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Richter Sampling Valves PA/F, PA/S Body ductile iron with PFA lining or investment cast stainless steel Bellows-sealed Safety packing gland Representative sampling

Richter sampling valves Fields of application Representative and safe sampling of pure and slightly solids-laden media in the chemical, pharmaceutical and other industries. The Richter series PA/F (fluoroplastic lining PFA) and PA/S (stainless steel version) are specially suitable for taking samples of corrosive and pure media, also slightly solids-laden media during the ongoing process prior to filling into other containers/further transport prior to feeding into the process for the regular monitoring of stocks in the piping and from containers Operating ranges from -75 to 400 F (-60 to 200 C) from vacuum to max. 235 psi (16 bar) Product features Top-entry design for very easy maintenance, the valve body can remain installed in the system Valve actuation: safety hand lever, removable. Pneumatic or electric actuator on request. Long plug tip: Counteracts clogging, e.g. caking media. Anti-adhesive, wetted surfaces thanks to PFA/PTFE (PA/F), can be steam-sterilised (must be checked on a case-to-case basis) External corrosion protection: Epoxy coating (PA/F), stainless steel valve bonnet and screws On request with stainless steel protective cabinet (see page 5) Type codes, materials Sampling valve manual actuation remote actuation perfluoroalkoxy (PFA) lined stainless steel version PA/... PAP/....../F.../S Differenciation to sampling ball valves Conventional sampling ball valves are not cavity-free: Residues remain in the area between the ball and the body lining and therefore, before a representative sample can be taken, rinsing must be performed several times and troublesome disposal of the initial samples is necessary promote an undesirable increase in the sedimentation of solids in the dead leg above the ball are usually not self-closing, no dead man s handle have a normal not self-adjusting packing gland seal, have no bellows sealing Travel stop, adjustable from outside finely metered sampling closing force can be increased at any time if the sealing action in the seat/plug area is insufficient (e.g. if sealing surfaces damaged) Safety spring return by means of a central spring suitable for all pressure ranges ( dead man s handle ) Safety packing gland acts independently re-adjustable from outside Lining virgin PFA wall thickness 0.12-0.14 (3-3.5 mm) high permeation resistance vacuum-proof anchored alternatively stainless steel 316 L (1.4435) body without lining Glandless due to heavy-duty PTFE bellows hermetic sealing of the product chamber bellows wall 0.1 (2.5 mm) thick, can also be used for highly permeating media Cavity-free tapered valve bottom representative sampling: only fresh medium is taken no prior rinsing necessary no formation of residue in entire valve Standard bottle connection with thread GL to DIN 168 modified pure PTFE secured against turning possibility of side connection for venting or overflow for PA/F: integrated FKM O-ring (Viton or equivalent) is not wetted further connection possibilities (see page 6) Removable safety hand lever disengages after actuation on request firmly installed with split pin in central bore lockable with lock or split pin alternative position: lever upwards Highly viscous media or applications with low operating pressure: Special plug and seat option (see page 6). For solids-laden media: Inclined or vertical position of the valve and, as a result, possibly special bottle connection is recommended (see page 6). 2

disengaged engaged 1 2 8 H 3 5 D k DN 6 4 nxd 2 H 1 optional 7 Sampling valve PA/F with thick-walled PFA lining L disengaged engaged F E optional D k DN nxd 2 H 1 H L Sampling valve PA/S of stainless steel design (without lining) 3

