Case 2:05-mc Document 1044 Filed 08/04/16 Page 1 of 35 IN THE UNITED STATES DISTRICT COURT WESTERN DISTRICT OF PENNSYLVANIA PITTSBURGH DIVISION

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1 Case 2:05-mc Document 1044 Filed 08/04/16 Page 1 of 35 IN THE UNITED STATES DISTRICT COURT WESTERN DISTRICT OF PENNSYLVANIA PITTSBURGH DIVISION UNITED STATES OF AMERICA, and the PENNSYLVANIA DEPARTMENT OF ENVIRONMENTAL PROTECTION, v. Plaintiffs, CONSOL Energy Inc., CNX Coal Resources LP, and Consol Pennsylvania Coal Company LLC, Defendants. ) ) ) ) ) ) ) ) ) ) ) Civil Ac No. COMPLAINT The United States of America ( United States ), by authority of the Attorney General of the United States and on behalf of the United States Environmental Protec Agency ( EPA ), and the Pennsylvania Department of Environmental Protec ( PADEP ) (collectively, Plaintiffs ), file this Complaint and allege as follows: INTRODUCTION 1. This is a civil ac brought pursuant to Sec 309(b) and (d) of the Federal Water Pollu Control Act ( Clean Water Act or the CWA ), 33 U.S.C. 1319(b) and (d), and Secs 601 and 605 of the Pennsylvania Clean s Law ( PCSL ), 35 P.S and Defendants have violated the CWA and the PCSL by discharging pollutants in viola of the condis and limitas of Naal Pollutant Discharge Elimina System ( NPDES ) permits issued pursuant to 33 U.S.C and 35 P.S and Plaintiffs seek permanent injunctive relief and civil penalties against Defendants to address their illegal discharges of pollutants, as authorized by Secs 309(b) and (d) of the CWA, 33 U.S.C. 1319(b) and (d), and 35 P.S and

2 Case 2:05-mc Document 1044 Filed 08/04/16 Page 2 of 35 JURISDICTION AND VENUE 3. This Court has jurisdic over the subject matter of this ac under Sec 309(b) of the Clean Water Act, 33 U.S.C. 1319(b), and under 28 U.S.C. 1331, 1345, 1355, and Venue is proper in the Western District of Pennsylvania pursuant to 28 U.S.C. 1391(b) and (c) and 1395(a), as well as Sec 309(b) of the Clean Water Act, 33 U.S.C. 1319(b), because it is the judicial district in which Defendants are doing business and in which the violas alleged in the Complaint occurred. 5. Notice of commencement of this ac has been given to Pennsylvania in accordance with Sec 309(b) of the CWA, 33 U.S.C. 1319(b). DEFENDANTS 6. CONSOL Energy Inc. ( Consol ) is a Delaware corpora with its principal place of business at CNX Center, 1000 Consol Energy Drive, Canonsburg, Pennsylvania CNX Coal Resources LP ( CNX ) is a Delaware corpora with its principal place of business at CNX Center, 1000 Consol Energy Drive, Canonsburg, Pennsylvania Consol Pennsylvania Coal Company LLC ( CPCC ) is a Delaware corpora with its principal place of business at 1000 Consol Energy Drive, Canonsburg, Pennsylvania STATUTORY AND REGULATORY REQUIREMENTS Clean Water Act 9. Sec 301(a) of the CWA, 33 U.S.C. 1311(a), prohibits the discharge of any pollutant by any person to waters of the United States, except, inter alia, in compliance with an 2

