MS QUALITIES: CITGO TRANSGARD ATF+4 has the following qualities: Full Synthetic Formulation provides outstanding protection under the most demanding conditions. Superior wear protection and anti-shudder durability, resulting in a more consistent viscosity profile for improved shift performance and extended transmission life. Improved Low Temperature Operating Range to provide smoother shifts and reduce wear on transmission components during cold weather operation. Increased Oxidation and Thermal Stability to prevent sludge formation and thereby maintain good transmission operation even after extended service at high temperatures. Extended Drain Intervals over previous ATF+3 standard. Transmission/Power Fluids APPLICATIONS: CITGO TRANSGARD ATF+4 has been tested and approved for use by FCA US LLC. It is recommended for top-up and refill of all automatic transmissions in Dodge, Chrysler and Jeep vehicles where ATF+4, ATF+3 or MS 7176 are called for. Do not use ATF+4 where DEXRON -III, DEXRON -IIE, or MERCON automatic transmission fluid is recommended. Consult owner s manual for fluid recommendations. TYPICAL PROPERTIES: Material Code CITGO TRANSGARD ATF+4 Gravity, ASTM D4052, API 34.9 Pounds Per Gallon 7.08 Flash Point, COC, ASTM D92, F ( C) 399 (204) Viscosity, ASTM D445, cst at 40 C cst at 100 C 7.4 cp at C 2,050 cp at -40 C 9,000 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -70 (-57) Color Red Meets Specification MS ATF+4 is a trademark of FCA US LLC, used under license number CITGO and TRANSGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

63 CITGO TRANSGARD CVT FLUID Date 03/18 DESCRIPTION: This Full Synthetic, Continuously Variable Transmission Fluid is specifically formulated to prolong and protect transmission life in modern high technology belt and chain-driven CVT transmissions. It helps maintain smooth operation, reduces transmission wear and degrades less over time. QUALITIES: Maintains viscosity control over the life of the fluid for smooth shifting and fuel economy. Prevents wear in metal contacts while maintaining the proper frictional values to transfer high levels of torque and prevent shudder. Excellent oxidation control to maximize fluid life and maintain chemical properties. APPLICATIONS: CITGO TRANSGARD CVT Fluid is recommended for use in most foreign and domestic belt and chain-driven CVT transmissions and is suitable for use in the following vehicles where CVT Fluid is recommended: Audi/VW TL52180, (G052180), TL52116 (G052516) Mazda JWS 3320 SUBARU i-cvt, ECVT, Lineartronic chain CVT, K0425Y0710, CV-30, NS-2 BMW , , EZL 799 Daihatsu Ammix CVTF-DC, DFC, DFE, TC Dodge/Jeep NS-2, CVT+4, Mopar CVT+4 GM/Saturn DEX-CVT Honda HMMF (without starting clutch) HCF-2, Honda Z-1 (CV-T model, without starting clutch, not SFU for Honda Fit & Jazz) Hyundai/Kia SP-III (CVT model), CVT-J1 Mini Cooper EZL, EZL 799A, ZF CVT V1 Mitsubishi DiaQueen CVTF-J1, J4, J4+, SP-III (CVT model only) Nissan NS-1, NS-2, NS-3 Punch CVT Shell Green 1V Suzuki CVTF 3320, TC, NS-2, CVTF Green 1,2, 1V Toyota TC, FE Volvo CVT 4959 NOT for Non-CVT transmissions. Consult owner s manual for fluid recommendations. Transmission/Power Fluids TYPICAL PROPERTIES: CITGO TRANSGARD CVT FLUID Material Code Gravity, ASTM D287, API 35.3 Density, Pounds Per Gallon 7.1 Flash Point, P.M. D93, C 190 Pour Point, ASTM D97, F ( C) -40 Viscosity, 40 C, cst, D C, cst, D Index, D Brookfield -40 C 13,000 Color Red CITGO and TRANSGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

64 CITGO TRANSGARD DEXRON -VI ATF Date 04/18 DESCRIPTION: CITGO TRANSGARD DEXRON-VI ATF is a full synthetic automatic transmission fluid approved and licensed by General Motors for use in its vehicles with automatic transmissions. This fluid is designed to provide twice the normal service life of a DEXRON-IIIH ATF. It offers enhanced performance for both new and older model transmissions. QUALITIES: Full synthetic formulation providing outstanding protection under the most demanding conditions Extends fluid and transmission life and offers the potential to extend drain intervals Outstanding oxidation life and thermal stability offering resistance to sludge and varnish formation Superior anti-wear protection Improved low temperature viscosity Optimized frictional properties to prevent shudder; and extend fluid and clutch durability Improved fuel economy versus DEXRON-IIIH fluids Increased shear stability Transmission/Power Fluids APPLICATIONS: CITGO TRANSGARD DEXRON-VI ATF is recommended for use in automatic transmissions manufactured by General Motors. The product is backward compatible and can be used in all General Motors cars and trucks where DEXRON-III, DEXRON-IIE and DEXRON-II type fluids were called for. TRANSGARD DEXRON-VI ATF was specifically designed for use in the Hydra-Matic 6-speed transmission. Do not use DEXRON-VI in applications calling for Ford MERCON, MERCON V, MERCON SP, or Type F. DEXRON-VI is not suitable for use in non-gm vehicles which called for DEXRON-III or DEXRON-II type fluids. In these applications CITGO recommends the use of TRANSGARD Multi-Purpose ATF. Consult owner s manual for fluid recommendations. TYPICAL PROPERTIES: CITGO TRANSGARD DEXRON -VI ATF Material Code Gravity, ASTM D 4052, API Pounds Per Gallon 7.05 Flash Point, COC, ASTM D92, F ( C) 403 (206) Pour Point, ASTM D97, F ( C) -65 (-54) Viscosity, ASTM D445, cst at 40 C 29.7 cst at 100 C 6.0 ASTM D2983, cp at -20 C 1,050 cp at -40 C 10,000 Viscosity Index, ASTM D Color Red CITGO and TRANSGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

65 CITGO TRANSGARD HEAVY-DUTY TRANSMISSION FLUIDS Date 04/18 DESCRIPTION: CITGO TRANSGARD Heavy-Duty Transmission Fluids are new generation Allison C-4 and CAT TO-4 transmission and drivetrain fluids. They are designed for heavy-duty construction equipment powershift transmissions, final drives and wet brakes. Compared to engine oil, TRANSGARD Heavy- Duty Transmission Fluids will improve transmission performance and power transfer under conditions of high horsepower output, increased loads, and higher transmission operating temperatures associated with heavy equipment. Base stocks and additives are carefully selected for compatibility with clutch face and seal materials. Available Viscosity Grades: 10W, 30, 50 and 60. QUALITIES: APPLICATIONS: BENEFITS: CITGO TRANSGARD Heavy-Duty Transmission Fluids provide longer transmission life than heavyduty engine oils. In meeting Allison C-4 (SAE 10W and 30 grades), Komatsu Micro-Clutch and Caterpillar TO-4 requirements, CITGO TRANSGARD Heavy-Duty Transmission Fluids offer improved performance while allowing product consolidation. They are offered in four viscosity grades to meet summer and winter powershift requirements. CITGO TRANSGARD Heavy-Duty Transmission Fluids compatibility with asbestos-free clutch materials offers extended clutch life. Due to their physical and chemical properties, TRANSGARD Heavy-Duty Transmission Fluids provide greater power transfer efficiency. These fluids are recommended for lubrication of winch, clutch plates, gears and bearings. They will help reduce brake chatter in wet brake applications. Formulated to meet the performance requirements of: Allison C-4 SAE 10W and 30 grades Caterpillar TO-4, CD/TO-2 all grades Komatsu Micro-Clutch all grades Use of CITGO TRANSGARD Heavy-Duty Transmission Fluids pay big dividends through reduced maintenance costs, longer equipment life, reduced downtime and higher production output. These are provided through reduced gear wear, improved friction control and greater rimpull. Rust and corrosion control protects gear cases and drive trains under the most severe conditions. The SAE 60 grade provides the greatest fluid film thickness for wear protection during severe operation. Transmission/Power Fluids (Continued) CITGO CITGO Petroleum Petroleum Corporation Corporation 800/ / Houston, Houston, Texas Texas Manufactured Manufactured in in USA USA C

66 CITGO TRANSGARD HEAVY-DUTY TRANSMISSION FLUIDS Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO TRANSGARD HEAVY-DUTY TRANSMISSION FLUIDS SAE Grade 10W Material Code Transmission/Power Fluids Gravity, ASTM D4052, API Density, lbs./gallon Flash Point, COC, ASTM D92, F ( C) 420 (216) 446 (230) 511 (266) 532 (278) Viscosity, ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D Brookfield Apparent Viscosity, 23,000 80,000 45, ,500 ASTM D2983, cp, at Temp, C Pour Point, ASTM D97, F ( C) -38 (-39) -27 (-33) +5 (-18) 0 (-18) Color, ASTM D1500 L3.0 L L7.0 CITGO and TRANSGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. CITGO CITGO Petroleum Petroleum Corporation Corporation 800/ / Houston, Houston, Texas Texas Manufactured Manufactured in in USA USA C

67 CITGO SYNDURANCE SYNTHETIC ALL SEASONS HEAVY-DUTY TRANSMISSION FLUID Date 04/18 DESCRIPTION: CITGO SynDurance All Seasons Heavy-Duty Transmission Fluid is a new generation, full synthetic, multigrade, transmission fluid designed for heavy-duty construction equipment with powershift transmissions, hydraulic systems, final drives and wet brakes that require Caterpillar TO-4 and Allisons C-4 type fluids. QUALITIES: The multigrade design reduces inventory by consolidating viscosity grades which eliminates seasonal change outs. The combination of full synthetic base oil and performance engineered additive technology extends transmission life and improves overall efficiency in powershift transmissions as compared to conventional TO-4 fluids. Fluid service life can also be extended when matched with the CITGO LubeAlert HD Oil Analysis Program. The multigrade design improves cold weather start up performance and provides superior wear protection while operating at wide temperature ranges. The unique product design extends clutch life and provides greater power transfer efficiency resulting in greater productivity and reduced fuel consumption. This fluid is recommended for lubrication of winch, clutch plates, gears and bearings. It also helps reduce brake chatter in wet brake applications. APPLICATIONS: BENEFITS: Formulated to meet the performance requirements of: Allison C-4 Caterpillar TO-4, CD/TO-2, TO-4M Komatsu Micro-Clutch Reduces overall operating costs as a result of: Improved drive train productivity and reduced fuel consumption Reduced inventory by consolidating viscosity grades with no seasonal change outs Longer component life Extended fluid change intervals up to two times that of conventional TO-4 fluids Transmission/Power Fluids TYPICAL PROPERTIES: CITGO SYNDURANCE SYNTHETIC ALL SEASONS HEAVY-DUTY TRANSMISSION FLUID Material Code Gravity, ASTM D4052, API 32.4 Density, lbs./gallon 7.0 Flash Point, COC, ASTM D92, F ( C) 453 (234) Viscosity, ASTM D445, cst at 40 C cst at 100 C 14.7 Viscosity Index, ASTM D Brookfield Apparent Viscosity, 37,000 ASTM D2983, cp, at Temp, C -39 Pour Point, ASTM D97, F ( C) -38 (-39) Color, ASTM D1500 L3.0 CITGO and SynDurance are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. CITGO CITGO Petroleum Petroleum Corporation Corporation 800/ / Houston, Houston, Texas Texas Manufactured Manufactured in in USA USA C

68 CITGO TRANSGARD MULTI-PURPOSE ATF Date 04/18 DESCRIPTION: CITGO TRANSGARD Multi-Purpose ATF is an automatic transmission fluid designed for electronicallycontrolled transmissions. This product is specifically designed for use in General Motors transmissions calling for DEXRON -III, DEXRON -IIE and DEXRON -II fluids. It can also be used in Ford transmissions calling for MERCON type ATF s. CITGO TRANSGARD Multi-Purpose ATF meets the performance requirements for Allison Transmission Division (C-4) and major hydraulic pump manufacturers requirements for anti-wear hydraulic fluids QUALITIES: Superior cold temperature performance characteristics. Wide range of seal compatibility. Excellent wear protection. Superior frictional characteristics with excellent friction retention and smooth shifting. Fortified against rust and corrosion. Excellent oxidation resistance. Meets requirements for foam protection. Dyed red for easy identification. Transmission/Power Fluids APPLICATIONS: CITGO TRANSGARD Multi-Purpose ATF is recommended for use in automatic transmissions manufactured by General Motors and Ford for model years 2006 and prior (except those calling for FORD Type F Fluid, MERCON SP, MERCON V, DEXRON -VI and CVT fluids). This product is suitable for use in foreign cars and trucks requiring the use of DEXRON -III, DEXRON -IIE, DEXRON -II fluids, and MERCON type ATF s. CITGO TRANSGARD Multi-Purpose ATF is suitable for use in powershift transmissions, torque converters, hydrostatic transmissions and applications such as in air compressors, hydraulic pumps, power steering boxes and other types of service where an ATF is recommended. CITGO TRANSGARD Multi-Purpose ATF is a truly multifunctional transmission fluid for passenger cars, trucks, construction and mining equipment, farm machinery and other mobile and industrial systems. Consult owner s manual for fluid specification. TYPICAL PROPERTIES: CITGO TRANSGARD MULTI-PURPOSE ATF Material Code Gravity, ASTM D4052, API 32.9 Pounds Per Gallon 7.15 Flash Point, COC, ASTM D92, F ( C) 424 (218) Pour Point, ASTM D97, F ( C) -54 (-48) Viscosity, ASTM D445, cst at 40 C 34.3 cst at 100 C 6.95 ASTM D2983, cp at 20 C 1,020 cp at -40 C 15,100 Viscosity Index, ASTM D Color Red CITGO and TRANSGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

69 CITGO TRANSGARD MULTI-VEHICLE HIGH-VISCOSITY ATF Date 04/18 DESCRIPTION: CITGO TRANSGARD Multi-Vehicle High-Viscosity ATF contains the highest quality synthetic base stocks combined with a state of the art additive system to provide superior performance in automatic and powershift transmissions. It is suitable for use in transmissions calling for Ford MERCON V, Ford MERCON (obsolete), General Motors DEXRON -IIIH (obsolete), and Allison C-4 type fluids. FEATURES/ BENEFITS: Superior oxidation and thermal stability Outstanding anti-wear performance for protection of transmission hardware Excellent cold temperature flow properties Compatible with a wide range of seal materials to prevent transmission leaks Can be used in most vehicles Provides inventory optimization (multi-vehicle compatible) without the use of ATF supplements APPLICATIONS: CITGO TRANSGARD Multi-Vehicle High-Viscosity ATF is suitable for use where the following applications are recommended: Ford MERCON and MERCON V* (In California, use TRANSGARD ATF, MERCON V) GM DEXRON -II and DEXRON -III Allison C-4, TES-295 (not OEM approved), TES-389 (not OEM approved) BMW LT-71141, ETL-7045E, LA-2634, ETL-8072B Nissan/Infiniti Nissan ATF Matic D, Matic J, Matic K and Matic W Mitsubishi Diamond J-2, SP-II and SP-III Hyundai/KIA SP-II and SP-III Toyota/Lexus Type T, T-III and T-IV Honda/Acura ATF-Z1 (except in CVTs) Mercedes Benz 236.3;.5;.6;.7;.8;.9;.91;.10; and.11; ATF 3403 M-115 Volkswagen/Audi G (A2); G052055; G (A1, A2); G (A2); G (A2); GUS ZF TE-ML 11A; 11B JASO 1A MAN 339A Mazda Type T-IV Subaru ATF-HP Renault Matic D2 Volvo ; / ; *Please note that California law prohibits manufacturers of multi-vehicle ATF from recommending products in certain applications where the viscometrics do not match those of the official OEM specification. CITGO therefore does not recommend the use of TRANSGARD Multi-Vehicle High Viscosity ATF in these applications in California. Do not use CITGO TRANSGARD Multi-Vehicle High-Viscosity ATF in vehicles calling for Type F, DEXRON VI, MERCON SP, MERCON LV, Toyota/Lexus WS, and CVT s. Consult owner s manual for fluid specification. (Continued) Transmission/Power Fluids C

70 CITGO TRANSGARD MULTI-VEHICLE HIGH-VISCOSITY ATF (Continued) Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO TRANSGARD MULTI-VEHICLE HIGH-VISCOSITY ATF Material Code Transmission/Power Fluids Viscosity, cst at 40 C 35 Viscosity, cst at 100 C 6.7 Viscosity Index 153 Specific 60 F Pour Point, ASTM D97, F ( C) -49 (-45) Brookfield -40 C, cp 16,280 Appearance Red CITGO and TRANSGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. This is not a licensed OEM product. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

71 CITGO TRANSGARD SYNTHETIC MULTI-VEHICLE LOW-VISCOSITY ATF Date 04/18 DESCRIPTION: QUALITIES: CITGO TRANSGARD Synthetic Multi-Vehicle Low-Viscosity ATF contains the highest quality synthetic base stocks combined with a state of the art additive system to provide superior performance in automatic and powershift transmissions. Superior oxidation and thermal stability Outstanding anti-wear performance for protection of transmission hardware Excellent cold temperature flow properties Compatible with a wide range of seal materials to prevent transmission leaks Can be used in most vehicles Provides inventory optimization (multi-vehicle compatible) without the use of ATF supplements. APPLICATIONS: CITGO TRANSGARD Synthetic Multi-Vehicle Low-Viscosity ATF is suitable for use where the following products are recommended: GM vehicles recommending AW-1. DEXRON -III and VI* (In California, use TRANSGARD DEXRON VI ATF) BMW , , , , , MERCON SP, LV* (Not recommended in California for MERCON LV) Scion FZ Toyota WS (JWS 3324) Honda DW-1, Type 3.0, Type 3.1 Nissan/Infiniti Matic S Hyundai SP-IV Saab AW-1 Mazda 6A EL, 6AX EL Mercedes MB ;.14;.15;.41 Mitsubishi ATF J-3, Dia Queen ATF-PA Porsche ZF Lifeguardfluid 6, 8 *Please note that California law prohibits manufacturers of multi-vehicle ATF from recommending products in certain applications where the viscometrics do not match those of the official OEM specification. CITGO therefore does not recommend the use of TRANSGARD Synthetic Multi-Vehicle Low Viscosity ATF in these applications in California. Transmission/Power Fluids Do not use CITGO TRANSGARD Synthetic Multi-Vehicle Low-Viscosity ATF in vehicles calling for Type F or CVT s. Consult owner s manual for fluid specification. (Continued) C

72 CITGO TRANSGARD SYNTHETIC MULTI-VEHICLE LOW-VISCOSITY ATF (Continued) Date 04/18 DESCRIPTION: QUALITIES: CITGO TRANSGARD Synthetic Multi-Vehicle Low-Viscosity ATF contains the highest quality synthetic base stocks combined with a state of the art additive system to provide superior performance in automatic and powershift transmissions. Superior oxidation and thermal stability Outstanding anti-wear performance for protection of transmission hardware Excellent cold temperature flow properties Compatible with a wide range of seal materials to prevent transmission leaks Can be used in most vehicles Provides inventory optimization (multi-vehicle compatible) without the use of ATF supplements. Transmission/Power Fluids APPLICATIONS: CITGO TRANSGARD Synthetic Multi-Vehicle Low-Viscosity ATF is suitable for use where the following products are recommended: GM vehicles recommending AW-1. DEXRON -III and VI* (In California, use TRANSGARD DEXRON VI ATF) BMW , , , , , MERCON SP, LV* (Not recommended in California for MERCON LV) Scion FZ Toyota WS (JWS 3324) Honda DW-1, Type 3.0, Type 3.1 Nissan/Infiniti Matic S Hyundai SP-IV Saab AW-1 Mazda 6A EL, 6AX EL Mercedes MB ;.14;.15;.41 Mitsubishi ATF J-3, Dia Queen ATF-PA Porsche ZF Lifeguardfluid 6, 8 *Please note that California law prohibits manufacturers of multi-vehicle ATF from recommending products in certain applications where the viscometrics do not match those of the official OEM specification. CITGO therefore does not recommend the use of TRANSGARD Synthetic Multi-Vehicle Low Viscosity ATF in these applications in California. Do not use CITGO TRANSGARD Synthetic Multi-Vehicle Low-Viscosity ATF in vehicles calling for Type F or CVT s. Consult owner s manual for fluid specification. (Continued) C

73 CITGO TRANSGARD TRACTOR HYDRAULIC FLUIDS Date 04/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO TRANSGARD Tractor Hydraulic Fluids (including CITGO TRANSGARD Lo-Temp Tractor Hydraulic Fluid) are multifunctional tractor hydraulic/transmission fluids which perform the following functions: Lubricate the transmission, differential and final drive gears. Act as a power steering, power brake, power take-off and implement drive fluid. Provide a medium with the correct friction and heat transfer characteristics for proper operation of the tractor wet brakes and power take-off unit. CITGO TRANSGARD Lo-Temp Tractor Hydraulic Fluid is specially designed to provide outstanding low temperature fluidity under the coldest conditions. It has the same performance benefits as CITGO TRANSGARD Tractor Hydraulic Fluid, but is intended for applications where a lower viscosity fluid is desired. It should not be used at ambient temperatures above 68 F. The following characteristics make CITGO TRANSGARD Tractor Hydraulic Fluids outstanding products for multi-functional application: Superior extreme pressure (EP) and antiwear performance protects tractor transmissions, axles and hydraulic pumps. The frictional characteristics are designed to minimize chatter while permitting the wet brakes to hold properly. This frictional balance also provides smooth engagement of the power take-off clutch. Special blend of base stocks helps maintain seals and gaskets. Balanced formulations provide excellent rust and corrosion protection as well as excellent oil oxidation stability for high-temperature service. CITGO TRANSGARD Tractor Hydraulic Fluids For use in equipment where the following fluids are recommended: AGCO Power Fluid 821XL Allison C-4 API GL-4 CAT TO-2 Case MS 1205, 1206, 1207,1209, 1210 Case New Holland: MAT 3525 Denison HF-0, HF-1, HF-2 Eaton Vickers I-286-S, M-2950-S Ford New Holland ESN-M2C134-D FNHA 2C 201 John Deere J20C/J20D (Low-Temp Only) Kubota UDT Massey Ferguson M-1135, M-1141, M-1143, M-1145 Volvo WB101 White Q-1826 ZF TE-ML-03E, -05, -06 Transmission/Power Fluids Suitable for use in: AGCO Case IH David Brown Ford John Deere KH Deutz Komatsu Kubota Mahindra Massey Ferguson New Holland Volvo White and others (Continued) C

74 CITGO TRANSGARD TRACTOR HYDRAULIC FLUIDS (Continued) Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO TRANSGARD TRACTOR HYDRAULIC FLUIDS Transmission/Power Fluids TRACTOR HYDRAULIC FLUID LOW-TEMP TRACTOR HYDRAULIC FLUID Material Code Gravity, ASTM D4052, API Density, lb/gal Flash Point, COC, ASTM D92, F ( C) 450 (232) 406 (208) Viscosity, ASTM D2983, cp at -4 F (-20 C) 4,500 1,500 Viscosity, ASTM D 2983, cp at -29 F (-35 C) 18,100 Viscosity, ASTM D 2983, cp at -40 F (-40 C) 15,300 ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -40 (-40) -54 (-48) Color, ASTM D ASTM D892, Sequence I, II, III Pass Pass CITGO and TRANSGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

75 CITGO ALUMINUM COMPLEX PL GREASE Date 04/18 DESCRIPTION: CITGO Aluminum Complex PL Greases are developed with unique semi-fluid formulas to provide exceptional flow performance. They are optimized to provide consistent lubricant flow for optimal protection of frac pump plungers. Properly lubricated plungers can operate at peak performance, maximizing up time. QUALITIES: Superior lubricant barrier to prevent seal failures Protects against friction and heat damage Exceptional extreme pressure (EP) protection Excellent anti-wear prolongs plunger life Outstanding resistance to rust and corrosion on copper and brass Performs well over a wide temperature range APPLICATIONS: For use with frac pump plungers where excellent adhesion, pumpability, corrosion resistance, wear and extreme pressure protection are needed. Designed to work with automatic lubricators. Consult owner s manual for proper lubricant selection. TYPICAL PROPERTIES: CITGO ALUMINUM COMPLEX PL GREASE Material Code NLGI Grade Worked Penetration, ASTM D Thickener Type Aluminum Complex Aluminum Complex Color Red Red Texture Smooth, Adhesive Smooth, Adhesive Rust Prevention, ASTM D1743 Pass Pass Copper Corrosion, ASTM D4048 1b 1b Four-Ball Wear, ASTM D2266, mm Four-Ball Weld, ASTM D2596, kgf US Steel 0 F, gpm 18 Approximate Temperature Range, F ( C) 0 to 325 (-18 to 163) 10 to 325 (-12 to 163) Base Oil Viscosity: 40 C, cst Greases CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. CITGO Petroleum Corporation 800/ Houston, Texas Manufactured in in USA USA C

76 CITGO CALSUPLEX MP GREASE Date 04/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Calsuplex MP Grease is specially formulated with a calcium sulfonate thickener in premium base oils to provide excellent performance in a wide variety of automotive, heavy duty, and industrial applications. It provides dependable performance in a broad range of applications including automotive chassis, wheel bearings, and industrial bearings. It provides excellent corrosion control for high moisture environments. Exceptional Corrosion Protection: CITGO Calsuplex MP Grease provides superior protection against corrosion in the presence of water. Extreme Pressure and Anti-Wear Protection: CITGO Calsuplex MP Grease provides excellent extreme pressure and anti-wear protection under severe conditions. Oxidation Resistance: Calsuplex MP Grease provides outstanding resistance to oxidation. Water Resistance: This product is highly resistant to water washout. CITGO Calsuplex MP Grease is recommended for a wide range of automotive and industrial applications including bearings, ball joints, and bushings. It meets the ASTM D4950 requirements for Wheel Bearing Grease Category GC and Chassis Grease Category LB. Consult owner s manual for proper lubricant selection. TYPICAL PROPERTIES: CITGO CALSUPLEX MP GREASE Greases SAP Code NLGI Grade 2 Worked Penetration, ASTM D Thickener Type Calcium Sulfonate Color Green Texture Smooth, Adhesive Dropping Point, ASTM D2265 F( C) 500 (260) Rust Prevention, ASTM D1743 Pass Water Washout, ASTM D1264, % 175 F 2.5 Low Temperature Torque, ASTM D4693, Nm 9.6 High Temperature Life, ASTM D3527, hrs. 120 Four-Ball Wear, ASTM D2266, mm.05 Four-Ball Weld, ASTM D2596, kgf 400 Four-Ball Load Wear Index, ASTM D2596, kgf 57.7 NLGI Certified, ASTM 4950 GC-LB ISO Viscosity Grade 150 CITGO, CITGARD and SynDurance are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

77 CITGO COTTON PICKER SPINDLE GREASE Date 03/18 DESCRIPTION: FEATURES: APPLICATIONS: CITGO Cotton Picker Spindle Grease is a unique semi-fluid formula developed to provide exceptional flow performance. It is optimized to provide consistent flow for optimal protection of the picker spindles. This fluidity allows it to lubricate in tough applications. Properly lubricated spindles can operate at peak performance, plucking cotton from bolls without tearing. Special semi-fluid, lithium-based grease that provides low friction and channeling resistance Flows freely, but resists excessive leakage from spindle bearings Performs well over a wide temperature range resulting in low cold-weather starting torque Soft consistency, channel resistant Resists leakage from bearings reducing cotton staining Easy to dispense or pump For use in low to normal temperatures under light loads. Consult owner s manual for proper lubricant selection. TYPICAL PROPERTIES: CITGO COTTON PICKER SPINDLE GREASE NLGI Grade 00 Material Code Thickener Type Lithium Stearate Texture Smooth, Short Fiber Color, Observed Light Green, Low-Staining Worked Penetration, ASTM D Approximate Temperature Range, F ( C) 5 to 200 (-15 to 93) Base Oil Viscosity: 40 C, cst 20 CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Greases C

78 CITGO JET LUBRICANT TM Date 04/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Jet Lubricant TM is a quality soap-thickened petroleum resin based compound for use as a Traction Motor Gear Lubricant in heavy duty, high speed locomotive gear boxes. It provides an adhesive film that protects gears under heavy loads. CITGO Jet Lubricant TM is formulated from petroleum resins to ensure good adhesion. CITGO Jet Lubricant TM is available in drums and in one pound polyethylene bags for ease of application. CITGO Jet Lubricant TM is an excellent lubricant for various open and closed gear cases and certain slow moving open gears used throughout the industry. GE Specification D50 E8C Consult owner s manual for proper lubricant selection. TYPICAL PROPERTIES: CITGO JET LUBRICANT TM Material Code Soap Type Sodium Texture Tacky Color Dark Brown Brookfield Viscosity, cp at 200 F 5,000-10,000 Timken OK Load, ASTM D2509, lbs 40 Four Ball EP Weld, ASTM D2596, kgf 250 Load Wear Index, ASTM D CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Greases C

79 CITGO LITHOPLEX CM & HM GREASES Date (Continued) 04/18 DESCRIPTION: QUALITIES: CITGO Lithoplex CM and Lithoplex HM greases provide outstanding protection in construction and mining applications where exceptional wear protection is required due to heavy shock load conditions. These premium quality lithium complex greases contain molybdenum disulfide for additional protection in harsh environments which reduces frictional and abrasive wear on components. The results are increased equipment life and lower maintenance costs. The CITGO Lithoplex grease family represents the latest technology in greases. These Lithoplex greases contain extreme pressure (EP) additives, anti-wear (AW) additives, oxidation inhibitors, and corrosion inhibitors. They are suitable for use at higher temperatures than conventional soap greases. Extreme Pressure and Wear Protection: Lithoplex CM and Lithoplex HM provide excellent extreme pressure and anti-wear protection. Lithoplex CM contains 3% moly disulfide and Lithoplex HM contains 5% moly disulfide to provide additional protection in harsh environments. These products are a good choice in applications where metal to metal friction and high loads exist. Corrosion Protection: Lithoplex CM and HM are formulated to resist corrosion, thereby extending equipment life. This is of particular importance in applications where moisture is present. Oxidation Resistant Formulation: These greases contain oxidation inhibitors to extend grease life and protect the application for longer periods. Polymer Fortified: Lithoplex CM and Lithoplex HM contain polymer for improved water resistance and improved adhesion. APPLICATIONS: Lithoplex CM contains three percent moly disulfide and Lithoplex HM contains five percent moly disulfide to meet equipment manufacturer s requirements. Applications include construction equipment, mining equipment, fifth wheels, industrial applications, bucket pins, crusher bearings, pin and bushings, pivot pins, track drive rollers. Consult owner s manual for proper lubricant selection. Greases (Continued) C

80 CITGO LITHOPLEX CM & HM GREASES (Continued) Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO LITHOPLEX CM & HM GREASES Lithoplex Lithoplex Lithoplex Lithoplex Product CM1 CM2 HM1 HM2 NLGI Grade Material Code Worked-60 Penetration Grease Type Lithium Lithium Lithium Lithium Complex Complex Complex Complex Color Gray Gray Gray Gray Texture Smooth, Smooth, Smooth, Smooth, Adhesive Adhesive Adhesive Adhesive Four-Ball Weld, ASTM D2596, kgf Four-Ball Load Wear Index, ASTM D Four-Ball Wear, ASTM D2266, mm Rust Protection, ASTM D1743 Pass Pass Pass Pass Water Washout, 175 F, ASTM D1264, % Loss Dropping Point, ASTM D2265, F Molybdenum Disulfide, % Viscosity: 40 C, cst CITGO and Lithoplex are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Greases C

81 CITGO LITHOPLEX Date 04/18 MP GREASES DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Lithoplex MP Greases represent the latest technology in greases. They are quality extreme pressure greases designed to be highly versitle and have long life. They provide dependable performance in a broad range of applications including automotive chassis, wheel bearing and other critical grease points. Excellent performance over a wide temperature range. CITGO Lithoplex MP Greases are multipurpose greases incorporating the following characteristics: Excellent Mechanical Stability Extremely stable lithium complex formula retains its consistency even in the most severe service. Extreme Pressure and Anti-Wear Protection Additives provide excellent extreme pressure and anti-wear protection under severe conditions. Corrosion Protection Lithoplex MP greases resist corrosion, thereby extending equipment life. This is of particular importance in applications where moisture is present. Oxidation Resistant Formulation Lithoplex MP greases contain oxidation inhibitors to extend grease life and protect the application for longer periods. Lithoplex MP Greases are compatible with conventional lithium soap greases. They contain extreme pressure (EP) additives and Molybdenum Disulfide (moly) to minimize wear in heavily loaded components. These greases satisfy a wide range of industrial and automotive applications including bearings, ball joints and bushings. Three NLGI consistencies are available. Lithoplex MP 1 and MP 2 Greases meet the ASTM D4950 requirements for Wheel Bearing Grease Category GC and Chassis Grease Category LB. Consult owner s manual for proper lubricant selection. AUTOMOTIVE WHEEL BEARING & CHASSIS LUBRICANT GC-LB Greases (Continued) (Continued) C

82 CITGO LITHOPLEX MP GREASES Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO LITHOPLEX MP GREASES Product Lithoplex MP0 Lithoplex MP1 Lithoplex MP2 NLGI Grade Material Code Worked Penetration, ASTM D Thickener Type Lithium Complex Lithium Complex Lithium Complex Color Gray Gray Gray Texture Smooth, Adhesive Smooth, Adhesive Smooth, Adhesive Four-Ball Weld, ASTM D2596, kgf Four-Ball Load Wear Index, ASTM D Four-Ball Wear, ASTM D2266, mm Rust Prevention, ASTM D1743, rating Pass Pass Pass Water Washout, 175 F, ASTM D1264, % Loss Dropping Point, ASTM D2265, F ( C) 500 (260) 530 (277) NLGI Certified, ASTM D4950 GC-LB GC-LB Viscosity: 40 C, cst CITGO and Lithoplex are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Greases C

83 CITGO LITHOPLEX PM GREASE Date 03/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Lithoplex PM Grease is designed to provide outstanding performance in industrial applications. This product provides excellent protection in severe applications of plain and rolling bearings that operate in mild to high temperatures. CITGO Lithoplex PM Grease is recommended for use in many other industrial, agricultural, and mining applications where exceptional wear protection and outstanding extreme pressure/high load protection is required. Corrosion Protection: CITGO Lithoplex PM Grease protects equipment from corrosion and passes the ASTM D1743 Corrosion Test. Extreme Pressure Protection: This product provides excellent protection in applications where high loads exist. CITGO Lithoplex PM Grease has a high Timken OK Load rating. Wear Protection: This product provides superior protection in applications where metal to metal friction exists. CITGO Lithoplex PM Grease has a low Four-Ball Wear Scar. Stays in Place: CITGO Lithoplex PM Grease is polymer fortified for improved adhesion. Water Resistance: The polymer fortification makes CITGO Lithoplex PM Grease highly resistant to water. CITGO Lithoplex PM Grease is a versatile lithium complex grease that will hold up in many situations where other products fail. This product is recommended for applications where outstanding wear protection, water resistance, corrosion resistance, and extreme pressure protection is required. Consult owner s manual for proper lubricant selection. TYPICAL PROPERTIES: CITGO LITHOPLEX PM GREASE NLGI Grade 2 Material Code Worked Penetration, ASTM D Thickener Lithium Complex Color Red Texture Smooth, Adhesive Dropping Point, ASTM D2265, F ( C) 500 (260) Rust Prevention, ASTM D1743, rating Pass Water Washout, ASTM D1264, % 175 F 2.5 Timken OK Load, ASTM D2509, Lb. 80 Four-Ball Wear, ASTM D2266, mm 0.48 Base Oil Viscosity: 40 C, cst 155 Greases CITGO and Lithoplex are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

84 CITGO LITHOPLEX Date 04/18 RED MP GREASES DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Lithoplex Red MP Grease represents the latest technology in greases. It is a quality Lithium Complex grease that is very versatile and provides long life with extreme pressure performance. Recommended for a wide variety of applications including automotive chassis and wheel bearings, industrial plain and rolling element bearings. Excellent performance over a wide temperature range. CITGO Lithoplex Red MP Grease is a multipurpose grease incorporating the following characteristics: Excellent Work Stability Extremely stable lithium complex formula retains its consistency even in the most severe service. Extreme Pressure and Anti-Wear Protection Additives provide excellent extreme pressure and anti-wear protection under severe conditions. Corrosion Protection Resists corrosion, thereby extending equipment life. This is of particular importance in applications where moisture is present. Oxidation Resistant Formulation Contains oxidation inhibitors to extend grease life and protect the application for longer periods. CITGO Lithoplex Red MP Grease is compatible with conventional lithium soap greases. It contains extreme pressure (EP) additives to minimize wear in heavily loaded components. This grease satisfies a wide range of industrial and automotive applications including bearings, ball joints and bushings. CITGO Lithoplex Red MP Grease meets the ASTM D4950 requirements for Wheel Bearing Grease Category GC and Chassis Grease Category LB. Labels display the NLGI Certification Mark GC-LB for Automotive Wheel Bearing & Chassis Lubricant. Consult owner s manual for proper lubricant selection. CLASSIFICATION: AUTOMOTIVE WHEEL BEARING & CHASSIS LUBRICANT GC-LB TYPICAL PROPERTIES: CITGO LITHOPLEX RED MP GREASE Greases Product Lithoplex Red MP NLGI Grade 2 Material Code Worked Penetration, ASTM D Thickener Type Lithium Complex Color Red Texture Smooth, Adhesive Four-Ball Weld, ASTM D2596, kgf 315 Four-Ball Load Wear Index, ASTM D Four-Ball Wear, ASTM D2266, mm 0.43 Rust Prevention, ASTM D1743 Pass Water Washout, ASTM D1264, % 175 F 1.4 Dropping Point, ASTM D2265, F ( C) 500 (260) NLGI Certified, ASTM D4950 GC-LB Base Oil Viscosity: 40 C, cst 205 CITGO and Lithoplex are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

85 CITGO LITHOPLEX Date 04/18 RT GREASES DESCRIPTION: QUALITIES: APPLICATIONS: APPROVALS: The CITGO Lithoplex RT Greases represent the latest technology in greases. They are premium quality lithium complex greases suited for a wide variety of industrial and automotive service applications including chassis and wheel bearings. These extreme pressure greases are recommended for use across several industries that include on-road, off-road and industrial applications. CITGO Lithoplex RT Greases are multipurpose greases incorporating the following characteristics: Excellent Work Stability Extremely stable lithium complex formula retains its consistency even in the most severe service. Extreme Pressure and Anti-Wear Protection Additives provide excellent extreme pressure and anti-wear protection under severe conditions. Corrosion Protection Lithoplex RT greases resist corrosion, thereby extending equipment life. This is of particular importance in applications where moisture is present. Oxidation Resistant Formulation Lithoplex RT greases contain oxidation inhibitors to extend grease life and protect the application for longer periods. CITGO Lithoplex RT Greases provide excellent performance in applications where good adhesion and water resistance are critical. Their red color and tacky, moly-free formula make them ideal for many problem applications. They are excellent for use in many industrial, agricultural, and automotive applications. Consult owner s manual for proper lubricant selection. Mack MG-C AUTOMOTIVE WHEEL BEARING & CHASSIS LUBRICANT GC-LB TYPICAL PROPERTIES: CITGO LITHOPLEX RT GREASES Product Lithoplex RT1 Lithoplex RT2 NLGI Grade 1 2 Material Code Worked Penetration, ASTM D Thickener Type Lithium Complex Lithium Complex Color Red Red Texture Smooth, Adhesive, Buttery Smooth, Adhesive, Buttery Four-Ball Weld, ASTM D2596, kgf Four-Ball Load Wear Index, ASTM D Four-Ball Wear, ASTM D2266, mm Rust Protection, ASTM D1743 Pass Pass Water Washout, ASTM D1264, % 175 F Dropping Point, ASTM D2265, F ( C) 500 (260) 530 (277) NLGI Certified, ASTM D4950 GC-LB GC-LB Oil 40 C, cst., with Oil Sol. Additives Greases CITGO and Lithoplex are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

86 CITGO LITHOPLEX ST GREASES Date 04/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Lithoplex ST Greases represent the latest technology in greases. They are high performance Lithium Complex greases that are industry tested to withstand high shock loads, extreme pressures and corrosive environments under a variety of mill conditions. Highly recommended for use in rolling mills, work rolls, strip mills, drive u-joint and conveyer bearings. Lithoplex ST greases are also recommended for use in other industrial equipment involving frequent contact with water. CITGO Lithoplex ST Greases are multipurpose greases incorporating the following characteristics: Excellent Work Stability Extremely stable lithium complex formula retains its consistency even in the most severe service. Extreme Pressure and Anti-Wear Protection Additives provide excellent extreme pressure and anti-wear protection under severe conditions. Corrosion Protection Lithoplex ST greases resist corrosion, thereby extending equipment life. This is of particular importance in applications where moisture is present. Oxidation Resistant Formulation Lithoplex ST greases contain oxidation inhibitors to extend grease life and protect the application for longer periods. CITGO Lithoplex ST Greases are high-temperature greases that provide exceptional water resistance and stability that is critical in many primary and secondary mill applications. CITGO Lithoplex ST Greases contain heavy base oils to provide for good load and wear protection. They provide excellent protection against corrosion making CITGO Lithoplex ST Greases a good choice in many high moisture environments. Consult owner s manual for proper lubricant selection. TYPICAL PROPERTIES: CITGO LITHOPLEX ST GREASES Greases Product Lithoplex ST Lithoplex ST NLGI Grade 1 2 Material Code Worked Penetration, ASTM D Thickener Type Lithium Complex Lithium Complex Color Green Green Texture Smooth, Adhesive Smooth, Adhesive Four-Ball Weld, ASTM D2596, kgf Four-Ball Load Wear Index, ASTM D Four-Ball Wear, ASTM D2266, mm Rust Prevention, ASTM D1743 Pass Pass Water Washout, ASTM D1264, % 175 F Timken OK Load, ASTM D2509, lb USS Grease Mobility, 0 F, gpm Base Oil Viscosity: 40 C, cst CITGO and Lithoplex are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

