एमआरप एल ग णव नय ण य गश ल उप दन व श:२०१७ MRPL QC LABORATORY PRODUCTS SPECIFICATIONS:2017
INDIAN STANDARD (IS) SPECIFICATIONS FOR DOMESTIC PRODUCTS: 2017 S.No Product Name Specification Number 1 Liquefied Petroleum Gases (LPG) 2 Motor Gasoline MG 91 BSIV IS 4576: 1999-Second Revision, Reaffirmed 2014, Amendment 1,2003 IS 2796:2014-5th Revision (Amendment No.1) April 2016 3 Aviation Turbine Fuel (ATF) Kerosene Type, Jet A-1 IS 1571:2008, 8 revision, reaffirmed 2013 and Defence Standard 91-091, Issue 9,dated 03.10.2016 & JIG(AFQRJOS) Issue 29,October 2016 4 Kerosine-SKO IS 1459: 2016, 3 rd Revision 5 Automotive Diesel Fuel (HSD)- BS IV/EURO IV IS 1460: 2005,5 th Revision (Amendment No.3) September 2012,reaffirmed 2011 6 Automotive Diesel Fuel IS 1460:2000-8 th Revision 7 Fuel Oil- MV2 Grade IS 1593: 1982, Reaffirmed 2014, Second Revision, Amendment 1 & 2 8 Paving Bitumen -VG 30 IS 73: 2013, 4 th Revision 9 Paving Bitumen -VG 10 IS 73: 2013, 4 th Revision 10 11 12 13 14 15 16
SPECIFICATION FOR LIQUEFIED PETROLEUM GAS (Commercial Butane-Propane Mixture) IS 4576 2014 1 Density@ 15 C g/ml Report ASTM D 2598 2 Vapour pressure at 40 C kpa 1050 Max. ASTM D 1267 3 4 Composition, Liquid - ASTM D 2163 i. C2 Hydrocarbons (Ethane) Vol% Report - ii. C3 Hydrocarbons (Propane) Vol% Report - iii. C4 Hydrocarbons (Iso- Butane) Vol% Report - iv. C4 Hydrocarbons (n- Butane) Vol% Report - v. C5 Hydrocarbons & Heavier Vol% Max 2.5 - vi. Unsaturated Hydrocarbons Vol% Report - OR - - Volatility evaporation temperature in C for 95 % by vol. at 760 mm Hg pressure C Max +2 ASTM D 1837 5 Total Volatile Sulphur ppm Max 150.0 ASTM D 3246 6 Copper Corrosion @ 38 C, for 1 hour. Not worse than No. 1 ASTM D 1838 7 Hydrogen Sulfide Pass ASTM D 2420 8 Free water Content None VISUAL
SPECIFICATION FOR MOTOR GASOLINE (UNLEADED REGULAR)MG 91 BHARAT STAGE IV IS 2796 2014 1 Grade BS IV MG 91 (Unleaded regular) 2 Color Visual Orange Visual 3 Density at 15 C Kg/m3 Range 720-775 ASTM D 4052 4 DISTILLATION: - ISO3405/ASTM D86 Recovery up to 70 C, {E70} Vol % Range 10-45 - Recovery up to 100 C, {E100] Vol % Range 40-70 - Recovery up to 150 C, {E150] Vol % Min 75 - Final Boiling Point (FBP) C Max 210 - Residue Vol % Max 2.0-5 Research Octane Number (RON) Min 91.0 ASTM D 2699 6 Motor Octane Number (MON) Min 81.0 ASTM D 2700 7 Gum Content(solvent Washed) g/m3 Max 40.0 ASTM D 381 8 Sulphur (Total ) mg/kg Max 50 ASTM D 5453 9 Lead Content (as Pb) g/l Max 0.005 ASTM D 5059 10 Reid Vapour pressure {RVP} @ 38 C kpa Max 60.0 11 Vapour Lock Index {VLI) (VLI=10*RVP + 7*E7O} a) Summer a) Other months IS 1448 P:39/ASTM D323 - - Max 750 Max 950 Calculation 12 Benzene percent by Volume Vol % Max 1.0 ASTM D 3606 13 14 Copper strip corrosion (for 3 hrs at 50 C) Water tolerance of Gasoline- Alcohol, blends temp. For Phase separation Not more than 1 - IS 1448, P: 15 / ISO 2160/ ASTM D 130 As per IS 2796-2008 Annex B a) Summer C Max 10 - b) Winter C Max Zero - 15 Oxidation Stability Minutes Min 360 16 Olefin Content Vol % Max 21.0 IS 1448: P:28 / ISO 7536/D 525 IS 1448:P:23/ ASTM D 1319
17 Aromatic Content Vol % Max 35.0 IS 1448:P: 23/ ASTM D 1319 18 Oxygen Content Mass % Max 2.7 ISO 1601 19 Oxygenates* Vol % ASTM D 4815/Annex C 20 Ethanol Content % Mass Max 4.75±0.25 ASTM D 4815/Annex E 21 Engine intake system cleanliness mg/kg Report - MFA used - Note: 1. * Contains no Oxygenates 2. Summer : May to July.