3 Case 2:05-mc Document 1044 Filed 08/04/16 Page 3 of 35 NPDES permit issued by EPA or an authorized state pursuant to Sec 402 of the CWA, 33 U.S.C Sec 402 of the CWA, 33 U.S.C. 1342, provides that the permit-issuing authority may issue an NPDES permit that authorizes the discharge of any pollutant to waters of the United States, upon the condi that such discharge will meet all applicable requirements of the CWA and such other condis as the permitting authority determines necessary to carry out the provisions of the CWA. 11. Sec 402(a)(2) of the CWA directs the Administrator to prescribe condis and limitas, including effluent limitas, for NPDES permits to assure compliance with the requirements of the CWA. 33 U.S.C. 1342(a)(2); see also 33 U.S.C Effluent limitas, as defined in Sec 502(11) of the CWA, 33 U.S.C. 1362(11), are restrics on quantity, rate, and concentra of chemical, physical, biological, and other constituents which are discharged from point sources. 12. Sec 301(b) of the CWA, 33 U.S.C. 1311(b), directs the Administrator to set effluent limitas for categories and classes of point sources based on the best practicable control technology or the best available technology economically achievable for such category or class. In 1985, EPA set effluent limitas guidelines ( ELGs ) for discharges from coal mining point sources. See 40 C.F.R. Part 434; 50 Fed. Reg (Oct. 9, 1985). The ELGs prescribe maximum for any 1 day and average of daily values for 30 consecutive days numeric effluent limits for, inter alia, iron, total suspended solids, ph, and manganese. Discharges with a ph above or below the range set forth in the applicable ELGs (generally within the range of 6.0 to 9.0 at all times) are violas of the daily maximum or daily minimum 3

4 Case 2:05-mc Document 1044 Filed 08/04/16 Page 4 of 35 limits in Defendants NPDES permits. 13. Sec 303(a) of the CWA, 33 U.S.C. 1313(a), requires that states adopt ambient water quality standards and establish water quality criteria for particular water bodies that will protect the designated uses of the water. When technology-based ELGs are insufficient to keep receiving waters within those levels, the NPDES permit must include stricter water quality based effluent limits that reflect water quality standards and criteria. 33 U.S.C. 1311(b)(1)(C); see also 25 Pa. Code Chapter 93 (Pennsylvania water quality standards). 14. Sec 309(b) of the CWA, 33 U.S.C. 1319(b), authorizes the Administrator to commence a civil ac for appropriate relief, including a permanent or temporary injunc, against any person who violates any permit condi or limita in a permit issued pursuant to Sec 402 of the CWA, 33 U.S.C Sec 309(d) of the CWA, 33 U.S.C. 1319(d), provides that any person who violates any permit condi or limita in a permit issued pursuant to Sec 402 of the CWA, 33 U.S.C. 1342, shall be subject to a civil penalty payable to the United States of up to $25,000 per day for each viola. 16. Pursuant to the Federal Civil Penalties Infla Adjustment Act of 1990, 28 U.S.C note, as amended by the Debt Collec Improvement Act of 1996, 31 U.S.C note, 69 Fed. Reg (February 13, 2004), 74 Fed. Reg. 626 (January 7, 2009), and 40 C.F.R. 19, EPA may seek civil penalties of up to $32,500 per day for each viola occurring between March 15, 2004 and January 12, 2009, and up to $37,500 per day for each viola occurring after January 12,

5 Case 2:05-mc Document 1044 Filed 08/04/16 Page 5 of 35 Pennsylvania Clean s Law 17. At all relevant times, the Commonwealth of Pennsylvania has been authorized by EPA pursuant to Sec 402(b) of the CWA, 33 U.S.C. 1342(b), to administer an NPDES program for regulating the discharges of pollutants to navigable waters within the jurisdic of the Commonwealth. Pursuant to 25 Pa. Code Chapter 92a, PADEP is the agency that administers the NPDES permit program in Pennsylvania. 18. Secs 301, 307, and 315 of the PCSL, 35 P.S , , and , prohibit the discharge by any person of any pollutant from a mine into waters of the Commonwealth of Pennsylvania, except, inter alia, in compliance with applicable water quality standards and effluent limitas as required by a Pennsylvania NPDES permit issued pursuant to the PCSL and its implementing regulas. 19. Sec 601 of the PCSL, 35 P.S , authorizes PADEP to commence a civil ac for injunctive relief to compel compliance with and enjoin violas of any provision of the PCSL or any term or condi of an NPDES permit issued under the PCSL. Sec 605 of the PCSL, 35 P.S , also provides that any person who violates any provision of an NPDES permit issued pursuant to the PCSL or its implementing regulas is subject to a civil penalty of up to $10,000 per day for each viola. GENERAL ALLEGATIONS 20. The Defendants named herein are persons within the meaning of Sec 502(5) of the CWA, 33 U.S.C. 1362(5), and 35 P.S Defendants own and/or operate the coal mining, processing, and shipping operas at the Bailey, Enlow, and Harvey (formerly known as BMX) mines in Greene 5