87 CITGO LITHOPLEX PL GREASES Date 04/18 DESCRIPTION: FEATURES: APPLICATIONS: CITGO Lithoplex PL Greases are developed with unique semi-fluid formulas to provide exceptional flow performance. They are designed to provide consistent lubricant flow for optimal protection of frac pump plungers. Properly lubricated plungers can operate at peak performance, maximizing up time. Superior lubricant barrier to prevent seal failures Protects against friction and heat damage Exceptional extreme pressure (EP) protection Excellent anti-wear prolongs plunger life Outstanding resistance to rust and corrosion on copper and brass Performs well over a wide temperature range For use with frac pump plungers where excellent adhesion, pumpability, corrosion resistance, wear and extreme pressure protection are needed. Designed to work with automatic lubricators. Consult owner s manual for proper lubricant selection. TYPICAL PROPERTIES: CITGO LITHOPLEX PL GREASES NLGI Grade Material Code Thickener Type Lithium Complex Lithium Complex Lithium Complex Texture Smooth, Short Fiber Smooth, Short Fiber Smooth, Short Fiber Color, Observed Green Green Green Worked Penetration, ASTM D Four-Ball Weld, ASTM D2596, kg Four-Ball Wear, ASTM D2266, mm Copper Corrosion, ASTM D4048 1a 1a 1a Rust Prevention, ASTM D1743 Pass Pass Pass US Steel 0 F, gpm Approximate Temperature Range, F ( C) 0 to 325 (-18 to 163) 0 to 325 (-18 to 163) 0 to 325 (-18 to 163) Base Oil 40 C, cst Greases CITGO and Lithoplex are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

88 CITGO LITHOPLEX Date 03/18 PTG GREASE DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Lithoplex PTG Grease is an excellent choice for the lubrication of bearings and gears found in power tools. It is a high quality grease that ensures peak performance of the tool in prolonged industrial or construction applications. Proper lubrication not only extends the effective service life of the tool, but also improves the operating efficiency. CITGO Lithoplex PTG Grease has the ability to resist sudden stress, sustain performance, and absorb shock loads without losing the ability to lubricate gears and bearings effectively. CITGO Lithoplex PTG Grease is a specially designed lubricant with the following characteristics: Long life Improved tool efficiency Extreme pressure and anti-wear Low bleed solution Excellent film strength Heat resistant Excellent thermal oxidation stability CITGO Lithoplex PTG Grease satisfies a wide range of industrial and home tool applications, lubricating bearings and gears. Consult owner s manual for proper lubricant selection. TYPICAL PROPERTIES: CITGO LITHOPLEX PTG GREASE Greases NLGI Grade 2 Material Code Worked Penetration, ASTM D Thickener Type Lithium Complex Color Amber Texture Smooth, Tacky Timken OK Lead, ASTM D2509, lb. 45 Four-Ball Weld, ASTM D2596, kgf 315 Four-Ball Wear, ASTM D2266, mm 0.54 Rust Protection, ASTM D1743 Pass Copper Corrosion Protection, ASTM D4048 1a Oil Separation, ASTM D1742 Nil Viscosity: 40 C, cst 630 CITGO and Lithoplex are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

89 CITGO LITHOPLEX WPM NO. 1 Date 03/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Lithoplex WPM No. 1 is a premium quality high performance lithium complex grease designed to provide outstanding protection in wood pellet mill applications. Extreme Pressure and Wear Protection: CITGO Lithoplex WPM No. 1 provides outstanding protection against wear and extreme pressure. Rust Protection: This product protects equipment against corrosion and passes the ASTM D1743 rust prevention test. Oxidation Resistant: CITGO Lithoplex WPM No. 1 is formulated with additives that protect against oxidation and extend the lubricant life. Water Resistance: CITGO Lithoplex WPM No. 1 is formulated with premium quality ISO 460 base oils that make this product highly water resistant. Additional benefits of the high viscosity base oils include providing an outstanding barrier between the metal surfaces and giving the grease an adhesive texture that keeps the product in place. CITGO Lithoplex WPM No. 1 is suitable for a variety of industrial, agricultural, mining, and construction applications. This product is particularly well suited for use in wood pellet mills. Consult owner s manual for proper lubricant selection. TYPICAL PROPERTIES: CITGO LITHOPLEX WPM NO. 1 Material Code NLGI Grade 1 Worked Penetration, ASTM D Thickener Type Lithium Complex Color Amber Texture Smooth/Adhesive Dropping Point, ASTM D2265, F ( C) 500 (260) Rust Prevention, ASTM D1743 Pass Four-Ball Wear, ASTM D2266, mm 0.43 Four-Ball Weld, ASTM D2596, kgf 315 Base Oil Viscosity 100 C, cst Base Oil Viscosity 40 C, cst Viscosity Index 95 CITGO is a registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Greases C

90 CITGO OVERDRIVE HD GREASE Date 03/18 DESCRIPTION: CITGO OverDrive HD Grease is designed for applications where outstanding protection is required. With engine oil drain and relubrication intervals being extended, it is important to use a grease that provides superior performance that will protect and stay put, even under a wide variety of conditions. OverDrive HD is the ultimate grease for extended service applications. QUALITIES: Corrosion Protection: OverDrive HD provides outstanding corrosion protection even in severe conditions where salt water is present. OverDrive HD passes the Emcor Dynamic Corrosion Test and the 5% Synthetic Sea Water Corrosion Test in addition to passing the standard ASTM D1743 Corrosion Test. Extreme Pressure and Wear Protection: This product provides excellent protection in applications where metal-to-metal friction and high loads exist. OverDrive HD offers an impressive Weld Point and a high Timken OK Load. Stays In Place: OverDrive HD is polymer fortified for improved adhesion. Stability: This product has outstanding stability and resists softening even in conditions where water contamination is present. OverDrive HD is highly resistant to water in conditions where rain or road splash are present. Grease Compatibility: OverDrive HD is formulated with a proprietary Lithium Complex thickener system that is compatible with many other greases that are currently on the market. APPLICATIONS: OverDrive HD Grease is an extremely versatile product that will hold up in situations where other products fail. It is recommended for use in fifth wheels, spring pins, chassis lubrication, king pins, and universal joints. OverDrive HD is recommended for applications where extreme stability, water resistance, corrosion resistance, wear protection, and EP protection are required. OverDrive HD is not recommended for use in disc brake wheel bearings. Due to the heavy base oil viscosity and tenacious polymer, OverDrive HD will stay put and provide excellent performance in many off-road construction and mining applications. Consult owner s manual for proper lubricant selection. Greases (Continued) C

91 CITGO OVERDRIVE HD GREASE Date 03/18 - (Continued) TYPICAL PROPERTIES: CITGO OVERDRIVE HD GREASE NLGI Grade 2 Material Code Thickener Type Lithium Complex Color Green Texture Smooth, Adhesive Dropping Point, ASTM D2265, F ( C) 430 (221) Worked Penetration, ASTM D Rust Prevention, ASTM D1743, rating Pass Emcor, ASTM D6138 Pass 5% Synthetic Salt Water Corrosion, ASTM D5969 Pass Water Washout, ASTM D1264, % Loss at 100 F 1.4 Water Spray Off, ASTM D4049, % Loss 15.1 Timken OK Load, ASTM D2509, lb. 65 Four-Ball Wear, ASTM D2266, mm 0.4 Four-Ball Weld, ASTM D2596, kgf 500 USS Grease Mobility, 0 F, gpm 12.5 Viscosity: 40 C, cst 540 CITGO and Overdrive HD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Greases C

92 CITGO PREMIUM COUPLING GREASE Date 04/18 DESCRIPTION: BENEFITS: CITGO Premium Coupling Grease is specially formulated with a lithium/polymer thickener in premium high viscosity base oils to provide excellent resistance to oil separation when used in high-speed grease lubricated couplings. Minimal Oil Separation: CITGO Premium Coupling Grease exhibits very low oil separation in ASTM D4425 high-speed centrifuge test. Excellent adhesion: This product is fortified with heavy base oils and a polymer additive to provide outstanding adhesion. Load Carrying: High viscosity base oils are utilized to provide outstanding load carrying ability. Versatility: This product is recommended for all types of grease lubricated couplings used in industrial equipment. It meets or exceeds the requirements of AGMA CG-1, CG-2 & CG-3 type coupling greases. Oxidation Resistance: Premium Coupling Grease provides outstanding resistance to oxidation. Water Resistance: This product is highly resistant to both water washout and water spray-off. Grease Compatibility: Premium Coupling Grease is formulated with a lithium/polymer thickener system that is compatible with many other coupling greases that are currently on the market. Greases APPLICATIONS: Premium Coupling Grease is recommended for grease lubricated couplings including gear couplings, grid couplings, and flexible chain couplings. Because of its water resistance and high viscosity base oils, it may be suitable for use in applications subjected to high water wash, heavy loads, and low speeds. Premium Coupling Grease is not recommended for use in rolling element bearings. Consult owners manual for proper lubricant recommendation. TYPICAL PROPERTIES: CITGO PREMIUM COUPLING GREASE SAP Code NLGI Grade 0-1 Worked Penetration, ASTM D Thickener Type Lithium/Polymer Color Amber Texture Smooth, Adhesive Dropping Point, F( C), ASTM D (169) Rust Prevention, ASTM D1743 Pass Copper Corrosion, ASTM D4048 1b Centrifugal Oil Separation, ASTM D4425 <8% Oxidation, ASTM D942, psi 100 hrs 3 Water Spray Off, ASTM D4049, % Loss <2% Four-Ball Wear, ASTM D2266, mm 0.4 Four-Ball Weld, ASTM D2596, kgf 400 Four-Ball Load Wear Index, ASTM D2596, kgf 63.4 Oil 100 C, cst, with Oil Sol. Additives 191 Oil 40 C, cst, with Oil Sol. Additives 4240 Viscosity Index with Oil Sol. Additives 148 CITGO, and CompressorGard are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

93 CITGO PREMIUM LITHIUM EP GREASES Date 04/18 DESCRIPTION: BENEFITS: CITGO Premium Lithium EP Greases are premium quality, lithium soap thickened greases containing extreme pressure, antiwear, antioxidant, and anticorrosion additives. These greases are formulated with high quality base stocks. The smooth, buttery texture of the grease in conjunction with high quality mineral oil provides excellent pumpability over a wide temperature range. The extreme pressure agent provides the protection required to handle severe conditions characterized by high shock loads. Oxidation and corrosion inhibitors, and a high quality soap yield a product with excellent shear stability, load carrying properties, corrosion resistance and oxidation stability. The combination of these properties makes CITGO Premium Lithium EP Greases extremely versatile, thereby reducing the number of products required. Substantial reductions in storage and handling costs are possible with these universal products, while at the same time reducing potential of costly equipment failures associated with misapplication of product. The service temperature range of these greases is 5 F to 250 F continuous, with peak intermittent temperatures up to 300 F. APPLICATIONS: CITGO Premium Lithium EP Greases are recommended for the lubrication of both journal and antifriction bearings in a wide variety of applications such as metallurgical industry equipment and general industrial machinery. CITGO Premium Lithium EP Greases are particularly adaptable for centralized lubrication systems and for bulk handling systems, both for bulk truck delivery and portable containers. They are approved under Chrysler Specification MS-3701 and Cincinnati Lamb P-64/P-72. NLGI Grades 1 and 2 meet the ASTM D4950 requirements for Chassis Grease Category LB. Consult owner s manual for proper lubricant selection. Greases (Continued) (Continued) C

94 CITGO PREMIUM LITHIUM EP GREASES Date (Continued) 04/18 - (Continued) APPROVALS: General Motors LS-2 Approval (EP 2, EP 1) Patterson Pump Company Split Case Pumps (EP 2) Falk Lifelign Gear Couplings Types G62 & G66 (EP 1, EP 0) Cincinnati P-72 (EP 1) Cincinnati P64 (EP 2) NSF H2 (EP 2, Semi-Fluid) NLGI Classification LB (EP 1, EP 2) AUTOMOTIVE WHEEL BEARING & CHASSIS LUBRICANT GC-LB TYPICAL PROPERTIES: CITGO PREMIUM LITHIUM EP GREASES Name Semi-Fluid EP-0 EP-1 EP-2 NLGI Grade Material Code Greases Thickener Type Lithium Lithium Lithium Lithium Texture Buttery Buttery Buttery Buttery Color Dark Amber Dark Amber Dark Amber Dark Amber Dropping Point, ASTM D566, F ( C) 350 (177) 375 (191) Worked Penetration, ASTM D Rust Prevention, ASTM D1743, rating Pass Pass Pass Pass Copper Corrosion, ASTM D4048, rating 1b 1b 1b 1b Timken OK Load, ASTM D2509, lbs Four-Ball Weld, ASTM D2596, kgf Base Oil Viscosity: 40 C, cst CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

95 CITGO RAILROAD CURVE GREASE Date 04/18 DESCRIPTION: CITGO Summer Railroad Curve Grease No. 1 and CITGO Winter Railroad Curve Grease No. 0 are anhydrous calcium soap thickened greases formulated with graphite to provide outstanding wear resistance. QUALITIES: APPLICATIONS: Excellent Flow Characteristics: CITGO Railroad Curve Grease has a smooth buttery texture that provides exceptional spray characteristics. CITGO Railroad Curve Grease sprays through the applicator nozzle in a consistent spray to coat the rail sides with a highly wear resistant film. The smooth consistency enables the product to flow through the applicator without clogging and without flow interruptions. Outstanding Wear Protection: This product contains graphite to provide outstanding wear protection to the rail curves. Water Resistance: CITGO Railroad Curve Grease is extremely resistant to water. This grease adheres to the rail, even in humid and rainy environments. CITGO offers two version of this product. CITGO Summer Railroad Curve Grease No. 1 stays in place during the harsh summer weather and CITGO Winter Railroad Grease No. 0 provides improved flow during the colder winter conditions. Both provide outstanding protection to the application. Consult owner s manual for proper lubricant selection. TYPICAL PROPERTIES: CITGO RAILROAD CURVE GREASE SUMMER RAILROAD WINTER RAILROAD CURVE GREASE NO. 1 CURVE GREASE NO. 0 NLGI Grade 1 0 Material Code Worked Penetration, ASTM D Thickener Type Anhydrous Calcium Anhydrous Calcium Color Gray Gray Texture Smooth, Buttery Smooth, Buttery Solid Additives Graphite Graphite Base Oil 40 C, cst Greases CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

96 CITGO SUPERGARD MARINE PLUS GREASE Date 03/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO SUPERGARD Marine Plus Grease is a smooth but tacky blue grease with outstanding water resistance. It is designed to provide excellent lubrication for greased chassis points and other wet-environment applications. SUPERGARD Marine Plus Grease combines an anhydrous calcium thickener, special polymer, and proprietary additive system to ensure superior performance in freshwater marine applications. Excellent water resistance Includes rust, corrosion and wear protection Extreme Pressure (EP), shock load and fretting wear (vibration) protection Compatible with commonly used lithium, lithium complex and anhydrous calcium based greases Polymer fortified for very good metal adhesion Recommended for marine applications including greased chassis points, boat lifts, etc. Lubricates well over a wide temperature range up to 250 F. It is not recommended for automotive disc brake wheel bearings. CITGO SUPERGARD Marine Plus Grease is also an excellent choice in non-marine applications where a general purpose EP grease with outstanding water resistance is desired, such as water pumps, fifth wheels and other equipment operating in wet conditions. Consult owner s manual for proper lubricant selection. TYPICAL PROPERTIES: CITGO SUPERGARD MARINE PLUS GREASE NLGI Grade 2 Material Code Greases Thickener Type Anhydrous Calcium Texture Smooth, Adhesive Color, Observed Blue Worked Penetration, ASTM D Dropping Point, ASTM D566, F ( C) 290 (143) Oil Separation, ASTM D1742, % loss 1 Rust Prevention, ASTM D1743, rating Pass Oxidation Stability, ASTM D942, psi 100 hrs. 5 Timken OK Load, ASTM D2509, lb. 50 Four-Ball Wear, ASTM D2266, mm 0.6 Approximate Temperature Range, F ( C) 0 to 250 (-18 to 121) Viscosity: 40 C, cst 1080 CITGO and SUPERGARD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

97 CITGO SYNDURANCE PREMIUM SYNTHETIC 460 GREASE #00 RED Date 03/18 DESCRIPTION: FEATURES: APPLICATIONS: APPROVALS: CITGO SynDurance Premium Synthetic 460 Grease #00 Red represents the latest in technology using synthetic PAOs in greases and is recommended for extended service applications; reducing operating costs and extending component life. It is designed as a high performance synthetic grease specifically for trailer wheel-ends operating under a wide range of conditions. It can also be utilized in industrial gear cases where operating temperatures are high, where conventional semi-fluid grease will not produce adequate lubricant life. Specially formulated to perform in demanding conditions of high and low temperatures, this grease offers the potential for energy savings and reduction in operating temperatures. High temperature stability Low temperature lubrication (lower starting torque) Excellent anti-oxidation resistance Anti-wear protection Excellent low friction properties Enhanced extreme pressure load carrying capacity Exceptional corrosion protection CITGO SynDurance Premium Synthetic 460 Grease #00 Red is compatible with most lithium and lithium complex greases. It is recommended for use in trailer axles, implement gear boxes, motorized wheelchair gear boxes and motorized conveyor gear boxes. It flows smoothly and evenly at temperature extremes from 40 C up to 190 C with appropriate re-lubrication intervals. Consult owner s manual for proper lubricant selection. Stemco Heavy Duty Axles TYPICAL PROPERTIES: CITGO SYNDURANCE PREMIUM SYNTHETIC 460 GREASE #00 RED NLGI Grade 00 Material Code Thickener Type Lithium Complex Texture Smooth Color, Observed Red Worked Penetration, ASTM D Rust Prevention, ASTM D1743, rating Pass Emcor Corrosion Protection, ASTM D (Pass) Sea Water Rust Prevention, ASTM D5969 Pass Four-Ball Wear, ASTM D2266, mm 0.41 Four-Ball EP Weld Point, ASTM D2596, kgf 315 Four-Ball Load Wear Index, ASTM D2596, kgf 59 Low Temperature Torque, ASTM D4693, N-m 2 Base Oil Viscosity: 40 C, cst 460 Greases CITGO and Syndurance are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

98 CITGO SYNDURANCE PREMIUM SYNTHETIC 460 GREASES Date 04/18 DESCRIPTION: The CITGO SynDurance product line represents the latest in technology using synthetic PAOs in greases and is recommended for extended service applications; reducing operating costs and extending component life. The CITGO SynDurance Premium Synthetic 460 Greases are available in two NLGI Grades: #00 and #2. The CITGO SynDurance Premium Synthetic 460 Grease #2 has superior water washout and spray off resistance, and is designed to prevent corrosion in fresh and sea water conditions. This is particularly important when exposed to corrosive anti-icing agents and water spray conditions. The CITGO SynDurance Premium Synthetic 460 Grease #00 is specifically engineered for trailer wheel-ends operating under a wide range of conditions. It can also be utilized in industrial gear boxes where operating temperatures are high, where conventional semi-fluid grease will not produce adequate lubricant life. Both NLGI Grades offer performance in demanding conditions of high and low temperatures, and offer the potential for energy savings and reduction in operating temperatures. Fully additized to provide superior extreme pressure (EP) and anti-wear characteristics, it is inhibited to resist corrosion and oxidation. Greases APPLICATIONS: The CITGO SynDurance Premium Synthetic 460 Greases are compatible with conventional lithium and lithium complex greases. They contain extreme pressure (EP) additives and provide superior corrosion protection. Consult owner s manual for proper lubricant selection. The CITGO SynDurance Premium Synthetic 460 Grease #2 satisfies a wide range of industrial applications including: Industrial Gear Boxes Paper Mills Industrial Bearings Heavy Duty Commercial On Road Fleets Fifth Wheels Pins and Bushings Slack Adjusters Kingpins Trailer Landing Gear Boxes Heavy Duty Off Road Dozers Forklifts Cranes Scrapers Excavators Loaders Backhoes Compactors Paving Cold Planers Forest Machines Articulated Trucks Agriculture Implements Tractors Combines Tillage Hay Balers Mowers Planting And Seeding Harvesting Skid Steers Sprayers And Spreaders Utility Vehicles Automotive Applications Wheel Bearings** Chassis** ** The CITGO SynDurance Premium Synthetic 460 Grease #2 meets the NLGI Service Classification of GC-LB and displays the NLGI Certification Mark as an Automotive Wheel Bearing and Chassis Lubricant The CITGO SynDurance Premium Synthetic 460 Grease #00 is recommended for use in trailer wheel ends, implement gear boxes, motorized wheelchair gear boxes as well as motorized conveyor gear boxes. It flows smoothly and evenly at temperature extremes from -40 C up to 190 C with appropriate re-lubrication intervals. (Continued) C

99 CITGO SYNDURANCE PREMIUM SYNTHETIC 460 GREASES Date (Continued) 04/18 - (Continued) APPROVALS: Stemco Heavy Duty Axles #00 SAF Holland LSZ Kingpin #2 AUTOMOTIVE WHEEL BEARING & CHASSIS LUBRICANT GC-LB TYPICAL PROPERTIES: CITGO SYNDURANCE PREMIUM SYNTHETIC 460 GREASES NLGI Grade 00 2 Material Code Thickener Type Lithium Complex Lithium Complex Texture Smooth, Adhesive Smooth, Adhesive Dropping Point, ASTM D Color, Observed Green Green Worked Penetration, ASTM D Rust Prevention ASTM D1743, Distilled Water Pass Pass Rust Prevention ASTM D5969, 5% Synthetic Sea Water Pass Pass Emcor Corrosion Protection ASTM D6138 Pass Pass Water Washout ASTM D1264 % 175 F 2 Water Spray-off ASTM D4049, % Loss 15 Low Temperature Torque, ASTM D4693, N-m 2 3 Four-Ball EP Weld, ASTM D2596, kgf USS -10 F, gpm 28 NLGI Classification GC-LB Base Oil Viscosity: 40 C, cst CITGO and SynDurance are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Greases C

100 CITGO SYNDURANCE ST SYNTHETIC GREASES Date 03/18 DESCRIPTION: FEATURES: APPLICATIONS: CITGO SynDurance ST Synthetic Greases are scientifically engineered for a wide variety of heavy duty applications. These high performance greases are formulated with a premium quality lithium complex thickener system which is combined with the exceptional features of synthetic base oils to significantly increase bearing life and equipment reliability. CITGO SynDurance ST Synthetic Greases are designed to provide excellent wear control, EP performance, and water resistance critical for a variety of applications. The corrosion protection available with these greases goes above and beyond in applications where corrosive environments are an everyday occurrence. CITGO SynDurance ST Synthetic Greases deliver superior protection in heavily loaded industrial, mining and construction applications by providing low temperature pumpability and low starting and running torque, resulting in reduction of operating temperatures and energy savings. Premium quality lithium complex thickener Outstanding low temperature performance and pumpability Superior water resistance Excellent high-temperature oxidation resistance Heavy Industrial Mining Steel Mills Construction DESIGNED TO PERFORM AND PROTECT: CITGO SynDurance ST Synthetic Greases are designed to protect against wear which increases equipment life. These greases have an impressive 500 kgf four-ball weld point which is an indicator of the outstanding extreme pressure protection. CITGO SynDurance ST Synthetic Greases provide twice the load protection compared to many leading competitor greases. Consult your owner s manual for proper lubricant selection. 4 Ball Weld load kgf passing (ASTM weight D-2596 kg test (ASTM method) D test method) Twice the load Greases Compe66ve SHC SynDurance ST Higher is better (Continued) C

101 CITGO SYNDURANCE ST SYNTHETIC GREASES (Continued) Date 03/18 - (Continued) TYPICAL PROPERTIES: CITGO SYNDURANCE ST SYNTHETIC GREASES Material Code ISO VIS Grade NLGI Consistency Number Color, Observed Red Red Red Red Worked Penetration, ASTM D Dropping Point, ASTM D2265 F ( C) >500 (260) >500 (260) >500 (260) >500 (260) Rust Prevention, ASTM D1743, rating Pass Pass Pass Pass Water Washout, ASTM D1264, % Loss Ball EP Weld Point, ASTM D2596, kgf Ball Load Wear Index, ASTM D2596, kgf Base Oil Viscosity: 40 C, cst CITGO and SynDurance are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Greases C

102 CITGO Date 04/18 ULTRALIFE CSEP 5M GREASE DESCRIPTION: CITGO UltraLife CSEP 5M Grease is an advanced calcium sulfonate complex grease engineered to provide outstanding EP (Extreme Pressure) performance, and superior corrosion protection in a variety of high temperature applications. It is specially formulated to protect even the most heavily loaded joints against galling, wear and corrosion, under dry or wet working conditions. CITGO UltraLife CSEP 5M Grease contains 5% molybdenum disulfide for added protection and longer service life in severe applications. The exceptional EP properties go beyond the norm, providing that extra protection needed in construction, mining, paper mills and other heavy industries. It has been designed to maximize component life and reduce re-lubrication frequency. The Four Ball EP Weld Point Test is a measure of how well a grease will stand up to the shock loading and direct metal-to-metal contact typically found in off-highway/construction/mining applications. As seen in the graph below, CITGO UltraLife CSEP 5M Grease outperforms the competition while matching the performance set by the leading OEM branded grease. Four Ball Weld Load kgf (ASTM D2596 Test Method) Competitor A Competitor B Leading OEM Brand UltraLife CSEP 5M Exceptional water resistance is very important to maintaining lubrication to the bearing or bushing. CITGO UltraLife CSEP 5M Grease resists water washout and softening, plus prevents corrosion in the presence of water. Greases FEATURES Adhesive and tacky, stays in place Superior water resistance Exceptional corrosion protection Minimizes abrasive wear Withstands shock loads, impact resistant APPLICATIONS: CITGO UltraLife CSEP 5M Grease provides excellent protection in severe applications such as construction, mining, aggregate mines, marine, forestry, pulp and paper mills, steel mills, and conveyor systems. Consult owner s manual for proper lubricant selection. (Continued) (Continued) C

103 CITGO ULTRALIFE CSEP 5M GREASE Date (Continued) 03/18 - (Continued) TYPICAL PROPERTIES: CITGO ULTRALIFE CSEP 5M GREASE NLGI Grade 2 Material Code Thickener Type Calcium Sulfonate % Molybdenum Disulfide 5 Dropping Point, ASTM D2265, F ( C) >500 (260) Rust Prevention, ASTM D1743, rating Pass Four Ball EP Weld Point, ASTM D2596, kgf 620 Water Washout, ASTM D1264, % 175 F <2 Operating Range, F ( C) -25 to 300 (-32 to 150) USS 0 F, gpm 20 Base Oil Viscosity: 40 C, cst 150 CITGO and UltraLife are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Greases C

104 CITGO AMPLEX OILS Date 04/18 DESCRIPTION: CITGO Amplex Oils are high quality, medium viscosity index oils for use in general purpose lubrication applications. QUALITITIES: CITGO Amplex Oils are made from highly refined medium viscosity index base stocks with low pour points. These oils exhibit a mild natural dispersant action, good seal swell and excellent solvency. APPLICATIONS: CITGO Amplex Oils are recommended as general purpose machinery lubricants, especially for use as a mild service circulating oil and lubrication of plain bearings where oil is applied by hand methods. CITGO Amplex Oil 22 has a very low pour point which makes it suitable for lubrication of certain industrial equipment where low ambient temperatures may be encountered. TYPICAL PROPERTIES: CITGO AMPLEX OILS Grade Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash Point, COC, ASTM D92, F ( C) 330 (166) 380 (193) 390 (199) 412 (211) Viscosity: ASTM D445, cst at 40 C ASTM D 445, cst at 100 C ASTM D2161, SUS at 100 F ASTM D 2161,SUS at 210 F Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -40 (-40) -20 (-29) -20 (-29) -15 (-26) Color, ASTM D1500 L CITGO and Amplex are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Industrial Fluids C

105 CITGO SENTRY OILS Date 03/18 DESCRIPTION: CITGO Sentry Oils are a complete line of highly-refined, non-additive mineral oils for bearing and other general purpose lubrication. QUALITIES: They are made with high viscosity index base stocks having high thermal stability. Available in several viscosity grades, these oils provide good lubrication with low maintenance costs, and have the necessary characteristics to permit their use in many applications. APPLICATIONS: CITGO Sentry Oils are recommended for general lubrication of industrial machinery, machine tools, engine bearings, and other plant equipment where a non-additive mineral oil is desired. Grades 19 through 68 are recommended for heat transfer applications and in hydraulic systems where pressures or temperatures are moderate. They can be used in many applications where high oil loss makes the use of a lower cost product desirable. CITGO Sentry Oils can be used as diluents for cutting oil bases, flushing oils, form oils for brick presses and steel concrete forms, lubricants for small electric motors, and other applications where a non-additive mineral oil is desired. TYPICAL PROPERTIES: CITGO SENTRY OILS Grade Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash Point, COC, ASTM D92, F ( C) 380 (193) 388 (198) 424 (218) 465 (241) 516 (269) 595 (313) Viscosity: ASTM D445, cst at 40 C ASTM D2161, SUS at 100 F Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) 5 (-15) 5 (-15) 5 (-15) 10 (-12) 8 (-13) 10 (-12) Color, ASTM D1500 L ISO VG No CITGO and Sentry are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C10036 Industrial Fluids 97

106 CITGO PACEMAKER OILS Date 04/18 DESCRIPTION: CITGO Pacemaker Oils are rust and oxidation (R&O) inhibited general purpose lubricants. They are manufactured with high viscosity index base stocks, contain anti-foam additives, and readily separate from water. QUALITIES: These oils are made from high quality, paraffinic base stocks. Their high viscosity index imparts superior temperature-viscosity characteristics. Long service life in closed circulating systems is assured by low carbon-forming tendency and excellent resistance to oxidation, rusting and foaming. APPLICATIONS: Appropriate viscosity grade Pacemaker Oils can be used as: Air line oil Circulating oil Gear oil Compressor oil Rust/oxidation inhibited (R&O) oil Low pressure hydraulic oil Non-detergent oil (Continued) Industrial Fluids C

107 CITGO PACEMAKER OILS Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO PACEMAKER OILS Grade Material Code Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, ASTM D92, F ( C) 395 (202) 395 (202) 395 (202) 442 (228) 442 (228) 442 (228) 442 (228) 442 (228) 579 (304) Viscosity ASTM D445 cst at 40 C cst at 100 C Viscosity Index ASTM D Pour Point ASTM D97 F( C) -22 (-30) -33 (-36) -22 (-30) -27 (-33) -22 (-30) 0 (-18) 0 (-18) 0 (-18) 10 (-12) Color, ASTM D1500 L0.5 L0.5 L0.5 L0.5 L1.0 L5.0 L5.0 L5.5 L5.5 Neutralization No. ASTM D Rust Test ASTM D665 Pass (1) Pass (1) Pass (1) Pass (1) Pass (1) Pass (2) Pass (2) Pass (2) Pass (2) Cincinnati Lamb Requirement P-45 P-38 P-55 P-54 P-57 ISO VG No C10034 AGMA Grade Notes: (1) Procedure A (distilled water) and Procedure B (synthetic sea water) - 24 hrs (2) Procedure A (distilled water) CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Industrial Fluids 99

108 CITGO PACEMAKER T OILS Date 03/18 DESCRIPTION: CITGO Pacemaker T Oils are extra inhibited high quality lubricants designed specifically as turbine oils. QUALITIES: These oils are made from high viscosity index paraffinic base stocks that are processed by modern hydrotreating methods. Their high viscosity index imparts superior temperature-viscosity characteristics. Long service life in closed circulating systems is assured by the high flash point and excellent resistance to oxidation, rusting, and foaming. Each grade of CITGO Pacemaker T Oil passes both procedures of the ASTM D665 Rust Test and will provide extended oxidation life as measured in the ASTM D943 Oxidation Test. APPLICATIONS: CITGO Pacemaker T Oils in proper viscosity grade are recommended for pressure-circulation systems of direct-connected steam turbines and for the bearings of turbo-generators. They are also recommended for the lubrication of steam turbines with single-reduction gear units, as found in marine service. CITGO Pacemaker T Oils are suitable for the lubrication of industrial gas turbines and gear units. CITGO Pacemaker T Oils are also highly recommended for use in compressor equipment, air lines, circulating oil systems, and gears where an R&O (Rust and Oxidation inhibited) type oil is specified. Pacemaker T-32 meets the performance recommendations of: General Electric GEK H Fives Cincinnati P-38 (Grade T-32) ALSTOM HTGD ASTM D4304 Type I, II, III British Standard BS 489 DIN Part 1, 2 DIN Part 1 ISO 8068 TSA TGA, TGE TSE ISO HH, HL SIEMENS AG TLV Standard Thermal Stability SIEMENS AG TLV High Thermal Stabiliity Solar ES9-244L grades C32 (150), C46 (5-215) (Grades T-32, T-46) respectively Pacemaker T-68 is suitable for mist applications as evidenced by the Alemite test. (Continued) Industrial Fluids (Continued) C

109 CITGO PACEMAKER T OILS Date (Continued) 03/18 - (Continued) TYPICAL PROPERTIES: CITGO PACEMAKER T OILS Grade T-32 T-46 T-68 T-115 Material Code Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, COC, ASTM D92, F ( C) 442 (228) 446 (230) 489 (254) 536 (280) Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445, cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -38 (-39) -38 (-39) -38 (-39) 0 (-18) Color, ASTM D1500 L1.0 L1.0 L Foam Test, ASTM D892 (1), Seq. I, II, III Pass Pass Pass Pass Aniline Point, ASTM D611, F ( C) 219 (104) 223 (106) 230 (110) 244 (118) Neutralization No., ASTM D Corrosion, ASTM D130, 3 hours at 212 F 1 B 1 B 1 B 1 B Oxidation, ASTM D943 (2), hours 10, ,000 + Water Separation, Dist. Water, ASTM D1401, at 130 F (54 C) (15) (15) (20) ASTM D 1401, at 180 F (82 C) (20) Rust Test, ASTM D665 (3) Pass Pass Pass Pass RPVOT, ASTM D2272, minutes , ISO VG No AGMA Grade Note: (1) 50 ml. max. at end of blowing period. No foam after 10 minutes setting. (2) Hours to reach acid number of 2.0 mg. of KOH per gram of oil. (3) Procedures A (distilled water) and B (synthetic sea water) 24 hours. CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C10035 Industrial Fluids 101

110 CITGO PACEMAKER ST-32 Date 04/18 DESCRIPTION: QUALITIES: CITGO Pacemaker ST-32 is a synthetic gas turbine lubricant formulated to meet the demands of high output stationary industrial gas turbines. High quality synthetic base oils are blended with carefully selected additives to impart antiwear, high temperature oxidation and corrosion inhibition, as well as rust protection. CITGO Pacemaker ST-32 exhibits exceptional low temperature performance, permitting superior fluidity during cold startups and cold weather operation. It is completely miscible and is compatible with petroleum based lubricants and components. Exceptionally good low temperature fluidity provides reduced wear and lowered power consumption during startup High viscosity index provides excellent temperature/viscosity performance over a wide temperature range High load carrying and antiwear characteristics for longer component life than mineral oil products Compatibility with petroleum based lubricants and system components such as seals, paints, gaskets and hoses Industrial Fluids APPLICATIONS: CITGO Pacemaker ST-32 meets the specifications of: Fives Cincinnati P-38 DIN Part 1 DIN Part 2 British Standard BS 489 GEK 46506D GEK 32568F Alstom HTGD Solar ES 9-224W Siemens TLV Siemens TLV Note: Not intended for aviation applications. TYPICAL PROPERTIES: CITGO PACEMAKER ST-32 ISO Viscosity Grade 32 Material Code Specific Gravity, 60 /60 F Density, lbs/gal 7.10 Viscosity, ASTM D445, cst at 040 C 30.5 cst at 100 C 5.74 Viscosity Index, ASTM D Flash Point, ASTM D92, F ( C) 486 (252) Pour Point, ASTM D97, F ( C) -71 (-57) Copper Corrosion, ASTM D130 1A Rust Protection, ASTM D665 DI Water, Proc. A Pass Salt Water, Proc. B Pass Foaming Tendency, Sequence I, II, III Pass Neutralization Number 0.1 Four Ball Wear, ASTM D4172, 40kg, mm 0.46 (Continued) CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

111 CITGO HY DURANCE AW FLUIDS Date 04/18 DESCRIPTION: CITGO HyDurance AW Fluids are superior anti-wear hydraulic and circulating oils specially formulated to provide outstanding resistance to sludge formation, are chemically stable, and exhibit excellent anti-wear protection and filterability. QUALITIES: CITGO HyDurance AW Fluids are formulated with high quality base stocks and premium additive components to offer trouble-free service in high-pressure, high-output industrial hydraulic circuits. CITGO HyDurance AW Fluids offer: Thermal Stability: Superior resistance to heat-related sludging in sensitive electro-hydraulic servos. Hydrolytic Stability: Will not contribute to the formation of metaletching acids or corrosive reactants. Rust and Corrosion Protection: Inhibited against rusting in both fresh and sea water and pass both A and B Sequences of the ASTM D665 Turbine Oil Rust Test. Wear Protection: Excellent antiwear protection to pumps, motors, valves, and other hydraulic circuit components. Approved against stringent equipment performance requirements. Anti Foam Performance: Resistant to foaming and will not foster abnormal air entrainment in properly designed hydraulic circuits. Demulsibility: Readily separate water permitting draining of contaminating water from circulating systems. Excellent Filterability: Premium performance in wet and dry filterability testing. CITGO HyDurance AW 68 Fluid (Continued) C10203 Industrial Fluids 103

112 CITGO HY DURANCE AW FLUIDS Date 04/18 - (Continued) APPLICATIONS: CITGO HyDurance AW Fluids are recommended for service in industrial and mobile hydraulic sytems when used in accordance with equipment manufacturers recommendations. They are designed to provide maximum service life to vane, piston, and gear pumps as well as other circuit components such as motors and servos. CITGO HyDurance AW Fluids are also recommended for use as a gear and bearing lubricant in industrial applications where rust and oxidation inhibited oils are required. Consult owner s manual for proper lubricant selection. CITGO HyDurance AW Fluids meet: ASTM D6158 HM (2005) General Motors LS-2 (1997) Fives Cincinnati P-68, 69, 70 JCMAS HK P041 (2004) Parker Denison HF-0 (Revision J) ISO HM (FDIS 2008) DIN (2006) SEB (2007) Eaton Brochure US Steel 126, 127, 136 Parker Denison HF-0 Thermal Stability V104C Vane Pump Wear Data CITGO HyDurance AW 32 CITGO HyDurance AW 32 Parker Denison HF-0 Demulsibility Parker Denison HF-0 Filterability CITGO HyDurance AW 46 CITGO HyDurance AW 46 Industrial Fluids (Continued) (Continued) C

113 CITGO HY DURANCE AW FLUIDS Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO HYDURANCE AW FLUIDS GRADE Material Code Gravity, ASTM D4052, API Density, lb/gal Flash Point, ASTM D92, COC, F ( C) 399 (204) 417 (214) 446 (230) 468 (242) 471 (244) 500 (260) Viscosity, cp at -40 C (1) cp at -35 C (1) cp at -20 C (1) cst at 40 C cst at 100 C Viscosity Index FZG (A/8.3/90), pass load, ISO Pour Point, ASTM D97, F ( C) -40 (-40) -27 (-33) -22 (-30) -17 (-27) -6 (-21) 0 (-18) Color, ASTM D1500 L0.5 L0.5 L0.5 L0.5 L3.0 L2.5 Water Separability, ASTM D1401 (2) Oxidation Test, ASTM D943, Hrs Rust Test, ASTM D665 A, B (3) Pass Pass Pass Pass Pass Pass Meets Fives Cincinnati Requirement P-68 P-70 P-69 AFNOR NF E HM22 HM32 HM46 HM68 HM100 HM150 ISO VG No Notes: (1) ASTM D2893 Brookfield Viscosity. (2) 30 minutes max. separation time to 3ml emulsion. Test temperature is 130 F for grades up through ISO 68. Test temperature is 180 F for ISO 100 and 150. (3) Pass - No Rust. CITGO and HyDurance are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C10203 Industrial Fluids 105