SPECIFICATION FOR AVIATION TURBINE FUEL JET A-1 IS 1571-2008 -DOMESTIC Also Meets Def Stan 91-091 Issue 9 and AFQRJOS issue 29, dated 03.10.2016 ` 1) APPEARENCE a) Visual Appearance b) Colour c) d) 2) Particulate Contamination, at point of manufacture, mg/l Particulate cumulative channel particle counts, ISO code as per table 1 of ISO 4406:1999 4um(c) 6um(c) 14um(c) 21um(c) 25um(c) 30um(c) COMPOSITION Number mg/l ISO code and counts Clear & Bright free from Solid matter & un dissolved water at ambient temperature. Report Max 1.0 Visual ASTM D 156/D 6045 IP 423/ASTM D 5452 Report IP 565 - - a) Total Acidity, mg KOH/g, Max mg KOH/g Max 0.015 IS 1448 P:113 b) Aromatics % vol, Max. Vol % 25.0 (22.0- Defence) IS 1448 P:23 c) Sulphur, Total % m/m, Max d) e) Sulphur Mercaptan, percent by mass, Max or Doctor Test, REFINING COMPONENT AT THE POINT OF MANUFACTURE. 1. Non Hydro processed components, % v/v 2.Severely Hydro processed component, % v/v Mass % Mass % Vol % Vol % Max 0.30 0.0030(0.002 Defence) or Doctor Negative Report Report ASTM D 4294/P:34 IS 1448 P:109/P:19
3) VOLATILITY - - a) Distillation IS 1448 P:18 Initial Boiling Point, at C, C Report 10 percent recovery, at C, v/v, Max. C Max 205.0-50 percent recovery at C,v/v C Report 90 percent recovery at C, v/v C Report Final Boiling Point C, Max. C Max 300.0 - Residue percent by volume, Max. Vol % Max 1.5 - Loss% volume, Max. Vol % Max 1.5 - b) Flash Point, C. Min. C Min 38.0 IS 1448 P:20 (Method B) c) Density @ 15 C, kg/m3 Kg/m3 Range 775.0 840.0 IS 1448 P:16 4) FLUIDITY - - a) Freezing point, C, Max. C Max Minus 47 IS 1448 P:11 b) 5) Kin. Viscosity at minus 20 C, mm 2 /s Max. COMBUSTION a) Specific energy MJ/kg, Min Or Product of API gravity and Aniline point, Min cst MJ/kg Max 8.000 IS 1448 P:25 Min 42.80 IS 1448 P:6/D 3338 Min 4800 IS 1448 P:3 b) Smoke point, mm, Min OR mm Min 25.0 ISO 3014/P:31 i) Smoke Point,mm, Min and mm Min 19.0 ISO 3014/P:31 ii) Naphthalene, percent v/v, Max. Vol % Max 3.00 P:118
6) 7) a) CORROSION Cu strip corrosion for 2 hrs at 100 C Thermal Stability, JFTOT at control Temperature of 260 C Filter pressure differential, mmhg, Max b) Tube Rating, visual 8) CONTAMINANTS a) b) c) Existent gum, mg/100 ml, Max. OR Existent gum with Air, mg /100 ml, Max Water Reaction Interface rating, Max. Micro Separator rating at point of Manufacture Number Not worse than No:1 IS 1448 P : 15 mmhg Max 25 Less than 3, No peacock or Abnormal colour deposits IS 1448 P : 97, ISO 6294 mg/100 ml Max 7 IS 1448 P: 29 Number 1b IS 1448 P :42 i) MSEP without SDA, Min OR Number Min 85 ii) MSEP with SDA, Min Number Min 70 9) CONDUCTIVITY 10) Electrical Conductivity ps/m (at the point,time and temp of delivery to the purchaser) LUBRICITY Wear Scar Diameter, mm max 11) ADDITIVES ps/m mm Range 50-600 Max 0.85(0.65 Defence) IS 1448 P : 142 ISO 6297 ASTM D 5001 i) ii) Static dissipater additive,mg/l #SDA 450(RDE/A/621),Max Anti oxidant, mg/l #$(RDE/A/609) mg/l Max 3.0 mg/l Range 17-24