6 Case 2:05-mc Document 1044 Filed 08/04/16 Page 6 of 35 and Washington Counties, Pennsylvania. The Bailey, Enlow, and Harvey Mines are large underground bituminous coal mines that are adjacent to each other and share a common coal prepara plant and coal refuse disposal areas. The Bailey, Enlow, and Harvey mines and related operas are collectively referred to in this Complaint as the Bailey Mine Complex. 22. CPCC applied for, and PADEP issued, the following NPDES permits to discharge pollutants from the Bailey Mine Complex into nearby receiving streams: PA ; PA ; PA ; PA ; and PA The NPDES permits were issued under both the Pennsylvania Clean s Law and the Clean Water Act. The NPDES permits contain effluent limitas prohibiting discharges of specified pollutants in excess of numeric monthly average, daily maximum, instantaneous maximum, and/or daily minimum limits. These limitas reflect ELGs and stricter water quality based effluent limits. 23. The NPDES permits identified in Paragraph 21 authorize discharges in compliance with effluent limits into specified receiving streams. The receiving streams are identified by NPDES permit number and outfall loca in Appendix A to this Complaint. 24. At all relevant times, Consol managed, directed, and controlled environmental compliance at the Bailey Mine Complex, including providing direct oversight and management of environmental compliance staff, corresponding with consultants and otherwise directing water treatment approaches, maintaining an environmental data management system for water quality data tracking, and communicating directly with state and federal regulators regarding environmental compliance issues. 25. On informa and belief, CNX is a master limited partnership formed by Consol in 2015 to manage and further develop its active thermal coal operas in Pennsylvania, 6

7 Case 2:05-mc Document 1044 Filed 08/04/16 Page 7 of 35 including the Bailey Mine Complex. On informa and belief, CNX has jointly owned and/or operated the Bailey Mine Complex since July 1, As a result of the coal mining and processing operas at the Bailey Mine Complex, Defendants generate coal slurry, wastewater, and other excess materials that are, or contain, various pollutants as that term is defined in Sec 502(6) of the CWA, 33 U.S.C. 1362(6), and 40 C.F.R These pollutants include aluminum, iron, manganese, total suspended solids, settleable solids, ph, and osmotic pressure. See Appendix A. 27. Defendants have discharged pollutants from various outfalls that are point sources within the meaning of Sec 502(14) of the Clean Water Act, 33 U.S.C. 1362(14), into the receiving streams identified in Appendix A of this Complaint. ENFORCEMENT BACKGROUND Outfall 301, No. PA Outfall 301 of Coal Refuse Disposal Permit No , PA , discharges drainage from coal refuse disposal areas Nos. 3 and 4 ( CRDA 3/4 ) in the Bailey Mine Complex, including drainage from a large slurry impoundment. On December 9, 2003, PADEP issued a revised permit that included average monthly, daily maximum, and instantaneous maximum osmotic pressure effluent limitas for Outfall On May 25, 2005, CPCC and PADEP entered into a Consent Order and Agreement with regard to the osmotic pressure effluent limitas for Outfall 301 (the CO&A ). The CO&A set forth a process for CPCC to request a site-specific osmotic pressure limita. The CO&A also imposed stipulated penalties in the amount of $250 per viola in the event that the discharge at Outfall 301 exceeded applicable osmotic pressure limitas prior 7

8 Case 2:05-mc Document 1044 Filed 08/04/16 Page 8 of 35 to any permit modifica. 30. CPCC subsequently decided not to pursue site-specific osmotic pressure limits and was unable to consistently meet the applicable osmotic pressure limits for Outfall On December 10, 2010, CPCC and PADEP entered into an amendment to the CO&A (the CO&A Amendment ). The CO&A Amendment required CPCC to submit an applica for permit modifica to include a water handling plan to remove the high osmotic pressure waters from Outfall On October 10, 2012, PADEP issued a Compliance Order to CPCC for failure to maintain necessary treatment facilities, based on exceedances of osmotic pressure limits for Outfall 301 in the prior three months. The Compliance Order required abatement by November 10, On March 9, 2013, PADEP issued a Consent Assessment of Civil Penalty to CPCC for exceeding its osmotic pressure permit limits for Outfall 301 in July, August, and September of Defendants have implemented a pump-back system as a temporary measure to address exceedances of the osmotic pressure limits for Outfall 301. The pump-back system uses the CRDA No. 3 slurry impoundment to store waters high in osmotic pressure and other pollutant parameters in order to prevent unlawful discharge. Due to excess water accumula and limited storage capacity, discharge of these contaminated waters from CRDA No. 3 may ultimately occur unless addial measures are taken. Outfall 501, No. PA Outfall 501, Coal Refuse Disposal Permit Number , No. 8