114 CITGO HY DURANCE AW ALL TEMP FLUIDS Date 04/18 DESCRIPTION: CITGO HyDurance AW All Temp Fluids are superior, high viscosity index, anti-wear hydraulic and circulating oils specially formulated to provide outstanding resistance to sludge formation, are chemically stable, and exhibit excellent anti-wear protection and filterability, and can be used over wide temperature ranges. QUALITIES: CITGO HyDurance AW All Temp Fluids are formulated with high quality base stocks and premium additive components to offer trouble-free service in high-pressure, high-output industrial hydraulic circuits. CITGO HyDurance AW All Temp Fluids offer: Thermal Stability: Superior resistance to heat-related sludging in sensitive electro-hydraulic servos. Hydrolytic Stability: Will not contribute to the formation of metaletching acids or corrosive reactants. Rust and Corrosion Protection: Inhibited against rusting in both fresh and sea water and pass both A and B Procedures of the ASTM D665 Rust Test. Wear Protection: Excellent anti-wear protection to pumps, motors, valves, and other hydraulic circuit components. Approved against stringent equipment performance requirements. Anti-Foam Performance: Resistant to foaming and will not foster abnormal air entrainment in properly designed hydraulic circuits. Demulsibility: Readily separate water permitting draining of contaminating water from circulating systems. Excellent Filterability: Premium performance in wet and dry filterability testing. CITGO HyDurance AW All Temp 46 Fluid (Continued) Industrial Fluids (Continued) C

115 CITGO HY DURANCE AW ALL TEMP FLUIDS Date 04/18 - (Continued) APPLICATIONS: CITGO HyDurance AW All Temp Fluids are recommended for service in industrial and mobile hydraulic systems when used in accordance with equipment manufacturers recommendations. They are designed to provide maximum service life to vane, piston, and gear pumps as well as other circuit components such as motors and servos. CITGO HyDurance AW All Temp Fluids are also recommended for use as a gear and bearing lubricant in industrial applications where rust and oxidation inhibited oils are required. CITGO HyDurance AW All Temp 32 Fluid is a special multigrade anti-wear fluid meeting FMC Hi-Performance Hydraulic Oil Grade 32 requirements. CITGO HyDurance AW All Temp Fluids 32 and 46 offer excellent low temperature pumpability and are recommended for use in mobile and other hydraulic equipment in heavy duty all weather service. CITGO HyDurance AW All Temp Fluids meet: ASTM D6158 HM (2014) SO HV (2009) DIN HVLP (2006) General Motors LS-2 (1997) Eaton Brochure Parker Denison HF-0 (Revision J) JCMAS HK P041 (2004) US Steel 126, 127, 136 SEB (2007) Parker Denison HF-0 Thermal Stability V104C Vane Pump Wear Data CITGO HyDurance AW All Temp 32 CITGO HyDurance AW All Temp 32 Parker Denison HF-0 Demulsibility Parker Denison HF-0 Filterability CITGO HyDurance AW All Temp 46 CITGO HyDurance AW All Temp 46 (Continued) C10238 Industrial Fluids 107

116 CITGO HY DURANCE AW ALL TEMP FLUIDS (Continued) Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO HYDURANCE AW ALL TEMP FLUIDS GRADE 32 (1) 46 Material Code ISO VG No Gravity, ASTM D4052, API Density, lb/gal Flash Point, ASTM D92, COC, F ( C) 385 (196) 423 (217) Viscosity, cp at -40 C (2) 13,900 39,770 cp at -35 C (2) 7,200 18,400 cp at -20 C (2) 2,424 cst at 40 C cst at 100 C Viscosity Index FZG (A/8.3/90), pass load, ISO Pour Point, ASTM D97, F ( C) -54 (-48) -49 (-45) Color, ASTM D1500 L1.0 L1.0 Water Separability, ASTM D (15) Oxidation Test, ASTM D943, Hrs >4800 Rust Test, ASTM D665 A, B (3) Pass Pass Notes: (1) Meets FMC Hi-Performance, Hydraulic Oil, Grade 32 requirements. (2) ASTM D2893 Brookfield Viscosity. (3) Pass - No Rust. CITGO and HyDurance are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Industrial Fluids C

117 CITGO HY DURANCE TM AW CP FLUID Date 03/18 DESCRIPTION: CITGO HyDurance AW CP Fluid is a premium multigrade anti-wear hydraulic fluid designed for applications where dielectric (insulating) properties are required. CITGO HyDurance AW CP Fluid offers wide temperature range service in mobile hydraulic equipment, particularly in low temperature conditions where excellent cold start up hydraulic system performance is required. QUALITIES: APPLICATIONS: High dielectric strength Superior low-temperature flow and pumpability Fluid film strength for warmer climates Excellent antiwear properties Foam resistant Rust and corrosion protection Long service life Water separation characteristics Excellent viscosity shear stability CITGO HyDurance AW CP Fluid is recommended for most outdoor and/or mobile hydraulic equipment requiring a fluid with high dielectric strength properties such as cherry picker lift applications. It provides excellent service in equipment used under a wide range of operating conditions and where hydraulic system response is critical such as: Tree trimming, fruit picking mobile equipment Firefighting lift trucks, buckets, etc. Aerial lift buckets Mobile hydraulic systems Garbage collection equipment Public utility vehicles Construction equipment in colder services CITGO HyDurance AW CP Fluid meets or exceeds the following: Dielectric Strength, ASTM D 877, 35 KV minimum ASTM D 6158 HM (2005) Parker Denison HF-0 (Revision J) DIN (2006) DIELECTRIC STRENGTH RATED Eaton Brochure WIDE TEMPERATURE PERFORMANCE General Motors LS-2 (1997) JCMAS HK P041 (2004) ISO HM (FDIS 2008) SEB (2007) (Continued) C10030 Industrial Fluids 109

118 CITGO HY DURANCE TM AW CP FLUID Date (Continued) 03/18 - (Continued) TYPICAL PROPERTIES: CITGO HYDURANCE TM AW CP FLUID Material Code Gravity, ASTM D4052, API 30.8 Density, lb/gal 7.26 Flash Point, COC, ASTM D92, F ( C) 367 (186) Color Blue-green Viscosity, ASTM D2983, cp at -40 C 20,450 cp at -23 C 1,590 cp at -18 C 860 ASTM D455, cst at 40 C 25.6 ASTM D 455, cst at 100 C 5.4 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -54 (-48) Aniline Pt., ASTM D611, F 204 Total Acid Number, ASTM D Oxidation Test ASTM D943, hrs 2775 Rust Test ASTM D665, A and B Pass Water Separability, ASTM D1401, at 130 F (54 C) (10) Dielectric Strength, ASTM D877, KV, minimum 35 CITGO is a registered trademark and HyDurance is a trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Industrial Fluids C

119 CITGO HY DURANCE AW NZ FLUIDS Date 04/18 DESCRIPTION: CITGO HyDurance AW NZ Fluids are high performance lubricants formulated with premium base stocks and ashless additives to provide outstanding protection for demanding hydraulic systems, especially those operating in environmentally sensitive areas. CITGO HyDurance AW NZ Fluids are zinc free. Zinc compounds are regulated as priority pollutants under provisions of the Clean Water Act and SARA Title 313. BENEFITS: Non-toxic in acute aquatic toxicity test (LC-50) per OECD TG 203 limit test. Inherently biodegradable. Zinc free formulation for less impact on the environment. Excellent thermal stability to virtually eliminate heat-related sludge deposits. Provide outstanding rust and corrosion protection. Separate readily from water. Contain inhibitors to minimize foaming and air entrainment. Provide premium anti-wear protection to pumps, motors and other hydraulic components. Offer extended fluid service life capability with a fortified premium formulation to handle severe operating conditions. CITGO HyDurance AW NZ 32 Fluid APPLICATIONS: CITGO HyDurance AW NZ Fluids offer premium non-zinc anti-wear protection to vane, piston and gear pumps, motors, valves and other hydraulic circuit components when used in accordance with manufacturer s recommendations. They meet or exceed the stringent performance requirements of: GM LS-2 Eaton Brochure DIN PART 2 Fives Cincinnati P-68, P-69, P-70 U.S. Steel 127, 136, 126 Parker Hannifin France (Denison) HF-0 CITGO HyDurance AW NZ Fluids can also be used in circulating systems of machine tools, presses, air compressors and other gear and bearing applications where rust and oxidation inhibited oils are required. They can be used in applications operating in environmentally sensitive areas where the use of a zinc free, ashless formulated fluid is desired such as: Marine Offshore Rigs, Tugs, Dredges, Hydraulic Lifts, Cranes, Pile-Drivers (Note: Does not meet EPA 2013 Vessel General Permit VGP EAL requirements) Forestry Scalpers, Excavators, Wheel Loaders Construction Bulldozers, Graders, Backhoes Mining Conveyors, Crawlers, Hole Drillers (Continued) C10137 Industrial Fluids 111

120 CITGO HY DURANCE AW NZ FLUIDS Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO HYDURANCE AW NZ FLUIDS Grade Material Code Gravity, ASTM D4052, API Density, lb/gal Flash Point, ASTM D92 (COC) C ( F) 215 (419) 206 (403) 242 (468) Viscosity, cst at 40 C cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, C ( F) -39 (-38) -36 (-33) -24 (-11) Color, ASTM D1500 L1.0 L1.0 L1.5 Total Acid No., ASTM D664, mgkoh/g Copper Corrosion, ASTM D130, 3h at 100 C 1A 1A 1A Rust Test, ASTM D665 A, B Pass Pass Pass Four Ball Wear, ASTM D4172, at 40 kg, mm Foam Test, Seq. I, ml Foam Test, Seq. II, ml Foam Test, Seq. III, ml Water Separability, ASTM D1401, at 130 F CITGO and HyDurance are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. NOTE: Contamination with other fluids can affect environmental benefits and system performance. Contamination with zinc containing and/or emulsifiable fluids may cause foaming, premature filter saturation, and a decrease in water separability. ZINC FREE INHERENTLY BIODEGRADABLE NON-TOXIC PER LC-50 AQUATIC TOXICITY TEST EXTENDED FLUID LIFE CAPABILITY Industrial Fluids C

121 CITGO HYDURANCE AW SUPER NZ FLUID Date 04/18 DESCRIPTION: CITGO HyDurance AW Super NZ Fluid is a high efficiency, wide temperature use range hydraulic fluid. It is formulated with premium base stocks and ashless additives to provide long fluid life and outstanding protection for demanding mobile equipment hydraulic systems. CITGO HyDurance AW Super NZ Fluid is zinc free. Zinc compounds are regulated as priority pollutants under provisions of the Clean Water Act and SARA Title 313. Multigrade performance offers ISO 68 viscosity characteristics at high operating temperatures and ISO 32 viscosity characteristics at low operating temperatures. QUALITIES: CITGO HyDurance AW Super NZ Fluid offers: Increased pump efficiency leading to improved productivity Zinc free and non-toxic in acute aquatic toxicity test (LC-50) per OECD TG 203 limit test for less environmental impact Multigrade performance for wide application temperature range Excellent shear and thermal stability provides extended fluid service life capability. Separates readily from water to allow draining of water from systems Premium rust and corrosion protection for harsh environments Excellent foam control for dependable performance Provides outstanding antiwear protection to pumps, motors and other hydraulic circuit components Recommended for use in Hitachi excavators with 4,000 hour service intervals. (Continued) (Continued) C10232 Industrial Fluids 113

122 CITGO HYDURANCE AW SUPER NZ FLUID Date (Continued) 04/18 - (Continued) APPLICATIONS: CITGO HyDurance AW Super NZ Fluid is designed for increased hydraulic efficiency while providing excellent service life in vane, piston, and gear pumps when used in accordance with equipment manufacturer recommendations. CITGO HyDurance AW Super NZ Fluid is highly recommended for high pressure mobile equipment hydraulic systems operating in wide temperature applications such as mining, construction and logging operations. CITGO HyDurance AW Super NZ Fluid meets performance requirements of: GM LS-2 Eaton Brochure 694 (formerly Vickers I-286-S and M-2950-S) DIN PART 3 U.S. Steel 127, 136, 126 Cincinnati Machine P-68, P-69, P-70 Parker Hannifin France (Denison) HF-0 Hitachi Excavators TYPICAL PROPERTIES: CITGO HYDURANCE AW SUPER NZ FLUID Material Code Gravity, ASTM D4052, API 31.5 Density, lb/gal 7.23 Flash Point, PM, ASTM D93, F ( C) 385 (196) Viscosity, ASTM D445, cst at 40 C 53.0 cst at 100 C 9.9 Viscosity Index, ASTM D Brookfield Viscosity, ASTM D2983, C 36,392 Pour Point, ASTM D97, F ( C) -49 (-45) Color Blue Copper Corrosion, ASTM D130, 3h at 100 C 1A Rust Test, ASTM D665 A, B Pass Four Ball Wear, ASTM D4172, at 40 kg, mm 0.50 Foam Test, ml, ASTM D892 Sequence I 10-0 Sequence II 25-0 Sequence III 0-0 Water 130F, ASTM D Acute aquatic toxicity (LC-50) per OECD TG 203 Pass Industrial Fluids C10232 Notes: Contamination with other fluids can affect environmental benefits and system performance. Contamination with zinc containing and/or emulsifiable fluids may cause foaming, premature filter saturation, and a decrease in water separability. Refer to equipment owner s manual for proper lubricant selection. CITGO and HyDurance are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. 114

123 CITGO HY DURANCE TM AW SYNTHETIC FLUIDS Date 04/18 DESCRIPTION: CITGO HyDurance AW Synthetic Fluids are premium ashless hydraulic fluids formulated with the highest quality synthetic base stocks and additives. These fluids offer outstanding chemical stability, anti-wear protection and resistance to sludge formation. QUALITIES: CITGO HyDurance AW Synthetic Fluids offer excellent low and high temperature performance providing a higher margin of equipment protection, beyond the capabilities of comparable mineral oils. The combination of synthetic base stocks and ashless additive package provide a product with exceptional oxidation stability allowing for extended drain and filter change intervals. High resistance to sludge formation helps assure clean and trouble free operation. Excellent thermal and oxidative stability reducing system deposits resulting in longer fluid life. High viscosity index and low pour point allows for operation over a wide temperature range without viscosity loss problems typical of mineral multigrade oils. Excellent corrosion protection. Exceptional demulsibility allows for the separation of large amounts of water from the system. Exceptional anti-wear properties CITGO HyDurance TM AW 46 Synthetic Fluid APPLICATIONS: CITGO HyDurance AW Synthetic Fluids are designed for use in vane, piston and gear pumps typically found in hydraulic and circulating systems. These fluids are designed to provide the excellent service life to pumps, servos and motors. CITGO HyDurance AW Synthetic Fluids meet or exceed the following manufacturer specifications: Eaton Brochure (formerly Vickers I-286-S, M-2950-S) Parker Denison HF-0, HF-1, HF-2 Fives Cincinnati P-70 (ISO 46), P-69 (ISO 68) U.S. Steel 127, 136 FULLY SYNTHETIC EXTREME TEMPERATURE PERFORMANCE (Continued) (Continued) C10149 Industrial Fluids 115

124 CITGO HY DURANCE TM AW SYNTHETIC FLUIDS Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO HYDURANCE TM AW SYNTHETIC FLUIDS Grade Material Code Specific Gravity, 60/60 F Density, lb/gal Viscosity, ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D Flash Point, ASTM D92, C ( F) 266 (510) 268 (514) Pour Point, ASTM D97, C ( F) -60 (-76) -57 (-70) Color, ASTM D Brookfield Viscosity cp at -18 C cp at -26 C 3340 Water Separation, ASTM D1401, at 130 F (54 C) 40/40/0 (5) 40/40/0 (5) Four Ball Wear, ASTM D4172, 40kg, mm Copper Corrosion, ASTM D130 1B 1B Rust Protection, ASTM D665 DI Water Pass Pass Sea Water Pass Pass Foam Sequence, ASTM D892, I, II, III Pass Pass CITGO is a registered trademark and HyDurance is a trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Industrial Fluids C

125 CITGO HY DURANCE AW/AL HVI 100 FLUID Date 03/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO HyDurance AW/AL HVI 100 Fluid is a superior anti-wear and anti-leak, high viscosity index hydraulic and circulating oil specially formulated to provide outstanding performance under wide temperature ranges. It has excellent resistance to sludge formation, is chemically stable, and exhibits premium protection and filterability. CITGO HyDurance AW/AL HVI 100 Fluid is formulated with high quality base stocks and premium additive components to offer trouble-free service in high-pressure, high-output hydraulic circuits operating under wide temperature conditions. It contains a seal conditioning agent to help prevent and minimize minor leaks and helps provide longer seal life. CITGO HyDurance AW/AL HVI 100 Fluid offers: Low Temperature Performance: Excellent fluidity over a wide temperature change. Thermal Stability: Superior resistance to heat-related sludging in sensitive electro-hydraulic servos. Hydrolytic stability: Will not contribute to the formation of metal-etching acids or corrosive reactants. Rust and Corrosion Protection: Inhibited against rusting in both fresh and sea water and pass both A and B Sequences of the ASTM D 665 Turbine Oil Rust Test. Wear Protection: Excellent antiwear protection to pumps, motors, valves and other hydraulic circuit components. Approved against stringent equipment performance requirements. Anti Foam Performance: Resistant to foaming and will not foster abnormal air entrainment in properly designed hydraulic circuits. Demulsibility: Readily separates water, permitting draining of contaminating water from circulating systems. Excellent filterability: Premium performance in wet and dry filterability testing. Seal conditioner for longer seal life. CITGO HyDurance AW/AL HVI 100 Fluid is recommended for service in industrial and mobile hydraulic systems when used in accordance with equipment manufacturers recommendations. CITGO HyDurance AW/AL HVI 100 offers excellent low temperature pumpability and is recommended for use in mobile and other hydraulic equipment in heavy duty all weather service. It is designed to provide enhanced service life to vane, piston and gear pumps as well as other circuit components such as motors and servos. CITGO HyDurance AW/AL HVI 100 Fluid is also recommended for use as a gear and bearing lubricant in industrial applications where rust and oxidation inhibited oils are required. CITGO HyDurance AW/AL HVI 100 Fluid meets or exceeds Parker Denison HF-0 (Revision J) Eaton Brochure DIELECTRIC STRENGTH RATED WIDE TEMPERATURE PERFORMANCE SEAL CONDITIONER (Continued) CITGO Petroleum Corporation 800/ Houston, Texas Manufactured in in USA USA C10210 Industrial Fluids 117

126 CITGO HY DURANCE AW/AL HVI 100 FLUID Date 03/18 - (Continued) TYPICAL PROPERTIES: CITGO HYDURANCE AW/AL HVI 100 FLUID Grade HVI 100 Material Code Gravity, ASTM D4052, API 30.5 Density, lb/gal 7.27 Flash Point, ASTM D92, COC, C ( F) 258 (496) Viscosity ASTM D2893 cp at -23 C 19,700 Viscosity ASTM D445 cst at 40 C cst at 100 C 14.3 Viscosity Index ASTM D Four Ball Wear, mm, ASTM D kg load kg load 0.46 Pour Point, ASTM D97, C ( F) -33 (-27) Water Separability, ASTM D1401 (1) Rust Test, ASTM D665 A, B (2) Pass Dielectric Strength, KV ASTM D877 (3) 35 Notes: (1) 30 minutes max. separation time to 3 ml emulsion. Test temperature is 180 F. (2) Pass - No Rust. (3) Minimum dielectric strength is 28 KV when packaged by CITGO Petroleum. Dielectric strength is sensitive to humidity and contamination; opened containers may exhibit lower values. Store sealed containers properly in dry environment. CITGO is a registered trademark and HyDurance is a trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Industrial Fluids CITGO Petroleum Corporation 800/ Houston, Texas Manufactured in in USA USA C

127 CITGO A/W HYDRAULIC OILS Date 03/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO A/W Hydraulic Oils are superior anti-wear hydraulic and circulating fluids specially formulated with thermally stable additives. These oils offer outstanding resistance to sludge formation, chemical stability, and anti-wear protection. CITGO A/W Hydraulic Oils are designed for service in high-pressure, high-output industrial hydraulic circuits. CITGO A/W Hydraulic Oils: Utilize thermally stable zinc-based additives, helping to protect against heat-related sludge formation in sensitive electro-hydraulic servo valves. These oils are recommended for use in CNC machine tools and other high-output equipment where sustained heat is prevalent. Inhibited against rust in both fresh and sea water and pass both Procedures A and B of the ASTM D665 Rust Test. Approved against stringent performance requirements including Eaton Brochure (formerly Vickers 2950-S, I-286-S), Fives Cincinnati P-68, P-69, and P-70, and Parker Denison HF-O Revision J. Resist foaming and will not foster abnormal air entrainment in properly designed hydraulic circuits. Readily separate water, allowing water contamination to be drained from the sump. CITGO A/W Hydraulic Oils are recommended for service in vane, piston, and gear pumps when used in accordance with equipment manufacturers recommendations. Designed to provide excellent service life to these pumps as well as to other circuit components such as motors and servos. CITGO A/W Hydraulic Oils are also recommended for use as a gear and bearing lubricant in industrial applications where rust and oxidation inhibited oils are required. TYPICAL PROPERTIES: CITGO A/W HYDRAULIC OILS Grade Material Code Gravity, ASTM D4052, API Density, lb/gal Flash Point, COC, ASTM D92, F ( C) 417 (214) 446 (230) 468 (242) Viscosity, ASTM D445 cst at 40 C cst at 100 C Viscosity Index Pour Point, ASTM D97, F ( C) -27 (-33) -22 (-30) -17 (-27) Color, ASTM D1500 L0.5 L0.5 L0.5 Water Separability, ASTM D Oxidation Test, ASTM D943, Hrs. >3000 >3000 >3000 Rust Test, ASTM D665 A, B Pass Pass Pass Eaton Brochure Yes Yes Yes Meets Parker Denison HF-O Requirement Yes Yes Yes Meets Fives Cincinnati Requirement P-68 P-70 P-69 AFNOR NF E HM32 HM46 HM68 ISO VG No CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks (Continued) are the property of their respective owners. C10029 Industrial Fluids 119

128 CITGO A/W HYDRAULIC OIL SUPER MV Date 03/18 DESCRIPTION: CITGO A/W Hydraulic Oil Super MV is a multi-grade high-efficiency hydraulic oil formulated to provide excellent oxidation stability, rust protection, foam resistance and wide temperature performance. QUALITIES: Improved overall hydraulic efficiency. A special seal conditioner assists in minimizing minor leaks and providing longer seal life. Pour point and Brookfield viscosity demonstrate excellent low temperature performance. These oils exhibit excellent water separation. Highly shear stable formula. APPLICATIONS: CITGO A/W Hydraulic Oil Super MV is designed to exceed the performance requirements of: ASTM D6158 HV Denison HF-O (Revision J) Eaton Brochure ISO HV DIN They are especially recommended for hydraulic systems operating in wide temperature ranges and can remain in service without seasonal-based oil changes. TYPICAL PROPERTIES: CITGO A/W HYDRAULIC OIL SUPER MV Material Code Gravity, ASTM D4052, API 31.7 Flash Point, ASTM D92, F ( C) 385 (196) Viscosity, ASTM D445, cst, at 40 C 35.6 Viscosity, ASTM D 445, cst, at 100 C 7.9 Viscosity, ASTM D2983, cp at -40 F 19,800 Viscosity, ASTM D 2983, cp at -23 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -54 (-48) Color, ASTM D1500 L0.5 Copper Corrosion, ASTM D130 1A Four Ball Wear, ASTM D4172, mm Scar at 40 kg 0.4 Water Separation, ASTM 130 F (54 C) Pass Foam Tendency, ASTM D892 Pass Rust Protection, Part A & B, ASTM D665 Pass CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Industrial Fluids C

129 CITGO AW 68 MINING HYDRAULIC OIL Date 04/18 DESCRIPTION: QUALITIES: CITGO AW 68 Mining Hydraulic Oil is an anti-wear hydraulic and circulating oil. CITGO CITGO AW 68 Mining Hydraulic Oil offers: Wear Protection Rust and Corrosion Protection Anti Foam Performance High Viscosity Index APPLICATIONS: CITGO AW 68 Mining Hydraulic Oil is recommended for service in surface and underground mining equipment. CITGO AW 68 Mining Hydraulic Oil is also recommended for industrial applications where an antiwear, rust and oxidation inhibited oil is desired. TYPICAL PROPERTIES: CITGO AW 68 MINING HYDRAULIC OIL ISO Grade 68 Material Code Viscosity, ASTM D445 cst at 40 C 71.8 cst at 100 C 10.7 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -31 (-35) CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C10207 Industrial Fluids 121

130 CITGO ELO 32 Date 03/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO ELO 32 is a superior antiwear hydraulic and circulating fluid specially formulated with high quality base stocks and improved thermally stable additives. This oil offers outstanding resistance to sludge formation, is chemically stable and exhibits excellent antiwear protection. CITGO ELO 32 offers excellent service in high-pressure, high-output industrial hydraulic circuits. Utilizes thermally stable zinc-type additives. This helps prevent the formation of heat-related sludging in sensitive electro-hydraulic servos associated with conventional zinc-type oils. This oil is wholly suitable for N/C machine tools and other high-output equipment where sustained heat is prevalent. Exhibits superior hydrolytic stability and will not contribute to the formation of metal-etching acids or corrosive reactants. Inhibited against rusting in both fresh and sea water and passes both Procedures A and B of the ASTM D665 Rust Test. Offers antiwear protection to pumps, motors, valves and other hydraulic circuit components. It is approved against stringent performance requirements including Fives Cincinnati P-68, Parker Denison HF-O, and Eaton Brochure (formerly M-2950-S and I-286-S). Resists foaming and will not foster abnormal air entrainment in properly designed hydraulic circuits. This oil also readily separates water permitting contaminating water to be drained from the sump. CITGO ELO 32 is recommended for service in vane, piston and gear pumps when used in accordance with the manufacturers recommendations. This oil is designed to provide maximum service life to these pumps as well as to other circuit components such as motors and servos. (Continued) Industrial Fluids C

131 CITGO ELO 32 (Continued) Date 03/18 - (Continued) TYPICAL PROPERTIES: CITGO ELO 32 GRADE 32 Material Code Gravity, ASTM D4052, API 32.6 Density, lb/gal 7.18 Flash Point, ASTM D92, COC, F ( C) 417 (214) Viscosity, cst at 40 C 32.3 cst at 100 C 5.59 Viscosity Index 111 Pour Point, ASTM D97, F ( C) -30 (-34) Color, ASTM D Water Separability, ASTM D1401 (1) Oxidation Test, ASTM D943, Hrs. >6,000 Rust Test, ASTM D665 A, B Pass Copper Corrosion, D130, 3 100C 1A (Pass) Foam Test, D892, Sequence 1, II, III Pass Meets Eaton Brochure Requirements Yes (formerly Vickers M-2950-S and I-286-S) Meets Parker Denison HF-O (Revision J) Requirement Yes Meets Fives Cincinnati Requirement P-68 AFNOR NF E HM32 ISO VG No. 32 Notes: (1) 30 minutes max. separation time to 3ml emulsion. CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C10177 Industrial Fluids 123

132 CITGO FR WG-40XD HYDRAULIC FLUID Date 04/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO FR WG-40XD Hydraulic Fluid is a premium water-glycol type fire-resistant fluid designed to provide excellent performance in hydraulic systems requiring fire resistance such as those found in steel industry operations. CITGO FR WG-40XD Hydraulic Fluid is specially formulated to provide excellent service over a wide range of operating conditions. It is particularly effective in demanding steel industry applications. CITGO FR WG-40XD is formulated to provide: Factory Mutual approved Excellent fire resistance, no flash or fire point Meets U.S. Steel Requirement No.171 Meets ASTM D2882 Sperry-Vickers V104C pump test Enhanced lubricity, with wear, foam and corrosion protection Excellent heat transfer properties CITGO FR WG-40XD Hydraulic Fluid may be used in most types of hydraulic systems requiring fire resistance. Applications include steel mills, die casting and power transmission plants. CITGO FR WG-40XD is recommended in fire resistant hydraulic systems operating with Eaton/Vickers, Parker/ Denison, Rexroth and other vane and piston pumps. Maintenance of viscosity of CITGO FR WG-40XD is recommended as follows: BRIX VISCOSITY (SUS) AT 100 F CITGO FR WG-40XD WATER ADJUSTMENT CHART VISCOSITY (cst) AT 40 C PERCENT WATER IN UNADJUSTED FLUID GALLONS OF WATER NEEDED PER 100 GALLONS OF UNADJUSTED FLUID IN SYSTEM Excess Water Excess Water N O R M A L CONDITION M O D E R A T E L E V E L S E V E R E L E V E L Industrial Fluids (Continued) C

133 CITGO FR WG-40XD HYDRAULIC FLUID Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO FR WG-40XD HYDRAULIC FLUID Material Code Specific Gravity, ASTM D129, at 60/60 F Density, lb/gal Flash Point, COC, ASTM D92, F ( C) None Viscosity, D2161, SUS at 100 F 200 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -40 (-40) Color Pink ph 9.5 Reserve Alkalinity, ASTM D1121 (1) 19.0 Four Ball Wear Test, ASTM D4172, 40 Kg load, Scar Dia., mm (2) 0.66 Foam Inhibitor Yes Notes: (1) Milliliters of 0.1N hydrochloric acid solution required to neutralize 10 milliliters of fluid to a ph of 5.5. (2) Test conditions: 1 hour, 130 F, 1800 rpm. CITGO and FR WG-40XD are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C10206 Industrial Fluids 125

134 CITGO GLYCOL FR-5046HP Date 04/18 DESCRIPTION: CITGO Glycol FR-5046HP is a high pressure polymer thickened water-glycol fluid which provides superior fire-resistance at pressures in excess of 5,000 psi. Pump test results (see Tables 1, 2, and 3) show low pump wear rates for CITGO Glycol FR-5046HP, essentially equivalent to or significantly better than phosphate esters and polyol esters. CITGO Glycol FR-5046HP, therefore, provides long pump life at high pressures, excellent fire safety, plus lower cost than synthetic fluids. QUALITIES: Fire Protection: CITGO Glycol FR-5046HP contains sufficient water to snuff out ignition which could occur in hydraulic systems operating under high pressure through a sudden line rupture or fluid contact with an ignition source. Factory Mutual research tests show that thickened glycol-water fluid provides superior fire resistance compared to synthetics such as phosphate ester and polyol ester fluids. Pump Performance: CITGO Glycol FR-5046HP imparts the necessary lubricity, corrosion protection, and overall performance demanded of a high-pressure antiwear hydraulic fluid. Higher Operating Temperature: The viscosity of CITGO Glycol FR-5046HP will not drop below pump minimum requirements, even at temperatures greater than 180 F, providing greater protection where piping, cylinders, and other components are exposed to high temperatures such as in steel mill applications. Bulk reservoir temperatures should still be maintained as low as possible to reduce water evaporation, preferably 135 F or less. It is important that water content be monitored and sufficient water added to maintain water content, bulk density, viscosity, and fire protection within the required range. Shear Stability: CITGO Glycol FR-5046HP exhibits essentially no viscosity loss (temporary or permanent) over a wide range of shear rates. (See Figure 1.) Additional features include high viscosity index, low pour point, excellent heat transfer, antifoam properties, and outstanding rust and corrosion protection. APPLICATIONS: The scope of applications for CITGO Glycol FR-5046HP include mobile equipment or stationary hydraulic systems in steel mills, foundries, die casting, power transmission plants, etc. CITGO s Glycol FR-5046HP can also be used in equipment operating in environmentally sensitive areas. FR-5046HP has been shown to have a lower environmental impact than mineral oil based products. Testing of the fluid has shown that it is relatively harmless to the aquatic species commonly tested. Additional testing has shown that FR-5046HP is relatively harmless to terrestrial species such as earthworms and plant seedlings. CITGO Glycol FR-5046HP is readily biodegradable per OECD 301B.. (Continued) Industrial Fluids (Continued) C

135 CITGO GLYCOL FR-5046HP Date (Continued) 04/18 - (Continued) Table 1 ASTM D2882 test results Wear Rate Fluid (mg/hr) Conventional water-glycol 0.65 Phosphate ester 0.05 Polyol ester 0.10 Antiwear oil 0.24 CITGO Glycol FR-5046HP 0.10 Test Conditions: Vickers 104 Vane pump run at 1250 rpm, 2,000 psi, 100 hr. with test pass criteria of 1 mg/hr wear rate max. Table 3 Sundstrand Series 22 axial-piston pump. CITGO Glycol FR-5046HP was also evaluated in a Sundstrand Series 22 axial-piston pump using a modified water stability test. The pump was rebuilt according to Sundstrand s Bulletin 9658 specifications. Test conditions were: Input speed rpm Load pressure 5,000 psi Charge pressure psi Case pressure 40 psi max. Stroke 1/2 of full Reservoir temperature* F Loop temperature* F Maximum inlet vacuum 5 psi Conditions differ from a standard test. Test duration was 225 hours and followed the sequence: startup at 500 psi for 2 hr; break-in at 3,000 psi for 1 hr; and full load at 5,000 psi for 222 hr. A flow degradation of 10% constitutes failure. Test data show that there was no significant flow degradation (<1%) over the full-load duration of the test. Subsequent examination of the pump components showed no significant wear or distress. These data show that high-pressure, thickened water-glycol hydraulic fluids can be used under conditions where phosphate esters and polyol esters are normally selected. Table 2 Modified Sperry Vickers 35V25 pump test Total weight loss (mg) Component Actual Recommended Ring Vanes 6 15 *Test Conditions: 12-Vane cartridge substituted for the 10-Vane Cartridge normally used and driven at 1,800 rpm for 49 hr. Figure 1 TYPICAL PROPERTIES: CITGO GLYCOL FR-5046HP Material Code Specific Gravity ASTM D1298 (20/20 C) Viscosity ASTM D445, cst at 0 C 340 Viscosity, cst at 40 C 46 Viscosity, cst at 65 C 22 Viscosity Index ASTM D2270 >210 ph 9.9 Pour Point, ASTM D97, C -50 Appearance Red Biodegradability, Mod. Sturm Test OECD 301B, 28 days 78% CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C10032 Industrial Fluids 127

136 CITGO CYLINDER OILS Date 04/18 DESCRIPTION: CITGO Cylinder Oils are compounded lubricants designed for use in steam cylinders, gas compressor cylinders, and worm gear drives. QUALITIES: CITGO Cylinder Oils are formulated with high viscosity index base stocks, and compounded for improved metal adhesion and lubricity. Because of their special formulation, these oils provide excellent lubrication even when in contact with steam at low-to-medium pressures. APPLICATIONS: CITGO Cylinder Oils are recommended for the lubrication of steam cylinders over a wide range of operating conditions and steam quality. All grades are recommended as lubricants for natural gas compressors having separate cylinder lubrication, especially recommended where high moisture natual gas is processed. Because of their lubricity, all grades may be utilized in certain types of worm gear drives. TYPICAL PROPERTIES: CITGO CYLINDER OILS Grade Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash Point, COC, ASTM D92, F ( C) 493 (256) 525 (274) 585 (307) 555 (290) Viscosity, ASTM D445, cst at 40 C cst at 100 C ASTM D2161, SUS at 100 F SUS at 210 F Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) 0 (-18) 16 (-9) 5 (-15) 5 (-15) Color, ASTM D1500 L3 L3 7 D8 Fatty Oil, % AGMA Grade Comp. 8 Comp. ISO VG No CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Industrial Fluids C

137 CITGO EP COMPOUNDS Date 04/18 DESCRIPTION: CITGO EP Compounds are designed for industrial gear lubrication extra-duty service in a wide variety of applications where extreme pressure load conditions prevail. Industrial Gear Oils BENEFITS: CITGO EP Compounds are formulated with highly refined base stocks and select ashless additives to assure premium extreme pressure properties and provide effective lubrication under most service conditions. These products can be used in mist lubrication systems and allow directed delivery of the oil and control of stray mist. CITGO EP Compounds have a high viscosity index, excellent demulsibility, solution stability and thermal stability properties. They also provide excellent resistance to oxidation and foaming and are noncorrosive. APPLICATIONS: CITGO EP Compounds have been formulated to meet recognized industrial gear oil requirements including: DIN Part 3 CLP US Steel 224 AGMA 9005-E02 ISO CKC/CKD David Brown S (E) GM LS2 EP Gear Oil Fives Group Machine Gear Oil They are recommended for lubrication of plain and antifriction bearings and gear drives that operate under extra-heavy-duty conditions. These lubricants can be applied via misting systems and are suitable for use in bearing oil circulating systems. Typical applications are steel mills, rubber mills, and similar heavy industries where ambient conditions include water, dirt, and scale. CITGO EP Compounds are formulated for the lubrication of industrial spiral bevel, helical, spur and herringbone gears. They are especially well-suited for use in multiple gear drives that operate at greatly increased pressure between the surfaces of the gear teeth or where severe shock or heavy loads are encountered. NOTE: Consult your owner s manual for proper lubricant selection. CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. (Continued) (Continued) C

138 Industrial Gear Oils CITGO EP COMPOUNDS Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES: CITGO EP COMPOUNDS Grade Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash Point, COC, ASTM D92, F ( C) 464 (240) 482 (250) 509 (265) 491 (255) 500 (260) 491 (255) 572 (300) 482 (250) Viscosity: ASTM D445, cst at 40 C ASTM D445, cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F( C) 5 (-15) 5 (-15) 5 (-15) 5 (-15) 5 (-15) 5 (-15) 15 (-9) 15 (-9) Color, ASTM D D Copper (Cu) Corrosion, ASTM D130 (1) 1 B 1 B 1 A 1 B 1 A 1 A 2 C 2 C Demulsibility, ASTM D2711B Water in Oil, % Total Free Water, ml Emulsion, ml Oxidation Test (2) Pass Pass Pass Pass Pass Pass Pass Pass Rust Test, ASTM D665A & B Pass Pass Pass Pass Pass Pass Pass Pass Timken OK Load, ASTM D2782, lbs Four Ball EP Test, Weld, ASTM D2783, kg Four Ball Wear at 20 kg, ASTM D4172, mm Foam Test, ASTM D892, Seq. I, II, III Pass Pass Pass Pass Pass Pass Pass Pass ISO VG No Between AGMA Grade 2 EP 3 EP 4 EP 5 EP 6 EP 7 EP 8 EP Between 8 & 8A EP Fives Cincinnati P-63 P-76 P-77 P-74 P-59 P-35 U.S. Steel Req. No. 224 Meets Meets Meets Meets Meets Meets Notes: (1) Three hours at 212 F. (2) Per U.S. Steel Requirement No. 224 (ASTM D2893, 312 hrs. at 99 C). CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

139 CITGO CITGEAR SYNTHETIC EP LUBRICANTS Date 03/18 DESCRIPTION: CITGO CITGEAR Synthetic EP Gear Lubricants are designed for highly loaded gear applications operating at high temperatures and/or very low temperatures, severe conditions, or requiring extreme pressure (EP) protection. Industrial Gear Oils QUALITIES: APPLICATIONS: Compared to conventional mineral oil based products, CITGEAR Synthetic EP lubricants offer exceptionally low pour points and high viscosity indexes. The high viscosity index provides higher viscosities and greater film thickness at high temperatures and lower viscosities at low temperatures for easy start-up. Extreme Pressure (EP) additives protect gears operating in boundary lubrication regime and guard against failures associated with heavy loading and severe operation. Exhibit low foaming tendencies, high oxidation resistance, and provide excellent rust and corrosion protection. CITGO CITGEAR Synthetic EP Gear Lubricants have lower coeffecients of friction than conventional mineral oils providing reduced energy consumption. Higher heat transfer properties than conventional oils often results in cooler running machinery. Compatible with essentially all commonly used elastomers, gaskets, seals such as nitrile, Buna N, Viton, Teflon, polyethylene, flourocarbon, polyacrylate, epoxy, and PVC. They will not deteriorate acrylic paints or lacquers. CITGO CITGEAR Synthetic EP Gear Lubricants are recommended for gears requiring EP protection, for applications which experience a wide range of temperatures and where a long lasting fluid is desired for extended drain intervals. They are particularly recommended for lubricating industrial enclosed gears, sealed-for-life systems, and heavily loaded plain or roller element bearings. With proper maintenance, useful service life may be extended beyond that associated with mineral oils. They are recommended for splash, idler immersion systems, forced drip and mechanical spray systems. No flushing or cleaning is required when converting from mineral oils to these synthetic products. Consult owner s manual for proper lubricant selection. CITGO and CITGEAR are registered trademarks of CITGO Petroleum Corporation. Viton is a registered trademark of DuPont Dow Elastomers. Teflon is a registered trademark of DuPont. (Continued) (Continued) C

