OptiMax Product Catalog OptiMax 1001 Standard Sets 1000 ml Glass Reactor Sets 500 ml Glass Reactor Sets 250 ml Glass Reactor Sets Accessories & Spares Dosing Unit SP-50 OptiMax Your Synthesis Workstation
Glossary of Terms Used Glossary of Terms Used ReactIR ETFE FFKM FPM PA PBT PE PEEK = Mid-IR spectroscopy = Ethylene tetrafluoroethylene = Perfluoro-elastomer = Fluoro-elastomer = Polyamide = Polybutylene terephthalate = Polyethylene = Polyetheretherketone POM PP GF25 PU PVC PVDF SAN VQM = Polyoxymethylene = Polypropylene = Polytetrafluoroethylene, 25% glass = Polyurethane = Polyvinylchloride = Polyvinylidene Fluoride = Styrene acrylonitrile = Silicone rubber 2
Contents General Introduction 2 4 OptiMax Starter Kit 5 OptiMax Thermostat System 6 11 OptiMax 1000 ml Two-Piece Glass Reactor Set 12 15 OptiMax 1000/500 ml Cover Set 16 18 OptiMax 500 ml Two-Piece Glass Reactor Set 19 22 OptiMax 250 ml Two-Piece Glass Reactor Set 23 25 OptiMax 1000 ml One-Piece Glass Reactor Set 26 28 OptiMax 500 ml One-Piece Glass Reactor Set 29 31 OptiMax 250 ml One-Piece Glass Reactor Set 32 34 OptiMax Spare Parts, Adapters, and Stirrers 35 40 OptiMax Accessories and Probes 41 Dosing Unit SP-50 Set 42 45 OptiMax HFCal Kit 46 47 icontrol Software for OptiMax 49 Compatibility List 50 51 3
General Introduction OptiMax Your Synthesis Workstation Editorial No oil baths, ice baths, and cryostats required Precise temperature control from 40 C to 180 C Small and mobile Wide range of different reactors and stirrers Simple and intuitive touch screen operation No learning curve Programmable Secure unattended operation Data logging making experiments traceable and reproducible Data export into icontrol and Microsoft Excel Introduction OptiMax is a synthesis workstation that is beyond traditional synthesis equipment. It is geared towards today s workflows in chemical and process development labs. It simplifies organic synthesis by eliminating cumbersome steps and ensures precise and accurate execution of chemical synthesis. It heats and cools efficiently without the need for cryostats, oil or ice baths, offers a large variety of different reactors and stirrers, and is operated by a simple touch screen. Even though its use is simple, experiments are carried out with highest precision, reproducible and traceable increasing productivity in chemical and process development significantly. A Remarkable Thermostat OptiMax is a single self-contained box with a built-in solid state thermostat covering the entire Temperature Range without an additional cryostat. The powerful Peltier-based thermostat provides the necessary performance to control the temperature of the reaction mixture accurately and reproducibly. It grants outstanding heating and cooling rates in the entire Temperature Range from 40 C to 180 C. Even strong chemical reactions are kept at constant temperature, ensuring that the experiment is carried out safely and the reaction kinetics remains unaffected. Operation OptiMax is operated completely effortless using a smart and intuitive touch screen. Changing experiment parameters, such as temperature or stirring speed is a matter of seconds and doesn t require any training. The experiment is either carried out stepby-step or programmed and completely unattended. The safety monitoring system ensures safe execution of the individual tasks without permanent supervision. All data and relevant information are displayed and recorded as the experiment proceeds. For further evaluation the recorded data can be transferred to either icontrol, the sophisticated PC software or Microsoft Excel. 4
OptiMax Starter Kit OptiMax Starter Kit The OptiMax starter kit is a ready-to-go setup that simplifies the part evaluation and ordering process. The starter kit combines all the key items for an easy-to-use 1000 ml two-piece reactor setup in just one part number. The OptiMax starter kit includes the following key components: OptiMax thermostat system incl. touchscreen Stirrer motor and adapter Tr temperature probe incl. adapter 1000 ml two-piece glass reactor Cover and reactor holders Pitched blade stirrer, downward, Alloy C-22 Bar type baffle, Alloy C-22 incl. adapter Stoppers and Keck clamps for all open ports Accessories holder The OptiMax starter kit can be combined individually with any additional items in this catalog. 51162830 OptiMax 1001 starter kit consists of the following items 51162701 OptiMax thermostat system 51162831 OptiMax 1000 ml two-piece glass reactor set 51162720 adapter for Tr, ph, and turbidity probe 51162839 Tr probe, Alloy C-22 51162886 Accessories holder set Details regarding these items can be found on the following pages. 5