SPECIFICATION FOR KEROSINE IS 1459-2016 1 Density @ 15 C g/ml Report IS 1448, P: 16 2 Colour (Saybolt) Number Min Plus 10 IS 1448 P:14 3 DISTILLATION Percent Recovered below 200 C % Vol Min 20.0 Final Boiling Point (FBP) C Max 300 - IS 1448, P: 18 4 Flash point (Abel) C Min 35.0 IS 1448, P: 20 5 Smoke point mm Min 18.0 IS 1448, P: 31 6 BURNING QUALITY - IS 1448, P: 5 Char value mg/kg of oil consumed Bloom on glass chimney, Colour, mg/kg Max 20.0 - Visual Not darker than Grey 7 Acidity, Inorganic mg KOH/g Nil IS 1448, P: 2 8 Total Sulphur % Mass Max 0.20 9 Copper Corrosion for 3 hrs at 50 deg. C. Number Not worse than No: 1 - ASTM D 4294/ISO 8754 IS 1448, P: 15
SPECIFICATION FOR AUTOMOTIVE DIESEL FUEL (BHARAT STAGE IV) IS 1460 2005 1 Acidity,Inorganic mg KOH/g Nil IS 1448, P: 2 2 Acidity,Total mg KOH/g To Report IS 1448, P: 2 3 Ash % Mass Max 0.01 IS 1448, P: 4 4 5 Carbon residue (Ramsbottom) On 10% Residue Note: Winter months: November to February % Mass Max 0.30 IS 1448, P:8 Cetane Number Number Min 51.0 IS 1448, P: 9 / ISO 5165 6 Cetane Index Number Min 46.0 ASTM D 4737 7 8 9 Pour Point Copper strip Corrosion for 3 hours @ 50 deg. C Distillation, % v/v, recovered @360 C C Max 3 C, for winter C Max 15 C, for summer ASTM D 5949/D5950 Not worse than No.1 IS 1448, P: 15 % Vol Min 95.0 ISO 3405 10 Flash Point (Abel/PMC) C Min 35.0/66.0 IS 1448, P: 20/P:21 11 Kinematic Viscosity@ 40 deg. C cst Range 2.0 to 4.5 IS 1448, P: 25 12 Sediments % Mass - P 30 13 Total Contamination mg/kg Max 24.0 EN 12662 14 Density @ 15 deg. C Kg/m3 Range 820-845 ASTM D 4052 15 Total Sulphur mg/kg Max 50 ASTM D 5453/D 4294 16 Water content mg/kg Max 200 ISO 12937 17 18 Cold Filter Plugging Point (CFPP) Lubricity corrected wear scar diameter(wsd 1.4) at 60 C C Max 6 C for winter C Max 18 C for Summer ASTM D 6371 Microns Max 460 ISO 12156-1/Cor 1 19 Oxidation Stability g/m3 Max 25.0 ASTM D 2274 20 Polycyclic Aromatic hydrocarbons (PAH) % Mass Max 11.0 IP 391 21 Oxygen Content % Mass Max 0.6 Annex B
SPECIFICATION FOR AUTOMOTIVE DIESEL FUEL (HIGH FLASH) IS 1460 2000 1 Acidity,Inorganic mg KOH/gm Nil IS 1448, P: 2 2 Acidity,Total mg KOH/gm Max 0.20 IS 1448, P: 2 3 Ash % Mass Max 0.01 IS 1448, P: 4 4 5 Carbon residue (Ramsbottom) On 10% Residue % Mass Max 0.30 IS 1448, P: 8 Cetane Number OR Min 48.0 IS 1448, P: 9 6 Cetane Index Min 46.0 ASTM D 4737 7 8 9 Pour Point Copper strip Corrosion for 3 hours @ 100 deg. C Distillation, % v/v, recovered: at 350 C at 370 C C C Max 12 C, for winter Max 18 C, for summer Not worse than No.1 % Vol Min 85.0 Min 95.0 IS 1448, P: 10 IS 1448, P: 15 IS 1448, P: 18 10 Flash Point (PMC) C Min 66.0 IS 1448, P: 21 11 Kinematic Viscosity @ 40 deg. C cst Range 2.0 to 5.0 IS 1448, P: 25 12 Sediment % Mass Max 0.05 IS 1448,P:30 13 Density @ 15 deg. C kg/m3 Range 820-860 IS 1448,P:16 14 Total Sulphur % Mass Max 0.25 ASTM D 4294 15 Water content % Vol Max 0.05 IS 1448,P:40 16 Cold Filter Plugging Point (CFPP) C C Max 6 C for winter Max 18 C for Summer IP 309 17 Total Sediments mg/100ml Max 1.5 ASTM D 2274