140 Industrial Gear Oils CITGO CITGEAR SYNTHETIC EP LUBRICANTS Date 03/18 - (Continued) TYPICAL PROPERTIES: CITGO CITGEAR SYNTHETIC EP GEAR LUBRICANTS Grade Material Code Specific Gravity ASTM D API Gravity ASTM D Pounds Per Gallon Viscosity ASTM D445 cst at 40 C cst at 100 C Viscosity Index ASTM D Brookfield at -40 ASTM D ,800 Flash Point, F ( C) ASTM D (224) 432 (222) 500 (260) 464 (240) 460 (238) 457 (236) Pour Point, F ( C) ASTM D97-71 (-57) -54 (-48) -54 (-48) -49 (-45) -44 (-42) -38 (-39) Copper Corr ASTM D130 1B 1B 1B 1B` 1B 1B Rust A/B ASTM D665 Pass Pass Pass Pass Pass Pass Demulsibility ASTM D1401 Pass Pass Pass Pass Pass Pass Timken OK Load ASTM D Four Ball Weld, Kg ASTM D Four Ball Wear ASTM D4172 at 40KG at 20KG Foam Test, Seq. I, II, III ASTM D982 Pass Pass Pass Pass Pass Pass Color ASTM D1500 L1.0 L1.0 L1.0 L1.0 L1.0 L1.0 AGMA Grade 3 EP 4 EP 5 EP 6 EP 7 EP 8 EP US Steel 224 Pass Pass Pass Pass Pass Pass SAE Grade 75W90 API Classfication GL-4 Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

141 CITGO CITGEAR SYNTHETIC HT LUBRICANTS Date 03/18 DESCRIPTION: CITGO CITGEAR Synthetic HT Gear Lubricants are fully synthetic products designed for gear applications operating at high temperatures and/or very low temperatures, severe conditions not requiring extreme pressure (EP) load protection. Industrial Gear Oils QUALITIES: APPLICATIONS: Compared to conventional mineral oil based products, CITGEAR Synthetic HT lubricants offer exceptionally low pour points and high viscosity indexes. High viscosity index provides higher viscosities and protective film thickness at high operating temperatures. Excellent low temperature properties for easy fluid pumping and equipment start-up in extreme cold environments. Highly resistant to oxidation, provides rust and corrosion protection and low foaming tendencies. Lower coefficients of friction than conventional mineral oils as determined in steel on steel measurements, which provides energy savings potential. Higher heat transfer properties than conventional mineral oils often results in cooler running machinery. Compatible with most conventional mineral oils. Compatible with essentially all elastomers, gaskets, seals such as nitrile, Buna N, Viton, Teflon, polyethylene, flourocarbon, polyacrylate, epoxy, and PVC. They will not deteriorate acrylic paints or lacquers. CITGO CITGEAR Synthetic HT Lubricants are recommended for lubrication of industrial blowers such as those manufactured by GE Energy (Roots), Gardner Denver, etc., and air and natural gas compressors. Note: CITGO CITGEAR Synthetic EP Gear Lubricants are recommended for gears requiring extreme pressure protection. CITGO and CITGEAR are registered trademarks of CITGO Petroleum Corporation. Viton is a registered trademark of DuPont Dow Elastomers. Teflon is a registered trademark of DuPont. (Continued) (Continued) C

142 Industrial Gear Oils CITGO CITGEAR SYNTHETIC HT LUBRICANTS Date (Continued) 03/18 - (Continued) TYPICAL PROPERTIES: CITGO CITGEAR SYNTHETIC HT LUBRICANTS Grade Material Code Specific Gravity ASTM D API Gravity ASTM D Pounds Per Gallon Viscosity, ASTM D445, cst at 40 C cst at 100 C Viscosity Index ASTM D Flash Point, F ( C) ASTM D (294) 550 (288) 565 (296) 554 (290) 554 (290) 540 (282) 572 (300) Fire Point, F ( C) ASTM D (306) 576 (302) 586 (308) 586 (308) 586 (308) 597 (314) 597 (314) Pour Point F ( C) ASTM D97-71 (-57) -65 (-54) -54 (-48) -49 (-45) -44 (-42) -44 (-42) -33 (-36) Copper Corr ASTM D130 1A 1A 1A 1A 1A 1A 1A Rust A/B ASTM D665 Pass Pass Pass Pass Pass Pass Pass Demulsibility ASTM D /40/0/15 40/40/0/15 40/40/0/10 40/40/0/15 40/40/0/15 40/40/0/10 40/40/0/15 Four Ball Wear at 40kg ASTM D at 20kg ASTM D Foam Test, Seq. I. II. III ASTM D892 Pass Pass Pass Pass Pass Pass Pass Color ASTM D1500 L1.0 L1.0 L1.0 L1.0 L1.0 L1.0 L1.0 AGMA Grade C

143 CITGO CITGEAR SYNTHETIC PAG GEAR FLUIDS Date 03/18 DESCRIPTION: CITGO CITGEAR Synthetic PAG Gear Fluids are premium polyalkylene glycol lubricants formulated to provide excellent performance in gear boxes, worm gears, bearings, blowers, reciprocating compressors, and hydraulic systems beyond the capabilities of mineral oils. Industrial Gear Oils QUALITIES: CITGO CITGEAR Synthetic PAG Gear Fluids offer: Outstanding thermal and oxidative stability, and resistance to sludge and deposit formation. High viscosity indexes and low pour points allow for a greater useable temperature range. Low coefficients of friction, for potential energy savings. Excellent heat transfer properites for cooler running machinery. Multipurpose industrial equipment capability. CITGO CITGEAR Synthetic PAG Gear Fluids are compatible with most seal materials in use today, for best results contact your seal manufacturer. APPLICATIONS: CITGO CITGEAR Synthetic PAG Gear Fluids are not miscible with mineral oils and should not be used as make-up for systems filled with conventional mineral oils. Mineral oils should not be used as top-off for systems which contain CITGEAR Synthetic PAG Gear Fluids. CITGEAR Synthetic PAG fluids are hygroscopic and do not separate from water. As a result, water does not settle to the bottom of the systems reservoir. The CITGO CITGEAR Synthetic PAG Gear Fluids are designed for use in: Heavy Duty Worm Gears Plain and Rolling Contact Bearings Industrial Enclosed Gears High Temperature Paper Machine Bearings Reciprocating and Rotary Screw Air and Natural Gas Compressors Plastic Calendar Operations TYPICAL PROPERTIES: CITGO CITGEAR SYNTHETIC PAG GEAR FLUIDS ISO GRADE Material Code Specific Gravity Density, lb/gal Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445, cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -54 (-48) -49 (-45) -44 (-42) -44 (-42) -38 (-39) Flash Point, ASTM D92, F ( C) 550 (288) 547 (286) 554 (290) 558 (292) 558 (298) Rust Protection, ASTM D665, A/B Pass Pass Pass Pass Pass 4-Ball Weld, ASTM D4172, mm at 40kg CITGO and CITGEAR are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. (Continued) C

144 Industrial Gear Oils CITGO EP GEAR SEMI SYNTHETIC 68 Date 04/18 DESCRIPTION: CITGO EP Gear Semi Synthetic 68 is designed for severe service in a wide variety of extreme pressure industrial applications. BENEFITS: Blended with synthetic components, severely hydrotreated base stocks and ashless additives. Provides excellent extreme pressure properties and anti-wear characteristics. CITGO EP Gear Semi Synthetic 68 has a high viscosity index, excellent demulsibility, solution stability and thermal stability. Provides excellent resistance to oxidation and foaming and is noncorrosive. APPLICATIONS: Recommended for lubrication of plain and antifriction bearings and gear drives that operate under extra-heavy-duty conditions. Formulated for the lubrication of industrial spiral bevel, helical, spur and herringbone gears. DIN Part 3 US Steel 224 AGMA 9005-E02 ISO CKC/CKD David Brown S GM LS 2 EP Gear Oil Fives Cincinnati Machine Gear TYPICAL PROPERTIES: CITGO EP GEAR SEMI SYNTHETIC 68 ISO Viscosity Grade 68 Material Code Gravity, ASTM D4052, API 30.7 Density, lb/gal at 60 F 7.27 Flash Point, COC, ASTM D92, F ( C) 195 (383) Viscosity: ASTM D445, cst at 40 C 66.0 ASTM D445, cst at 100 C 8.6 Viscosity Index, ASTM D Pour Point, ASTM D97, F( C) -21 (-30) Color, ASTM D Rust Test, ASTM D665A & B Pass Timken OK Load, ASTM D2782, lbs. 65 Four Ball EP Test, Weld 315 Four Ball Wear at 20 kg Foam Test, ASTM D892, Seq. I, II, III 0-0, 0-0, 0-0 ISO VG No. 68 AGMA Grade 2 EP CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

145 CITGO CITGEAR WT 320 Date 03/18 DESCRIPTION: CITGO CITGEAR WT 320 is a synthetic gear lubricant designed specifically for wind turbine gear lubrication. CITGO CITGEAR WT 320 meets industrial gear oil standard DIN Industrial Gear Oils QUALITIES: APPLICATIONS: CITGO CITGEAR WT 320 offers: Wear protection for gear and bearing components Protection against micropitting High viscosity index (VI) for wide temperature performance Oxidation stability and rust/corrosion protection Suppression of foam and air/oil dispersion Seal compatibility per DIN and ISO 1817(Flender) CITGO CITGEAR WT 320 is recommended for wind turbine gear lubrication and can also be used in industrial gear applications requiring extreme pressure (EP) protection, operating under a wide range of temperatures, and where a long lasting fluid is desired. Approved for: Flender gear units by Siemens MD (Rev.15) Approval No. A-CI Hansen gearboxes FAG Schaeffler bearings in wind turbines (passed 4 step test) TYPICAL PROPERTIES: CITGO CITGEAR WT 320 ISO VISCOSITY GRADE 320 Material Code Gravity, ASTM D4052, API 27.3 Density, lb/gal at 60 F 7.42 Flash Point, COC, ASTM D92, F ( C) 210 (410) Viscosity ASTM D445 cst at 40 C 328 cst at 100 C 38.2 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -27 (-33) Color, ASTM D1500 L1.0 Foam Test, ASTM D892, Seq. I, II, III 0-0, 10-0, 0-0 Water F, ASTM D /40/0/30 Former AGMA Grade 6 EP CITGO and CITGEAR are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

146 Industrial Gear Oils CITGO CITGEAR XCO OILS Date 04/18 DESCRIPTION: CITGO CITGEAR XCO Oils are premium lubricants that provide excellent bearing and gear lubrication performance in steel industry applications such as high speed rod mills. BENEFITS: APPLICATIONS: CITGO CITGO CITGEAR XCO Oils are formulated with high quality paraffinic base oils and additive systems that assure: Excellent oil/water separation which allow water removal from gear and bearing systems High level of wear protection for critical machinery Outstanding rust and corrosion protection in wet environments Excellent oxidation stability for long service life Premium anti-foam properties High thermal stability minimizes formation of heat related sludge and varnishes CITGO CITGEAR XCO Oils are recommended for use in high speed rod mill circulation systems and other gear and bearing lubrication applications. CITGO CITGEAR XCO Oils are recommended for use in Danieli and Morgan (Siemens AG) high speed rod mills. TYPICAL PROPERTIES: CITGO CITGEAR XCO OILS Grade Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash Point, ASTM D92, COC, F ( C) 482 (250) 522 (272) 561 (294) 554 (290) Viscosity, ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -6 (-21) 10 (-12) 10 (-12) 10 (-12) Color, ASTM D1500 L1.0 L4.0 L4.0 L5.0 Rust Test, ASTM D665 A and B Pass Pass Pass Pass Water Separation, ASTM D1401 at 180 F (ml Emulsion at 30 minutes) 3.0 Max. 3.0 Max. 3.0 Max. 3.0 Max. Foam Test, ASTM D892, Sequence I, II, III Pass Pass Pass Pass Four Ball Wear, ASTM D kg CITGO and CITGEAR are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

147 CITGO PACEMAKER SD OILS Date 03/18 DESCRIPTION: CITGO Pacemaker SD Super Demulsibility Oils are high quality circulating lubrication oils, with superior oil/water separation characteristics, oxidation stability, and rust and corrosion protection specifically designed for steel mill applications. Available in viscosity grades 220, 320, 460 and 680. CITGO Pacemaker Oils exceed Siemens AG requirements for Morgoil Advanced Bearing Lubricant Super Demulsibility specification. Industrial Gear Oils QUALITIES: APPLICATIONS: CITGO Pacemaker SD Oils are formulated to provide: Outstanding water removal characteristics Long service life in circulating systems Corrosion protection and foam control Excellent filterability Deposit control CITGO Pacemaker SD Oils are recommended for circulating systems requiring AGMA R&O type lubricants operating in severe conditions such as water contamination. These products allow rapid oil separation from water at steel mill operating temperatures, especially in Siemens AG (formerly Morgan Construction Company) steel mill roll bearings. CITGO Pacemaker SD Oils can be used as: Gear oils Compressor oils Rust/oxidation inhibited (R&O) oils Roll bearing lubricant (blooming, slabbing, hot and cold strip mills) Morgoil lubrication system oils MESTA system oils Morgoil and MESTA are registered trademarks of Siemens AG. (Continued) C

148 Industrial Gear Oils CITGO PACEMAKER SD OILS Date 03/18 - (Continued) TYPICAL PROPERTIES: CITGO PACEMAKER SD OILS Grade Material Code Gravity, ASTM D4052, API Density, lb/gal Flash Point, ASTM D92, COC, F ( C) 464 (240) 464 (240) 554 (290) 554 (290) Viscosity: ASTM D445, cst at 40 C ASTM D 445, cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) 0 (-18) 5 (-15) 5 (-15) 5 (-15) Color, ASTM D Rust Test, ASTM D665 A Pass Pass Pass Pass Demulsibility, ASTM D2711 (ml Emulsion at 125 F) 1.0 max. 1.0 max. 1.0 max. 1.0 max. Water Separation, ASTM D1401 at 180 F (ml Emulsion at 40 minutes) 3.0 max. 3.0 max. 3.0 max. 3.0 max. Foam Test, ASTM D892, Seq. I, II, III Pass Pass Pass Pass AGMA Grade CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. (Continued) C

149 CITGO CITGEAR MGW-OGL Date 04/18 DESCRIPTION: CITGO CITGEAR MGW-OGL is an asphaltic open gear lubricant designed to protect heavily loaded open gears. CITGO CITGEAR MGW-OGL provides a heavy, dense film that includes extreme pressure additives that ensure smooth operation even on gears that operate under harsh conditions. This gear lubricant contains a solvent for ease in handling and application. Industrial Gear Oils QUALITIES: CITGO CITGEAR MGW-OGL offers the following qualities: Resistance to sludge and deposit formation. High film strength Excellent wear protection Extends gear life Protects against rust and corrosion Water wash-off protection Suitable for use in airless spray systems Non-chlorinated APPLICATIONS: Grinding mill gear and pinion, ball grinding mill gear and pinion, girth gears, SAG mill gears, cement kiln open gears APPROVAL: Shanghai Heavy Industries TYPICAL PROPERTIES: CITGO CITGEAR MGW-OGL Material Code Texture Smooth Color Black Flash Point, ASTM D92, F ( C) (without diluent) 475 (246) Flash Point, ASTM D92, F ( C) (with diluent) 240 (116) Viscosity ASTM D C, cst (without diluent) Viscosity ASTM D C, cst (with diluent) Four Ball Weld EP, ASTM D2783, kg 500 Four Ball Wear, ASTM D4172, mm 0.33 Four Ball LWI, ASTM D2783, kgf 83 Copper Corrosion, ASTM D130 3B Rust Prevention, ASTM D665 Pass FZG, ASTM D5182, Load Stages Passed >12 USS 0º C, gls 1.65 CITGO and CITGEAR are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

150 CITGO AUTOKUT AS SERIES Date 04/18 DESCRIPTION: CITGO Autokut AS Series are transparent, highly active metal removal fluids designed for severe machining operations. Citgo Autokut AS series is available in four different viscosity grades to meet the requirements of a modern engineering facility. Metalworking Fluids FEATURES: BENEFITS: Contains active sulfur and other anti-weld components High levels of lubricity Low odor Chlorinated paraffin free Light in color Contains a stable oil mist suppressant Improved productivity and lower costs of operation Excellent surface finish at high feeds and speeds Improved worker acceptability Reduction in disposal costs and reduced risk of rust Aids visibility of operation Improves working environment and worker safety by minimizing mist formation NOTE: Not recommended for yellow or non-ferrous metals APPLICATIONS: CITGO Autokut AS Series are formulated for machining operations involving alloyed, stainless and chrome steels. These products are intended for severe machining operations such as broaching, tapping and cold-heading. Lower viscosity grades are used for higher speed lighter duty applications and higher viscosity is used for slower speed heavier duty operations. Material Compatibility P - Steels M - Stainless Steel K - Cast Iron Recommended Highly Recommended (Continued) (Continued) C

151 CITGO AUTOKUT AS SERIES Date (Continued) 04/18 - (Continued) TYPICAL PROPERTIES - CITGO AUTOKUT AS SERIES Grade AS 15 AS 32 AS 46 AS 68 Material Code Gravity, ASTM D4052, API Gravity, Specific, ASTM D1298, 60/60 F Density, lb/gal Flash Point, COC, ASTM D92, F ( C) 349 (176) 363 (184) 356 (180) 356 (180) Viscosity, cst at 40 C cst at 100 C SUS at 100 F SUS at 210 F Color, ASTM D Pour Point, ASTM D97, F ( C) (-43) -22 (-30) (-26) (-26) Copper Corrosion, ASTM D130, 3 hrs at 212 F Active Sulfur Yes Yes Yes Yes Phosphorus No No No No Lubricity Additive Yes Yes Yes Yes Metalworking Fluids CITGO and Autokut are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

152 CITGO AUTOKUT IS SERIES Date 04/18 DESCRIPTION: CITGO Autokut IS Series are non-staining metal removal oils designed for machining non-ferrous metals and many ferrous metals. CITGO Autokut IS Series are available in two viscosity grades to meet the requirements of a modern engineering facility. The lower viscosity grade is used for higher speed lighter duty applications and the higher viscosity is used for slower speed heavier duty operations. Metalworking Fluids FEATURES: BENEFITS: Excellent lubricity and mild EP Compatible with all metals Chlorine free Light in color Contain a stable oil mist suppressant Improved productivity and lower costs of operation Non staining on ferrous and non-ferrous metals Benefits environmental needs and reduces disposal costs Light color aids visibility of operation Improves working environment and worker safety by minimizing mist formation APPLICATIONS: CITGO Autokut IS 15 is a low viscosity oil, primarily recommended for all machining operations on aluminum and magnesium and their alloys. This light viscosity product has additional applications in deep drilling and the honing of steel, cast iron and alloyed copper. CITGO Autokut IS 46 is designed for more severe duty applications and contains a high level of non-staining extreme pressure agent to permit its use over a wide variety of materials, and over a wide range of cutting depths, feeds and speeds. It can also be used in turning, sawing, milling and drilling of non-ferrous metals as well as some plain carbon steels and free-machining steel alloys. Material Compatibility P - Steels M - Stainless Steel K - Cast Iron N - Non-ferrous Recommended Highly Recommended (Continued) C

153 CITGO AUTOKUT IS SERIES Date 04/18 - (Continued) TYPICAL PROPERTIES - CITGO AUTOKUT IS SERIES Grade IS 15 IS 46 Material Code Gravity, ASTM D4052, API Gravity, Specific, ASTM D1298, 60/60 F Density, lb/gal Flash Point, COC, ASTM D92, F ( C) 361 (183) 428 (220) Viscosity, cst at 40 C cst at 100 C SUS at 100 F SUS at 210 F Color, ASTM D Pour Point, ASTM D97, F ( C) -44 (-42) -6 (-21) Copper Corrosion, ASTM D130, 3 hrs at 212 F 1 A/B 1 A/B Active Sulfur No No Phosphorus No No Lubricity Additive Yes Yes Metalworking Fluids CITGO and Autokut are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

154 CITGO AUTOKUT EXTRUSION OIL Date 04/18 DESCRIPTION: CITGO Autokut Extrusion Oil is a heavy duty fluid designed for a variety of metal forming and other metalworking operations. Metalworking Fluids FEATURES: BENEFITS: Contains advanced lubrication and anti-weld components Compatible with all metals Residues are easily cleaned High viscosity Free of chlorinated components Benefits environmental needs and reduces disposal costs Improved productivity and lower costs of operation, improving surface finish and extending tool life Non staining on ferrous and non-ferrous metals Conventional cleaners can be used to remove unwanted residues Oil remains in the areas intended during the operation process APPLICATIONS: CITGO AutoKut Extrusion Oil is formulated for a variety of drawing, stamping, forming and extrusion applications over a wide range of machining applications and metallurgies. Material Compatibility P - Steels M - Stainless Steel K - Cast Iron N - Non-ferrous Recommended Highly Recommended TYPICAL PROPERTIES - CITGO AUTOKUT EXTRUSION OIL Material Code Gravity, ASTM D4052, API 23.9 Gravity, Specific, ASTM D1298, 60/60 F Density, lb/gal 7.6 Flash Point, COC, ASTM D92, F ( C) 432 (222) Viscosity, ASTM D445, cst at 40 C cst at 100 C 15.3 ASTM D2161, SUS at 100 F 546 SUS at 210 F 79 Color, ASTM D Pour Point, ASTM D97, F ( C) 15.8 (-9) Copper Corrosion, ASTM D130, 3 hrs at 212 F 1 A/B Active Sulfur No Phosphorus No Lubricity Additive Yes CITGO and Autokut are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or (Continued) trademarks are the property of their respective owners. C

155 CITGO AUTOKUT TRI-PURPOSE Date 04/18 DESCRIPTION: CITGO Autokut Tri-Purpose is a transparent, non-corrosive, multi-purpose cutting oil. It is equally effective for use as a cutting oil and as a lubricant in screw machines and other automatic type machine tools. FEATURES: BENEFITS: Tri-functional, can be used as a gear lubricant, cutting oil and hydraulic fluid Contains a stable oil mist suppressant Contains advanced lubrication and anti-weld components Compatible with all metals Chlorine free Light in color Premium rust and oxidation protection Tri-functionality reduces costs by consolidating inventory and minimizing cross-contamination risks Improves working environment and worker safety by minimizing mist formation Improves productivity and lower costs of operation, with improved tool life and surface finish Non staining on ferrous and non-ferrous metals Benefits environmental needs and reduces disposal costs Aids visibility of operation Versatility in gear and hydraulic applications Metalworking Fluids APPLICATIONS: CITGO Autokut Tri-Purpose is a cutting oil, hydraulic fluid and a gear lubricant. It is specifically designed for automatic screw machines and is recommended for machining non-ferrous metals and ferrous alloys having machinability rating of approximately 50% or higher. It can be used in all automatic screw machines and in similar equipment for: Drilling, Counter-Boring, Turning, Shaving, Reaming, Tapping, Forming and Stamping. Material Compatibility P - Steels M - Stainless Steel K - Cast Iron N - Non-ferrous Recommended Highly Recommended CUTTING HYDRAULIC GEAR Multi-use Fluid (Continued) C

156 CITGO AUTOKUT IS SERIES Date 04/18 - (Continued) TYPICAL PROPERTIES - CITGO AUTOKUT IS SERIES Metalworking Fluids Grade IS 15 IS 46 Material Code Gravity, ASTM D4052, API Gravity, Specific, ASTM D1298, 60/60 F Density, lb/gal Flash Point, COC, ASTM D92, F ( C) 361 (183) 428 (220) Viscosity, cst at 40 C cst at 100 C SUS at 100 F SUS at 210 F Color, ASTM D Pour Point, ASTM D97, F ( C) -44 (-42) -6 (-21) Copper Corrosion, ASTM D130, 3 hrs at 212 F 1 A/B 1 A/B Active Sulfur No No Phosphorus No No Lubricity Additive Yes Yes CITGO and Autokut are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

157 CITGO TRUKUT GP 205 Date 04/18 DESCRIPTION: CITGO Trukut GP 205 is a conventional general purpose cutting fluid designed to be readily mixed with water to form a stable emulsion. Designed for a variety of machining operations, it is suitable for use on ferrous and non-ferrous metals. FEATURES: BENEFITS: Forms stable emulsions in various water qualities Multi-metal and general purpose applications Good residual corrosion properties Free from chlorinated paraffins Excellent corrosion prevention properties Product performance is constant and machine remains clean Wide application range reduces the need for several products Increases the time between in process operations and protects the machine tool parts from rust Reduces disposal costs Reduces the need for in-process corrosion protection fluids Metalworking Fluids APPLICATIONS: CITGO Trukut GP 205 is recommended for milling, turning, drilling, grinding and other metalworking operations on ferrous and non-ferrous metals where efficiency of an emulsifiable oil is preferred. Trukut GP 205 has excellent cooling and rust prevention properties. It is also a preferred grinding fluid. Concentrate Diluted with Water Material Compatibility P - Steels M - Stainless Steel K - Cast Iron N - Non-ferrous Recommended Highly Recommended Refractometer Reading Refractometer Chart Concentration Refractometer Reading at 10% = 10.0 o Brix Refractometer Factor = 1.0 (Continued) C

158 CITGO TRUKUT GP 205 Date 04/18 - (Continued) TYPICAL PROPERTIES - CITGO TRUKUT GP 205 Metalworking Fluids Material Code Gravity, Specific, ASTM D1298, 60/60 F 0.91 Density, lb/gal 7.59 Flash Point, COC, ASTM D92, F ( C) 320 (160) Viscosity, cst at 40 C 35 Color, ASTM D Pour Point, ASTM D97, F ( C) 32 (0) ph at 5% in Deionized 9.6 Corrosion (modified Iron Chip Rust test) Pass Copper Corrosion, ASTM D130, 3 hrs at 212 F 1B Emulsion Stability, 24 hrs at 77 F Deionized Water Pass Hard Water Pass Solution Stability, 24 hrs at 30 F Pass Appearance Yellow METAL MACHINABILITY GROUPS Machining Operation 1 Non-Ferrous, Soft Metals 2 Nickel Alloys, Nitralloy Steels, Cast Irons and Alloy Steels (up to 200 Brinell) 3 Stainless Steels, Monel Metals, Cast Irons and Alloy Steels (200 to 300 Brinell) 4 Titanium Alloys, High Tensile Nickel Alloys, Austentic Stainless Steels, Tool Steel and High Tensile Alloy Steels (300 to 400 Brinell) Turning, Boring, Milling, Forming, Drilling, Sawing 5-7% 5-7% 8-12% 8-12% Tapping, Thread Rolling, Reaming, Screw Cutting, Broaching 5-7% 5-7% 8-12% 8-12% Gear Shaping, Form and Thread Milling, Shaving, Hobbing, and Trepanning 5-7% 5-7% 8-12% 8-12% Internal and External Grinding, Form and Thread Grinding 5-7% 5-7% 5-7% 5-7% Stamping 5-10% 5-10% 5-10% 5-10% Note: Dilution ratios shown are approximate and may require higher or lower water concentrations depending on a number of factors including the type of metal cut, machine speed, the severity of the operation, metal hardness, etc. CITGO and Trukut are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

159 CITGO TRUKUT HD 220 Date 04/18 DESCRIPTION: CITGO Trukut HD 220 is a heavy-duty cutting and grinding fluid designed to be diluted with water to form an emulsion. It is recommended for use on ferrous and non-ferrous metals. FEATURES: BENEFITS: Contains robust boundary lubrication and lubricity technology Affords efficient cooling Helps prevent bacterial growth Forms stable emulsions in various water qualities Low staining. Multi-metal and application compatibility Free from chlorinated paraffins Excellent corrosion prevention properties Improves tool life and surface finish Increases productivity Extends odor-free sump life Predictable machining performance Wide application range reduces the need for several products Reduces disposal costs Reduces the need for in-process corrosion protection fluids Concentrate Diluted with Water Metalworking Fluids APPLICATIONS: CITGO Trukut HD 220 is well suited for CNC Machining where a single cutting fluid may be needed to function in a wide variety of operations and metallurgies. It performs in multiple cutting operations including turning, boring, drilling, grinding, and threading. Material Compatibility P - Steels M - Stainless Steel K - Cast Iron N - Non-ferrous Recommended Highly Recommended Refractometer Reading Refractometer Chart Concentration Refractometer Reading at 10% = 10.0 o Brix Refractometer Factor = 1.0 (Continued) C

160 CITGO TRUKUT HD 220 Date 04/18 - (Continued) TYPICAL PROPERTIES - CITGO TRUKUT HD 220 Metalworking Fluids Material Code Gravity, Specific, ASTM D1298, 60/60 F 0.94 Density, lb/gal 7.83 Flash Point, COC, ASTM D92, F ( C) 311 (155) Viscosity, cst at 40 C 111 Color, ASTM D1500 L5.0 Pour Point, ASTM D97, F ( C) 32 (0) ph at 5% in Deionized 9.0 Corrosion (modified Iron Chip Rust test) Pass Copper Corrosion, ASTM D130, 3 hrs at 212 F 1B Emulsion Stability, 24 hrs at 77 F Deionized Water Pass Hard Water Pass Solution Stability, 24 hrs at 30 F Pass Appearance Amber METAL MACHINABILITY GROUPS Machining Operation 1 Non-Ferrous, Soft Metals 2 Nickel Alloys, Nitralloy Steels, Cast Irons and Alloy Steels (up to 200 Brinell) 3 Stainless Steels, Monel Metals, Cast Irons and Alloy Steels (200 to 300 Brinell) 4 Titanium Alloys, High Tensile Nickel Alloys, Austentic Stainless Steels, Tool Steel and High Tensile Alloy Steels (300 to 400 Brinell) Turning, Boring, Milling, Forming, Drilling, Sawing 5-7% 5-7% 6-8% 8-10% Tapping, Thread Rolling, Reaming, Screw Cutting, Broaching 6-9% 5-7% 6-8% 8-10% Gear Shaping, Form and Thread Milling, Shaving, Hobbing, and Trepanning 5-7% 5-7% 6-8% 8-10% Internal and External Grinding, Form and Thread Grinding 5-7% 5-7% 5-7% 5-7% Stamping 10% 10% 20% 20% Note: Dilution ratios shown are approximate and may require higher or lower water concentrations depending on a number of factors including the type of metal cut, machine speed, the severity of the operation, metal hardness, etc. CITGO and Trukut are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

161 CITGO CITCOOL SS-HD Date 04/18 DESCRIPTION: CITGO CITCOOL SS-HD is a water extendable semi-synthetic coolant recommended for heavy-duty applications. The product is suitable for job shops where one coolant is needed to machine a variety of metals in multiple operations. FEATURES: BENEFITS: Forms stable emulsions in various water hardness up to 1000ppm Low foaming tendencies Medium oil content Free of chlorine, secondary amines, phenols, nitrates, PCB s, and heavy metals Product performance is constant and machine remains clean Reliable in-service performance and long sump life Heavy-duty machining capability Ease of disposal and friendly work environments Metalworking Fluids APPLICATIONS: CITGO CITCOOL SS-HD is recommended for general machining including thread cutting and forming, deep hole drilling and boring, reaming, and grinding of cast irons, ferrous alloys and stainless steels, free cutting aluminum alloys, oil resistant plastics, and other non-ferrous materials. Concentrate Diluted with Water Material Compatibility P - Steels M - Stainless Steel K - Cast Iron N - Non-ferrous * Recommended Highly Recommended *Might stain some sensitive aluminum alloys. e.g and 7000 series Refractometer Reading Refractometer Chart Concentration Refractometer Reading at 10% = 6.8 o Brix Refractometer Factor = 1.47 (Continued) C

162 CITGO CITCOOL SS-HD Date 04/18 - (Continued) TYPICAL PROPERTIES - CITGO CITCOOL SS-HD Metalworking Fluids Material Code Appearance, Concentrate (neat) Amber Fluid Dilution (5% in DI water) Semi-Translucent Gravity, Specific, ASTM D1298, 60/60 F 1.02 Mineral Oil Content % 20 ph at 3% concentration 9.5 (5%) Defoaming ml (5% in 50 ppm water) Nil (60 sec.) METAL MACHINABILITY GROUPS (1) Machining Operation 1 Non-Ferrous, Soft Metals (2) 2 Nickel Alloys, Nitralloy Steels, Cast Irons and Alloy Steels (up to 200 Brinell) 3 Stainless Steels, Monel Metals, Cast Irons and Alloy Steels (200 to 300 Brinell) 4 Titanium Alloys, High Tensile Nickel Alloys, Austentic Stainless Steels, Tool Steel and High Tensile Alloy Steels (300 to 400 Brinell) Turning, Boring, Milling, Forming, Drilling, Sawing 5-7% 5-7% 8-10% 8-10% Tapping, Thread Rolling, Reaming, Screw Cutting, Broaching 5-7% 5-7% 8-10% 8-10% Gear Shaping, Form and Thread Milling, Shaving, Hobbing, and Trepanning 5-7% 5-7% 8-10% 8-10% Internal and External Grinding, Form and Thread Grinding 5-7% 5-7% 5-7% 5-7% Stamping 5-20% 5-20% 5-20% 5-20% Notes: (1) Dilution ratios shown are approximate and may require higher or lower water concentrations depending on a number of factors including the type of metal cut, machine speed, the severity of the operation, metal hardness, etc. (2) CITCOOL SS-HD might stain sensitive aluminum alloys such as 2000 and 7000 series alloys. CITGO and CITCOOL are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

163 CITGO CITCOOL 33 Date 03/18 DESCRIPTION: CITGO CITCOOL 33 is a heavy-duty synthetic coolant designed to be diluted in water to the proper concentrations to afford excellent operations in high-performance machining. FEATURES: BENEFITS: Balanced lubricity and boundary lubrication components Readily soluble in water Oil free Distinct transparent green Fully synthetic Contains effective bactericide and fungicide Rejects tramp oil Improves tool life and surface finish with enhanced EP and wear protection Easy mixing and clean up, and improved solution stability even in harder water Odor and rancidity free, no gummy residues, and eliminates oil mists in the workplace Good work piece visibility Superior heat transfer to improve tool life and part tolerances Inhibits initial bacterial and fungal growth in service Concentrate Diluted with Water Tramp oils are readily removed; eliminating a source for bacteria and fungus to grow, resulting in no rancid ordors and extending sump life Metalworking Fluids APPLICATIONS: CITGO CITCOOL 33 is designed primarily for use in machining titanium, ferrous metals, and their alloys, and stainless steel. It is non-corrosive to brass and copper so also recommended for these metals. Material Compatibility P - Steels M - Stainless Steel Recommended Highly Recommended *Not recommended for aluminum, magnesium and their alloys due to possible staining. Refractometer Reading Refractometer Chart Concentration Refractometer Reading at 10% = 3.9 o Brix Refractometer Factor = 2.56 (Continued) C

164 CITGO CITCOOL 33 Metalworking Fluids Date 03/18 - (Continued) TYPICAL PROPERTIES - CITGO CITCOOL 33 Material Code Appearance, Concentrate (neat) Clear, Green Dilution (5% in DI water) Clear, Green (1) Gravity, Specific, ASTM D1298, 60/60 F 1.07 Density, lb/gal 8.9 Viscosity, ASTM D445, cst at 40 C 3.7 ASTM D2161, SUS at 100 F 17 ph, Concentrate 9.5 Falex Load, 5% in tap water, ASTM D3233, lbs Rust Test, 3% in tap water, ASTM D4627 Pass Solution Stability (5%), 24 hrs. at 30 F No Separation Copper Corrosion (5%), 3 hrs. at 122 F, ASTM D130 1B Foam Test, ASTM D892, Seq. I 90-0 Seq. II 10-0 Seq. III 20-0 Note: 1) Dilute solutions can be hazy if tap water is used depending upon water hardness. METAL MACHINABILITY GROUPS (1) Machining Operation Turning, Boring, Milling, Forming, Drilling, Sawing 1 Non-Ferrous, Soft Metals (2) 5-7% 2 Nickel Alloys, Nitralloy Steels, Cast Irons and Alloy Steels (up to 200 Brinell) 5-7% STORAGE, HANDLING AND SPECIAL CONSIDERATIONS: Preferred storage is indoors away from sun and heat. Do not allow to freeze. Under long term storage, product may discolor. 3 Stainless Steels, Monel Metals, Cast Irons and Alloy Steels (200 to 300 Brinell) 7-9% 4 Titanium Alloys, High Tensile Nickel Alloys, Austentic Stainless Steels, Tool Steel and High Tensile Alloy Steels (300 to 400 Brinell) 7-9% Tapping, Thread Rolling, Reaming, Screw Cutting, Broaching 5-7% 5-7% 8-10% 8-10% Gear Shaping, Form and Thread Milling, Shaving, Hobbing, and Trepanning 5-7% 5-7% 8-10% 8-10% Internal and External Grinding, Form and Thread Grinding 5-7% 5-7% 5-7% 5-7% Stamping 10% 10% 20% 20% Notes: (1) Dilution ratios shown are approximate and may require higher or lower water concentrations depending on a number of factors including the type of metal cut, machine speed, the severity of the operation, metal hardness, etc. (2) CITCOOL 33 is not recommended for machining aluminum alloys or magnesium (due to possible staining). CITGO and CITCOOL are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

165 CITGO RUST-O-LENE LT Date 03/18 DESCRIPTION: CITGO Rust-O-Lene LT is a rust preventative oil formulated with effective rust inhibitors and high quality base oils. It exhibits excellent metal wetting and water displacement properties and is designed for temporary protection of metal parts during manufacturing and storage. CITGO Rust-O-Lene LT can also be used as a hydraulic and circulating oil where added rust protection is required. FEATURES: BENEFITS: May be applied by dipping, spraying or brushing Excellent water displacement properties Excellent metal wetting Multi-purpose fluid Effective application on any part configuration Protects parts after machining with aqueous cutting fluids Provides a high degree of prevention of fingerprint or perspiration acid corrosion Can be used as an hydraulic and circulating oil where robust corrosion protection is needed Metalworking Fluids APPLICATIONS: CITGO Rust-O-Lene LT is used for rust protection of semi-finished or finished metal parts and assemblies that require longer term protection while stored indoors. It can be used by hydraulic and circulating systems for industrial equipment requiring better protection from rust. Material Compatibility P - Steels M - Stainless Steel K - Cast Iron N - Non-ferrous Recommended Highly Recommended TYPICAL PROPERTIES - CITGO RUST-O-LENE LT Protected Metal Unprotected Metal Material Code Gravity, ASTM D4052, API 30 Solvent Present No Flash Point, COC, ASTM D92, F ( C) 385 (196) Viscosity, ASTM D445, cst at 40 C 52 ASTM D2161, SUS at 100 F 241 Rust Protection, Humidity Cabinet (hours) 1300 CITGO and Rust-O-Lene are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

166 CITGO RUST-O-LENE ST Date 03/18 DESCRIPTION: CITGO Rust-O-Lene ST is a rust preventative oil formulated with highly effective rust inhibitors, a high flash solvent and high quality base oils. It provides a protective film after solvent evaporation and is designed for short term protection of metal parts during manufacturing and storage indoors. Metalworking Fluids FEATURES: BENEFITS: May be applied by dipping, spraying or brushing Excellent water displacement properties Excellent metal wetting properties High quality base oil and high flash point solvent carrier Effective application on any part configuration Protects parts after machining with aqueous cutting fluids Provides a high degree of prevention of fingerprint or perspiration acid corrosion Forms a protective film after solvent evaporation APPLICATIONS: CITGO Rust-O-Lene ST is used for rust protection of semi-finished or finished metal parts and assemblies where temporary or in transit protection is required. Material Compatibility P - Steels M - Stainless Steel K - Cast Iron N - Non-ferrous Recommended Highly Recommended TYPICAL PROPERTIES - CITGO RUST-O-LENE ST Protected Metal Unprotected Metal Material Code Gravity, ASTM D4052, API 41.6 Solvent Present Flash Point, COC, ASTM D92, F ( C) 160 (72) Viscosity, ASTM D445, cst at 40 C 3 ASTM D2161, SUS at 100 F 36 Rust Protection, Humidity Cabinet (hours) 1300 NOTE: CITGO RUST-O-LENE ST cannot be sold in the California South Coast Air Quality Management District (SCAQMD) due to the VOC level from the solvent. Yes CITGO and Rust-O-Lene are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

167 CITGO AR SLUSHING OIL Date 04/18 DESCRIPTION: CITGO AR Slushing Oil is a light colored, low viscosity rust preventative coating oil. It utilizes a highly effective metal protection system to provide excellent rust protection for steel stored for intermediate periods under cover. The light viscosity promotes complete surface coverage and quick drainage of excess oil. The low pour point facilitates cold weather storage and handling. TYPICAL PROPERTIES: CITGO AR SLUSHING OIL Material Code Gravity, API ASTM D Density, lb/gal 7.19 Flash Point ASTM D93, PM 360 Flash Point ASTM D92, COC 392 Fire Point ASTM D92, COC 437 Viscosity ASTM D445 cst at 40 C 18 cst at 100 C 3.8 Viscosity ASTM D2161 SUS at 100 F 95 SUS at 210 F 39 Viscosity Index ASTM D Carbon Residue ASTM D189, WT% 0.04 Color, ASTM D Pour Point ASTM D97, F -35 Copper Corrosion ASTM D130 1A Rust Test ASTM D665B, Salt Water Pass Humidity Cabinet Test ASTM D1748, hrs Metalworking Fluids CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