9 Case 2:05-mc Document 1044 Filed 08/04/16 Page 9 of 35 PA discharges drainage from coal refuse disposal area No. 5 (CRDA No. 5) in the Bailey Mine Complex, including from a large slurry impoundment. No. PA includes effluent limitas on discharges of aluminum, iron, and manganese from Outfall On October 10, 2012, PADEP issued a compliance order to CPCC for failure to maintain necessary treatment facilities, based on exceedances of aluminum, iron, and manganese limits for Outfall 501 in July of The Compliance Order required abatement by November 10, On January 30, 2013, PADEP issued a Consent Assessment of Civil Penalty to CPCC for exceeding its aluminum, iron, and manganese permit limits for Outfall 501 in July of No. PA also includes osmotic pressure effluent limitas. Pursuant to a request from PADEP, Defendants have implemented a pump-back system as a temporary measure to prevent future exceedances of osmotic pressure permit limits for Outfall 501. The pump-back system uses the CRDA No. 5 slurry impoundment to store contaminated waters in order to prevent unlawful discharge. Due to excess water accumula and limited storage capacity, discharge of contaminated waters from CRDA No. 5 may ultimately occur unless addial measures are taken. CLAIM FOR RELIEF 39. Paragraphs 1-38 are realleged and incorporated by reference. 40. During the period relevant to this Complaint, Defendants have discharged and likely will continue to discharge pollutants in excess of effluent limitas specified in 9

10 Case 2:05-mc Document 1044 Filed 08/04/16 Page 10 of 35 applicable NPDES permits. 41. From January 1, 2006 to June 30, 2015, Consol and CPCC exceeded effluent limitas contained in NPDES permits applicable to discharges from the Bailey Mine Complex at least 188 times for daily effluent limitas and at least 170 times for monthly effluent limitas. See Appendix A. 42. From July 1, 2015 to March 31, 2016, Consol, CNX, and CPCC exceeded effluent limitas contained in NPDES permits applicable to discharges from the Bailey Mine Complex at least one time for daily effluent limitas and one time for monthly effluent limitas. See Appendix A. 43. For each exceedance of an effluent limita, Defendants are in viola of the Clean Water Act for discharging in viola of the condis and limitas of the applicable NPDES permit issued under Sec 402 of the CWA, 33 U.S.C Defendants discharges of pollutants in excess of effluent limitas contained in the applicable NPDES permits constitute violas of 35 P.S and Unless enjoined, Defendants violas will continue. 46. Pursuant to Sec 309(b) of the CWA, 33 U.S.C. 1319(b), and 35 P.S , Defendants are liable for permanent injunctive relief. 47. Pursuant to Sec 309(d) of the CWA, 33 U.S.C. 1319(d), Defendants are liable for civil penalties of up to $32,500 per day of viola for all violas occurring between March 15, 2004 and January 12, 2009, and up to $37,500 per day of viola for all violas occurring after January 12, Under 35 P.S , Defendants are liable for civil penalties up to $10,000 10