Richter sampling valves Components and materials Item Designation Material 100 Body PA/F: ductile cast iron ASTM A395/ EN-JS 1049 with PFA lining Temperature/pressure ranges PA/S: investm. cast stainl. steel 316 L/1.4435 104 Transition flange stainl. steel (only ND 1 1 /2 (40), not shown) 106 Cover stainless steel 203 Lever stainless steel 205 Seat PA/F: ductile cast iron ASTM A395/ EN-JS 1049 with PFA lining 206 Bellows w. plug modified pure PTFE 226 Bottle connection modified pure PTFE 302/1 Guide ring PTFE carbon PA/S: investm. cast stainl. steel 316 L/1.4435 400/1 O-ring, not wetted FKM (Viton or equivalent) 402/1 Packing ring PTFE 405/1 Thrust ring stainless steel 503 Packing gland stainless steel follower 509/1 Groove nut stainless steel 513 Spring bonnet stainless steel 514 Spring bush stainless steel 515 Actuation stainless steel 561/1 Grooved pin stainless steel 855 Stem stainless steel 902/1 Stud screw stainless steel 904/1 Setscrew stainless steel 920/3 Hex. check nut stainless steel 952 Pressure spring stainless steel 963 Star knob plastic/stainless steel 964 Ball head plastic 514 515 561/1 106 100 203 Viscosity/operating pressure diagram p (bar) 16 14 12 10 8 6 964 Standard design with tapered plug Design for viscous media (see page 6) 963 920/3 513 952 509/1 904/1 902/1 503 405/1 402/1 302/1 855 206 205 400/1 226 p (psi) 235 205 175 145 115 85 Temperature F ( C) 70 (20) 300 (150) 400 (200) Pressure psi (bar) 235 (16) 220 (15) 205 (14) Cv values (US gpm), k v100 values (m 3 /h) Cv (k v100 ) Cv (k v100 ) Valve Sampling at max. valve stroke inch DN flow rate Tapered plug Flat plug 1 25 17.5 (15) 1 1 /2 40 54.8 (47) 0.448 (0.385) 2.98 (2.56) 2 50 75.7 (65) Other valve sizes on request 4 2 1 0.1 1 5 10 50 100 500 1000 1.8 1.5 Density 1 (g/cm 3 ) 0.7 0.4 0.001 0.0050.01 0.05 0.1 0.5 1 Kinematic viscosity (mm 2 /s) Dynamic viscosity (Pas) Installation and connecting dimensions and weights for series PA/F and PA/S Face-to-face ISO 5752 series 1 (DIN EN 558-1 series 1, formerly DIN 3202/F1) Flanges drilled to ASME/ANSI B 16.5 Cl.150, on request to ISO 7005-1 PN16 (formerly DIN 2532/33), JIS 10 K DN D k n x d 2 H H 1 E L F approx. weight PA/F PA/S (appr.) PA/F* PA/S* inch mm inch mm inch mm inch mm inch mm inch mm inch mm inch mm inch mm inch mm lbs kg lbs kg 1 25 4.52 115 3.35 85 4x 5 /8 4 x 16 7.48 190 4.84 123 4.17 106 7.87 200 6.3 160 9.25 235 22 10 20 9 1 1 /2 40 5.9 150 4.33 110 4x 5 /8 4 x 16 9.84 250 5 127 7.87 200 7.87 200 6.89 175 40 18 ** ** 2 50 6.5 165 4.92 125 4x 3 /4 4 x 19 7.68 195 5.16 131 4.8 122 7.87 200 9.05 230 9.06 230 40 18 31 14 * manually actuated, ** availability on request Other valve sizes on requst 4

Options Sampling valves with stainless steel protective cabinet Sampling valves with actuator Septum bottle adapter for high-purity media The protective cabinets are produced in standard sizes and with various accessories, also custom-made. Installation directly on the valve, can also be retrofitted. Fig.: Option with spring-loaded bottle holder. Pneumatic and electric actuators. Makes as per customer's choice. For design details, see page 6 Body heating Handwheel instead of lever actuation Flat plug for slightly solids-laden media O-ring 230 e.g. for crystallising media, heating jacket made of stainless steel, mounted (PA/F) or welded on (PA/S) Permits particularly finely metered sampling over the entire flow range of the valve. No automatic spring return. The integrated FFKM (Kalrez or equivalent) O-ring still seals if small solid particles are jammed in the sealing surface area. Viton, Kalrez = Trademark of DuPont Richter = Trademark of Richter Chemie-Technik GmbH 5

Special versions of the models PA/F and PA/S Special design for highly viscous media or applications with low operating pressure The standard version of the PA valve with a tapered plug has a travel of 0.12 (3 mm), producing an angular gap of 0.02 (0.5 mm) over a length of 3 /4 (20 mm). However, taking samples of higher viscous media and media with a low operating pressure requires an enlarged passage cross section. With a travel of 0.12 (3 mm) the special flat plug produces a full cross section of the outlet opening of 0.4 (10 mm). The suitable valve plug is selected according to the viscosity/operating pressure diagram (see page 4). Richter should be consulted in the case of different application parameters. Flat plug Choice of connection possibilities for sampling bottles Venting bore Sampling bore Adapter for horizontal valve installation Adapter for vertical valve installation 6 Twin adapter for two different bottle sizes Adapter for hose nozzle A spring-loaded threadless bottle clamping feature can also be provided in conjunction with a protective cabinet; see page 5. Bottle connections: Standard GL to DIN 168 and customised special versions. Presented by: Adapter with O-ring, prevents the ingress of ambient atmosphere Adapter for septum bottle (see picture page 5) Richter Pumps & Valves Inc. A Unit of IDEX Corporation 406 State Street Cedar Falls, 50613 IA, USA Tel. +1(319) 268-8038, Fax +1(319) 268-8048 Integrated needle for perforating the septum Headquarter: Richter Chemie-Technik GmbH Otto-Schott-Str. 2, D-47906 Kempen, Germany Tel. +49 (0) 21 52/146-0, Fax +49 (0) 21 52/146-190 www.richter-ct.com, richter-info@idexcorp.com Publication No. 160us 11.10 Richter Chemie-Technik GmbH. Subject to change without notice. Printed in Germany.