168 CITGO QUENCHOL Date 04/18 DESCRIPTION: CITGO Quenchol 521 and 624 are highly stable quench oils designed especially for use in steel heat treating operations. They are formulated with premium high viscosity index base oils and additives to provide outstanding service life and performance. Metalworking Fluids QUALITIES: APPLICATIONS: CITGO Quenchol products provide: Excellent thermal stability and oxidation resistance Premium wetting ability and cooling capability Uniform heat dissipation for quality hardened steel production Less viscosity change during the quenching operation compared to low viscosity index oils CITGO Quenchol products offer superior service in steel quenching operations requiring a premium mineral quench oil. TYPICAL PROPERTIES: CITGO QUENCHOL Quenchol Quenchol Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash Point, ASTM D92, F ( C), Min. 354 (179) 410 (210) Viscosity: ASTM D445, cst at 40 C ASTM D 445,cSt at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) 16 (-9) 16 (-9) Color, ASTM D1500 D8.0 D8.0 Quenching Time (Quenchometer), ASTM D3520, Sec. (1) Quenchalyzer, ASTM D6200 Max. Cooling Rate, C/sec Temp. at Max. Cooling Rate, C Cooling Rate at 300 C, C/sec Time to reach 600 C, sec Time to reach 400 C, sec Time to reach 200 C, sec Note: (1) Test method ASTM D3520 is no longer available. Values shown are for historic reference only. CITGO and Quenchol are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

169 CITGO SLIDERITE OILS Date (Continued) 03/18 DESCRIPTION: CITGO SlideRite Oils are designed for use on slideways of machine tools. QUALITIES: CITGO SlideRite Oils contain special non-corrosive additives which provide the necessary qualities to protect against the occurrence of stick-slip. They impart good metal-wetting, adhesiveness, and EP characteristics which effectively eliminate chatter and scoring in the operation of machine tool ways. Some slideway lubricants tend to form an emulsion with coolants in machining centers, making it difficult to maintain clean and effective coolants. However, CITGO SlideRite Oils are specially designed to minimize this problem. As a result, these oils are particularly recommended for use in applications where synthetic coolants or soluble oil emulsions are used. CITGO SlideRite Oils are light colored, have a very mild odor, and provide good visibility of slideways. The ISO VG 32, ISO VG 68 and ISO VG 220 grades of CITGO SlideRite Oils have been formulated to meet requirements of the Fives Group (formerly Cincinnati Machine) specifications covering machine tool way lubricants. Grade Fives Cincinnati Specification CITGO SlideRite 32 P-53* CITGO SlideRite 68 P-47 CITGO SlideRite 220 P-50 Metalworking Fluids *NOTE: Fives Group Specification P-53 is a Combination Hydraulic and Way Oil Specification. APPLICATIONS: CITGO SlideRite 32 is suitable for use in central systems for lubricating hydraulic pump units and slideways and can be used where a premium grade light viscosity oil is needed. CITGO SlideRite 68 is suitable for use as a slideway lubricant where a heavy-medium viscosity oil is specified. CITGO SlideRite 220 and CITGO SlideRite 320 are suitable for use as a slideway lubricant where a heavy viscosity oil is specified. (Continued) C

170 CITGO SLIDERITE OILS Date 03/18 - (Continued) TYPICAL PROPERTIES: CITGO SLIDERITE OILS Grade Metalworking Fluids Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash Point, ASTM D92, F ( C), COC 392 (200) 428 (220) 455 (235) 482 (250) Viscosity, ASTM D445, cst at 40 C cst at 100 C ASTM D2161, SUS at 100 F SUS at 210 F Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -27 (-33) -17 (-27) +10 (-12) +10 (-12) Color, ASTM D1500 L1.5 L2.5 L2.5 L3.5 Texture Tacky Tacky Tacky Tacky Stick-Slip Coefficient Ratio, Max. (1) Gleittechnik Demulsibility Test Pass Pass Pass Pass ISO VG No Fives Group Specification P-53 P-47 P-50 Note: (1) Ratio of the coefficients of kinetic friction to static friction. CITGO and SlideRite are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

171 CITGO TUL-KUT OIL BASE CUTTING OIL CONCENTRATE Date 04/18 DESCRIPTION: CITGO Tul-Kut Oil Base is a special additive concentrate designed for fortifying cutting oils in the field. CITGO Tul-Kut Oil Base is designed without chlorine containing components to minimize any hazards to the environment. FEATURES: APPLICATIONS: Non-staining to yellow metals (copper and copper-containing alloys) Non-corrosive Good solubility in mineral oil base fluids Highly concentrated level of performance additive Long history of proven performance Non-chlorinated CITGO Tul-Kut Oil Base is used to refortify cutting oils. Generally, 3 to 5 percent of concentrate is sufficient. Higher concentrations can be used for extremely difficult machining operations. CITGO Tul-Kut Oil Base can be diluted with kerosene or low viscosity oils to compound products when customers prefer to do their own blending for honing and lapping. Metalworking Fluids TYPICAL PROPERTIES: CITGO TUL-KUT OIL BASE Material Code Gravity, ASTM D4052, API 12.0 Gravity, Specific, 60/60 F, ASTM D Density, lb/gal at 60 F 8.21 Flash Point, ASTM D92, F ( C) 400 (204) Viscosity, ASTM D445, cst at 40 C 370 cst at 100 C 40 Color, ASTM D1500 D8 (Dark) Pour Point, ASTM D97 equivalent, F ( C) 60 (16) Sulfur, ASTM D2622, w% 10.5 Copper Corrosion, ASTM D130 (3 hrs. at 212 F, 10% in 100 SUS at 100 F base oil) 2 CITGO and Tul-Kut are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

172 CITGO PACEMAKER 15SL GAS ENGINE OIL Date 03/18 DESCRIPTION: CITGO Pacemaker Gas Engine Oil 15SL SAE 15W-40 is a long life low ash stationary natural gas engine oil formulated with synthetic base stocks and an advanced additive system. It is specially formulated to provide lubrication in engines that have been converted to natural gas fuel, such as those in LP and agricultural irrigation pump service. Excellent oxidation and nitration resistance helps avoid sludge and oil thickening, which can plug oil filters and cause excessive foaming. QUALITIES: Compared with conventional engine oils, CITGO Pacemaker Gas Engine Oil 15SL SAE 15W-40 offers: Dramatically extended oil service life High shear stability Special additives designed to minimize slider follower wear Deposit control and wear protection of pistons, rings and liners Effective oxidation and nitration control Industrial Gas Engine Oils APPLICATIONS: CITGO Pacemaker Gas Engine Oil 15SL SAE 15W-40 is specially formulated to provide extended fluid life and engine lubrication in stationary engines converted to natural gas such as irrigation pump service and LP applications. TYPICAL PROPERTIES: CITGO PACEMAKER GAS ENGINE OIL 15SL SAE Grade 15W-40 Commodity Code Gravity, API, ASTM D Pounds per Gallon 7.22 Flash Point, COC, F ( C) 489 (254) Viscosity, ASTM D445, 40 C 107 Viscosity, ASTM D445, 100 C 15.1 Viscosity Index ASTM D Pour Point, F ( C), ASTM D97-60 (-51) Color, ASTM D1500 L6 Sulfated Ash, m%, ASTM D Total Base Number, ASTM D Zinc, ppm 900 CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

173 CITGO PACEMAKER 700 SERIES GAS ENGINE OIL Date 03/18 DESCRIPTION: CITGO Pacemaker Gas Engine Oil 700 Series oils are medium ash type oils formulated from high VI base stocks and select additives to provide excellent wear protection and deposit control in high speed, severe service engines. The additive package contains zinc for a high level of antiwear performance plus additional antioxidant for improved oxidation and nitration stability and resistance to thermal breakdown needed for long service life. QUALITIES: Provide excellent valve face and seat lubrication. Improved engine cleanliness and sludge control performance in heavy-duty, high temperature and continuous engine operation. Improved oxidation and nitration resistance. Better wear protection, especially in valve train, and better protection from ring and valve sticking. Higher TBN will offer greater protection against acid increase and corrosive wear which means longer oil life. APPLICATIONS: CITGO Pacemaker Gas Engine Oil 700 Series oils are recommended for naturally-aspirated to turbocharged, medium and high speed, high output four-cycle engines in field gathering service. They are also recommended for engines in cogeneration service, digester gas-fueled, dual-fueled (i.e. diesel/natural gas) and diesel-fueled service. CITGO Pacemaker Gas Engine Oil 700 Series oils are recommended for use in lean/clean burn engines. They are NOT recommended for engines equipped with catalytic converters. CITGO Pacemaker Gas Engine Oil 700 Series oils can also be used to lubricate the compressor cylinders in natural gas service. Industrial Gas Engine Oils (Continued) C

174 CITGO PACEMAKER 700 SERIES GAS ENGINE OIL Date 03/18 - (Continued) TYPICAL PROPERTIES: CITGO PACEMAKER GAS ENGINE OIL 700 SERIES Product Name SAE Grade 15W Material Code Industrial Gas Engine Oils Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, COC, ASTM D92, F ( C), Min. 460 (238) 453 (234) Viscosity, ASTM D445, cst at 040 C cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -27 (-33) +5 (-15) Color, ASTM D1500 L6.5 L6.5 Carbon Residue, % (base stock) Sulfated Ash, ASTM D874, m% Total Acid No., ASTM D Total Base No., ASTM D Phosphorus, m% Oxidation Inhibitor Yes Yes Corrosion Inhibitor Yes Yes Detergent-Dispersant Yes Yes Metal Deactivator Yes Yes Antiwear Yes Yes CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

175 CITGO PACEMAKER 800 SERIES GAS ENGINE OIL Date 04/18 DESCRIPTION: CITGO Pacemaker Gas Engine Oil 800 Series oils are low ash/low phosphorus stationary natural gas engine oils formulated to provide maximum resistance to oxidation, corrosion and foaming, and excellent antiwear performance. QUALITIES: APPLICATIONS: Premium high viscosity index base stocks with low carbon residue to minimize carbon and varnish formation and maximize oil oxidation life. Contain no bright stock. Promote reduced spark plug deposits. Contain special detergent-dispersant additive package for excellent cleaning action to keep piston rings free in their grooves, thereby extending engine overhaul periods and engine life. Offer excellent resistance to oil nitration. Contain low phosphorous level suitable for use with catalytic converter systems. Provide lower oil consumption and reduced maintenance costs. Are suitable for use in compressor cylinder lubrication. Provide excellent protection against corrosion of vital engine and compressor components. CITGO Pacemaker Gas Engine Oil 800 Series oils are recommended primarily for use in the lubrication of spark-ignited 4-cycle stationary natural gas engines and compressor cylinders. These oils are recommended for high and medium speed naturally aspirated and turbo charged 4-cycle stationary engines manufactured by Caterpillar, Waukesha, Superior, Cooper-Bessemer; Cummins, Dresser-Rand (Categories I, II and III), as well as low-speed engines manufactured by Cooper-Bessemer and Worthington C4-Cycle. Low ash level/low phosphorous formulation is suitable for use with catalyte converter systems. Industrial Gas Engine Oils (Continued) C

176 CITGO PACEMAKER 800 SERIES GAS ENGINE OIL Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO PACEMAKER GAS ENGINE OIL 800 SERIES Product Name SAE Grade 15W Material Code Industrial Gas Engine Oils Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, COC, ASTM D92, F ( C) 446 (230) 466 (241) 511 (266) Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445, cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -27 (-33) -27 (-33) +5 (-15) Color, ASTM D Carbon Residue, % (base stock) Sulfated Ash, ASTM D874, m% Total Acid No., ASTM D664, mg KOH/g Total Base No., ASTM D2896, mg KOH/g Phosphorus, ppm CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

177 CITGO PACEMAKER 1000 SERIES GAS ENGINE OIL Date 04/18 DESCRIPTION: CITGO Pacemaker Gas Engine Oil 1000 Series oils are ashless stationary natural gas engine lubricants fortified with an ashless dispersant, corrosion inhibitor, oxidation inhibitor and antiwear additive package. They are available in a single viscosity grade at the midpoint between SAE 30 and SAE 40 grades and an SAE 15W-40 grade. QUALITIES: APPLICATIONS: CITGO Pacemaker Gas Engine Oil 1000 Series Oils provide: Use of high viscosity index base stock with low carbon residue minimizes carbon and varnish formation and maximizes oil oxidation life Contain no bright stock Ashless formulation provides maximum protection against spark plug fouling Ashless dispersant system provides excellent cleaning action which keeps piston rings free in their grooves, thereby extending overhaul periods and engine life Excellent resistance to oil oxidation Superior corrosion protection to vital engine and compressor components Use in compressor cylinder lubrication Superior protection against ring belt and port deposits in 2-cycle engine designs CITGO Pacemaker Gas Engine Oil 1000 Series oils are applicable for use in a wide variety of 2- and 4-cycle gas engine designs. They meet the performance requirements for Dresser-Rand Categories I and II, as well as requirements for other gas engine manufacturers requiring ashless type engine oils. CITGO Pacemaker Gas Engine Oil 1035LP is specially formulated to provide enhanced low temperature properties. This low pour point product provides excellent cold temperature flow properties and is well suited where low temperature fluidity is needed but a monograde viscosity is preferred. Industrial Gas Engine Oils The CITGO Pacemaker Gas Engine Oil 1000 Series has a history of outstanding performance in gas processing, gas transmission and other applications calling for a high quality ashless natural gas engine oil. (Continued) C

178 CITGO PACEMAKER 1000 SERIES GAS ENGINE OIL Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO PACEMAKER GAS ENGINE OIL 1000 SERIES Product Name LP SAE Grade 15W-40 30/40 30/40 Material Code Industrial Gas Engine Oils Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, COC, ASTM D92, F ( C), Min. 471 (244) 543 (284) 460 (238) Fire Point, COC, ASTM D92, F ( C), Min. 514 (268) 563 (295) 563 (295) Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445, cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -22 (-30) +10 (-12) -27 (-33) Color, ASTM D1500 L2.0 L2.0 L1.5 Carbon Residue, % (base stock) Total Acid No., ASTM D664, mg KOH/g Total Base No., ASTM D2896, mg KOH/g Phosphorus, ppm Antiwear Yes Yes Yes Corrosion Inhibitor Yes Yes Yes Dispersant Yes Yes Yes Foam Suppressor Yes Yes Yes Oxidation Inhibitor Yes Yes Yes CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

179 CITGO PACEMAKER GAS ENGINE OIL 1200 SERIES Date 03/18 DESCRIPTION: CITGO Pacemaker Gas Engine Oil 1200 Series oils are premium quality, ashless stationary natural gas engine oils fortified with a latest generation dispersant additive package in combination with corrosion, oxidation and foam inhibitors, and a premium antiwear additive package. They provide excellent performance in 2-cycle engines and also provide superior service in many 4-cycle engines. QUALITIES: APPLICATIONS: The use of high viscosity index base stocks with low carbon residue minimizes carbon and varnish formation and serves to provide maximum oxidation resistance. Contain no bright stock. Provide superior protection against ring belt and port deposits in 2-cycle engines. Use ashless formulation minimizes spark plug fouling. Are highly dispersant, which provides excellent engine cleanliness. By keeping piston rings free in their grooves, extended engine overhaul periods and engine life can be achieved. Offer excellent resistance to oil nitration and oxidation. Promote lower oil consumption, fewer deposits and reduced maintenance costs. Provide superior corrosion protection to vital engine and compressor components. CITGO Pacemaker Gas Engine Oil 1200 Series oils provide superior antiwear protection, varnish and deposit control in naturally aspirated and turbocharged 2-cycle and 4-cycle gas engines. These products meet the performance characteristics required for Dresser-Rand Categories I and II gas engines as well as other 2- and 4-cycle units of major equipment manufacturers requiring ashless type oils. These premium qualities make CITGO Pacemaker Gas Engine Oil 1200 Series the best choice for universal ashless gas engine oils in a wide variety of low- and high-speed 2- and 4-cycle engines. Industrial Gas Engine Oils (Continued) C

180 CITGO PACEMAKER GAS ENGINE OIL 1200 SERIES Date 03/18 DESCRIPTION: CITGO Pacemaker Gas Engine Oil 1200 Series oils are premium quality, ashless stationary natural gas engine oils fortified with a latest generation dispersant additive package in combination with corrosion, oxidation and foam inhibitors, and a premium antiwear additive package. They provide excellent performance in 2-cycle engines and also provide superior service in many 4-cycle engines. Industrial Gas Engine Oils QUALITIES: APPLICATIONS: The use of high viscosity index base stocks with low carbon residue minimizes carbon and varnish formation and serves to provide maximum oxidation resistance. Contain no bright stock. Provide superior protection against ring belt and port deposits in 2-cycle engines. Use ashless formulation minimizes spark plug fouling. Are highly dispersant, which provides excellent engine cleanliness. By keeping piston rings free in their grooves, extended engine overhaul periods and engine life can be achieved. Offer excellent resistance to oil nitration and oxidation. Promote lower oil consumption, fewer deposits and reduced maintenance costs. Provide superior corrosion protection to vital engine and compressor components. CITGO Pacemaker Gas Engine Oil 1200 Series oils provide superior antiwear protection, varnish and deposit control in naturally aspirated and turbocharged 2-cycle and 4-cycle gas engines. These products meet the performance characteristics required for Dresser-Rand Categories I and II gas engines as well as other 2- and 4-cycle units of major equipment manufacturers requiring ashless type oils. These premium qualities make CITGO Pacemaker Gas Engine Oil 1200 Series the best choice for universal ashless gas engine oils in a wide variety of low- and high-speed 2- and 4-cycle engines. (Continued) C

181 CITGO PACEMAKER GAS ENGINE OIL 1600 SERIES Date 03/18 DESCRIPTION: CITGO Pacemaker Gas Engine Oil 1600 Series oils are superior low ash, low phosphorus stationary natural gas engine oils with a balanced advanced additive package. These new generation oils deliver a superior level of cleanliness with excellent wear protection with a low ash formula that complies with manufacturers warranties and non selective catalytic converter requirements. Formulated with the latest generation additives and highest quality base stocks available, CITGO Pacemaker Gas Engine Oil 1600 Series oils are unsurpassed in performance. QUALITIES: Contain special dispersants and detergents to help ensure a cleaner, longer running engine. Control deposits and minimize wear of pistons, rings, and liners. Retain TBN to neutralize combustion acids from sour gas. Effectively control oxidation and nitration which create sludge that thickens the oil, plugs filters and causes excessive foaming. Minimize valve recession to provide longer head life. APPLICATIONS: CITGO Pacemaker Gas Engine Oil 1600 Series oils are low ash oils suitable for a wide range of engines operating on virtually any variation of natural or synthetic gas, gas from digester or landfill sources or fuels containing low levels of sulfur and chloroflurocarbons (CFC). Note: In high CFC/sour gas applications, an oil with a higher base reserve may be required. These oils are recommended for high and medium speed 4-cycle engines manufactured by Caterpillar, Waukesha, Superior, Cooper-Bessemer; Cummins, Dresser-Rand (Categories I, II and III), as well as low-speed engines manufactured by Cooper-Bessemer and Worthington C4-Cycle. CITGO Pacemaker Gas Engine Oil 1640LP is a specially formulated SAE 40 grade product that exhibits superior low temperature properties, compared with other monograde oils. This low pour product is particularly well suited for applications where improved low temperature fluidity is needed, but a monograde oil is recommended by the engine manufacturer. Industrial Gas Engine Oils (Continued) C

182 CITGO PACEMAKER GAS ENGINE OIL 1600 SERIES Date 03/18 - (Continued) TYPICAL PROPERTIES: CITGO PACEMAKER GAS ENGINE OIL 1600 SERIES Product Name LP SAE Grade 15W Material Code Industrial Gas Engine Oils Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, COC, ASTM D92, F ( C) 446 (230) 466 (241) 511 (266) 511 (266) Viscosity, ASTM D445, cst at 40 C Viscosity, AST McSt at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -27 (-33) -27 (-33) +10 (-12) -33 (-36) Color, ASTM D1500 L5.0 L4.5 L4.5 L4.5 Carbon Residue, % (base stock) Sulfated Ash, ASTM D874, m% Total Base No., ASTM D2896, mg KOH/g Total Acid No., ASTM D664, mg KOH/g Phosphorous, ppm CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

183 CITGO PACEMAKER 1700 SERIES GAS ENGINE OIL Date 04/18 DESCRIPTION: CITGO Pacemaker Gas Engine Oil 1700 Series oils are superior new generation low ash, low phosphorus stationary natural gas engine oils with an advanced additive package that deliver a superior level of cleanliness and excellent wear protection with a low ash formula that complies with manufacturers warranties and non selective catalytic converter requirements. Formulated with latest generation additive technology and highest quality Group II base stocks. CITGO Pacemaker Gas Engine Oil 1700 Series oils offer outstanding performance. In CITGO rigorous field testing, these oils have shown superior protection against nitration and oxidation, plus resistance to viscosity increase for longer drain intervals. QUALITIES: APPLICATIONS: Contain special dispersants and detergents help ensure a cleaner, longer running engine. Control deposits and minimize wear of pistons, rings, and liners. Retain TBN to neutralize combustion acids from sour gas. Contain specialized antioxidant/base oil combination effectively inhibits oxidation and nitration in severe service. Control sludge that thickens the oil, plugs filters and causes excessive foaming. Minimize valve recession to provide longer head life. CITGO Pacemaker Gas Engine Oil 1700 Series oils are low ash oils suitable for a wide range of engines operating on virtually any variation of natural or synthetic gas, gas from digester or landfill sources or fuels containing low levels of sulfur and chloroflurocarbons (CFC). Note: In high CFC/sour gas applications, an oil with a higher base reserve may be required. These oils are recommended for high and medium speed 4-cycle engines manufactured by Caterpillar, Waukesha, Superior, Cooper-Bessemer, Cummins, Dresser-Rand (Categories I, II and III), as well as low-speed engines manufactured by Cooper Bessemer and Worthington C4-Cycle). CITGO Pacemaker Gas Engine Oil 1740LP is a specially formulated SAE 40 grade product that exhibits superior low temperature properties, compared with other monograde oils. This low pour product is particularly well suited for applications where improved low temperature fluidity is needed, but a monograde oil is recommended by the engine manufacturer. Industrial Gas Engine Oils (Continued) C

184 CITGO PACEMAKER 1700 SERIES GAS ENGINE OIL Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO PACEMAKER GAS ENGINE OIL 1700 SERIES Product Name LP SAE Grade 15W Material Code Industrial Gas Engine Oils Gravity, ASTM D4052, API Pounds Per Gallon Flash Point, COC, ASTM D92, F ( C) 446 (230) 466 (241) 473 (245) 480 (249) Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445, cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -22 (-30) -16 (-27) +10 (-12) -26 (-33) Color, ASTM D1500 L6.0 L5.0 L5.0 L5.0 Carbon Residue, % (base stock) Sulfated Ash, ASTM D874, m% Total Base No., ASTM D2896, mg KOH/g Total Acid No., ASTM D664, mg KOH/g Phosphorous, ppm CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

185 CITGO PACEMAKER GAS ENGINE OIL 1900 XL SERIES Date 04/18 DESCRIPTION: CITGO Pacemaker Gas Engine Oil (GEO) 1900 XL series are next-generation, premium-performance low ash and low phosphorus lubricants for stoichiometric and lean-burn stationary natural gas engines. CITGO Pacemaker GEO 1900 XL series are designed for highly loaded 4-cycle natural gas engines operating under severe conditions and provides premium performance over older technology lubricants in high nitration conditions typically found in stoichiometric engine operation. QUALITIES: APPLICATIONS: Exceptional resistance to oxidation and nitration Extended oil drain intervals capability (up to two times vs. other premium oils operating in severe conditions) helps maximize production and lowers operating cost through less down time, and reduced lubrication cost Exceptional deposit control and protection against piston scuffing and ring and liner wear TBN retention to neutralize combustion acids from sour gas Minimized valve recession for longer head life Improved TAN control Catalyst compatible CITGO Pacemaker GEO 1900 XL series low ash lubricants meet rigorous demands of modern natural gas engines operating in a variety of natural gas fuel qualities. Recommended for high and medium speed 4-cycle engines manufactured by: Caterpillar Worthington (low-speed engines) Waukesha Cooper-Bessemer (low-speed engines) Superior Cummins Jenbacher Dresser-Rand (Categories I, II, III) Wärtsilä Industrial Gas Engine Oils (Continued) C

186 CITGO PACEMAKER GAS ENGINE OIL 1900 XL SERIES Date 04/18 - (Continued) Proven in Severe Service Caterpillar 300 Series and Waukesha VHP Series stoichiometric engines are historically severe in nitration. In field operation, results show CITGO Pacemaker GEO 1940 XL delivered up to 200% longer engine oil life compared to other premium oils. Nitration - Hours to OEM Limit Caterpillar 300 Series Oxidation - Hours to OEM Limit Caterpillar 300 Series Industrial Gas Engine Oils Premium Oil C Pacemaker GEO 1940 XL Nitration - Hours to OEM Limit Waukesha VHP Series Premium Oil C Caterpillar 300 Series Stoichiometric Engines Pacemaker GEO 1940 XL Oxidation - Hours to OEM Limit Waukesha VHP Series Premium Oil A Premium Oil B Pacemaker GEO 1940 XL 0 Premium Oil A Premium Oil B Pacemaker GEO 1940 XL Waukesha VHP Series Stoichiometric Engines (Continued) C

187 CITGO PACEMAKER GAS ENGINE OIL 1900 XL SERIES Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO PACEMAKER GAS ENGINE OIL 1900 XL SERIES Product Name 1930 XL 1940 XL SAE Grade Material Code Gravity, ASTM D4052, API Pounds Per Gallon Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445, cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -33 (-36) -33 (-36) Color, ASTM D1500 L5.0 L5.0 Sulfated Ash, ASTM D874, m% Total Base No., ASTM D2896, mg KOH/g Total Acid No., ASTM D664, mg KOH/g Phosphorus, ppm CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Industrial Gas Engine Oils C

188 CITGO PACEMAKER GAS ENGINE OIL LFG LA 40 Date 03/18 DESCRIPTION: QUALITIES: APPLICATIONS & APPROVALS: CITGO Pacemaker Gas Engine Oil LFG LA 40 is a superior low ash, low phosphorus gas engine oil, designed for high output, 4-cycle natural gas engines operating on landfill and digester gas. As demonstrated in field service, this premium low ash package can significantly extend oil drain intervals, while minimizing the negative effects of ash deposits on sensitive engine components. Specifically designed for high BMEP engines Low ash formula minimizes combustion chamber deposits Specially formulated with modern chemistry to neutralize combustion acids from landfill gas and digester gas Controls deposits and minimizes wear of pistons, rings and liners CITGO Pacemaker Gas Engine Oil LFG LA 40 is recommended for a wide range of engines that operate on landfill and digester gas, including engines manufactured by Caterpillar, Waukesha, GE Jenbacher, Deutz and Cummins. CITGO Pacemaker Gas Engine Oil LFG LA 40 has been approved by GE Jenbacher for use in type 2, 3, 4 and 6 engines (fuel classes B and C) and appears in their Technical Instruction TA Industrial Gas Engine Oils BENEFITS: Optimized ash content helps control combustion chamber deposits to maintain the power output of high BMEP engines for reduced maintenance and longer engine life. Exceptional piston, ring and liner wear control Significantly extends drain intervals Excellent base retention Strong corrosion resistance Neutralizes acidic components such as Total Organic Halide as Chloride (TOHCI) and H2S at moderate levels. TYPICAL PROPERTIES: CITGO PACEMAKER GAS ENGINE OIL LFG LA 40 SAE Grade 40 Material Code Gravity, ASTM D4052, API 29.3 Density, lb/gal at 60 F 7.33 Flash Point, ASTM D92, COC, F ( C) 525 (274) Viscosity, ASTM D445, cst at 40 C 123 Viscosity, cst at 100 C 13.5 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -11 (-24) Color, ASTM D1500 L5.0 Carbon Residue, % (base stock) 0.02 Sulfated Ash, ASTM D874, % 0.55 Total Base No., ASTM D2896, mg KOH/g 5 Total Acid No., ASTM D664, mg KOH/g 1.16 CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

189 CITGO RAILROAD CAR JOURNAL OIL NO. 9 Date 04/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Railroad Car Journal Oil No. 9 is a quality lubricating oil designed specially for use as a railroad car journal oil to cover a wide range of service requirements. Rust Protection It guards against rust and corrosion under adverse conditions, especially when cars are idle. Low Pour Point, High Viscosity Index This oil flows freely at very low temperatures, yet provides effective lubrication in high temperature service. CITGO Railroad Car Journal Oil No. 9 conforms to the requirements of AAR Specification M for All-Year Journal Box Lubricating Oil. It is designed for the lubrication of locomotive and railroad car journal bearings. TYPICAL PROPERTIES: CITGO RAILROAD CAR JOURNAL OIL NO. 9 Material Code Gravity, ASTM D4052, API 30.3 Density, lb/gal at 60 F 7.28 Flash Point, COC, ASTM D92, F ( C) 442 (228) Viscosity, ASTM D445, cst at 40 C 64 cst at 100 C 8.8 ASTM D2161, SUS at 100 F 354 SUS at 210 F 58 Viscosity Index, ASTM D Pour Point, Max, ASTM D97, F ( C) -22 (-30) Color, ASTM D1500 L1.0 CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Railroad Lubricants (Continued) C

190 CITGO RD-969 AND RD-1069 DIESEL ENGINE OILS Date 04/18 DESCRIPTION: CITGO RD-969 and RD-1069 are high dispersancy, reduced ash engine oils intended for use in railroad locomotive diesel engines and other medium-speed stationary and marine diesel engines of similar design. They meet the LMOA Generation 6 (GE Generation IV Long Life) quality requirements. The Oronite OLOA additive system is utilized. QUALITIES: Improved detergent/dispersent dramatically improves cleanliness Superior oxidation and thermal stability inhibition prevents excessive viscosity increase 9 TBN designed for low and ultra- low sulfur fuels Non-zinc formulation to protect silver bearing materials Non-chlorinated to reduce used oil recycling costs High viscosity index base in both oils for: better oxidation resistance good low-temperature performance Outstanding protection from deposits Maximum oil drain intervals Enhanced particulate matter emissions control PERFORMANCE CAPABILITIES: LMOA Generation 6 EMD approved for Pointers Listing GE Generation IV Long Life Railroad Lubricants APPLICATIONS: These oils meet the specifications of the major railroad diesel engine builders including General Electric and Electro-Motive Division (EMD) of General Motors Corporation. They also meet the requirements of the manufacturers of many large medium-speed diesel engines used in marine and stationary service. They provide superior lubrication of most diesel engines used in inland marine service in towboats and work boats. General Electric diesel EMD diesel ALCO diesel Enterprise diesel Fairbanks-Morse diesel Superior diesel Colt Pielstick Sulzer diesel Baldwin-Lima-Hamilton (Continued) C

191 CITGO RD-969 AND RD-1069 DIESEL ENGINE OILS Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO RD-969 AND RD-1069 DIESEL ENGINE OILS Product RD-969 RD-1069 SAE Grade 40 20W-40 Material Code Gravity, ASTM D4052, API Gravity, ASTM D1298, Specific 60/60 F Density, lbs./gallon Flash Point, ASTM D92, COC, F ( C) 518 (270) 482 (250) Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445, cst at 100 C Viscosity Index, ASTM D Visc ASTM D5293, CCS, cp at -15 C - 6,800 Pour Point, ASTM D97, F ( C) 0 (-18) -11 (-24) Color, ASTM D1500 D8 D8 Sulfated Ash, ASTM D874, m% Total Acid No., ASTM D664, mg KOH/g Total Base No., ASTM D2896, mg KOH/g Zinc, ppm <10 <10 Chlorine, ppm <50 <50 CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Railroad Lubricants C

192 CITGO RD-2069 LE DIESEL ENGINE OIL Date 04/18 DESCRIPTION: CITGO RD-2069 LE Diesel Engine Oil is a new generation railroad diesel engine oil that supports the EPA Tier 4 emissions requirements and is performance engineered for use in railroad locomotive diesel engines and other medium-speed stationary and marine diesel engines of similar design. CITGO RD-2069 LE Diesel Engine Oil is approved for LMOA Generation 7 (supersedes the performance requirements of LMOA Generation 6). The CITGO RD-2069 LE Diesel Engine Oil utilizes the Oronite OLOA additive system. QUALITIES: Improved detergent/dispersent dramatically improves cleanliness Superior oxidation and nitration thermal stability inhibition prevents excessive viscosity increase 11 TBN designed for low and ultra-low sulfur fuels Non-zinc formulation to protect silver bearing materials Non-chlorinated to reduce used oil recycling costs High viscosity index base in oil provides: better oxidation resistance good low-temperature performance Outstanding protection from deposits Maximum oil drain intervals Enhanced particulate matter emissions control Improved fuel economy versus single grade engines oils Better start up cold temperature lubrication versus single grade engine oils PERFORMANCE CAPABILITIES: LMOA Generation 7 (Supersedes LMOA Generation 6) Railroad Lubricants APPLICATIONS: CITGO RD-2069 LE Diesel Engine Oil meets the performance for General Electric Transportation (GE) for Tier 4 locomotives and older models as well as Electro-Motive Division (EMD) Tier 3 locomotives and older models. This oil is formulated with the latest generation of additive technology advancements with a proven track record of providing superior lubrication in a variety of diesel engines used in coastal and inland marine service. Consult owner s manual for proper lubricant selection. (Continued) C

193 CITGO RD-2069 LE DIESEL ENGINE OIL Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO RD-2069 LE DIESEL ENGINE OIL SAE Grade 20W-40 Material Code Gravity, ASTM D4052, API 28.7 Gravity, ASTM D1298, Specific 60/60 F Density, lbs/gallon 7.34 Flash Point, ASTM D92, COC, F ( C) 496 (258) Viscosity, ASTM D445, cst at 40 C 140 cst at 100 C 15.2 Viscosity Index, ASTM D ASTM D5293, CCS, cp at -15 C 7,800 Pour Point, ASTM D97, F ( C) -27 (-33) Color, ASTM D1500 L4.5 Sulfated Ash, ASTM D874, m% 1.15 Total Acid No., ASTM D664, mg KOH/g 0.7 Total Base No., ASTM D2896, mg KOH/g 11 Zinc, ppm <10 Chlorine, ppm <50 CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. Railroad Lubricants C

194 CITGO DIAMOND OILS Date 04/18 DESCRIPTION: CITGO Diamond Oils are low viscosity, light color, low fluid-friction lubricants, designed primarily for use in machinery in the textile industry. The properties of these oils also make them suitable for a number of other applications. QUALITIES: APPLICATIONS: CITGO Diamond Oils provide lubrication and low fluid-friction loss required for excellent performance in high-speed spindle bearings and are compatible with all types of filtration systems. Their superior oxidation stability under moderate temperature conditions and excellent water separation capability make them outstanding machine oils for use where lubrication and temperature conditions are mild. CITGO Diamond Oils are recommended for general machinery lubrication, for knitting machinery needle heads, textile machinery spindles and twister rings, sewing machines and small electric motors. They can be used in all types of dispensing systems including centralized mist and air-line lubricators. TYPICAL PROPERTIES: CITGO DIAMOND OILS ISO Vis Grade Material Code Gravity, ASTM D4052, API Flash Point, ASTM D92, C Viscosity, ASTM D445, cst at 40 C Pour Point, ASTM D97, F ( C) -35 (-32) 15 (-9) Color, ASTM D1500 L0.5 L1.5 Water Separation time, ASTM D1401, Minutes at 130 F CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Functional Products C

195 CITGO HYDRAULIC/PRESS OIL 68 Date 04/18 DESCRIPTION: BENEFITS: APPLICATIONS: CITGO Hydraulic/Press Oil 68 is formulated with highly refined, premium base oils and an ashless antiwear additive system to provide outstanding protection for demanding printing press hydraulic systems. CITGO Hydraulic/Press Oil 68 does not rely on zinc-type antiwear additives which is an important consideration in various press applications. CITGO Hydraulic/Press Oil 68: Contains no heavy metals such as zinc Offers thermal stability to virtually eliminate heat-related sludge deposits Provides rust and corrosion protection Separates readily from water Contains inhibitors to minimize foaming and air entrainment Provides antiwear protection to pumps, motors and other hydraulic circuit components Extends fluid service life with a balanced additive system to handle severe operating conditions Contains an anti-leak agent to aid in maintaining the condition and life of elastomer materials Offers great compatibility with CITGO Press Oil 68 CITGO Hydraulic/Press Oil 68 is recommended for printing press service in vane, piston and gear pumps when used in accordance with the manufacturers recommendations. CITGO Hydraulic/Press Oil 68 is within the viscosity range covered in Goss SBM 5078 for gear and bearing lubricants. Use of Hydraulic/Press Oil 68 assures unintended mixing will not result in viscosity degradation of the lubricant covered by Goss SMB TYPICAL PROPERTIES: CITGO HYDRAULIC/PRESS OIL 68 Grade 68 Material Code Gravity, ASTM D4052, API 29.3 Density, lb/gal 7.33 Flash Point, (COC), ASTM D92, F ( C) 468 (242) Viscosity, ASTM D445, cst at 40 C 67.6 Viscosity, ASTM D 445,cSt at 100 C 8.5 Vscosy,ASTM D2161, SUS at 100 F 351 Vscosy ASTM D 2161,SUS at 210 F 55 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -11 (-24) Color, ASTM D1500 L1.5 Total Acid No., ASTM D664, mg KOH/g 0.10 Copper Corrosion, 3 hr at 100 C, ASTM D130 1A Rust Test, ASTM D665 A, B Pass Four Ball Wear, ASTM D2266, at 40 kg, mm 0.50 Foam Test, Seq. I, ml 0-0 Foam Test, Seq. II, ml 20-0 Foam Test, Seq. III, ml 0-0 Water Separability, at 130 F, ASTM D1401 (ml-ml-ml) CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C10082 Functional Products 187

196 CITGO PRESS OIL 68 Date (Continued) 04/18 DESCRIPTION: CITGO Press Oil 68 is formulated with premium, highly refined base oils, a unique selection of performance additives, and synthetic components to meet the demanding gear and bearing lubrication requirements found in printing press systems. BENEFITS: Provides extreme pressure and antiwear protection on gears and bearings. Exhibits outstanding thermal and oxidative stability. Provides rust and corrosion protection. Prevents sticking of eccentrics. Offers increased gear protection against shock loading and wear. Contains inhibitors to minimize foaming and air entrainment. Provides excellent adhesion and cohesion on metal parts. Extends fluid service life with a balanced additive system to handle severe press operating conditions. Contains no heavy metals. Offers improved viscosity control, minimum viscosity shear. APPLICATIONS: CITGO Press Oil 68 is recommended for service for high speed gearing and bearing applications found in the printing industry. CITGO Press Oil 68 exceeds the performance requirements of Goss SBM 5078 and Man Roland Presses. TYPICAL PROPERTIES: CITGO PRESS OIL 68 Grade 68 Material Code Functional Products Gravity, ASTM D4052, API 29.2 Density, lb/gal 7.33 Flash Point, (COC), ASTM D92, F ( C) 439 (226) Viscosity, ASTM D445, cst at 40 C 68.1 Viscosity, ASTM D 445, cst at100 C Vscos ASTM D2161, SUS at 100 F 320 Vscos ASTM D 2161, SUS at210 F 62 Viscosity Index ASTM D Pour Point, ASTM D97, F ( C) -27 (-33) Color, ASTM D1500 L2.5 Copper Corrosion, 3 hr at 100 C, ASTM D130 1A Rust Test, D665 A, B Pass Four Ball Wear at ASTM D4172, 40 kg, mm 0.36 Four Ball Wear Index, ASTM D Four Ball Wear, Index (Weld Point), Kg 250 Timken OK Load, ASTM D2782, lb. 50 Foam Test, Seq. I, ml 0-0 Seq. II, ml 50-0 Seq. III, ml 0-0 Tackifier Yes CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

197 CITGO HYTHERM OIL 46 Date 04/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Hytherm Oil 46 is a premium quality heat transfer oil formulated with high viscosity index paraffinic base stocks and a special high temperature detergent/dispersant additive package. CITGO Hytherm Oil 46 provides high specific heat and good thermal conductivity at all temperatures for highly efficient heat transfer. CITGO Hytherm Oil 46 contains rust and oxidation inhibitors and a special additive package to help maintain system cleanliness and operational performance, reducing downtime and maintenance costs. CITGO Hytherm Oil 46 meets the exacting requirements of both open and closed heat transfer systems, at temperatures up to 600 F. CITGO HYTHERM OIL 46 PHYSICAL DATA Specific Thermal Specific Heat Conductivity Viscosity Temp., F Gravity BTU/lb/ F BTU/hr/ft 2 / F cst TYPICAL PROPERTIES: CITGO HYTHERM OIL 46 ISO VIS Grade (SAE Grade) 46 Material Code Gravity, ASTM D4052, API 31.5 Density, lb/gal at 60 F 7.25 Flash Point, ASTM D92, F 453 Viscosity, ASTM D445, cst, at 40 C 48.5 cst, at 100 F 7.0 Viscosity Index, ASTM D Pour Point, ASTM D97, F 16 Color, ASTM D Acid No., ASTM D974 <0.01 Volume Factor, % per F Distillation, F, ASTM D2887, IBP, F 650 5% % % % 944 CITGO and Hytherm are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C10083 Functional Products 189