11 Case 2:05-mc Document 1044 Filed 08/04/16 Page 11 of 35 per day for each viola. PRAYER FOR RELIEF WHEREFORE, Plaintiffs, the United States of America and the Pennsylvania Department of Environmental Protec, respectfully pray that this Court: 1. Permanently enjoin Defendants from discharging pollutants except as expressly authorized by the CWA and the limitas and condis of NPDES permits. 2. Order Defendants to take all necessary steps to comply with the CWA, the PCSL, and the limitas and condis of the applicable NPDES permits. 3. Assess civil penalties against Defendants up to $32,500 per day for each viola that occurred between March 15, 2004 and January 12, 2009, and up to $37,500 per day for each viola that occurred after January 12, Assess civil penalties against Defendants up to $10,000 per day for each viola under 35 P.S Grant such other relief as the Court may deem appropriate. Respectfully submitted, FOR THE UNITED ~T"~1.TES~F AMERICA J HN-. CRUD~T-- ~ss' ant Attorney Genera E ironment &Natural Resources Division U.S. Department of Juke TsAURA A. TH~MS, Senior Attorney, Bar No. DC STAGY COLEMAN, Trial Attorney, Bar No. DC

12 Case 2:05-mc Document 1044 Filed 08/04/16 Page 12 of 35 Environmental Enforcement Sec Environment & Natural Resources Division United States Department of Justice P.O. Box 7611 Washington, D.C Tel: (Laura Thoms) (Stacy Coleman) Fax: usdoj.gov 12

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15 Case 2:05-mc Document 1044 Filed 08/04/16 Page 15 of 35 PA /2010 TSS Monthly 30 mg/l % 39 58'18.04" 80 25'31.38" Enlow PA /2009 TSS Monthly 35 mg/l % 40 0'22.07" 80 23'35.87" UT Long Run PA /2010 TSS Monthly 35 mg/l % 40 0'22.07" 80 23'35.87" UT Long Run PA /3/2007 Settleable Solids Daily 0.5 ml/l % 39 59'16.83" 80 20'59.28" UT Enlow PA /2008 Iron Monthly 3 mg/l % 40º 02' 13" 80º 22' 38" UT Rocky Run TSF PA /2008 Aluminum Monthly 2.53 mg/l % 40º 02' 13" 80º 22' 38" UT Rocky Run TSF PA /2008 TSS Monthly 35 mg/l % 40º 02' 13" 80º 22' 38" UT Rocky Run TSF PA /2009 TSS Monthly 35 mg/l % 40º 02' 13" 80º 22' 38" UT Rocky Run TSF PA /2009 TSS Monthly 35 mg/l % 40º 02' 13" 80º 22' 38" UT Rocky Run TSF PA /2011 TSS Monthly 35 mg/l % 40º 02' 13" 80º 22' 38" UT Rocky Run TSF PA /2011 TSS Monthly 35 mg/l % 40º 02' 13" 80º 22' 38" UT Rocky Run TSF PA /2/2011 TSS Daily 70 mg/l % 40º 02' 13" 80º 22' 38" UT Rocky Run TSF UT Templeton PA /2009 TSS Monthly 35 mg/l % 40 03'38" 80 21'53" TSF PA /2014 TSS Daily 70 mg/l % 40 03'38" 80 21'53" UT Templeton TSF PA /2014 TSS Monthly 35 mg/l % 40 03'38" 80 21'53" UT Templeton TSF PA /2016 Aluminum Daily 2.4 mg/l % 40 03'38" 80 21'53" UT Templeton TSF PA /2012 TSS Monthly 35 mg/l % 40 2'12.34" 80 19'34.52" UT Short Creek TSF Page 1 of 21