SPECIFICATION FOR FURNACE OIL MV2 Grade IS 1593 1982 1 Acidity, Inorganic Mg KOH/gm Nil IS 1448, P: 2 2 Ash % Mass Max 0.1 IS 1448, P: 4 3 Gross Calorific Value Cal/gm Report IS 1448, P: 7 4 Relative Density @ 15/15 C g/ml Report IS 1448, P: 32 5 Flash Point (PMC) C Min 66.0 IS 1448, P: 21 6 Kinematic Viscosity at 50 C cst Max 180 IS 1448, P: 25 7 Sediment % Mass Max 0.25 IS 1448, P: 30 8 Total Sulphur % Mass Max 4.0 NOTE: Tests indicated in Sl. No. 11-14 is as per customer requirements. ASTM D 4294 IS 1448,P:33 9 Water content % Vol Max 1 0 IS 1448, P: 40 10 Pour Point C Report ASTM D 97 11 Cleanliness Number Report ASTM D 4740 12 Micro Carbon Residue % Mass Report ASTM D 4530 13 Asphaltenes % Mass Report IP 143 14 Net calorific value Cal/gm Report IS 1448 P:6
SPECIFICATION FOR PAVING BITUMEN (VG 30) IS 73-2013 Sl. No. TESTS UNIT REQUIREMENT TEST METHOD 1 Density at 27 C g/ml Report IS 1202 Density at 15 C g/ml Report IS 1202 2 Absolute Viscosity at 60 C poises Range 2400-3600 IS 1206(Part 2) 3 Kinematic viscosity at 135 C cst Min 350 IS 1206(Part 3) 4 Flash Point (COC) C Min 220 IS 1448 P:69 5 6 Solubility in Trichloroethylene Penetration at 25 C,100 g,5 sec % Min 99.0 IS : 1216 0.1 mm Min 45 I S: 1203 7 Softening Point (R&B) C Min 47 I S: 1205 8 Tests on Residue from thin film oven tests/ RTFOT i) Viscosity ratio at 60 C Calculation Max 4.0 IS 1206(Part 2) ii) Ductility at 25 C, cm, after Rotating thin film oven test cm Min 40 IS 1208
SPECIFICATION FOR PAVING BITUMEN (VG 10) IS 73-2013 1 Density at 27 C g/ml Report IS 1202 Density at 15 C g/ml Report 2 Absolute Viscosity at 60 C poises Range 800-1200 IS 1206(Part 2) 3 Kinematic viscosity at 135 C cst Min 250 IS 1206(Part 3) 4 Flash Point (COC) C Min 220 IS 1448, P:69 5 6 Solubility in Trichloroethylene Penetration at 25 C,100 g,5 sec % Min 99.0 IS : 1216 0.1 mm Min 80 I S: 1203 7 Softening Point (R&B) C Min 40 I S: 1205 8 Tests on Residue from thin film oven tests/ RTFOT i) Viscosity ratio at 60 C Calculation Max 4.0 IS 1206(Part 2) ii) Ductility at 25 C, cm, after Rotating thin film oven test cm Min 75 IS 1208
SPECIFICATION FOR PAVING BITUMEN (VG 40) IS 73-2013 Sl. No. TESTS UNIT REQUIREMENT TEST METHOD 1 Density at 27 C g/ml Report IS 1202 Density at 15 C g/ml Report IS 1202 2 Absolute Viscosity at 60 C poises Range 3200-4800 IS 1206(Part 2) 3 Kinematic viscosity at 135 C cst Min 400 IS 1206(Part 3) 4 Flash Point (COC) C Min 220 IS 1448 P:69 5 6 Solubility in Trichloroethylene Penetration at 25 C,100 g,5 sec % Min 99.0 IS : 1216 0.1 mm Min 35 I S: 1203 7 Softening Point (R&B) C Min 50 I S: 1205 8 Tests on Residue from thin film oven tests/ RTFOT i) Viscosity ratio at 60 C Calculation Max 4.0 IS 1206(Part 2) ii) Ductility at 25 C, cm, after Rotating thin film oven test cm Min 25 IS 1208