198 CITGO ICE MACHINE OIL 68 Date 04/18 DESCRIPTION: BENEFITS: APPLICATIONS: CITGO Ice Machine Oil 68 is a highly refined, pour depressed, paraffinic oil developed especially to lubricate ammonia compressors in industrial refrigeration systems. Demulsibility properties provide quick and complete separation of lubricant from water or refrigerant Foam inhibited with non-silicon additive Helps protect against formation of harmful deposits on exhaust ports and other compressor parts Protects bearings and other metal surfaces from corrosion Minimizes formation of sludge and varnish build-up CITGO Ice Machine Oil 68 is designed primarily for the complete lubrication of industrial type evaporating ice machines and crankcases, cylinders and bearings of refrigeration compressors using ammonia refrigerant. Meets requirements of Frick Co. Refrigeration Oil #3. In addition to its use in refrigeration compressors, CITGO Ice Machine Oil 68 is recommended for general oiling of bearings, open chains and linkages operating under conditions of mild unit loading and mild temperatures and humidity, where an additive type oil is not required. TYPICAL PROPERTIES: CITGO ICE MACHINE OIL 68 Material Code Gravity, ASTM D4052, API 31.0 Flash Point, ASTM D92, F ( C) 425 (218) Viscosity, ASTM D2161, SUS at 100 F 350 Viscosity, ASTM D445, cst at 40 C 68 Pour Point, ASTM D97, F ( C) -30 (-34) Color ASTM D CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Functional Products C

199 CITGO NORTH STAR REFRIGERATION OILS Date 04/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO North Star Refrigeration Oils are premium quality naphthenic oils, blended for use in refrigeration compressors. Special properties provide excellent refrigeration compressor lubrication including: Light color Low acid number Low pour and floc points Excellent foam resistance Good seal control Control stability and compatibility with refrigerants CITGO North Star Refrigeration Oils are recommended for use in refrigeration compressors and other low-temperature applications, including air conditioning systems. They are recommended for other extremely low temperature applications requiring low temperature fluidity and floc points of -50F or lower. Not recommended for use with hydrofluorocarbons (HFC) such as R-134A. TYPICAL PROPERTIES: CITGO NORTH STAR REFRIGERATION OILS GRADE Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash Point, ASTM D92, F ( C), COC 370 (188) 392 (200) Viscosity, ASTM D445, cst at 40 C cst at 100 C ASTM D2161, SUS at 100 F SUS at 210 F Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -44 (-42) -49 (-45) Floc Point, F ( C) -62 (-52) -56 (-49) Color, ASTM D1500 L1.0 L1.5 Aniline Point, ASTM D611, F ( C) 178 (81) 181 (83) Neutralization No., ASTM D Foam Inhibitor Yes Yes Foam, ASTM D892, Sequence I Sequence II Sequence III CITGO and North Star are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C10085 Functional Products 191

200 CITGO NORTH STAR REFRIGERATION OIL 68 Date 04/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO North Star Refrigeration Oil 68 is a lubricant designed for use in refrigeration compressors. Special properties to provide good refrigeration compressor lubrication include: Very light color Very low acid number Low pour and floc points Excellent foam resistance Good seal conditioning Control stability and compatibility with refrigerants CITGO North Star Refrigeration Oil 68 is recommended for use in refrigeration compressors and other low-temperature applications, including air conditioning systems. It is recommended for extremely low temperature applications requiring low floc points. Not recommended for use with hydrofluorocarbons (HFC) such as R-134A. TYPICAL PROPERTIES: CITGO NORTH STAR REFRIGERATION OIL 68 GRADE 68 Material Code Gravity, ASTM D4052, API 28.8 Density, lb/gal at 60 F 7.36 Flash Point, ASTM D92, F ( C), COC 405 (207) Viscosity, ASTM D445, cst at 40 C 65 cst at 100 C 8.3 ASTM D2161, SUS at 100 F 335 SUS at 210 F 54 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -42 (-44) Color, ASTM D1500 L0.5 Neutralization No., ASTM D Foam Inhibitor Yes Foam, ASTM D892, Sequence I 10-0 Sequence II 10-0 Sequence III 10-0 CITGO and North Star are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Functional Products C

201 CITGO BAR & CHAIN OIL Date 03/18 DESCRIPTION: CITGO Bar & Chain Oil is a suitable choice for home and commercial users. It contains components to reduce wear, guard against rust and enhance metal adhesion to reduce spatter. Designed for use over a wide temperature range. BENEFITS: Lubricates and Cools Chain and Bar Formulated to Reduce Spatter Guards Against Rust Provides Wear Protection NOTE: NOT FOR USE IN ENGINES! TYPICAL PROPERTIES: CITGO BAR & CHAIN OIL Material Code SAE Grade >20 Gravity, ASTM D4052, API 28 Pounds/Gallon at 60 F 7.3 Flash Point, ASTM D92, COC, F ( C) 284 (140) Pour Point, ASTM D97, F ( C) -29 (-20) Viscosity ASTM D445 cst at 40 C 68 cst at 100 C, 9.5 Appearance Dark Amber CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C10227 Functional Products 193

202 CITGO CONCRETE FORM OIL Date 04/18 DESCRIPTION:CITGO Concrete Form Oil is a light colored, non-staining, low volatile organic content (VOC) oil for use on concrete forms where an excellent surface finish is desired. QUALITIES: APPLICATIONS: CITGO Concrete Form Oil is specially formulated with high quality base stocks and additives including a combination spreading and release agent which: Provides excellent surface finish. Provides even spreading of the oil on wood or steel forms and prevent cement sticking to forms. Prevents staining, build-up and corrosion of forms. Meets U. S. EPA AIM and OTC Phase I State VOC requirements. CITGO Concrete Form Oil may be used for all concrete form applications. With excellent nonstaining characteristics, it is recommended for applications requiring excellent surface finish including production of burial vaults, white stone furniture and other specialty concrete products. Meets EPA AIM VOC Requirements VOC EPA Method 24 TYPICAL PROPERTIES: US EPA AIM VOC Limit OTC Phase I State Limit CITGO Form Oil CITGO CONCRETE FORM OIL Material Code Functional Products Gravity, ASTM D4052, API 27 Density, lb/gal at 60 F 7.43 Flash Point, COC, Min., ASTM D92, F ( C) 384 (196) Viscosity, ASTM D445, cst at 040 C 20 Viscosity, ASTM D 445,cSt at 100 C 3.8 Vscost ASTM D2161, SUS at 100 F 106 Vscost ASTM D 2161,SUS at 210 F 39 Viscosity Index, ASTM D Pour Point, Max, ASTM D97, F ( C) -33 (-36) Color, ASTM D Saponification No., ASTM D Copper Corrosion, ASTM D130 1A CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

203 CITGO SATISOL CONCRETE FORM RELEASE Date 04/18 DESCRIPTION: CITGO SATISOL Concrete Form Release is a high performance water emulsifiable, concrete form release agent. SATISOL meets Federal and State Regulations for VOC release. QUALITIES: CITGO SATISOL provides: Less Environmental Impact Reduces Spalling, Bug Holes, Voids Minimizes Form Cleaning and Maintenance Non-Staining Increased Form Life Non-Corrosive U.S. EPA AIM and OTC Phase I State VOC requirement APPLICATIONS: CITGO SATISOL is designed to be stable in both hard and soft water; as such, no special water is needed to make the working solution. The concentrate is designed to be used at a treat rate of 4 to 1 (water/oil); exceptional results have been obtained at this treat rate. The concentrate must be adequately mixed to insure proper thickening and performance. Do not allow material to freeze. Mixing Instructions: The Satisol Concentrate should always be added to the water and mixed thoroughly to insure proper emulsion formation. TYPICAL PROPERTIES: CITGO SATISOL CONCRETE FORM RELEASE Material Code Specific Gravity, ASTM D4052, at 60 F Density lbs/gal 7.70 Color Dark Amber Appearance Slight Haze Viscosity, ASTM D445, cst at 40 C 33.5 SUS at 100 F 158 Pour Point ASTM D97 (Neat), F ( C) -60 (-51) Flash Point ASTM D92 (Neat), F ( C), 323 (162) Copper Corrosion ASTM D130, 25% Solution 1A Rust Test, ASTM D665A, 25% Solution Pass Volatile Organic Compounds ASTM D2369, Neat Solution 14% Volatile Organic Compounds, Grams/Liter, Neat Solution 130 Freeze Pt. (25% solution) F ( C) 30 (-1) CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C10141 Functional Products 195

204 CITGO ROCK DRILL OILS Date 04/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Rock Drill Oils are premium lubricants designed for protection of pneumatic equipment subjected to excessive moisture or water spray. CITGO Rock Drill Oils work to ensure outstanding equipment protection by providing: Excellent metal wetting (preferential to water) and extra adhesiveness for more effective lubrication. Extreme Pressure (EP) wear protection, optimized with emulsification properties, guards against wear in high moisture conditions. Premium rust and corrosion protection and antifoam properties. High viscosity index, low pour point temperature and excellent stability enhance lubrication of pneumatic equipment over a wide range of conditions. CITGO Rock Drill Oils meet the general requirements of major manufacturers of rock drills, jack hammers, and other types of pneumatic percussion equipment manufactured by Ingersoll-Rand, Gardner-Denver, Mincon, and others. TYPICAL PROPERTIES: CITGO ROCK DRILL OILS ISO Grade Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash Point, ASTM D92, F ( C) 410 (210) 486 (252) 504 (262) Viscosity, cst at 040 C Viscosity, cst at 100 C Viscosity Index Pour Point, ASTM D97, F ( C) -17 (-27) -11 (-24) 10 (-12) Copper Corrosion, ASTM D 130 1A 1A 1A Timken EP Test, ASTM D2782, lbs. >65 >65 >65 Falex Load Test, ASTM D3233, ft-lbs. >2000 >2000 >2000 Steam Emulsion Number, seconds >1200 >1200 >1200 CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Functional Products C

205 CITGO WIRELINE LUBRICANTS Date 04/18 DESCRIPTION: QUALITIES: APPLICATIONS: CITGO Wireline Lubricants are premium viscous, tacky lubricants and sealants designed specifically for use in in oil and gas well logging operations and other wireline applications where a lubricating dynamic seal is required. Formulated with advanced corrosion inhibitors to protect against corrosion in harsh high pressure down-hole environments where exposure to moisture, H2S, and corrosive fluids occur. CITGO Wireline Lubricants are available in several viscosity grades for ease of application in varying temperature conditions. CITGO Wireline Lubricants offer: Excellent sealing capability Excellent adhesion to prevent sling off, splatter and drip Outstanding corrosion protection Ease of application Excellent low temperature performance CITGO Wireline Lubricants are recommended as a lubricant/sealant for braided wirelines, cables and slicklines used in down-hole operations including oil and gas well logging, pipe recovery, and reservoir analyses. TYPICAL PROPERTIES: CITGO WIRELINE LUBRICANTS Material Number Grade Specific Gravity, 60 F Pounds per Gallon Color Appearance Light Amber Amber Amber Amber Amber Flash Point, C ( F) 170 (340) 204 (400) 227 (440) 227 (440) 230 (446) Viscosity 40 C , C Pour Point, C ( F) -33 (-27) -18 (0) -15 (5) -18 (0) -21 (-6) Rust Test, D-665B Pass Pass Pass Pass Pass Texture Tacky Liquid Tacky Liquid Tacky Liquid Tacky Liquid Tacky Liquid Material Number Grade Specific Gravity, 60 F Pounds per Gallon Color L0.5 Appearance Amber Amber Amber Amber Flash Point, C ( F) 230 (446) 189 (373) 230 (446) 174 (345) Viscosity 40 C 5,000 7,500 9, C Pour Point, C ( F) -24 (-11) -28 (-18) -21 (-6) -18 (0) Rust Test, D-665B Pass Pass Pass Pass Texture Tacky Liquid Tacky Liquid Tacky Liquid Tacky Liquid NOTE: These products are NOT designed to be used as wire rope lubricants on draglines, cranes, elevators, shovels, drilling rigs, suspension bridges, or cable stayed bridges. CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C10208 Functional Products 197

206 Compressor Lubricants CITGO COMPKLEEN SYNTHETIC CLEANER Date 04/18 DESCRIPTION: CITGO CompKleen Synthetic Cleaner is a high performance cleaner designed to loosen, remove, and suspend the varnish, sludge, and carbon typically found in rotary screw and rotary vane compressors. These deposits can result in operational problems plus increased maintenance and operational cost. BENEFITS: CITGO CompKleen Synthetic Cleaner is designed for use as a supplemental lubricant additive to remove sludge, varnish, and carbon from the compressor system while in operation. Using CITGO CompKleen Synthetic Cleaner virtually eliminates the need for disassembling for cleaning. For maximum benefit, use CITGO CompKleen Synthetic Cleaner prior to each lubricant change. USAGE DIRECTIONS: Add one gallon of CITGO CompKleen Synthetic Cleaner concentrate for every 10 gallons of compressor oil in the unit; drain enough oil from the system unit to allow for the addition of the concentrate. Continue to operate the compressor for 40 to 60 hours, allowing the treated oil to circulate through the system to loosen, dissolve and suspend the deposits. It is very important that the fluid be drained from the system while hot to avoid re-depositing the contaminants. After draining the fluid, replace the filters and refill with the proper CITGO lubricant. Flushing the system before refilling may be necessary if the deposits were especially heavy. CITGO CompKleen can also be used to clean and remove deposits from hydraulic systems, gear boxes, heat transfer systems, and machine tools. NOTE: It is the user s responsibility to follow instructions, and ensure proper and complete drainage. Product sampling and testing are highly recommended. For additional technical information and assistance, please contact the CITGO Lubricants Product Answer Line at or TYPICAL PROPERTIES: CITGO COMPKLEEN SYNTHETIC CLEANER Material Code API Gravity, ASTM D4052, API 12.2 Density lb/gal 8.20 Color ASTM, D Viscosity, ASTM D445, cst at 40 C 66 cst at 100 C 7.3 Flash Point PM ASTM D93, F ( C) 410 (210) CITGO and CompKleen are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

207 CITGO COMPRESSOR OILS 35LP AND 45LP Date 04/18 DESCRIPTION: CITGO Compressor Oils 35LP and 45LP are high-quality non-foaming, non-detergent compressor cylinder lubricants engineered for the requirements of air and gas compressors and older stationary natural gas engines that utilize activated clay filtration. CITGO Compressor Oils 35LP and 45LP employ high VI paraffinic base stocks with additives to inhibit oxidation, rust and corrosion, and possess additional demulsibility characteristics. Compressor Lubricants QUALITIES: APPLICATIONS: High viscosity index provides superior viscosity-temperature characteristics Low pour point for cold climate operations Low carbon forming tendencies together with oxidation resistance minimizes exhaust valve deposits CITGO Compressor Oils 35LP and 45LP are recommended for cylinder lubrication of reciprocating air and natural gas compressors. TYPICAL PROPERTIES: CITGO COMPRESSOR OILS 35LP AND 45LP 35LP 45LP Material Code Gravity, ASTM D4052, API Density, lb/gal Flash Point, ASTM D92, F ( C) 554 (290) 475 (246) Viscosity, ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -17 (-27) -27 (-33) Color, ASTM D1500 L2.0 L0.5 Total Acid No. mgkoh/g, ASTM D Foam Test, ASTM D892, Seq. I, ml Seq. II, ml Seq. III, ml RPVOT, Oxidation, ASTM D2272, minutes CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

208 Compressor Lubricants CITGO COMPRESSOR OIL 7585 Date 03/18 DESCRIPTION: CITGO Compressor Oil 7585 is a compressor lubricant specifically designed to provide excellent protection against oxidation and corrosion for reciprocating compressors operating in sour, wet, high pressure natural gas service. QUALITIES: APPLICATIONS: CITGO Compressor Oil 7585 is formulated to a high viscosity index to provide good low temperature start-up viscosity yet provide high film strength under high-temperature operating conditions. CITGO Compressor Oil 7585, contains a special additive system to reduce lubricant displacement by water or liquid hydrocarbons, resist the corrosive effects of hydrogen sulfide and other sour gas components, and fight deposit formation to ensure compressor cleanliness. CITGO Compressor Oil 7585 can tolerate a wide variety of natural gas quality. CITGO Compressor Oil 7585 satisfies the lubricant requirements of single and multi-stage reciprocating compressors in raw, scrubbed or processed natural gas service, and excels where once through lubrication is needed in wet acidic gas service. CITGO Compressor Oil 7585 is widely used for compressing production natural gas, high pressure carbon dioxide, hydrogen sulfide, refinery tail gas, and wellhead gas, where the gas stream may be wet and dirty. TYPICAL PROPERTIES: CITGO COMPRESSOR OIL 7585 Material Code Gravity, ASTM D4052, API 28.8 Flash Point, ASTM D92, F ( C) 410 (210) Viscosity, ASTM D445, cst at 40 C 267 cst at 100 C 24.0 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) 14 (-10) CITGO is a registered trademark of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

209 CITGO COMPRESSORGARD DE Date 03/18 DESCRIPTION: CITGO CompressorGard DE lubricants are formulated from premium diester base stocks and incorporate the latest developments in additive technology. They are designed to satisfy the lubrication requirements for most air compressors in service today. Compressor Lubricants BENEFITS: CITGO CompressorGard DE lubricants are engineered to provide superior oxidation and thermal characteristics which, when compared with mineral oils, offer: Better low temperature fluidity for cold climate operations. Better thermal conductivity reduces lubricant operating temperatures, extending fluid service. Less wear due to lower friction coefficient. Greater resistance to thermal or mechanical stress creates fewer deposits, reducing maintenance. Reduced oil carryover and reduced valve deposits due to low vapor pressure and increased solvency. APPLICATIONS: CITGO CompressorGard DE 32 and 68 are recommended for use in oil flooded rotary vane and screw type air compressors where these viscosity fluids are needed. The high thermal stability and oxidation stability minimize the formation of deposits, sludge and lacquers, especially in the heat exchangers. CITGO CompressorGard DE 100, 125 and 150 are especially designed for both the crankcase and cylinder lubrication of reciprocating compressors. The combination of low volatility and excellent thermal and oxidation stability provide for significantly cleaner discharge valves. Cleaner valves mean reduced maintenance and reduced risk of compressor fires or explosions caused by these deposits. MATERIALS COMPATIBILITY Materials Recommended Not Recommended Seals Fluorocarbon, Fluorosilicone, Butadiene, Butyl, Ethyl Propylene, Nitrile Buna N (>30%), Isoprene, Natural Rubber, Neoprene, Polysulfide, Teflon, Viton Nitrile Buna N (<30%), Polyacrylate, Polyacrylic, SBR Rubber Paints Epoxy, Oil Resistant Alkyd Acrylic, PVC Plastics Celcon, Delrin, Fluorocarbon, Polystyrene, PVC, ABS, nylon polycarbonate Viton is a registered trademark of DuPont Dow Elastomers. (Continued) C

210 Compressor Lubricants CITGO COMPRESSORGARD DE Date 03/18 - (Continued) TYPICAL PROPERTIES: CITGO COMPRESSORGARD DE ISO Viscosity Grade Material Code Specific Gravity Gravity, ASTM D4052, API Density, lb/gal Viscosity, cst at 40 C Viscosity, cst at 100 C Viscosity Index Flash Point, ASTM D92, F ( C) 522 (272) 554 (290) 532 (278) 511 (266) Fire Point, ASTM D92, F ( C) 561 (294) 572 (300) 554 (290) 568 (298) Pour Point, ASTM D97, F ( C) -38 (-39) -33 (-36) -38 (-39) -33 (-36) Color, ASTM D1500 L1.0 L1.0 L1.0 L1.0 Carbon Residue, ASTM D524, % Four Ball Wear, ASTM D4172 mm at 20 kg mm at 40 kg CITGO and CompressorGard are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

211 CITGO COMPRESSORGARD GE Date 04/18 DESCRIPTION: CITGO CompressorGard GE products are formulated with a special combination of polyglycol and Alkylated Hydrocarbon to address thermal degradation and deposit formation commonly associated with conventional rotary screw compressor coolants. Compressor Lubricants BENEFITS: APPLICATIONS: The unique synthetic blend combination found in CITGO CompressorGard GE products has been proven to offer superior performance in the areas of oxidation resistance and deposit control. CompressorGard GE products further eliminate the varnish, sludge and frequent lubricant changes commonly associated with hydrocarbon-type compressor oils. CITGO CompressorGard GE 32 has been formulated specifically to address the needs of Sullair Rotary Screw Compressors. CITGO CompressorGard GE 46 has been formulated specifically to address the needs of Ingersoll- Rand Rotary Screw Compressors. TYPICAL PROPERTIES: CITGO COMPRESSORGARD GE Grade Material Code Gravity, ASTM D4052, API Density, lbs/gal Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445, cst at 100 C Viscosity Index, ASTM D Color Blue Green Blue Green Flash Point, ASTM D92, F ( C), COC 457 (236) 457 (236) Pour Point, ASTM D97, F ( C) -60 (-51) -60 (-51) Autoignition Temperature, ASTM D2155, F ( C) 730 (388) 750 (399) Rust Prevention, ASTM D665 A/B Pass Pass Foam Test, Sequence I. II. III Pass Pass CITGO and CompressorGard are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

212 Compressor Lubricants CITGO COMPRESSORGARD H-SERIES Date 04/18 DESCRIPTION: CITGO CompressorGard H-Series fluids are formulated with the highest quality synthetic base stocks to address thermal degradation and deposit formation commonly observed in reciprocating compressors operating in natural gas compression service. BENEFITS: APPLICATIONS: CITGO CompressorGard H-Series products provide: Protection against wear, thermal and oxidative deposits. Excellent rust and corrosion protection in the presence of hydrogen sulfide and offer excellent low temperature service. CITGO CompressorGard H-Series products are designed for use in reciprocating compressors in hydrogen and natural gas service. CITGO CompressorGard H-Series products are non-catalyst poisoning and can be used in the compression of gas streams that come in contact with catalyst beds. TYPICAL PROPERTIES: CITGO COMPRESSORGARD H-SERIES ISO Viscosity Grade Material Code Gravity, API Density lbs/gal Viscosity, ASTM D445 cst at 40 C cst at 100 C Viscosity Index Flash Point, ASTM D92, F ( C) 518 (270) 558 (292) Pour Point, ASTM D97, F ( C) -54 (-48) -54 (-48) Rust Prevention, ASTM D665 A Pass Pass Foam, Sequence I 10/0 10/0 Sequence II 15/0 15/0 Sequence III 0/0 0/0 Water Separation, ASTM D1401, at 180 F (82 C) 40/40/0 (5) 40/40/0 (10) CITGO and CompressorGard are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

213 CITGO COMPRESSORGARD IPG Date 04/18 DESCRIPTION: CITGO CompressorGard IPG 100 is a high-quality polyether polyol synthetic compressor lubricant engineered for the compression of propane. CITGO CompressorGard IPG 100 offers good water separation characteristics, excellent wear protection and oxidation resistance. Compressor Lubricants BENEFITS: CITGO CompressorGard IPG 100 is miscible with propane in the low temperature areas of the system like the expansion valve and evaporator for efficient cooling. The naturally high viscosity index of CITGO CompressorGard IPG 100 when compared to mineral oils provides enhanced lubrication through increased viscosity at high temperatures. APPLICATIONS: CITGO CompressorGard IPG ISO 100 is recommended for use in rotary screw, vane and reciprocating compressors in propane refrigeration service. TYPICAL PROPERTIES: CITGO COMPRESSORGARD IPG ISO Viscosity Grade 100 Material Code Gravity, ASTM D4052, API 10.6 Density, lb/gal 8.29 Specific Gravity 0.99 Flash Point, ASTM D92, F ( C) 525 (274) Viscosity, ASTM D445, cst at 40 C 100 Viscosity, ASTM D 445, cst at 100 C 17.5 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -49 (-45) Water Separation, ASTM D C (180 F) Pass Foam Test, ASTM D892, Sequence I, II, III Pass Four Ball Wear, ASTM D4172, mm Scar 0.49 Copper Corrosion, ASTM D130 1A CITGO and CompressorGard are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

214 Compressor Lubricants CITGO COMPRESSORGARD PAG Date 04/18 DESCRIPTION: CITGO CompressorGard PAG products are designed especially for high pressure reciprocating compressors operating with natural gas, carbon dioxide, hydrogen, helium, nitrogen, ammonia and other polar gasses. QUALITIES: BENEFITS: APPLICATIONS: CITGO CompressorGard PAG products are resistant to hydrocarbon dilution and absorption of the gas stream. As a result, condensed hydrocarbon liquids in the cylinder area do not wash the lubricant from the cylinder walls. Other lubricants which absorb these liquids lose viscosity, which can result in severe mechanical damage. The high viscosity index and low pour points allow usage over a wide temperature range. Permits reduced maintenance costs and decreased downtime due to improved lubrication. Minimizes problems downstream in separators, meters, filters, etc. due to lower lubricant consumption. Allows easier handling and lower disposal costs. Reduces absorption of lubricating oil into the gas at higher pressures. Minimizes viscosity degradation when saturated with high pressure gas. Provides excellent resistance to wash-off by liquid hydrocarbon gases. Offers compatibility with well bore fluids and treating chemicals, therefore reducing incidence of well impairment. CITGO CompressorGard PAG products are excellent for flooded rotary screw and vane compressors used to compress natural gas, carbon dioxide and other gaseous hydrocarbons. CITGO CompressorGard PAG products of appropriate grade viscosity are also suitable for use as a reciprocating compressor cylinder lubricant when processing these and other gases requiring chemical resistance. TYPICAL PROPERTIES: CITGO COMPRESSORGARD PAG ISO Viscosity Grade Material Code Gravity, API Specific Gravity Density, lb/gal. 60/60 F Viscosity, ASTM D445, cst at 40 C ASTM D 4cSt at 100 C Viscosity Index, ASTM D Flash Point, ASTM D92, F ( C) 555 (291) 547 (286) 554 (290) Pour Point, ASTM D97, F ( C) -54 (-48) -49 (-45) -49 (-45) Color, ASTM D1500 L 0.5 L 0.5 L 0.5 Copper Strip Corrosion, ASTM D130 1A 1A 1A Rust Protection, ASTM D665A Pass Pass Pass Four Ball Wear, ASTM D kg Foam Resistance, ASTM D892 Sequence I, II, III Pass Pass Pass Carbon Residue, mg CITGO, and CompressorGard are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. Values shown are typical values only and do not constitute a specification. The information contained herein is subject to change without notice. C

215 CITGO COMPRESSORGARD PAO Date 04/18 DESCRIPTION: CITGO CompressorGard PAO lubricants are formulated with high-quality polyalphaolefin (synthesized hydrocarbon) base fluids and incorporate technologically advanced additives to provide effective and efficient compressor performance. Available in ISO grades 32, 46, 68, 100 and 150. Compressor Lubricants BENEFITS: APPLICATIONS: Reduced danger of compressor fire and explosions resulting from deposit formation Outstanding oxidation and thermal stability Exceptionally low pour point Low varnish-forming tendencies Wide operating temperature range High viscosity index Excellent antiwear properties Extended service life Lower maintenance costs Excellent rust protection Fully compatible with elastomers, paints, seals and petroleum oil Low toxicity Excellent demulsibility CITGO CompressorGard PAO lubricants are designed for use with the following types of compressors: Rotary Vane, Rotary Screw and Centrifugal. Rotary Compressors Rotary vane and rotary screw compressors are lubricated by injecting the oil directly into the airstream where it is in intimate contact with high-temperature air. The excellent thermal and oxidation properties of CITGO CompressorGard PAO lubricants make them ideal to guard against sludge and varnish deposit formation and accumulation. They give outstanding performance in maintaining a cleaner compressor interior, which means reduced component wear and, thus, increased compressor efficiency and safety. Centrifugal Compressors Centrifugal (Dynamic) compressors are often mated with integral gear sets, requiring a lubricant with good load carrying ability and low foaming tendencies. These compressors are often remotely located. CITGO CompressorGard PAO lubricants contain a carefully selected and proven additive package and low vapor forming tendencies to assure that excellent performance can be achieved over an extended drain interval and extended compressor life when compared to petroleum oil. (Continued) C

216 Compressor Lubricants CITGO COMPRESSORGARD PAO Date 04/18 - (Continued) TYPICAL PROPERTIES: CITGO COMPRESSORGARD PAO ISO Grade Material Code API Gravity Specific Gravity Density, lb/gal, 60/60 F Viscosity, ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D Flash Point, ASTM D92, F ( C) 522 (272) 504 (262) 543 (284) 550 (288) 550 (288) Pour Point, ASTM D97, F ( C) -87 (-66) -71 (-57) -65 (-54) -65 (-54) -54 (-48) Color, ASTM D1500 L0.5 L0.5 L0.5 L0.5 L0.5 Copper Corrosion, ASTM D130 1A 1A 1A 1A 1A Rust Protection, ASTM D665 DI Water Pass Pass Pass Pass Pass Salt Water Pass Pass Pass Pass Pass Four Ball Wear, ASTM D4172, mm at 40 Kg Foam Resistance, ASTM D892 Sequence I, II, III Pass Pass Pass Pass Pass Water Separation, ASTM D1401 at 130 F (54 C) 40/40/0 (5) 40/40/0 (10) 40/40/0 (10) - - at 180 F (82 C) /40/0 (10) 40/40/0 (15) Carbon Residue, mg CompressorGard PAO lubricants are not compatible with silicone or polyalkylene glycol compressor lubricants. Consider CompressorGard PAG lubricants when compressing gases with condensed hydrocarbon liquids. CITGO and CompressorGard are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

217 CITGO COMPRESSORGARD PS 68 Date 04/18 DESCRIPTION: CITGO CompressorGard PS 68 is a premium synthetic blend compressor lubricant formulated with ultra high purity hydrotreated base stocks and a proprietary synthetic component to aid in controlling sludge and deposit formation in compressor applications. CompressorGard PS 68 is designed specifically for use in compressor applications, but can be used in multi-purpose applications. Compressor Lubricants BENEFITS: APPLICATIONS: Resists fluid breakdown caused by high operating temperatures. Improves condensate separator efficiency due to excellent demulsibility. Reduces fluid carryover and make-up oil costs due to low-volatility, ultra high purity hydrotreated mineral oils and synthetic base stocks. Reduces and controls deposits with high performance, ashless additives. Improves equipment reliability by eliminating harmful varnish, sludge and carbon deposits on rotors and separators. CITGO s CompressorGard PS 68 is designed for use in: Rotary vane, rotary screw, and centrifugal compressors. Hydraulic applications where anti-wear hydraulic oils are called for Bearing applications. TYPICAL PROPERTIES: CITGO COMPRESSORGARD PS 68 ISO Viscosity Grade 68 Material Code Specific Gravity ASTM D /60 F Density, lb/gal Viscosity, ASTM D445 cst at 40 C cst at 100 C 8.38 Viscosity Index, ASTM D Flash Point, ASTM D92, C ( F) 260 (500) Pour Pont, ASTM D97, C ( F) -36 (-33) Color, ASTM D Water Separation, ASTM D1401, 130 F (54 C) 40/40/0 (5) Four Ball Wear, ASTM D4172, mm at 40 kg Copper Strip Corrosion, ASTM D130 1A Rust Protection, ASTM D665 DI Water, Proc. A Pass Sea Water, Proc. B Pass Foam, ASTM D892, Sequence I, II, III, Pass C

218 Compressor Lubricants CITGO COMPRESSORGARD SS Date 04/18 DESCRIPTION: CITGO CompressorGard SS fluids are semi-synthetic lubricants designed for rotary screw and reciprocating compressors in natural gas service. The thermal and oxidation stability of these products are superior to conventional petroleum products. CITGO CompressorGard SS fluids contain a balanced additive system to inhibit rust and corrosion, reduce bearing wear, minimize foaming and inhibit the corrosive effects of hydrogen sulfide. QUALITIES: APPLICATIONS: When compared with conventional petroleum products, CITGO CompressorGard SS fluids offer: Low vapor pressure to reduce oil carryover to the compressed gas stream. Oxidation and thermal stability to reduce valve deposit formation that in turn lowers the risk of fires and reduces valve maintenance. Wide operating temperature range attributable to high viscosity index and low pour point. Inhibition against hydrogen sulfide corrosion for longer component life. CITGO CompressorGard SS fluids are compatible with the same system elastomers and seals as used with petroleum products. CITGO CompressorGard SS fluids are recommended for use in rotary screw, vane and reciprocating compressors. TYPICAL PROPERTIES: CITGO COMPRESSORGARD SS ISO Viscosity Grade Material Code API Gravity, API ASTM D Density, lb/gal Specific Gravity, 60 /60 F Flash Point, ASTM D92, F ( C) 504 (262) 504 (262) Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445,cSt at 100 C Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -38 (-39) -36 (-38) Copper Corrosion, ASTM D130 1A 1A Four Ball Wear, 1200 rpm ASTM D4172, mm Scar at 40kg Rust Test, ASTM D665 Pass Pass Foam Test, ASTM D892 Sequence I 0/0 0/0 Sequence II 10/0 10/0 Sequence III 0/0 0/0 CITGO and Compressorgard are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

219 CITGO COMPRESSORGARD XA 200 Date 03/18 DESCRIPTION: CITGO CompressorGard XA 200 is specifically designed for use in reciprocating compressors subjected to sour, wet, high pressure gases found in refineries, gas compression stations and fertilizer plants. Compressor Lubricants BENEFITS: APPLICATIONS: CITGO CompressorGard XA 200 offers: State of the art premium rust and corrosion inhibitor; does not contain barium Outstanding demulsification properties Excellent thermal and hydrolytic stability Resistance to gelling when contaminated with water Quick release of entrained gases Resistance to corrosive attacks by hydrogen sulfide, wet carbon dioxide and other sour gas components CITGO CompressorGard XA 200 is an excellent lubricant for use in reciprocating compressors subjected to high-pressure carbon dioxide and hydrogen sulfide service, in urea fertilizer compression synthesis-gas compression, refinery tail-gas compression, wellhead gas compression and high-pressure sulfur dioxide applications. TYPICAL PROPERTIES: CITGO COMPRESSORGARD XA 200 Material Code API Gravity, ASTM D Density, lb/gal 7.26 Flash Point, ASTM D92 (COC) F ( C) 468 (242) Viscosity, ASTM D445, cst at 40 C 180 Viscosity, ASTM D 445, cst at 100 C 22 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) -17 (-27) Color, ASTM D Copper Corrosion, ASTM D130, 3h at 100 C 1A Rust Test, ASTM D665 A, B Pass Foam Test, ASTM D892, Sequence I, II, III Pass CITGO and CompressorGard are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

220 Compressor Lubricants CITGO GASCOM R OIL Date 04/18 DESCRIPTION: CITGO Gascom R Oil is formulated to satisfy the lubrication requirements of gas compressors used for wet, scrubbed or processed gases. QUALITIES: APPLICATIONS: CITGO Gascom R Oil is formulated with high VI base stocks and special lubricity additives which reduces lubricant displacement by water and/or liquid hydrocarbons. CITGO Gascom R Oil can tolerate a wide variety of gas quality. CITGO Gascom R Oil satisfies the lubricant requirements of single or double-acting reciprocating compressors in raw, scrubbed or processed natural gas service. CITGO Gascom R Oil can also be used as a mild stamping and drawing lubricant where enhanced lubricity is needed. TYPICAL PROPERTIES: CITGO GASCOM R OIL ISO VIS Grade 220 Material Code Specific Gravity, 60 /60 F Gravity, ASTM D4052, API 28.6 Flash Point, ASTM D92, F ( C) 450 (232) Viscosity, ASTM D445, cst at 40 C 234 cst at 100 C 20.4 ASTM D2161, SUS at 100 F 1350 SUS at 210 F 100 Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C) 5 (-9) Color, ASTM D CITGO and Gascom are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

221 CITGO PACEMAKER HV OILS Date 04/18 DESCRIPTION: CITGO Pacemaker HV Oils are high quality, high boiling range, low vapor pressure, petroleum fluids. These oils are designed especially for use in high vacuum, vacuum pump applications where a mineral-type high quality oil is required. Compressor Lubricants QUALITIES: CITGO Pacemaker HV Oils have high initial boiling points and low vapor pressures. They are produced with special processes and quality assurance procedures to help ensure excellent vacuum pump performance. These products have inherently high oxidation resistance, thermal stability and low chemical reactivity. Special product handling assures very low moisture and volatiles contamination which could adversely affect vapor pressure characteristics. Care should be taken to keep containers of CITGO Pacemaker HV Oils tightly sealed and stored in areas that do not have wide variations in temperature. APPLICATIONS: CITGO Pacemaker HV-39 is designed for direct drive vacuum pumps such as WELCH, YELLOW JACKET, PRECISION, LEYBOLD-HERAEUS, EDWARDS and ALCATEL where lower viscosity vacuum pump oil is required to prevent heat build-up, provide high ultimate vacuum, and handle high vacuum pump speeds. Pacemaker HV-68 is designed for belt driven vacuum pumps such as WELCH and CENCO. TYPICAL PROPERTIES: CITGO PACEMAKER HV OILS Grade HV-39 HV-68 Material Code Gravity, ASTM D4052, API Density, lb/gal at 60 F Flash Point, COC, ASTM D92, F ( C) 435 (224) 465 (241) Viscosity, ASTM D445, cst at 40 C Viscosity, ASTM D 445,cSt at 100 C Viscosit,ASTM D2161, SUS at 100 F Viscosit,ASTM D 2161,SUS at 210 F Viscosity Index, ASTM D Pour Point, ASTM D97, F ( C), Max. +5 (-15) 0 (-18) Color, ASTM D1500 L0.5 L0.5 Neutralization No., ASTM D974, mg KOH/ml <0.05 <0.05 Copper Corrosion, ASTM D130, 3 hours at 100 C 1A 1A Carbon Residue, ASTM D4530, wt, % <0.01 <0.02 Vapor Pressure, ASTM D5190, 100 F (37 C) CITGO and Pacemaker are registered trademarks of CITGO Petroleum Corporation. All other registered trademarks or trademarks are the property of their respective owners. C

222 CITGO PROCOIL OILS Date 04/18 DESCRIPTION: CITGO Procoil products are highly refined light color, very low sulfur, paraffinic process oils. Process Oils QUALITIES: APPLICATIONS: CITGO Procoil products have: Low volatility, low aromaticity and high flash points. Very light color and excellent antioxidant response. High viscosity index for relatively low rate of viscosity change with changes in temperature. CITGO Procoil products are recommended as carriers, diluent oils, processing aids or functional oils in a wide range of formulations and chemical processes. CITGO Procoil products are used where superior stability, high flash, low pour and low volatility characteristics are desired. TYPICAL PROPERTIES: CITGO PROCOIL OILS Material Code Gravity, ASTM D4052, API Specific Gravity 60/60 F Pounds Per Gallon Flash Point, ASTM D92, F ( C) 400 (205) 415 (214) 440 (227) 510 (265) Viscosity, ASTM D2161, SUS at 100 F SUS at 210 F ASTM D445, cst at 40 C cst at 100 C Viscosity Index, ASTM D Aniline Point, ASTM D611, F (C) 227 (108) 221 (105) 231 (111) 245 (118) Ash, ASTM D Carbon Residue, ASTM D Total Acid Number, ASTM D Pour Point, ASTM D97, F ( C) 5 (-15) 5 (-15) 5 (-15) 10 (-12) Color, ASTM D1500 L0.5 L0.5 L Molecular Weight, ASTM D Sulfur, ASTM D2622, wt% C

223 WHICH OIL IS RIGHT FOR YOU? Reference Information 215

224 The current and previous ILSAC standards and API Service Categories are listed here. Vehicle owners should refer to their owner s manuals before consulting these charts. Oils may have more than one performance level. For automotive gasoline engines, the latest ILSAC standard or API Service Category includes the performance properties of each earlier category and can be used to service older engines where earlier category oils were recommended. ILSAC STANDARD FOR PASSENGER CAR ENGINE OILS Name Status Service GF-5 Current Introduced in October 2010, designed to provide improved high temperature deposit protection for pistons and turbochargers, more stringent sludge control, improved fuel economy, enhanced emission control system compatibility, seal compatibility, and protection of engines operating on ethanol-containing fuels up to E85. GF-4 Obsolete Use GF-5 where GF-4 is recommended. GF-3 Obsolete Use GF-5 where GF-3 is recommended. GF-2 Obsolete Use GF-5 where GF-2 is recommended. GF-1 Obsolete Use GF-5 where GF-1 is recommended. Reference Information GASOLINE ENGINES (Follow your vehicle manufacturer s recommendations on oil performance levels) Category Status Service SN Current Introduced in October 2010, designed to provide improved high temperature deposit protection for pistons, more stringent sludge control, and seal compatibility. API SN with Resource Conserving matches ILSAC GF-5 by combining API SN performance with improved fuel economy, turbocharger protection, emission control system compatibility, and protection of engines operating on ethanol-containing fuels up to E85. SM Current For 2010 and older automotive engines. SL Current For 2004 and older automotive engines. SJ Current For 2001 and older automotive engines. SH Obsolete OBSOLETE: For 1996 and older automotive engines. SG Obsolete CAUTION: Not suitable for use in most gasoline-powered automotive engines built after May not provide adequate protection against build-up of engine sludge, oxidation, or wear. SF Obsolete CAUTION: Not suitable for use in most gasoline-powered automotive engines built after May not provide adequate protection against build-up of engine sludge. SE Obsolete CAUTION: Not suitable for use in most gasoline-powered automotive engines built after SD Obsolete CAUTION: Not suitable for use in most gasoline-powered automotive engines built after Use in more modern engines may cause unsatisfactory performance or equipment harm. SC Obsolete CAUTION: Not suitable for use in most gasoline-powered automotive engines built after Use in more modern engines may cause unsatisfactory performance or equipment harm. SB Obsolete CAUTION: Not suitable for use in most gasoline-powered automotive engines built after Use in more modern engines may cause unsatisfactory performance or equipment harm. SA Obsolete CAUTION: Contains no additives. Not suitable for use in most gasoline-powered automotive engines built after Use in modern engines may cause unsatisfactory performance or equipment harm. Engine Oil Licensing and Certification System 1220 L Street, NW Washington, DC USA Telephone: Copyright 2016 American Petroleum Institute, all rights reserved. API, the API logo, the Motor Oil Matters Seal, the API Service Symbol (Donut), the API Service Symbol with CI-4 PLUS logo, the API Certification Mark (Starburst), the Mom Knows Best and the Motor Oil Matters phrases are either trademarks or registered trademarks of API in the United States and/or other countries. API Global Marketing & Creative: PDF 216