16 Case 2:05-mc Document 1044 Filed 08/04/16 Page 16 of 35 PA /2013 TSS Monthly 35 mg/l % 40 2'12.34" 80 19'34.52" UT Short Creek TSF UT Buffalo PA /2010 TSS Monthly 35 mg/l % 40 5'1.6" 80 14'29.1" Creek HQ- UT Buffalo PA /2013 Osmotic Pressure Daily 100 mosm/kg % 40 5'1.6" 80 14'29.1" Creek HQ- UT Buffalo PA /2013 Aluminum Daily 0.75 mg/l % 40 5'1.6" 80 14'29.1" Creek HQ- PA /2013 Aluminum Monthly 0.38 mg/l % 40 5'1.6" 80 14'29.1" UT Buffalo Creek HQ- UT Buffalo PA /2013 Osmotic Pressure Monthly 50 mosm/kg % 40 5'1.6" 80 14'29.1" Creek HQ- UT Buffalo PA /2015 Aluminum Monthly 0.38 mg/l % 40 5'1.6" 80 14'29.1" Creek HQ- PA /2006 TSS Monthly 35 mg/l % 39º 57' 59" 80º 24' 36" Tally Run PA /2007 Manganese Monthly 1.5 mg/l % 39º 57' 59" 80º 24' 36" Tally Run PA /24/2007 Manganese Daily 3.0 mg/l % 39º 57' 59" 80º 24' 36" Tally Run PA /2008 Manganese Monthly 1.5 mg/l % 39º 57' 59" 80º 24' 36" Tally Run PA /16/2008 Manganese Daily 3.0 mg/l % 39º 57' 59" 80º 24' 36" Tally Run PA /2010 TSS Monthly 35 mg/l % 39º 57' 59" 80º 24' 36" Tally Run PA /17/2010 TSS Daily 70 mg/l % 39º 57' 59" 80º 24' 36" Tally Run PA /2010 Iron Monthly 1.5 mg/l % 39º 57' 59" 80º 24' 36" Tally Run PA /2010 TSS Monthly 35 mg/l % 39º 57' 59" 80º 24' 36" Tally Run PA /2006 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2006 TSS Monthly 35 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2006 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2006 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2006 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2006 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2007 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /17/2007 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2007 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run Page 2 of 21

17 Case 2:05-mc Document 1044 Filed 08/04/16 Page 17 of 35 PA /8/2007 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2007 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2007 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2007 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2007 Iron Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2008 TSS Monthly 35 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2008 Iron Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2008 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /3/2008 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /16/2008 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run #REF! PA /2008 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /22/2008 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2008 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2008 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2008 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /10/2008 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2008 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /18/2008 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2009 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /12/2009 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2009 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2009 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2010 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2010 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2010 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /21/2010 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /27/2010 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2011 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /25/2011 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /28/2011 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2011 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run Page 3 of 21

18 Case 2:05-mc Document 1044 Filed 08/04/16 Page 18 of 35 PA /7/2011 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2011 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /21/2011 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /28/2011 Manganese Daily 3.0 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2011 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /15/2011 Manganese Daily 3 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /26/2011 Manganese Daily 3 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2011 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /14/2011 Manganese Daily 3 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2011 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2011 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /12/2011 Manganese Daily 3 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2011 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2012 Manganese Monthly 1.5 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2012 Manganese Daily 3 mg/l % 39º 58' 02" 80º 24' 34" Tally Run PA /2012 Manganese Monthly 0.5 mg/l % 39 58'11.67" 80 24'45.24" Tally Run PA /2006 TSS Monthly 35 mg/l % 39 58'16.26" 80 25'11.75" Tally Run PA /2010 Iron Monthly 1.5 mg/l % 39 58'16.26" 80 25'11.75" Tally Run PA /2008 TSS Monthly 30 mg/l % 39 53'13.02" 80 29'27.66" UT SF Dunkard PA /2011 ph/field Daily % 39 53'49.02" 80 25'53.27" Kent Run TSF PA /2006 Aluminum Monthly 0.75 mg/l % 39º 57' 32" 80º 22' 33" PA /7/2006 Aluminum Daily 1.5 mg/l % 39º 57' 32" 80º 22' 33" PA /2006 Aluminum Monthly 0.75 mg/l % 39º 57' 32" 80º 22' 33" PA /2006 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /23/2006 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" Page 4 of 21

19 Case 2:05-mc Document 1044 Filed 08/04/16 Page 19 of 35 PA /2006 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2006 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2006 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /26/2006 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /2006 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2006 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /9/2006 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /17/2006 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /17/2006 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /25/2006 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /25/2006 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2006 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2007 Aluminum Monthly 0.75 mg/l % 39º 57' 32" 80º 22' 33" PA /5/2007 Aluminum Daily 1.5 mg/l % 39º 57' 32" 80º 22' 33" PA /23/2007 Aluminum Daily 1.5 mg/l % 39º 57' 32" 80º 22' 33" PA /2007 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" Page 5 of 21

20 Case 2:05-mc Document 1044 Filed 08/04/16 Page 20 of 35 PA /2007 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2007 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2007 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /28/2007 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2007 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2007 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /6/2007 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /10/2007 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /21/2007 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /24/2007 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /2007 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2007 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /8/2007 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /19/2007 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /29/2007 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /2007 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" Page 6 of 21