OptiMax Thermostat System OptiMax Thermostat System Power Supply Voltages Back-/Frontlight Heating/Cooling Temperature Mode OptiMax 1001 reactor block available only in a thermostat system set Powder-coated stainless steel with FEP/PFA coated cover plate 100 240 VAC 12 LEDs Solid state thermostat Jacket control, reaction mixture control, crystallization and distillation (constant or ramp) Temperature Range 40 C to 180 C, jacket temperature (Tj) 388 mm x 414 mm x 539 mm (w, d, h), 388 mm x 414 mm x 780 mm (w, d, h with overhead stirrer) Weight 35 kg, including touchscreen 51162701 OptiMax thermostat system set consisting of Order Number Product Description Quantity OptiMax 1001 reactor block 1 51161873 7 TFT OptiMax touchscreen 1 51191728 Pen for OptiMax touchscreen 1 51162690 Overhead stirrer drive complete 1 51161099 Lab bar, 600 mm x 14 mm 4 51162860 Reactor block plug for bottom drain valve opening 1 51161187 PVC tube for coolant, length 2.5 m 2 51191125 PVC tube, soft, for reflux condenser, length 5 m 1 51161186 PVC tube for gas inlet, length 2 m 1 51191915 Flow indicator for coolant 1 51191916 Reducing connector for purge gas tubing 3 51190324 Quick connect coupling for purge gas inlet 5 51192126 Hose clamp for PVC tube 4 USB memory stick for data export 1 51161782 Bubble counter 1 51161603 Magnetic bubble counter holder 1 51191945 Purge gas regulation valve 1 11132570 OptiMax touchscreen protective cover 1 51191235 Identification clips for adhesive labels to label individual sensors, reactors etc. 1 51192208 Glass adapter ST19/26-GL14 2 51190317 Screw cap GL14, with aperture 2 51103947 Sealing ring with vulcanized-on washers for GL14 cap 2 51191373 Y-piece for gas tubing 1 51162895 OptiMax LOGBook, includes Operating Instructions, Guides, and other product-related documents 1 6
OptiMax Thermostat System 51161873 7 TFT OptiMax touchscreen including protective cover PA, aluminium 195 mm x 135 mm x 60 mm (w, d, h) 51161187 PVC tube for coolant PVC Ø 8/12 mm, length 2.5 m 51191728 Pen for touch screen operation Length 140 mm 51191125 PVC tube, soft, for reflux condenser PVC Ø 8/12 mm, length 5 m 51162690 Overhead stirrer drive complete Aluminium anodized, Speed 30 rpm to 1200 rpm 51161186 PVC tube for purge gas inlet PVC Ø 4/6 mm, length 2 m 51161099 Lab bar 600 mm x 14 mm Stainless steel, 1.4435 Ø 14 mm x 600 mm 51191915 Flow indicator for coolant SAN Temperature Max. 30 C For tubes with inner Ø 6 mm to 9 mm available on special request only USB 2.0 memory stick for data export Memory 2 GB 55 mm x 15 mm x 6 mm available on special request only 51191916 Reducing connector for purge gas tubing PP Temperature Max. 30 C For tubes with inner Ø 7 mm to 11 mm; 4 mm to 7 mm 7
OptiMax Thermostat System 51162860 Reactor block plug for bottom drain valve opening GF25 Ø 56 mm x 35 mm O-ring needed 51192209 51161782 Bubble counter Borosilicate glass Ø 30 mm x 150 mm 51 192 209 O-ring for 51162860 plug FPM Ø 50.39 mm x 3.53 mm, AS No. 226 51161603 Magnetic bubble counter holder PET 30 mm x 33 mm x 68 mm 51190324 Quick connect coupling for purge gas in-/outlet Stainless steel For tubes with inner Ø 4 mm 51191945 Purge gas regulation valve PA 6.6, NBR Tube Ø 6 mm 51192126 Hose clamp for PVC tube Stainless steel Ø 14 mm to 9.5 mm available on special request only 51191235 Identification clips for adhesive labels to label individual sensors, reactors etc. For cables with Ø 2 mm to 4.5 mm 8
OptiMax Thermostat System 11132570 OptiMax touchscreen protective cover Barex resin 51192208 Glass adapter ST19/26-GL14 Glass Height 50 mm 51190317 Screw cap GL14, with aperture PBT Aperture Ø 9.5 mm 51103947 Sealing ring with vulcanized-on washers for GL14 cap Silicone rubber VQM, -coated Ø 12 mm, aperture 6 mm 51191373 Y-piece for gas tubing Acetal resin For tubes with inner Ø 4 mm 51162895 OptiMax LOGBook Quantity Includes OptiMax Operating Instructions, Guides, and other product-related documents 1 of each 9
OptiMax Thermostat System OptiMax Thermostat System Spare Parts 51161883 7 TFT OptiMax touchscreen including protective cover PA, aluminium 195 mm x 135 mm x 60 mm (w, d, h) 51162841 Overhead stirrer motor standard Aluminium anodized, Speed 30 rpm to 1200 rpm ± 5 rpm 51162763 Security ring to hold stirrer shaft PEEK Speed Inner Ø 10 mm 51162643 Stirrer adapter, ST24 (Valfon 117) Inner Ø 10 mm 51162820 Loosening nut for 51162643 stirrer adapter PEEK Inner Ø M26 51192163 Bearing sleeve for overhead stirrer PEEK/ Inner Ø 10 mm 51192164 Compression spring for overhead stirrer PEEK Inner Ø 10 mm 10