225 DIESEL ENGINES (Follow your vehicle manufacturer s recommendations on oil performance levels) Category Status Service CJ-4 Current For high-speed four-stroke cycle diesel engines designed to meet 2010 model year on-highway and Tier 4 nonroad exhaust emission standards as well as for previous model year diesel engines. These oils are formulated for use in all applications with diesel fuels ranging in sulfur content up to 500 ppm (0.05% by weight). However, the use of these oils with greater than 15 ppm (0.0015% by weight) sulfur fuel may impact exhaust aftertreatment system durability and/or drain interval. CJ-4 oils are especially effective at sustaining emission control system durability where particulate filters and other advanced aftertreatment systems are used. Optimum protection is provided for control of catalyst poisoning, particulate filter blocking, engine wear, piston deposits, low- and high-temperature stability, soot handling properties, oxidative thickening, foaming, and viscosity loss due to shear. API CJ-4 oils exceed the performance criteria of API CI-4 with CI-4 PLUS, CI-4, CH-4, CG-4 and CF-4 and can effectively lubricate engines calling for those API Service Categories. When using CJ-4 oil with higher than 15 ppm sulfur fuel, consult the engine manufacturer for service interval. CI-4 Current Introduced in For high-speed, four-stroke engines designed to meet 2004 exhaust emission standards implemented in CI-4 oils are formulated to sustain engine durability where exhaust gas recirculation (EGR) is used and are intended for use with diesel fuels ranging in sulfur content up to 0.5% weight. Can be used in place of CD, CE, CF-4, CG-4, and CH-4 oils. Some CI-4 oils may also qualify for the CI-4 PLUS designation. CH-4 Current Introduced in For high-speed, four-stroke engines designed to meet 1998 exhaust emission standards. CH-4 oils are specifically compounded for use with diesel fuels ranging in sulfur content up to 0.5% weight. Can be used in place of CD, CE, CF-4, and CG-4 oils. CG-4 Obsolete OBSOLETE: Introduced in For severe duty, high-speed, four-stroke engines using fuel with less than 0.5% weight sulfur. CG-4 oils are required for engines meeting 1994 emission standards. Can be used in place of CD, CE, and CF-4 oils. CF-4 Obsolete OBSOLETE: Introduced in For high-speed, four-stroke, naturally aspirated and turbocharged engines. Can be used in place of CD and CE oils. CF-2 Obsolete OBSOLETE: Introduced in For severe duty, two-stroke-cycle engines. Can be used in place of CD-II oils. CF Obsolete OBSOLETE: Introduced in For off-road, indirect-injected and other diesel engines including those using fuel with over 0.5% weight sulfur. Can be used in place of CD oils. CE Obsolete CAUTION: Not suitable for use in most diesel-powered automotive engines built after CD-II Obsolete CAUTION: Not suitable for use in most diesel-powered automotive engines built after Reference Information CD Obsolete CAUTION: Not suitable for use in most diesel-powered automotive engines built after CC Obsolete CAUTION: Not suitable for use in most diesel-powered engines built after CB Obsolete CAUTION: Not suitable for use in most diesel-powered engines built after CA Obsolete CAUTION: Not suitable for use in most diesel-powered engines built after SAE VISCOSITY GRADES: PASSENGER CAR MOTOR OIL Multigrade oils such as SAE 5W-30 and 10W-30 are widely used because, under all but extremely hot or cold conditions, they are thin enough to flow at low temperatures and thick enough to perform satisfactorily at high temperatures. Note that vehicle requirements may vary. Follow your vehicle manufacturer s recommendations on SAE oil viscosity grade. If lowest expected outdoor temperature is 0 C (32 F) 18 C (0 F) Below 18 C (0 F) Typical SAE viscosity grades for passenger cars 0W-20, 0W-30, 5W-20, 5W-30, 10W-30, 10W-40, 20W-50 0W-20, 0W-30, 5W-20, 5W-30, 10W-30, 10W-40 0W-20, 0W-30, 5W-20, 5W

226 Reference Information HDEO: Full Synthetic to Conventional Category Full Synthetic SynDurance Plus 5W-30 5W-40 Synthetic Blend CITGARD W-30 15W-40 Premium Conventional CITGARD W-40 Conventional CITGARD HD 15W-40 JT-8 5W-40 Delvac 1 ESP 5W-30 5W-40 JT-8 SHD 10W W-40 15W50 Delvac Extreme FE 10W-30 15W-40 Delvac W-30 15W-40 Mobil HDO 15W-40 10W-30 Rotella T 6 5W-40 Rotella T5 10W30 10W40 Rotella T-4 10W-30 15W-40 Rotella T3 Rimula 15W-40 Delo 400 XSP 5W-30 5W-40 Delo 400 XLE 10W-30 15W-30 Delo 400 SDE 15W40 Elixon 5W-30 Triton ECT Kendall SHP 5W-40 Hypuron 10W W-40 Tection Extra 15W-40 Guardol ECT Kendall Super-D XA Phillip 66 Supreme Firebird EC Kendall Super-D- EC 15W-40 10W- 30 URSA 15W-40 Phillip 66 EC Fleet Supreme EC 15W-40 Premium Blue Extreme Premium Blue 8100 ES 10W-30 Premium Blue 8100 ES 15W-40 Valvoline Premium Blue 15W-40 Valvoline Motor Oil All Fleet 15W-40 All recommendations set forth herein are based solely upon information and materials available at the time of publication. CITGO Petroleum Corporation makes no representations or warranties of any kind regarding the completeness or current accuracy of its competitors information set forth herein. Competitor formulations, claims, and approvals are subject to change without notice. All trademarks other than CITGO, CITGARD, CompressorGard and Pacemaker are registered trademarks of their owners, which are not affiliated with CITGO. 218

227 SAE Viscosity Grade SAE J300 SAE VISCOSITY GRADES FOR ENGINE OILS Low-Tempurature Cranking Viscosity (3) (mpa s) Max Low-Tempurature ( C) Pumping Viscosity (4) (mpa s) Max with No Yield Stress Low-Shear- Rate Kinematic Viscosity (5) (mm 2 /s) at 100 C Min Low-Shear- Rate Kinematic Viscosity (5) (mm 2 /s) at 100 C Max High-Shear- Rate Kinematic Viscosity (5) (mpa s) at 100 C Min 0W 6200 at at W 6600 at at W 7000 at at W 7000 at at W 9500 at at W at at < < < < < < (0W-40 and 10W-40 grades) < (15W-40, 20W- 40 and 25W-40, 40 grades) < < Notes 1 mpa s = 1 cp; mm 2 /s = 1 cst 1. All values, with the exception of the low-tempurature cranking viscosity, are critical specifications as defined by ASTM D3244 (see text, Section 7.) 2. ASTM D5293: Cranking viscosity The non-critical specification protocol in ASTDM D3244 shall be applied with a P value of ASTM D4684: Note that the presence of any yield stress detectable by this method constitutes a failure regardless of viscosity. 4. ASTM D ASTM D4683, ASTM D4741, ASTM D5481, or CEC L SAE Viscosity Grade s SAE J306 AUTOMOTIVE GEAR LUBRICANT VISCOSITY CLASSIFICATION Maximum Temperature for a Viscosity of cp, C (1,2) Kinematic Viscosity at 100 C, cst (3) Minimum (4) Kinematic Viscosity at 100 C, cst (3) Maximum 70W -55 (5) W W W < < < < < < NOTE 1cP = 1 mpa s; 1 cst = 1mm 2 /s 1. Using ASTM D Additional low-temperature viscosity requirements may be appropriate for fluids intended for use in light duty synchronized manual transmissions. See text. 3. Using ASTM D Limit must also be met after testing in CEC L-45-A-99. Method C (20 hours.) 5. The precision of ATSM Method D2983 has not been established for determinations made at temperatures below -40 C. This fact should be taken into consideration in any producer-consumer relationship. *SAE J2360 replaced MIL-PRF-2105E as a world-wide standard for Automotive Gear Lubricants for Commercial and Military use. The gear lubricant shall meet the limits for classification described in SAE J306. Reference Information 219

228 CITGO Grease Characteristics Chart NLGI Grade Base Oil Type (Mineral, Semisyn. or Synthetic) EP/AW (Enhanced Load Carrying) Reference Information Water Resistance Rust Protection Saltwater Rust Protection Low Temperatures High Temperatures Jet Lubricant TM Semi-Fluid Min. + Lithoplex CM Greases 1 Min Min Lithoplex HM Greases 1 Min Min Lithoplex MP Greases 0 Min Min Min Lithoplex PL Greases 000 Min Min Min Lithoplex PM Grease 2 Min Lithoplex Red MP Grease 2 Min Lithoplex RT Greases 1 Min Min Lithoplex ST Greases 1 Min Min OverDrive HD Grease 2 Min Premium Lithium EP Semi-Fluid Min Greases 0 Min Min Min. + + Railroad Curve 0 Min. + + Greases 1 Min. + SUPERGARD Marine Plus Grease 2 Min SynDurance Premium 00 Syn Synthetic 460 Greases 2 Syn SynDurance Premium Synthetic 460 #00 00 Syn Grease Red SynDurance ST 1 Syn Synthetic Greases, ISO Syn SynDurance ST 1 Syn Synthetic Greases, ISO Syn UltraLife CSEP 5M Grease 2 Min Suitable ++ Recommended 220

229 NLGI GREASE CLASSIFICATIONS The following table shows the worked penetration values for the various NLGI grades of grease. NLGI Number ASTM Worked Penetration at 77 F ±1 (25 C±0.5 ) ASTM D 4950 STANDARD CLASSIFICATION AND SPECIFICATIONS FOR AUTOMOTIVE SERVICE GREASES Service Category L Chassis Grease LB Chassis and universal joints subject to water contamination and heavy loads. Usable temperature -40 F to 248 F with relubrication intervals greater than 2000 miles. Reference Information Service Category G Wheel Bearing Grease GC Lubricate wheel bearings over a wide temperature range. Temperatures from -40 F with frequent excursions to 320 F and occasional to 392 F. AUTOMOTIVE WHEEL BEARING & CHASSIS LUBRICANT GC-LB AUTOMOTIVE CHASSIS LUBRICANT LB 221

230 Sodium Soap Reference Information GREASE THICKENER COMPATIBILITY CHART Aluminum Complex Calcium Stearate Calcium 12-Hydroxy Calcium Complex Calcium Sulfonate Clay Lithium Stearate Lithium 12-Hydroxy Lithium Complex Polyurea General Guide - Exceptions Are Possible Aluminum Complex C I B I I I I I I I* I Calcium Stearate I C C I B I C B C I* I Calcium 12-Hydroxy B C C B C I C C C I* I Calcium Complex I I B C I I I I B C I Calcium Sulfonate I B C I C I I B B I I Clay I I I I I C I I I I I Lithium Stearate I C C I I I C C C I* I Lithium 12-Hydroxy I B C I B I C C C I* I Lithium Complex I C C B B I C C C I* I Polyurea I* I* I* C I I I* I* I* C I Sodium Soap I I I I I I I I I I C C - Compatible B - Borderline I - Incompatible I* - Dependent Upon Type 222

231 CITGO Technical Bulletin Guide to Synthetic Industrial Lubricants The term synthetic lubricant can apply to a wide range of non-petroleum derived materials used as lubricant base stocks. The most common are synthetic hydrocarbons, the polyalphaolefins, or PAOs. These oils are very similar chemically to petroleum base oils (mineral oils), but because they are synthesized from specific starting materials, they are typically very uniform in molecular size and shape and do not contain the impurities often found in mineral oils, including wax molecules. PAOs are better at low temperature due to the absence of wax (low pour point) and better at high temperature due to superior thermal and oxidative stability. They also have higher viscosity indexes than mineral oils, making them applicable over a wider range of temperatures. Because PAOs are so commonly used in lubricant formulations, the API gave them their own base oil group API Group IV. All other synthetic lubricant base stocks fall into another API base oil group Group V. Those materials include various types of esters, polyalkylene glycols (PAGs), alkylated aromatics, etc. Each type of synthetic fluid has advantages and disadvantages. One of the biggest challenges is compatibility. Compatibility not only between the various fluid types, but also compatibility with seals and other elastomeric or plastic components, compatibility with paints and coatings, and even sometimes compatibility with the metallic parts being lubricated. In general, mineral oils, PAOs, and most esters are miscible and compatible. However, most PAGs are not compatible with mineral oils or PAOs, and mixing can have disastrous results. Esters can be very aggressive towards elastomers and plastics as well as paints and coatings. The use of an ester based lubricant may require that the seals in the equipment be changed to a more resistant elastomer. PAGs can also be aggressive towards seals and paints, and special elastomers may be needed. Reference Information The use of synthetic lubricants is often done to extend the oil change interval. If the oil change interval is based on oil thermal or oxidative degradation of the oil, then the use of a synthetic lubricant is likely justified, and will lower overall operating cost. However, if the oil change interval is based on contamination of the lubricant with water, wear metals, environmental contaminants, etc., then using a synthetic lubricant will likely not extend the service interval. In fact, contamination of certain types of esters with water can result in hydrolysis, the breakdown of the ester into the organic acid and alcohol 223

232 components from which it was made. That breakdown can result in an increase in acid number, component corrosion, viscosity loss, and other negative impacts. Selecting a synthetic lubricant can be a daunting task. Many factors must be considered when selecting the appropriate type of synthetic fluid for a specific application. As stated above, PAO based products are the most common synthetic lubricants. Many PAO based lubricants also contain some type of ester fluid to improve the solubility of additives in the finished lubricant. These PAO/ester products find service in a wide range of applications, ranging from industrial gear oils to compressor fluids. Ester based synthetic fluids are used in some air compressor fluids where the discharge temperature is high and the solvency of the ester fluid helps to reduce deposits and keep critical surfaces clean. PAG fluids are often used in compressor fluids for natural gas or other hydrocarbon gases. PAG fluids are more resistant to dilution by the hydrocarbon gases, and tend to maintain viscosity better under operating conditions. Factors to take into consideration when selecting a synthetic lubricant include: Reference Information Viscosity grade and viscosity index Most synthetic lubricants have a higher viscosity index compared to mineral oil based products. It may be possible to use a lower viscosity grade synthetic that maintains viscosity better at higher temperatures. Thermal and oxidative stability If the lubricant is to be used at high temperature, a product with excellent thermal and oxidative stability should be selected. Low temperature properties If the synthetic lubricant is being considered for low temperature applications, the pour point of the product must be considered. Flammability Some synthetic lubricants offer reduced flammability, due to higher flash and fire points compared to mineral oils of similar viscosity grade. Lower tendency to form deposits Due to their superior solvency, ester based fluids tend to remove existing deposits and reduce the formation of new deposits. PAG based fluids are also very resistant to the formation of deposits. PAO based fluids can actually have a higher deposit formation tendency due to their inherently poorer solvency compared to many other types of lubricants. Material compatibility Compatibility with elastomers and plastics, paints and coatings, and the metals being lubricated must be considered when selecting a synthetic lubricant. Adverse reactions Reactions such as hydrolysis of ester based fluids must be considered when selecting a synthetic lubricant. Miscibility Some synthetic fluids are not miscible with mineral oils or other synthetics, making a change more difficult. A proper change-over procedure must be followed in those cases. 224

233 Cost The cost of the synthetic lubricant must be balanced against the potential for a longer oil change interval or improved operating conditions of the equipment. Synthetic lubricants are often well worth the additional initial cost. Reference Information 225

234 Reference Information Compatibility of Common Elastomers and Plastics with CITGO Products Elastomer/Plastic Abbreviation Trade Names Mineral Oil Example Products HyDurance AW, Pacemaker T, EP Compound Polyacrylate ACM HyTemp Very Good Synthetic Hydrocarbon CITGEAR Synthetic EP, CITGEAR Synthetic HT, CompressorGard PAO Synthetic Ester CompressorGard DE Polyalkylene Glycol CompressorGard PAG, CITGEAR Synthetic PAG Ethylene-Acrylic AEM Vamac Good Good Good Ethylene-Propylene-Diene Monomer EPM, EPDM Duttral, Nordel, Vistalon Water/Glycol FR WG-40XD, Glycol FR-5046HP Poor Poor Poor Excellent to Good Recommended Fluoroelastomers FKM, FPM Viton, Fluorel Very Good Very Good Very Good Excellent to Good Suitable Nitrile (Acrylonitrile-Butadiene) NBR, XNBR, HNBR NBR, Purbunan, Buna-N, Chemigum, Hycar, Paracril, Nipol, Krynac, Europrene Perfluoroelastomers FFKM Kalrez, Parafluor Very Good Very Good Good Good Poor to Good Fair Suitable Polychloroprene CR Neoprene Fair Fair to Good Poor Good Suitable Silicones MQ, VMQ, PMQ, FMQ VMQ Poor to Good Poor to Good Poor to Fair Good to Excellent Styrene-Butadiene SBR SBR, Buna-S Poor Poor to Good Poor Poor Suitable Polyester Good Good Poor to Fair Polytetrafluoroethylene PTFE Teflon Very Good Very Good Very Good Suitable Polyamide PA Nylon, Zytel Poor to Good Poor to Good Poor Polycarbonate PC Good Natural Rubber NR Poor to Fair Poor to Fair Poor Suitable Polyethylene PE (LDPE, HDPE) Good Good Good Polypropylene PP Good to Poor Butyl Rubber IIR Very Poor to Poor Very Poor to Poor Poor to Fair Polyvinyl Chloride PVC PVC Poor to Good Poor to Good Poor Chlorosulfonated Polyethylene CSPE, CSM Hypalon Fair Polyether Ester TPC-ET Hytrel Good Polyurethane PU Good to Fair Polyoxymethylene, Polyacetal, acetal resin, polytrioxane, polyformaldehyde, and paraformaldehyde POM Delrin, Kepital, Celcon, Hostaform and Ultraform Excellent - Good Fluorosilicone FSI Good Excellent Ethylene-Propylene Rubber EPR Poor Poor Good Fluorovinyl Methyl Silioxane FVMQ Fluorosilicone Good to Excellent 226

235 Compressor OEM Fluid Cross-reference OEM Product Name CITGO Product Name Mat. Code Competitive Product Co Atlas Copco Atlas Copco HD Roto Fluid CompressorGard PAO Mineral Special Processed Oil, ISO 46 Atlas Copco HD Roto Fluid Plus CompressorGard PAO Group III, ISO 46 Atlas Copco Paroil M CompressorGard PAO Mineral Oil, anti-wear, ISO 46 Atlas Copco Paroil S 46 CompressorGard PAO PAO, ISO 46 Atlas Copco Paroil S 68 CompressorGard PAO PAO, ISO 68 Atlas Copco Roto-H Plus CompressorGard PAO Mineral oil, ISO 32 Atlas Copco Roto-Inject CompressorGard PAO Ashless, AW mineral oil, ISO 46 Atlas Copco Roto Xtend Duty Fluid CompressorGard PAO PAO, ISO 46 Atlas Copco Roto Xtreme Duty No Product Polyol Ester, ISO 46 Fluid Champion RotorLub 8000 CompressorGard PAO PAO, ISO 46 RotorLub 4000FG Clarion CompressorGard PAO, ISO 46, Food Grade RotorLub 4000 CompressorGard PAO Mineral Oil, ISO 46 Compair/Kellogg CompAir CN 300 No Product Naphthenic mineral oil, ISO 100 CompAir CS 100 CompressorGard DE Diester, ISO 32 CompAir CS 200 CompressorGard DE Diester, ISO 68 CompAir CS 300 CompressorGard DE Diester, ISO 100 CompAir CS 400 CompressorGard DE Diester, ISO 150 CompAir Hydrovane 2000 CompressorGard DE Rotary compressor mineral oil, ISO 100; [Kellogg- American (A CompAir Co.) recommends an ISO 100 diester for Hydrovane Rotary Vane 3 HP to 50 HP comp. - check if mineral oil was previously used; drain and flushing recommended] Compair/LeROI CompAir LeRoi CompLube 10 CompressorGard PAO PAO/Polyol ester mixture, ISO 46 CompAir LeRoi RVL 5 CompressorGard PAO 100 PAO/ester, ISO 100 CompAir LeRoi SSL-46 Plus CompressorGard PAO PAO, ISO 46 CompAir LeRoi SSL-50 CompressorGard PAO Semi-synthetic; PAO Mineral Oil blend, ISO 46 All recommendations set forth herein are based solely upon information and materials available at the time of publication. CITGO Petroleum Corporation makes no representations or warranties of any kind regarding the completeness or current accuracy of its competitors information set forth herein. Competitor formulations, claims, and approvals are subject to change without notice. All trademarks other than CITGO, CITGARD, CompressorGard, Pacemaker, HyDurance and Clarion are registered trademarks of their owners, which are not affiliated with CITGO. Reference Information 227

236 Reference Information Compressor OEM Fluid Cross-reference - (Cont d.) OEM Product Name CITGO Product Name Mat. Code Competitive Product Co Gardner Denver Gardner Denver Aeon 500 CompressorGard PAO Mineral oil, ISO for reciprocating compressors Gardner Denver Aeon 800 CompressorGard PAO R&O, Mineral oil, ISO 46 - for rotary screw compressors Gardner Denver Aeon 2000 CompressorGard PAO R&O Mineral oil, ISO 46 Gardner Denver Aeon 4000 CompressorGard PAO Mineral/synthetic blend, ISO 46 Gardner Denver Aeon 5000 CompressorGard DE Diester, ISO 68 - for reciprocating compressors Gardner Denver Aeon 6000 FG Clarion CompressorGard USDA H1, FDA 21CFR , PAO, ISO 46 Gardner Denver Aeon 9000 SP CompressorGard PAO PAO, ISO 46 Ingersoll-Rand Ingersoll-Rand All Season Select CompressorGard DE Diester, ISO 100 Ingersoll-Rand OCV-Zero Fluid No Product ISO VG 15, diester fluid Ingersoll-Rand Original SSR CompressorGard DE Diester, ISO 68, discontinued product Coolant Ingersoll-Rand Pro-Tec CompressorGard PAO (stationary compressor) Ingersoll-Rand Pro-Tec CITGARD W (portable compressor) Ingersoll-Rand Rotalube 1000 CompressorGard PAO Mineral oil, ISO 46 Ingersoll-Rand SL-200 HyDurance AW NZ For Oil-Free Sierra Compressors, Mineral oil, SAE 20, ISO 46, Ashless Hydraulic Ingersoll-Rand SSR Ultra Coolant CompressorGard GE Polyalkylene glycol/ester, 56.2 cst at 40C Ingersoll-Rand SSR Ultra Plus CompressorGard GE Polyolester, ISO 32 Coolant Ingersoll-Rand T-30 Select CompressorGard DE Diester, ISO 150 Ingersoll-Rand Techtrol Gold CompressorGard GE Polyalkylene glycol/polyol ester, ISO 32 Ingersoll-Rand XL-300 CompressorGard PAO R&O Mineral oil, ISO 150, discontinued product Ingersoll-Rand XL-700 CompressorGard DE Diester, ISO 100 Ingersoll-Rand XL-740 HT CompressorGard DE Diester, ISO 150 All recommendations set forth herein are based solely upon information and materials available at the time of publication. CITGO Petroleum Corporation makes no representations or warranties of any kind regarding the completeness or current accuracy of its competitors information set forth herein. Competitor formulations, claims, and approvals are subject to change without notice. All trademarks other than CITGO, CITGARD, CompressorGard, Pacemaker, HyDurance and Clarion are registered trademarks of their owners, which are not affiliated with CITGO. 228

237 Compressor OEM Fluid Cross-reference - (Cont d.) OEM Product Name CITGO Product Name Mat. Code Competitive Product Co Mineral/synthetic blend (5-10% polyol ester), ISO 100 Kaeser Kaeser Sigma 4000 M-100 Pacemaker T-115, CompressorGard PAO 100 Kaeser Sigma 4000 M-150 Pacemaker T-150, CompressorGard PAO 150 Kaeser Sigma 4000 M-460 Pacemaker T-46, CompressorGard PAO , , , Mineral/synthetic blend (5-10% polyol ester), ISO 150 Mineral/synthetic blend, ISO 46 Kaeser Sigma 8000 S-100 CompressorGard DE Diester, ISO 100 Kaeser Sigma 8000 S-150 CompressorGard DE Diester, ISO 150 Kaeser Sigma 8000 S-320 CompressorGard PAO PAO, ISO 32 Kaeser Sigma 8000 S-460 CompressorGard PAO PAO, ISO 46 Kaeser Sigma 8000 S-680 CompressorGard PAO PAO, ISO 68 LeROI Leroi SSL-32 CompressorGard PAO Mineral Oil, not sure what vis grade, no web information available, cross reference info conflict Leroi SSL-46 CompressorGard PAO PAO ISO /mineral oil blend, 35 40C Leroi SSL-50 CompressorGard PAO PAO/mineral oil blend, 37 40C Leroi SSL-68 HT No Product Polyol ester, ISO 68 Quincy Quincy Quin-Cip 100 CompressorGard PAO R&O Mineral oil for reciprocating compressors, ISO small recips, discharge less than 150 C Quincy Quin-Cip 32 CompressorGard PAO R&O Mineral oil for reciprocating compressors, ISO 32 - small recips, discharge less than 150 C Quincy Quin-Cip 68 CompressorGard PAO R&O Mineral oil for reciprocating compressors, ISO 68 - small recips, discharge less than 150 C Quincy Quin-Syn CompressorGard PAO PAO, ISO 46 Quincy Quin-Syn F Clarion CompressorGard PAO, ISO 46, H-1 Quincy Quin-Syn HP CompressorGard GE Polyol ester, ISO 46 Quincy Quin-Syn PG CompressorGard GE Polyalkylene glycol/ester, ISO 46 Quincy Quin-Syn Plus Clarion CompressorGard Food Grade PAO, ISO 46 Quincy Quin-Syn IV CompressorGard PAO Mineral oil/synthetic PAO blend, ISO 46 Quincy Quin-Syn XP No Product Polyol ester, ISO 68 All recommendations set forth herein are based solely upon information and materials available at the time of publication. CITGO Petroleum Corporation makes no representations or warranties of any kind regarding the completeness or current accuracy of its competitors information set forth herein. Competitor formulations, claims, and approvals are subject to change without notice. All trademarks other than CITGO, CITGARD, CompressorGard, Pacemaker, HyDurance and Clarion are registered trademarks of their owners, which are not affiliated with CITGO. Reference Information 229

238 Reference Information Compressor OEM Fluid Cross-reference - (Cont d.) OEM Product Name CITGO Product Name Mat. Code Competitive Product Co Sullair Sullair 24KT No Product Silicon, ISO 32 Sullair AWF CITGARD W Mineral oil, extends warranty to 5 years, 5W-20 Sullair AWF CompressorGard PAO Mineral oil, extends warranty to 5 years, 5W-20 Sullair SRF 1/4000 CompressorGard PAO Paraffinic Mineral oil viscosity cst at 40C Sullair SRF II/8000 CompressorGard PAO Paraffinic Mineral oil viscosity 35.6 cst at 40C Sullair Sullube CompressorGard GE Polyalkylene glycol/ester blend, SAE 5W-20 Sullair Sullube 32 CompressorGard GE Polyalkylene glycol/ester blend, ISO 32, renamed Sullube Sullair Sullube 60 No Product Polyalkylene glycol/ester blend, ISO 68 Sullivan-Palatek AFX 32 CompressorGard GE Polyol Ester blend, ISO 46 Sullivan-Palatek Palasyn 45 CompressorGard PAO PAO, ISO 46 Sullivan-Palatek Pallube 32 ComprssorGard GE Polyalkylene glycol/ester blend, ISO 32 Before making any recommendations or cross reference recommendations for CITGO products, it is strongly suggested that the requirements of the specific compressor application be reviewed. In some cases, the wrong product may be in service, thus crossing the product to an applicable CITGO product may lead to future compressor problems or even compressor failures. All recommendations set forth herein are based solely upon information and materials available at the time of publication. CITGO Petroleum Corporation makes no representations or warranties of any kind regarding the completeness or current accuracy of its competitors information set forth herein. Competitor formulations, claims, and approvals are subject to change without notice. All trademarks other than CITGO, CITGARD, CompressorGard, Pacemaker, HyDurance and Clarion are registered trademarks of their owners, which are not affiliated with CITGO. 230

239 CITGO Technical Bulletin Understanding ISO Cleanliness Rating System for Hydraulic Fluids (ISO Standard 4406) It is estimated that 70-80% of hydraulic component wear can be traced to solid particle contamination. The most common sources of these are wear debris from pumps, valves, cylinder rods, the sticking of valves, and oxidation. A primary step toward gaining control over wear problems is to determine how many, and what size particles are present in the hydraulic fluid. The means most widely used to represent fluid cleanliness is the ISO Code Level of the ISO Cleanliness Rating System. This method of identifying the level of contaminants in a fluid uses a two digit XY code where X represents particles larger than 5um and Y represent particles larger than 15um. Using Chart 1 you can determine the cleanliness level of a given fluid. If, for example, a fluid had x (>5um) = 1895 particles per milliliter and Y (>15um) = 152 particles per milliliter, the fluid would have an ISO cleanliness rating of 18/14. The lower the code numbers, the cleaner the fluid. Some organizations have extended the two standard code (XY) to three levels by including a code level for (>2um) particles as well. This three level system is illustrated in Chart 2. The three level system is being considered by the ISO committee that oversees this standard. Chart 3 illustrates some recommended cleanliness code levels for selected types of hydraulic components. Some caution should be taken when extracting samples for particle counting of any fluid. The sample should be as representative of the entire hydraulic system as possible, and the sample container should be glass and super clean. Many containers are certified clean but are not clean from solid particulate; they are biologically clean (sterile) but may contain many particles. ISO Standard 3722 should be followed for certifying bottle cleanliness. Chart 1 ISO 4406 Code Levels Particle count range (per ml) ISO Code Minimum (included) Minimum (excluded) , ,000 20, ,000 40, ,000 80, , , , , , , ,000 1,300, ,300,000 2,500,000 Reference Information 231

240 Reference Information 232

241 233 Reference Information

242 CITGO Technical Bulletin Particle Counting Accuracy Particulate contamination interferes with a lubricant s ability to provide friction and wear protection. Controlling the level of particulates in a lubricant will improve a system s performance, as well as reduce downtime. Reference Information Measurement of particle contamination within a lubricant is usually performed by lightdetecting automatic particle counters. These counters use the properties of light to perform counts and are highly sensitive to sample preparation. However, even using proper sample preparation techniques, particle counters can detect phantom particles that cannot be removed by filtration. This results in high particle detection that is a function of the formulation of the lubricant itself, and not of the cleanliness of the fluid. It is important to note that there are other methods of performing particle counting that are not susceptible to phantom counts, so there is always a check that can be performed against light detecting automatic particle counters should results come into question. The reason for the popularity of light detecting automatic particle counters is the speed of the test compared to the more labor intensive, yet more accurate testing. ISO Cleanliness Code ISO 4406 describes a method of coding solid particles in an oil sample. Results are delivered in a three number code. The first code number represents the number of particles per milliliter of fluid at a size of four microns. The second code number represents the number of particles per milliliter of fluid at a size of six microns. The third code number represents the number of particles per milliliter of fluid at a size of 14 microns. The range between the upper and lower limits for each code number is listed in the table below and limits increase per code by a factor of two. This means that for each increase of one ISO code number, the number of particles approximately doubles. For example, an ISO code of 18/16/14 indicates there are 1301 to 2500 particles at a size of four microns, 321 to 640 particles at a size of six microns, and 81 to 160 particles at a size of 14 microns. Also, please note that it is common for certain applications to refer to ISO cleanliness results with only two codes. In this case, the number of particles at a size of 4 microns is irrelevant, and the two number code refers to the number of particles at six and 14 microns, respectively. 234

243 Scale Particles per million Number more than less or equal 22 20,000 40, ,000 20, ,000 10, ,500 5, ,300 2, , Table 1. Source: Practicing Oil Analysis (January 2008) Chemical Description Function Weight % 50 TBN calcium sulfonate Rust inhibitor TBN calcium sulfonate Detergent 1.2 Succinimide Dispersant 1.1 Zinc dithiophosphate Antiwear agent 1.1 Boronated succiminide Dispersant 0.9 Polyacrylate Foam inhibitor 0.05 Polydimethylsiloxane Foam inhibitor 0.02 Detergent-inhibitor package DEO additive (75% conc.) 18.8 Table 2. Source: Practicing Oil Analysis (January 2008) Measuring Fluid Cleanliness Light detecting particle counters use a beam of light to quantify the contamination level of fluids. Basically, when particles block the path of the beam of light, a count is made. However, the path of the light beam can be disturbed by means other than particles. For example, water droplets in oil will deflect the light beam, and will be counted as a particulate and increase the ISO code. Water, although a contaminant of the lubricant, is not a particulate in the traditional sense as it can not be captured and removed by filtering. Test Procedure Common lubricant additives were introduced into base oils at concentrations typical of the use of the additive. The concentration of each additive is listed in Table 2. The base oil was filtered through a 3 micron filter until it reached a cleanliness of ISO X/16/13 or cleaner. After the fluid reached that level of cleanliness, the additive was introduced to the base oil. The fluid was then circulated for 30 minutes, and sample was taken after 15 minutes to measure ISO cleanliness. After 30 minutes, fluid was then filtered for an additional 30 minutes, and then ISO cleanliness was measured. Results are listed in Table 3. Reference Information These test results show that all base oils were relatively clean prior to introducing the additive. The greatest increases were seen with the diesel engine oil package, and the polydimethylsiloxane (silicone antifoam). All other increases were relatively small and responded to filtration. 235

244 Conclusion The test results indicate that silicone antifoam agent produces phantom counts in light detecting particle counters. Silicone antifoams work by forming an insoluble micelle within air bubble walls that causes the thinning and collapse of the air bubble wall. These insoluble micelles are what the particle counter is actually reading as particles. Much like water, these micelles will not be collected by a filter and reform on the other side of the filter. Additive Base oil at start of test, 100 F Group I, ISO Code Filter off 15 minutes of filtration After 30 minutes of fltration 50 TBN calcium sulfonate 15/13/<7 13/11/9 13/12/9 400 TBN calcium sulfonate 15/13/10 15/14/11 13/9/<7 Succinimide 13/11/8 16/14/11 16/14/11 Zinc dithiophosphate 16/15/12 17/15/11 17/15/11 Boronated succiminide 16/14/11 17/15/11 17/14/12 Polyacrylate 14/12/8 16/12/10 >28/22/16 Polydimethylsiloxane 15/13/9 >28/22/21 20/16/7 Diesel engine additive package Table 3. Source: Practicing Oil Analysis (January 2008) 17/14/<7 22/19/14 Reference Information Silicone antifoams are common in lubricants, so consideration must be given before ISO cleanliness testing can be put into perspective. Knowing that phantom counts can occur can save you loads of frustration and money attempting to filter lubricants that are actually clean. CITGO s technical help team can always assist in interpreting ISO Cleanliness results, and help to explain whether results are due to cleanliness or due to formulation. Please call the CITGO Lubricant Product Answer Line at for help interpreting ISO cleanliness, or for further explanation. Acknowledgments Thomas S. Wanke, Milwaukee School of Engineering Paul W. Michael, Milwaukee School of Engineering Michael A Mccambridge, Milwaukee School of Engineering 236

245 CITGO Technical Bulletin Use of Fire Resistant Hydraulic Fluids The use of industrial fluid power or hydraulics has increased substantially not only in U.S. industry but also in worldwide industry. In addition to this increase in fluid power usage, we have seen some rather drastic changes in the operating conditions of industrial hydraulic circuitry. Increased production demands, larger work pieces, and higher output machinery have all had the net effect of elevating hydraulic system operating pressures in most industries. This, in itself, has imposed greater performance demands on hydraulic fluids. Fluids that were designed to perform at 1000 psi cannot adequately satisfy the requirements of today s pressures of 2000 psi and higher. With these changes in hydraulic system conditions, we also find a substantial increase in the volumes of fire resistant fluids being employed by industry. This has been brought about, in part, by increased regulations at all levels of government to insure safe working conditions. In addition to these regulatory codes, management has a keen awareness of the devastating cost resulting from plant fires. As system pressures go higher, the chance of hydraulic line rupture increases and the potential for fire becomes greater. Therefore, a modern fire resistant hydraulic fluid must offer the consumer not only maximum fire protection, but must also give him the optimum lubrication and wear protection necessary for pumps and other hydraulic hardware running at these elevated pressures. Reference Information CITGO FR WG 40XD and FR-5046HP are water-glycol fire resistant fluids developed and designed specifically to operate in high system pressures in the 2000 and 5000 psi range respectively. CITGO Glycol FR-5046 is specifically formulated to meet the high pressure requirements for mobile equipment and meets the specification for Caterpillar where a water-glycol product is required. These unique formulations contain more than a sufficient amount of water to prevent the propagation of fires in the event of a hydraulic line rupture near an ignition source. Moreover, CITGO Glycol FR fluids have all the necessary lubrication and anti-wear properties required of a hydraulic fluid for service in high-pressure, high-output systems. Other advantages include: Excellent corrosion protection both liquid and vapor phase to the metals commonly used in hydraulic systems. The superior heat transfer characteristics of water. 237

246 The viscosity-temperature properties, combined with a very low pour point, prevent or minimize cavitation and cold start pump wear problems associated with fluids having poorer viscosity-temperature properties. Compatible with most conventional seals, gaskets, and O rings. Can be satisfactorily mixed with other water-glycol type fluids. Resistant to oxidation and chemical breakdown. Will not separate with normal use and storage. FIRE RESISTANCE Fire resistance is imparted to CITGO FR WG-40XD and FR-5046HP through its water content which creates a snuffing blanket of steam if the fluid comes in contact with an ignition source. Because of the water content, these products have the ability to prevent flame propagation when a fire occurs. CITGO FR WG-40XD and FR-5046HP have been tested and approved by Factory Mutual Research. Reference Information In order to insure continued fire resistance, the water content of CITGO Glycol FR fluids must be maintained above 35%. This is true of any water-glycol fluid. In order to insure against excessivewater evaporation in open hydraulic systems, operating temperatures should be maintained as low as possible and should not exceed 150 F (65.5 C). Water control methods are provided in this bulletin for the addition of water to a particular fluid in service. HEAT TRANSFER Water and water containing compositions such as CITGO Glycol FR fluids are superior heat transfer media. Water-glycol fluids have marked advantages over mineral oils or synthetic FR fluids in this respect. SHEAR STABILITY CITGO Glycol FR fluids contain water soluble polymers which give the fluids their viscosity properties. The close tolerances in hydraulic pumps and other hardware have a tendency to break down certain polymers. This action is mechanical shearing. The special polymers used in formulating CITGO Glycol FR fluids are completely resistant to this mechanical shearing, and the fluids will not undergo viscosity change due to shearing. VISCOSITY INDEX The viscosity index of a fluid defines the degree to which the fluid resists thinning out at 238

247 elevated temperatures. In the viscosity index rating system, the lower the VI number of an oil or fluid, the greater the differential between the fluid s viscosity measured at 100 F and its viscosity measured at 210 F. Therefore, fluids with high VI numbers show a much lower viscosity difference than low VI fluids. CITGO Glycol FR fluids have viscosity indexes of 180 and 210 respectively when tested using the ASTM D 2270 procedure. Shown below is a comparison between CITGO Glycol FR fluids and other commonly used hydraulic fluids. Fluid Type Viscosity Index R & O Oil 95 A/W Hydraulic Oil 95 Automatic Transmission Fluid W-30 Motor Oil 140 Synthetic FR Fluid 70 CITGO FR WG-40XD 180 CITGO Glycol FR-5046HP >210 The temperature-viscosity relationship of CITGO Glycol FR fluids assures the user of minimum fluid thin-out at operating temperatures, hence, better lubricity. POUR POINT The pour point of a fluid is the measured temperature at which the fluid will no longer flow under prescribed test conditions. CITGO Glycol FR fluids have pour points below -40 F. In addition, these fluids can be repeatedly frozen and thawed without any loss whatsoever in homogeneity. The excellent low-temperature flow properties of CITGO Glycol FR fluids, coupled with high viscosity indexes, offer the user the maximum in fluid performance over a wide temperature range. The excellent low-temperature properties minimize pump problems on cold start and the high VI assures adequate viscosity and lubricity at running conditions. Reference Information The following chart illustrates the fluidity characteristics of CITGO FR WG-40XD and FR-5046HP compared with other fluid types. 239