21 Case 2:05-mc Document 1044 Filed 08/04/16 Page 21 of 35 PA /2007 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /7/2007 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /2008 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2008 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2008 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2008 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /8/2008 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /15/2008 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /23/2008 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /23/2008 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /29/2008 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /2008 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2008 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /5/2008 Aluminum Daily 1.5 mg/l % 39º 57' 32" 80º 22' 33" PA /5/2008 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /12/2008 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" Page 7 of 21

22 Case 2:05-mc Document 1044 Filed 08/04/16 Page 22 of 35 PA /20/2008 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /25/2008 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /2008 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2/2008 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2009 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /25/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /10/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /19/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /20/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /24/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /28/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" Page 8 of 21

23 Case 2:05-mc Document 1044 Filed 08/04/16 Page 23 of 35 PA /2009 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2009 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /1/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /9/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /17/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2009 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /21/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /24/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /28/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /31/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /4/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /11/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" Page 9 of 21

24 Case 2:05-mc Document 1044 Filed 08/04/16 Page 24 of 35 PA /25/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2009 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /9/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /16/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /23/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /29/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /30/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /6/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /13/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /20/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /25/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2009 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /4/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" Page 10 of 21

25 Case 2:05-mc Document 1044 Filed 08/04/16 Page 25 of 35 PA /11/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /18/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /23/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /30/2009 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2010 Aluminum Monthly 0.75 mg/l % 39º 57' 32" 80º 22' 33" PA /2010 TSS Monthly 35 mg/l % 39º 57' 32" 80º 22' 33" PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /8/2010 Aluminum Daily 1.5 mg/l % 39º 57' 32" 80º 22' 33" PA /8/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /8/2010 TSS Daily 70 mg/l % 39º 57' 32" 80º 22' 33" PA /15/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /22/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /28/2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /29/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /5/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" Page 11 of 21

26 Case 2:05-mc Document 1044 Filed 08/04/16 Page 26 of 35 PA /12/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /19/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /5/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /19/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /26/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /1/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /9/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /23/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /30/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /7/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /13/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /21/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /28/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" Page 12 of 21

27 Case 2:05-mc Document 1044 Filed 08/04/16 Page 27 of 35 PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /3/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /11/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /18/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2010 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /9/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /16/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /23/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /6/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /13/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /20/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /27/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" Page 13 of 21

28 Case 2:05-mc Document 1044 Filed 08/04/16 Page 28 of 35 PA /3/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /10/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /17/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /24/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /1/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2010 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /8/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /8/2010 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /15/2010 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /15/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2010 TSS Monthly 35 mg/l % 39º 57' 32" 80º 22' 33" PA /2010 TSS Daily 70 mg/l % 39º 57' 32" 80º 22' 33" PA /2010 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /5/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" Page 14 of 21

29 Case 2:05-mc Document 1044 Filed 08/04/16 Page 29 of 35 PA /12/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /19/2010 Manganese Daily 2.2 mg/l % 39º 57' 32" 80º 22' 33" PA /19/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /26/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2010 Manganese Monthly 1.1 mg/l % 39º 57' 32" 80º 22' 33" PA /2010 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /23/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /30/2010 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /14/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /11/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /15/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /25/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" Page 15 of 21

30 Case 2:05-mc Document 1044 Filed 08/04/16 Page 30 of 35 PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /3/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /17/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /24/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /1/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /8/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /15/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /22/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /29/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /5/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /12/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /16/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" Page 16 of 21

31 Case 2:05-mc Document 1044 Filed 08/04/16 Page 31 of 35 PA /23/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /30/2011 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2011 Aluminum Daily 1.5 mg/l % 39º 57' 32" 80º 22' 33" PA /2011 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2012 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2012 Aluminum Monthly 0.75 mg/l % 39º 57' 32" 80º 22' 33" PA /2012 Aluminum Daily 1.5 mg/l % 39º 57' 32" 80º 22' 33" PA /2012 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2012 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2012 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2012 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2012 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2012 Osmotic Pressure Monthly 50 mosm/kg % 39º 57' 32" 80º 22' 33" PA /2012 Osmotic Pressure Daily 100 mosm/kg % 39º 57' 32" 80º 22' 33" Page 17 of 21