248 100,000 20,000 5,000 1,000 VISCOSITY SUS A Reference Information 40 Viscosity Tempurature Properties of Hydraulic Fluids A. CITGO FR WG-40XD and FP-5046HP B. Conventional High VI Mineral Hydraulic Oil C. Typical Synthetic Type Fluid B C TEMPURATURE F CORROSION PROTECTION CITGO Glycol FR fluids are formulated with special corrosion inhibitors to provide corrosion protection in both the liquid phase and the vapor phase. Vapor phase protection is especially desirable when machines do not operate around the clock or are subject to short- and long-term shutdowns. CITGO Glycol FR fluids provide corrosion protection to aluminum, copper, brass, cast iron, steel and other metals commonly used in hydraulic circuitry. LUBRICITY CHARACTERISTICS A high level of anti-wear protection is built into CITGO Glycol FR fluids. This permits usage in hydraulic systems operating up to 5000 psi (with FR-5046HP), providing the hydraulic pumps are designed to operate on water-glycol fluids. Prior to converting 240

249 any system to a water-glycol fluid from a conventional or synthetic fluid, the equipment manufacturer should always be consulted to make sure that the circuit hardware is suitable for water-glycol fluids. The excellent anti-wear properties of CITGO Glycol FR fluids have been well demonstrated in actual field performance and in laboratory testing. The fluids meet all specifications of U.S. Steel Requirement No. 171 including the ASTM D psi pump test. The following chart compares CITGO Glycol FR fluids to other hydraulic fluids in this high pump. CITGO Glycol FR fluids offer the maximum wear protection available in a water-glycol hydraulic fluid. COMPATIBILITY WITH OTHER WATER-GLYCOLS CITGO Glycol FR fluids are compatible with and miscible in other water-glycol fire resistant fluids. This assumes that the competitive fluid has been adequately maintained with the proper amount of water and rust inhibitor and is reasonably free of contamination. It is highly recommended that all systems containing a competitive water-glycol fluid be laboratory tested by CITGO prior to installing CITGO Glycol FR fluids. These fluids will be tested for the following properties: 1. Water Content 2. Rust Inhibitor Level 3. Viscosity 4. Dirt Level 5. Particle Size Reference Information Your CITGO representative will be glad to initiate this work including all necessary sample containers, labels, etc. SYSTEM CONVERSION When converting a system to CITGO Glycol FR fluids from either a conventional mineral oil based fluid or another type of fire resistant or synthetic fluid, it is important that the following procedures be used. Compliance with these conversion procedures will permit the changeover to proceed with minimum difficulty and will extend the service life of the fluid. 1. Make absolutely sure that the pump on the equipment is suitable for water-glycol service. Consult the manufacturer. 2. Completely drain all fluid from the sump, lines, coolers, actuators, etc. Wipe clean. 241

250 3. Remove any interior paint which is not compatible with water-glycol type fluids. Sand blast sump interior down to white metal and apply water-glycol compatible paint system. 4. Replace any seals or O rings which are not generally recommended for waterglycol fluids. 5. Reconnect lines, accumulators, coolers, etc., using either Teflon pressure tape or a suitable pipe joint compound. Make sure any grease used is water resistant. 6. Replace any filters which are not suitable for water-glycol service. If there is any doubt, the filter supplier should be contacted for recommendations. 7. Install a mesh strainer on the pump inlet. Usually a 60-mesh screen is adequate. DO NOT PUT A FILTER ON THE PUMP INLET. Due to the high bulk density of waterglycol fluids and the resultant suction lift demands, the pump inlet must never be restricted without prior discussion with the pump manufacturer. Cavitation can result from a restricted pump inlet. Reference Information 8. When converting from a conventional petroleum fluid, perform step 2, fill system with CITGO Glycol FR fluid to a minimum level to maintain pump suction and operate the system for 30 minutes at reduced pressures. When converting from a synthetic type or oil-synthetic fluid, first perform step 2, then pre-flush the system with a light, straight mineral oil. Repeat step 2 and then flush with CITGO Glycol FR fluid. 9. Drain system immediately and fill to operating level with CITGO Glycol FR fluid. 10. Where a system already contains another water-glycol fluid, it is permissible to start using CITGO Glycol FR fluid directly as makeup providing the existing fluid is of an acceptable cleanliness level and contains the proper amount of water and rust inhibitor. Prior to adding CITGO Glycol FR fluid to a system containing another water-glycol fluid, it is strongly recommended that the fluid in the system first be analyzed by CITGO s laboratory. Your CITGO representative will furnish all necessary bottles, labels, etc., to facilitate this testing. 11. Start up the system and slowly bring it up to normal operating system pressure and conditions. 12. Periodically check filters and strainers for the first few weeks of operation. These components could get clogged with sludge and deposits resulting from the flushing of the system fluid. If the system has been changed from an oil or synthetic type fluid, the CITGO Glycol FR fluid may take on a pink, milky appearance. This is normal and will occur with any water-glycol fluid. This is due to slight emulsification of oil or synthetic fluid left in the system after flushing. Normally this emulsion will break, allowing free oil to be skimmed from the surface in the sump if it is mineral oil or drained from the bottom if it is a synthetic. 242

251 TOXICITY AND HANDLING CITGO Glycol FR fluids contain no nitrosamines or other established or suspected carcinogens. CITGO Glycol FR fluids contain diethylene glycol. Should either of these products be ingested or swallowed, vomiting should be induced immediately, and a physician should be contacted at once. Breathing of the vapors should be avoided. These products could cause skin irritation or sensitization in some humans so it is recommended that plastic or rubber gloves be utilized in handling. After handling, washing with soap and water is recommended. CITGO Glycol FR fluids contain a basic amine type corrosion inhibitor. Compounds of this type will cause eye irritation. In case of contact, rinse the eyes with large amounts of cool water and contact a physician at once. CITGO Glycol FR fluids are slippery liquids and spills constitute a definite safety hazard. Small spills should be cleaned up immediately by either washing or hosing with water or by treating the affected area with commercially available spill absorbents. Large spills must be treated like a petroleum spill. SEAL AND O RING COMPATIBILITY CITGO Glycol FR fluids can be operated with a wide variety of seal and gasket materials. Elastomers such as natural rubber, Buna N, Buna S, and Neoprene are unaffected by the fluid. Materials such as Viton, Teflon, and other similar types are also satisfactory. The only seal and gasket configurations not acceptable are leather, cork, cellulose, or other substances which will absorb water and either swell or deteriorate as a result. Reference Information RESERVOIR PAINTS AND COATINGS All water-glycol type fluids will tend to dissolve or deteriorate many conventional paints and coating systems commonly used in sumps and reservoirs. When converting any system over to CITGO Glycol FR fluids, any paint or coating used in the system which is known to be incompatible with water-glycol systems should be removed and replaced with a coatings system which is compatible with water-glycols. Several of the leading paint suppliers manufacture systems which are acceptable for water-glycol usage. These suppliers should be contacted for application and paint types to be used. 243

252 PIPE JOINT COMPOUNDS AND GREASES CITGO Glycol FR fluids and all other water-glycol fluids may tend to dissolve or soften certain pipe thread dopes. It is recommended that either Teflon pressure tape or pipe compounds which have water-glycol compatibility be used. The use of soda based greases in and around hydraulic circuits should be avoided due to their propensity to emulsify with water-glycol fluids. Grease selection should be restricted to greases having good water tolerance such as lithium, calcium, or aluminum complex. WATER CONTROL AND MAKEUP It is necessary to maintain the water level of CITGO Glycol FR fluids within acceptable limits. Excessive water reduces the fluid s viscosity and its ability to lubricate and to seal internal pump clearances. The latter leads to fluid backwash. Insufficient water will render the fluid non-fire resistant as well as raise its viscosity and bulk density, both of which will contribute to pump cavitation. Reference Information Three acceptable methods may be used to control the water level of CITGO Glycol FR fluids: 1) indirectly by viscosity determination, 2) by refractometer of Brix reading and 3) directly by laboratory methods using the Karl Fischer titration. The water level of CITGO Glycol FR fluids cannot be determined by distillation procedures. The viscosity approach is not applicable to systems containing more than trace amounts of oil or systems where the fluid is not predominantly CITGO Glycol FR fluid. Portable viscosity gauges are available at nominal costs to determine viscosity at machine-side. It is important that the gauges be standardized for CITGO Glycol FR fluid. The following tables can be used with acceptable accuracy to determine the amount of water required to adjust the fluid to acceptable limits. Only distilled, deionized, or controlled boiler feed water should be used as makeup. The use of hard tap water, well or spring water should be avoided since the dissolved minerals in these waters will react with the additive system in the fluid causing fluid haziness and formation of soap-like insoluble material. Never use water that has been processed through a water softener. 244

253 BRIX READINGS VS. % WATER AND VISCOSITIES FOR CITGO FR WG-40XD This chart is only valid when the system contains all CITGO FR WG-40 XD BRIX VISCOSITY (SUS) AT 100 F CITGO FR WG-40XD WATER ADJUSTMENT CHART VISCOSITY (cst) AT 40 C PERCENT WATER IN UNADJUSTED FLUID GALLONS OF WATER NEEDED PER 100 GALLONS OF UNADJUSTED FLUID IN SYSTEM NORMAL CONDITION MODERATE LEVEL SEVERE LEVEL Reference Information Excess Water Excess Water 245

254 BRIX READINGS VS. % WATER AND VISCOSITIES FOR CITGO GLYCOL FR-5046HP This chart is only valid when the system contains all CITGO Glycol FR HP Reference Information BRIX # % WATER VIS. cst 40 C VIS. SUS 100 F WATER ADJUSTMENT PER 100 GALLONS OF FLUID OK OK OK OK OK Fluid with viscosity below 31.6 cst at 40 C or Brix readings below 42.0 contain excess 246

255 water and only new CITGO Glycol FR-5046HP should be used as makeup. Only distilled, deionized, or steam condensate water should be used. For larger or smaller systems than 100 gallons use appropriate multiples or fractions for water addition based on the actual amount of fluid in the system. ALKALINITY CONTROL CITGO Glycol FR fluids contain alkaline corrosion inhibitors. The fluids are blended to contain a surplus of the additive which is called the alkaline reserve. The inhibitors will slowly evaporate from the fluid which gives vapor phase protection. The hotter the system operating temperature, the greater the evaporation loss. The inhibitor loss usually goes hand in hand with the water evaporation loss. As a rule of thumb, if system operating temperatures are maintained at 120 F or lower, and a normal amount of new CITGO Glycol FR fluid is being added as makeup, no alkaline adjustment will be necessary. Conversely, in systems running at higher temperatures, the inhibitor loss may occur at a greater rate than normal new fluid makeup can replenish. When this occurs, a portion or all of the fluid may require replacement. The amount of inhibitor in CITGO Glycol FR fluid is a measurement of the alkaline content of the fluid. It is defined technically as the number of milliliters of 0.1N hydtrochloric acid necessary to neutralize 100 ml of fluid to a ph of 5.5. This can only be determined by a laboratory titration. The normal alkaline reserve of new CITGO Glycol FR fluid ranges from 160 to 180 ml of 0.1N hydrochloric acid required to neutralize 100 ml of the fluid to the ph of 5.5. It is safe to continue to use CITGO Glycol FR fluid so long as the alkaline content does not fall below 120 in the titration. Reference Information If the user of CITGO Glycol FR fluid suspects his inhibitor loss may be excessive due to high operating temperatures and lacks the laboratory equipment necessary to check the alkaline reserve, the CITGO representative will arrange for sampling of systems and a CITGO laboratory analysis of the fluids. GOOD FLUID MAINTENANCE CITGO Glycol FR fluids will retain their optimum fire protection, impart excellent resistance against rusting and corrosion, and prolong the service life of hydraulic components only with good fluid maintenance. Proper water content assures fire resistance. Maintaining the alkaline reserve gives maximum corrosion protection. Proper filtration of dirt and sludge is essential for a well maintained fire resistant fluid. CITGO has provided the consumer with superior products in CITGO Glycol FR fluids. Poor or inadequate fluid maintenance will result in reduced fluid performance and can certainly lead to reduced or lost production and costly downtime. 247

256 CITGO Technical Bulletin Water Glycols Compatibility Water-glycol fluids are excellent fire-resistant fluids. They are normally used in applications where there is the possibility of exposure of the fluid to high temperatures or open flames. They can be used at lower ambient temperatures where fluids are likely to be subjected to cold weather. However, these fluids should not be used where bulk fluid temperatures will exceed 150 F, as the water evaporation will result in an increase in viscosity as well as the loss of fire resistance. Water-glycol fluids are compatible with standard seals, but may react with certain metals. Care must be taken with pump choices or where pump limitations are suitable and require no boundary lubrication. Reference Information MATERIAL COMPATIBILITY MATERIAL FR-40 XD FR-5046HP INVERT EMULSIONS HWCF PHOSPHATE ESTERS POLYOL ESTERS OIL SYNTHETICS Elastomer, Neoprene Y Y Y N N N Elastomer, Buna N Y Y Y N Y N Elastomer, Butyl Y N Y Y N N Elastomer, E.P.R. Y N Y Y N N Elastomer, Polyurethane * * * N Y N Elastomer, Silicone Y Y Y Y Y Y Elastomer, Teflon Y Y Y Y Y Y Elastomer, Viton Y Y Y Y Y Y Filter Media, Cellulosic, Phenolic Treated Y Y Y Y Y Y Filter Media, Fiberglass Y N Y Y Y Y Metals, Ferrous Y Y Y Y Y Y Metals, Bronze * 1 Y * 1 Y * 1 Y Metals, Zinc N Y N Y Y Y Metals, Cadmium N Y N Y Y Y Metals, Lead N N N Y N Y Metals, Brass, Copper Y Y Y Y Y Y Metals, Aluminum, Unanodized N Y N Y Y Y Metals, Aluminum, Anodized Y Y Y Y Y Y Y = Compatible * = Low or marginal compatibility N = Not compatible 1Bronze with lead content over 20 percent limited to 120F 248

257 COMPARATIVE VISCOSITY CLASSIFICATIONS ISO Viscosity Grade C Min. cst Max. cst F No Requirement* Min. SUS Max. SUS Vis. No 100 C Min. cst Max. cst AGMA Lubricant Number C Min. cst Max. cst F No Requirement* Min. SUS Max. SUS C No Requirement* Min. cst Max. cst *Viscosities given are not required; however, for informational purposes, viscosities listed are calculated assuming an oil with V.I. of 95. Reference Information 249

258 Viscosity Blending Chart Instructions Example: Determine the relative viscosities, at a common temperature, of the two base oils to be blended. Base oil 1: 30cst at 40C Base oil 2: 100cst at 40C Draw a line between the viscosity values of the two components. A vertical line is then drawn to indicate the percentage of the Higher Viscosity component and Lower Viscosity component to intersect this line. At the intersection, draw a horizontal line to the viscosity scale. This will indicate the viscosity of the combination of the two components. In the example above, the lighter product is Base oil 1 (30cst) while the higher viscosity product Base Oil 2 (100cst). We could obtain 60cst at 40C with a 55/45 blend of Base oil 2 and Base oil 1. Reference Information 250

259 Lower Viscosity Components, Centistokes (cst) Higher Viscosity Components, Centistokes (cst) Reference Information 251

260 Reference Information P Steels M Stainless Steels K Cast Iron N Non Ferrous S HRSA H Hard Metals Materials Indexable tooling Plain Steels CITCOOL SS HD Low Alloy CITCOOL SS HD High Alloy CITCOOL SS HD Steel Castings CITCOOL SS HD Aluminum alloys, Copper alloys Heat Resistance, Super Alloys (nickelbased) High Hardness alloys, work Hardening Alloys CITCOOL SS HD CITCOOL SS HD TRUKUT HD220 TRUKUT GP205 CITCOOL 33 CITCOOL SS HD CITCOOL 33 CITCOOL SS HD Metalworking Product Application Guide - Water Miscible Products Drilling HSS CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD TRUKUT HD220 CITCOOL 33 CITCOOL SS HD CITCOOL 33 CITCOOL SS HD Deep Hole Drilling CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD TRUKUT HD220 CITCOOL 33 CITCOOL SS HD CITCOOL 33 CITCOOL SS HD Operation Cut Tap Form Tap End milling Reaming Hobbing Sawing Grinding CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD TRUKUT HD220 CITCOOL 33 CITCOOL SS HD CITCOOL 33 CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD TRUKUT HD220 CITCOOL 33 CITCOOL SS HD CITCOOL 33 CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD TRUKUT HD220 TRUKUT GP205 CITCOOL 33 CITCOOL SS HD CITCOOL 33 CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD TRUKUT HD220 CITCOOL 33 CITCOOL SS HD CITCOOL 33 CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD TRUKUT HD220 CITCOOL 33 CITCOOL SS HD CITCOOL 33 CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD CITCOOL SS HD TRUKUT HD220 TRUKUT GP205 CITCOOL 33 CITCOOL SS HD CITCOOL 33 CITCOOL SS HD TRUKUT GP205 TRUKUT GP205 TRUKUT GP205 TRUKUT GP205 TRUKUT GP205 TRUKUT GP205 TRUKUT GP205 TRUKUT GP205 TRUKUT GP205 The product recommendations on this chart are general guidelines. Consult the CITGO Product Answer Line with details of your specific operation and metallurgy. CITGO never recommends mixing competitive metalworking products with CITGO metalworking products. Some product changes may require sampling of the existing fluid and extensive cleaning and flushing of the system. 252

261 Metalworking Product Application Guide - Straight Oils P Steels M Stainless Steels K Cast Iron N Non Ferrous S HRSA H Hard Metals Materials Screw Machine Operations Plain Steels AUTOKUT TRI-PURPOSE Low Alloy AUTOKUT TRI-PURPOSE High Alloy AUTOKUT TRI-PURPOSE Steel Castings AUTOKUT TRI-PURPOSE Aluminum alloys, Copper alloys Heat Resistance, Super Alloys (nickelbased) High Hardness alloys, work Hardening Alloys AUTOKUT TRI-PURPOSE AUTOKUT TRI-PURPOSE AUTOKUT TRI-PURPOSE AUTOKUT TRI-PURPOSE AUTOKUT TRI-PURPOSE Swiss Machining Operations AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT IS Series AUTOKUT AS Series AUTOKUT AS Series Deep Hole / Gun Drilling AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT IS Series AUTOKUT AS Series AUTOKUT AS Series Operation Thread Forming AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT IS Series AUTOKUT AS Series AUTOKUT AS Series Gear Hobbing Gear Shaping Grinding AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT IS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT IS Series AUTOKUT AS Series AUTOKUT AS Series AUTOKUT IS 15 AUTOKUT IS 15 AUTOKUT IS 15 AUTOKUT IS 15 AUTOKUT IS 15 AUTOKUT IS 15 AUTOKUT IS 15 AUTOKUT IS 15 AUTOKUT IS 15 The product recommendations on this chart are general guidelines. Consult the CITGO Product Answer Line with details of your specific operation and metallurgy. CITGO never recommends mixing competitive metalworking products with CITGO metalworking products. Some product changes may require sampling of the existing fluid and extensive cleaning and flushing of the system. Reference Information 253

262 Metal Removal Product Offering Product Type Citgo Products Typical Applications Market Share Straight oils Autokut IS Multiple metals 19% Autokut AS Ferrous alloys Autokut Tri-Purpose Screw Machine Soluble Oils Trukut GP 205 Multi-metal GP 28% Trukut HD 220 Multi-metal HD Semi-Synthetics CITCOOL SS HD Fe and most AL 29% Synthetics CITCOOL 33 Concentrate Ferrous applications 24% Reference Information Metallurgy and Machinability Ferrous Nonferrous Ferrous Nonferrous Ferrous Nonferrous (>100%) (100-70%) (70-50%) (50-40%) (<40%) (<100%) Most Wrought 1112* xx, 2330, 2340 Most Stainless Titanium Aluminums Steels Most Cast , 31xx, 41xx 2512, , 3310 Ti-5Al-2.5Sn Aluminums Leaded Brass , 4340, 48xx 50100, 51100, Ti-6Al-4V Magnesium Alloys 4023, 4024, xx, 46xx, 51xx 61xx, 8645, Ti-6Al-6V-2Sn Zinc Cast Steel 86xx, 87xx 8750, 9445 Tool Steel Ti-8Al-1Mo-1V Silicon Bronze Cast Iron 91xx, 98xx 1008, 1010, 1015 Ti-8Mn Brass Stainless Iron Ductile Iron 1050, 1070 Ti-13V-11Cr-3Al 3310, 18-8 Nickel Wrought Iron Copper *Machinability rating is determined by normal cutting speed, surface finish, and tool life. Ratings are normalized to the machinability of B1112 steel, which has been benchmarked as 100% by the American Iron and Steel Institute. Metals with a rating lower than 100% are less machinable than B1112; metals with a rating greater than 100% are more machinable than B

263 Stationary Natural Gas Engine Oil Cross Reference Pacemaker GEO 1940XL Pegasus 1005 HDAX 7200 LA, HDAX 9200 LA El Mar LA 4 EXD No Product Pacemaker GEO 1740 Pegasus 905 HDAX 5200 LA El Mar LA 4 Mysella S5 N40 Pacemaker GEO 1640 Pegasus 805 HPLX 3200 LA 40 El Mar Low Ash Mysella S3 N40 Pacemaker LFG LA 40 Pegasus Ultra 605 HDAX LFG 6500 No Product No Product Pacemaker GEO 740 Pegasus 710 HDAX 5300 MA 40 El Mar Mid Ash Mysella S3 S Pacemaker GEO 1000 Pegasus 701 HDAX 3100, Ashless El Mar Ashless, Heavy Duty Pacemaker GEO 1200 Pegasus 701 HDAX 5100, Ashless El Mar Ashless, Supreme Mysella S2 Z Mysella S2 Z All recommendations set forth herein are based solely upon information and materials available at the time of publication. CITGO Petroleum Corporation makes no representations or warranties of any kind regarding the completeness or current accuracy of its competitors information set forth herein. Competitor formulations, claims, and approvals are subject to change without notice. All trademarks other than CITGO and Pacemaker are registered trademarks of their owners, which are not affiliated with CITGO. Reference Information 255

264 Reference Information CITGO STATIONARY NATURAL GAS COMPRESSOR LUBRICANT CHART BETTER COLD CLIMATE FLOW ANTI-EMULSION FORMULA HIGH MOISTURE GAS HYDROCARBON DILUTION RESISTANT SOUR GAS SWEET GAS COMPRESSOR OIL 4 STROKE GAS ENGINE OIL ATTRIBUTE PACEMAKER 1640AE X X X X COMPRESSORGARD PAG X X X X X X X CITGEAR SYNTHETIC PAG X X X X X X X COMPRESSORGARD PAO X X X X X X X CITGEAR SYNTHETIC HT X X X X X X X COMPRESSOR OIL 35LP, 45LP X X X X X PACEMAKER OILS 100, 150, 220 X X X X CYLINDER OIL 150-5, X X X X X COMPRESSORGARD XA200 X X X X CITGO STATIONARY NATURAL GAS COMPRESSION APPLICATION CHART MID ASH, % LOW ASH, % ASHLESS, <0.1% CATALYST COMPATIBLE EXTENDED OIL LIFE CAPABILITY HIGH OXIDATION CONDITIONS HIGH NITRATION CONDITIONS ANTI- EMULSION ENGINE & COMPRESSOR OIL FORMULATED FOR LFG/ BIOGAS SOUR GAS SWEET GAS 4 STROKE GAS ENGINE OIL 2 STROKE GAS ENGINE OIL Product Low Ash PACEMAKER GEO 1900XL X X X X X X X X PACEMAKER GEO 1700 X X X X X X X X PACEMAKER GEO 1600 X X X X X PACEMAKER GEO 800 X X X X X X X X PACEMAKER GEO LFG LA X X X X X X X PACEMAKER 1640AE X X X X X X Mid Ash PACEMAKER GEO 700 X X X X X X Ashless PACEMAKER GEO 1000 X X X X PACEMAKER GEO 1200 X X X X 256

265 Pacemaker GEO Application Chart ENGINE/MANUFACTURER STROKE PER CYCLE PACEMAKER GEO LFG LA PACEMAKER GEO 700 PACEMAKER GEO 800 PACEMAKER GEO 1000 PACEMAKER GEO 1200 PACEMAKER GEO 1600 PACEMAKER GEO 1700 PACEMAKER GEO 1900XL CATERILLAR GCM34 4 X X X X G X X X X G X X X X G X X X X G X X X X X X MWM TCG SERIES, NATURAL GAS 4 X X X X MWM TCG SERIES, BIOGAS 4 X PERKINS, NATURAL GAS 4 X X X X PERKINS, BIOGAS 4 X FAIRBANKS MORSE 2 X X GENERAL ELECTRIC JENBACHER, NATURAL GAS 4 X X X JENBACHER, BIOGAS 4 X WAUKESHA VGF F18, H24, L36, P48 4 X X X X G, GL, GLD WAUKESHA VGF GSI, GSID 4 X X X X WAUKESHA VHP F3521, L5790, L7042, 4 X X X X X P9390 G, GSI, GL WAUKESHA VHP F3514, F3524, L5794, 4 X X X X L7044, GSI, L5774, L5794, LT WAUKESHA VHP 5794, 7044GSI WITH 4 X X X X FACTORY SUPPLIED CATALYST WAUKESHA 275 GL/GL+ 12V, 16V 4 X X X X X WAUKESHA APG 16V150LTD 4 X X X X WAUKESHA APG 12V220GL, 4 X X X X 18V220GL WAUKESHA COGENERATION 4 X X X X WAUKESHA BIOGAS 4 X SUPERIOR 825, 12SGTD, 16SGTD 4 X X X X AJAX DPC 140LE, 180LE, 280LE, 2 X X 360LE, 540LE, 720LE, 2200LE SERIES,2800LE SERIES, C 302, E 565 MTU All recommendations set forth herein are based solely upon information and materials available at the time of publication. CITGO Petroleum Corporation makes no representations or warranties of any kind regarding the completeness or current accuracy of its competitors information set forth herein. Competitor formulations, claims, and approvals are subject to change without notice. All trademarks other than CITGO and Pacemaker are registered trademarks of their owners, which are not affiliated with CITGO. Reference Information 257

266 Reference Information Pacemaker GEO Application Chart ENGINE/MANUFACTURER STROKE PER CYCLE PACEMAKER GEO LFG LA PACEMAKER GEO 700 PACEMAKER GEO 800 PACEMAKER GEO 1000 PACEMAKER GEO 1200 PACEMAKER GEO 1600 PACEMAKER GEO 1700 PACEMAKER GEO 1900XL 4000L61 / L62 / L63 4 X X X 4000 L32 / L33 4 X X 4000 L64 4 X SIEMENS DRESSER RAND CATEGORY I 4 X X X X DRESSER RAND CATEGORY II 4 X X X X DRESSER RAND CATEGORY III 4 X X X X GUASCOR 4 X X X X CLARK 2 X X WORTHINGTON, 2 STROKE 2 X X WORTHINGTON, 4 STROKE 4 X X X X WÄRTSILÄ 4 X X X X All recommendations set forth herein are based solely upon information and materials available at the time of publication. CITGO Petroleum Corporation makes no representations or warranties of any kind regarding the completeness or current accuracy of its competitors information set forth herein. Competitor formulations, claims, and approvals are subject to change without notice. All trademarks other than CITGO and Pacemaker are registered trademarks of their owners, which are not affiliated with CITGO. 258

267 CITGO Technical Bulletin EPA amendments to the NESHAP for stationary reciprocating internal combustion engines (RICE) On January 14, 2013, the Environmental protection Agency finalized amendments to the National Emissions Standards for Hazardous Air Pollutants (NESHAP) for stationary reciprocating internal combustion engines (RICE) and amendments to the NSPS (New Source Performance Standards) applicable to Stationary Engines. These final amendments address several issues affecting RICE engine owners and operators. The full compliance date for these rules was October 19th, 2013 for owners of Spark Ignition (SI) stationary engines. For reference, these rules are codified in the Federal Register at; 40 CFR Part 63 Subpart ZZZZ (NESHAP) 40 CFR Part 60 Subpart JJJJ (NSPS for SI engines) These final amendments have determined that certain classifications of SI engines typically used in sparsely populated areas for oil and gas production can comply with these rules by maintenance practices, instead of emissions based performance standards. This is in addition to SI engines that were previously eligible for compliance with maintenance practices. To determine whether your engine is eligible for compliance by maintenance practices, please contact your EPA compliance representative. Reference Information One of the requirements of compliance by maintenance practices is that the owner/ operator change oil every 1440 or 2160 hours, depending on engine size. Drains can be extended beyond 1440 or 2160 hours, if the operator can provide supporting oil analysis records that the oil remains within the EPA s condemning limits; Total Acid Number (TAN) Increase of 3.0 mgkoh/g from TAN when oil is new Viscosity Change of ±20% from new oil viscosity %Water Content (By Volume) Greater than 0.5% 259

268 As per the rules referenced the previous table; Oil analysis must be performed and conducted at the same frequency specified for oil changes. If the oil is condemned, the oil must be changed within 2 business days. The operators or the owners must keep the records of all the oil analysis. The EPA s condemning limits are relatively wide and CITGO encourages engine owners/ operators to also keep in consideration the engine manufacturer s recommendations for oil change limits. CITGO s GEO LubeAlert oil analysis program for natural gas engine oils includes a number of important tests that can aid in NESHAP compliance as well as provide early detection of critical equipment issues. CITGO has anticipated your extra testing needs, and we stand ready to assist our LubeAlert users with the EPA requirements referenced above. Reference Information Please contact our Product Answer Line at with any additional questions. 260

269 CITGO SENSITIVE PRODUCT LIST The following list contains products which CITGO has determined are sensitive in nature. Repackaging of the products on this list is either prohibited, or requires CITGO approval. The reprinting of labels and other material is also prohibited or subject to approval. CITGO GREASES The repackaging of CITGO greases requires approval from Technical Services. The reprinting of CITGO grease labels and other material also requires approval. CITGO INDUSTRIAL FLUIDS The following CITGO Industrial fluids are prohibited from repackaging and the printing of labels and other material: CITGO HyDurance AW CP Fluid CITGO FR WG-40XD Hydraulic Fluid CITGO Glycol FR-5046HP The following CITGO Industrial fluids require Technical Services approval before repackaging or the printing of labels and other materials: CITGO HyDurance AW NZ Fluids CITGO HyDurance AW Super NZ Fluids CITGO HyDurance AW Synthetic Fluids Reference Information CITGO INDUSTRIAL GEAR OILS The following CITGO Industrial Gear Oils require Technical Services approval before repackaging or the printing of labels and other materials: CITGO CITGEAR OGL-A CITGO CITGEAR MGW-OGL CITGO CITGEAR SYNTHETIC EP LUBRICANTS CITGO CITGEAR SYNTHETIC HT LUBRICANTS CITGO CITGEAR SYNTHETIC PAG GEAR FLUIDS CITGO EP GEAR SEMI-SYNTHETIC 68 CITGO CITGEAR WT

270 CITGO SMALL ENGINE OILS The repackaging of CITGO Small Engine Oils requires approval from Technical Services. The reprinting of CITGO Small Engine Oils labels and other material also requires approval. CITGO AUTOMOTIVE GEAR OILS The following CITGO Automotive Gear Oils are prohibited from repackaging and the printing of labels and other material: CITGO Synthetic Gear Lubricants The following CITGO Automotive Gear Oils require Technical Services approval before repackaging or the printing of labels and other materials: CITGO CITGEAR Synthetic HD Gear Lubricants CITGO ENGINE OILS (PCMO) The following CITGO Engine oils (PCMO) require Technical Services approval before repackaging or the printing of labels and other materials: CITGO SUPERGARD Synthetic Motor Oils Reference Information CITGO ENGINE OILS (HDEO) The following CITGO Engine oils (HDEO) require Technical Services approval before repackaging or the printing of labels and other materials: CITGO CITGARD SynDurance PLUS Synthetic Heavy Duty Engine Oils CITGO TRANSMISSION/POWER FLUIDS The following CITGO Transmission / Power fluids are prohibited from repackaging and the printing of labels and other material: CITGO TRANSGARD ATF, MERCON V CITGO TRANSGARD ATF +4 CITGO TRANSGARD DEXRON -VI ATF The following CITGO Transmission / Power fluids require Technical Services approval before repackaging or the printing of labels and other materials: CITGO QuatraSyn Synthetic Transmission Fluid CITGO SynDurance All Seasons Heavy-Duty Transmission Fluid CITGO TRANSGARD CVT Fluid CITGO TRANSGARD Multi-Vehicle High-Viscosity ATF CITGO TRANSGARD Synthetic Multi-Vehicle Low-Viscosity ATF 262

271 CITGO RAILROAD LUBRICANTS The following CITGO Railroad lubricants require Technical Services approval before repackaging or the printing of labels and other materials: CITGO Railroad Car Journal Oil No. 9 CITGO RD-969 & RD-1069 Diesel Engine Oil CITGO RD-2069 LE Diesel Engine Oil CITGO FUNCTIONAL PRODUCTS The following CITGO Functional products require Technical Services approval before repackaging or the printing of labels and other materials: CITGO Press Oil 68 CITGO SATISOL Concrete Form Release CITGO Wireline Lubricants CITGO Ice Machine Oil 68 CITGO North Star Refrigeration Oils CITGO Pacemaker HV Oils CITGO METALWORKING FLUIDS All CITGO METALWORKING Fluids require Technical Services approval before repackaging or the printing of labels and other materials. CITGO INDUSTRIAL GAS ENGINE OILS All CITGO Industrial Gas Engine Oils require Technical Services approval before repackaging or the printing of labels and other materials. Reference Information CITGO COMPRESSOR LUBRICANTS The following CITGO Compressor lubricants require Technical Services approval before repackaging or the printing of labels and other materials: CITGO CompKleen Synthetic Cleaner CITGO CompressorGard DE CITGO CompressorGard GE CITGO CompressorGard H CITGO CompressorGard IPG CITGO CompressorGard PAG CITGO CompressorGard PAG 150 VR CITGO CompressorGard PAO CITGO CompressorGard PS Fluids CITGO CompressorGard SS CITGO Pacemaker ST

272 GHS Label Compliance was required by June 1, 2015 In order to meet the requirements of the new U.S. OSHA Hazard Communication regulations that have adopted the Globally Harmonized System (GHS) of classification and labeling of chemicals, CITGO is making changes to workplace labels for containers that hold five or more gallons, or 35 or more pounds, including pails, kegs, and drums. Reference Information How does this affect you? All marketers who have a CITGO repackaging agreement and print product shipping labels require a specific color printer and compliant labels. The required CITGO printer is the Lexmark C792E and can be purchased along with the new labels through Jeff VanDonsel at Reliance, ext You can also order labels on MarketNet under Account Management>>Product Labels>>Print GHS Labels. 264

273 CITGO Technical Bulletin Lubricant Storage Five Key Lubricant Storage Tips 1. Keep it clean 2. Keep it cool 3. Keep it dry 4. Know how to spot contamination/storage instability 5. Practice FIFO (first in, first out) 1. Keep it clean Contamination sources: - Air, airborne particle & water ingression - Dirty transfer containers/equipment Label transfer containers and funnels (consider color coding) and keep them as specific as possible (engine, hydraulic, etc). Containers should be sealable! Reference Information Use separate pumps for separate types of products and flush well with the next product. Keep clean rags, sampling equipment, small containers in a storage cabinet. Keep drums indoors if possible, with a desiccant breather in humid environments. Outdoor drums: lie sideways on notched planks, keep bungs sealed & positioned at 3&9 o clock to prevent air entrainment through drum breathing. 2. Keep it cool Exposure to temperature extremes shortens shelf life by reducing effectiveness of some additives keep temperature moderate (32-77F optimal). 265

274 - Products containing water (emulsifiable cutting oils, fire resistant fluids) or fatty oils (cylinder oils, some cutting oils) should be kept above freezing to avoid component separation. - Avoid storage near heaters, ovens, etc. Avoid light exposure use the original container when possible. Temperature variation causes containers to breathe when they expand and contract (drawing in air, dirt and moisture). Reference Information (Image source: Noria Corporation) 3. Keep it dry Water contamination in oil reduces equipment and oil life through: - Excessive wear - Corrosion - Filter plugging - Oxidation - Additive depletion - Increased viscosity Pumps, transfer containers, funnels and any other equipment contacting lubricants must be dry. Lubricants absorb moisture from humid air and condensation. Keep containers out of washing areas. Drums will quickly rust through if stored on a damp surface elevation on planks or pallets is advised, whether indoors or out. 266

275 Outdoor drums must be covered with a shelter or tarp. Upright storage is not recommended for fluids, but if necessary use drum covers (preferred) or tilt the drum so water does not pool (less preferred). 4. Know how to spot contamination/storage instability New oil should be bright and clear. Milky appearance: water contamination Significant color change from new oil: possible oxidation or oil mixing Haze or significant sediment: possible particulate contamination Gel or sticky liquid at bottom: additive settling Significant change in odor: oxidation or bacteria Normal oil aging: - Gradual color change - Minor settling of additives - Oil separation on grease surface (okay to discard oil; store cartridges upright to minimize separation) 5. Practice FIFO (first in, first out) To minimize exposure to harmful environmental conditions, use first in/first out inventory practices, especially for drums. Label containers with the date received. Reference Information Follow the manufacturer s guidelines for shelf life. Does your CITGO container still have a batch code? The CITGO Answer Line can help you determine when the product was manufactured. - Format: 4-5 numbers, letter (usually C or O), 4 numbers (Ex: 02351C2344) - Call or or Photos welcome. 267

276 CITGO Technical Bulletin How to Take a Sample The Sample: Oil samples should be representative of the system from which they are taken. This can be accomplished by following a few simple procedures. 1. Ideally the equipment being sampled should be brought to operating temperature prior to collecting the sample. This will assure that any insoluble and semi-soluble materials are suspended evenly throughout the system. Samples taken from equipment that has been inactive for long periods are not representative. Reference Information 2. If possible, take the sample while the machine is in operation, from an area where the oil is flowing before the filter. 3. Do not collect a sample from a reservoir shortly after an oil change or the addition of a large amount of makeup oil. 4. Samples for ongoing analysis should always be taken in the same manner and from the same point. 5. Do not take samples from the fluid surface or from the very bottom of the reservoir unless you desire identification of a contaminant layer occurring there. 6. Always use a clean, dry container provided by CITGO. Make sure contamination does not enter the container while the sample is being taken. Dust and rain storms can cause misinterpretations. 7. Grease samples must also be representative of the system from which they are taken. A clean scoop or paddle may be used to transfer the grease to a suitable container for shipping. 8. Completely fill out the identification form. It is important to note all fields. Hours on the oil and make up oil will determine the severity of the wear metal results. The oil must be properly identified. Add a note if the sample was taken under special circumstances, such as from the oil filter or after failure. 9. Send in the sample promptly. Do not save samples to send in multiple samples together. If there are critical problems you will receive notification. 10. Follow up on any recommendation that is made by the report. No action may be the 268

277 correct follow up. An employee trained to monitor the results and the process is a very valuable asset. Sample Container: Use appropriate containers provided by the CITGO Product Technology Laboratory to avoid contamination. Store them in a clean, dry place until ready to use them. These can be provided to you by your Territory Sales Manager or your Technical Representative. Sampling Methods Sample (vacuum) Gun Method Used correctly, a sample gun or vampire allows the user to draw representative oil samples quickly and with a minimum amount of effort. Measure a sufficient length of new clean tubing to reach from the gun into the equipment s sump or reservoir. Since the tubing is supplied in coils, it may be necessary to straighten it. If the unit has a dipstick, the tubing should be measured against the dipstick to assure proper length. Note: Install new tubing after each use to avoid sample cross contamination. Good practice dictates the use of a new length of tubing for each sample. If you run out of tubing or for some other reason must use the tubing again, flush it once Loosen the nut on the sample gun head, insert one end of the tubing through the nut to about 1/2 inch past the threaded part of the gun head and tighten the nut. Screw a clean bottle into the gun adapter. Reference Information Holding the pump upright, fill the bottle to within 1/2 inch of the top. Beak the vacuum by partially unscrewing the bottle or using the vacuum button. Remove the bottle, screw the cap on flush it and wipe the bottle clean. Fill out the bottle label and affix it to the bottle. Sample Valve/Petcock Method Care should be taken to install the valve at the proper point in the lube system. (Consult equipment dealer or manufacturer.) If the valve or petcock outlet is internally threaded, a pipe plug should be installed; if externally threaded, a cap should be installed or the valve handle secured to prevent accidental opening and loss of fluid during operation. This will also keep out dirt and debris. The valve exterior and area around it should be wiped or brushed clean prior to drawing a sample. Drain about one quart of fluid into a clean container to later be discarded back into the reservoir or waste oil tank. This procedure clears the valve of sediment or stagnant fluid. Now catch your sample in a new clean, dry bottle, filling it to within 1/2 inch of the top. Screw the cap on tightly, wipe clean and attach the completed label. 269

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