Accessories for OptiMax System Accessories for OptiMax System 51162839 Alloy C-22 temp. sensor, incl. chip Alloy C-22 Ø 1/4 (6.35 mm), 300 mm 51162886 Accessories holder set to be attached to the lab bar of your OptiMax system for stirrer motor (ST24), for Ø 12 mm probes (ST19), for Ø 6 mm probes (ST14) Stainless steel, GF25 Quantity in a set 2 x holders 1 x adapter with ST14 aperture 4 x adapters with ST19 aperture 1 x adapter with ST24 aperture 51162720 adapter, eccentric for Tr and turbidity probe, including 51162716 sealing ring Inner Ø 6 mm, ST14 can also be used for Ø 1/4 6.35 mm inserts 51162716 Sealing ring for 51162720 adapter Inner Ø 6 mm can also be used for Ø 1/4 6.35 mm inserts 51161778 Purge gas set for overhead stirrer available only as a set Stainless steel, PVC, PP Temperature PP max 30 C Quantity in a set 1 x bulkhead connector 2 x quick connect couplings (for tubes inner Ø 4 mm) 1 x reducing connector (for tubes inner Ø 7 mm to 11 mm and 4 mm to 7 mm) 1 x PVC tube (inner Ø 4 mm) 51190319 Plastic hose, straight with silicone rubber seal, for GL14 screw cap PP, VQM For tube inner Ø 6 mm to 9 mm 51162885 Touchscreen cable extension to be ordered with base unit or assembled by a field service engineer Length 3 m 11
OptiMax 1000 ml Two-Piece Glass Reactor Set OptiMax 1000 ml Glass Reactor Set Two-Piece 51162831 1000 ml two-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 1000 ml two-piece glass reactor set consisting of The 1000 ml two-piece glass reactor is equipped with a bottom drain valve and has a working volume of 1000 ml, a nominal volume of 1310 ml and a starting volume of 200 ml. Order Number Product Description Quantity 51162634 Glass reactor, 1000 ml 1 51162782 Reactor holder for 1000 ml reactor 1 51162671 Glass cover, for 1000/500 ml reactor, 7 ports 1 51162780 Cover holder for 1000/500 ml reactor cover 1 51162673 Reactor clamp for 1000/500 ml reactor 1 51192205 O-ring for 1000/500 ml reactor 1 51162722 Stirrer shaft for 1000/500 ml reactor, Alloy C-22 1 103504 Pitched stirrer blade, Alloy C-22, downward 1 51162637 Bar type baffle for 1000 ml reactor, Alloy C-22 1 51104154 adapter for baffle 1 51162685 Drain union, bended 1 51192169 Pinch clamp S19 1 71518 Glass stopper ST29/32 2 71517 Glass stopper ST19/26 3 51190878 Glass stopper ST14/23 1 51192168 Keck clamp ST29 2 51192167 Keck clamp ST24 1 51191429 Keck clamp ST19 3 51191505 Keck clamp ST14 1 12
OptiMax 1000 ml Two-Piece Glass Reactor Set ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST24/29 Overhead stirrer ST29/32 ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/8 15.875 mm ST29/32 ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/8 15.875 mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/4 6.35 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm 51162634 1000 ml glass reactor Borosilicate glass,, PEEK, silicone Working Volume Max. 1000 ml Nominal Volume 1310 ml Temperature 40 C to 180 C Inner Ø 101 mm, height 172 mm, wall 3 mm 51162671 Glass cover for 1000/500 ml reactor, seven ports 1 x ST14/23, 3 x ST19/26, 2 x ST29/32, center ST24/29 Borosilicate glass Temperature 40 C to 180 C Inner Ø 98 mm 51162782 Reactor holder for 1000 ml reactor Stainless steel 1.4404, PE 51162780 Cover holder for 1000/500 ml reactor cover Stainless steel 1.4404, PE Inner Ø 121 mm x 22 mm 51162673 Reactor clamp for 1000/500 ml reactor Stainless steel 1.4404, Glastherm HT 220 (Thermalite 220M) 51192205 O-ring for 1000/500 ml reactor Elastomer Vollkern Silicone VQM, FEP-coated Temperature 60 C to 200 C Ø 107.5 mm x 3.53 mm, AS No. 244 13
OptiMax 1000 ml Two-Piece Glass Reactor Set 51162685 Drain union, bended Borosilicate glass Inner Ø 9 mm, spherical joint S19 51192169 Pinch clamp S19 drain union clamp Stainless steel 71518 Glass stopper ST29/32 Glass 71517 Glass stopper ST19/26 Glass 51190878 Glass stopper ST14/23 Glass 51192168 Keck clamp ST29 POM 51192167 Keck clamp ST24 POM 51191429 Keck clamp ST19 POM 51191505 Keck clamp ST14 POM 14
OptiMax 1000 ml Two-Piece Glass Reactor Set 51162722 Stirrer shaft for 1000/500 ml reactor M8 thread Alloy C-22 Ø 10 mm, length 400 mm 103504 Pitched stirrer blade for 1000/500 ml reactor downward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm 51104154 adapter for baffle, eccentric for baffle, including 103047 sealing ring Inner Ø 10 mm, ST19 51162637 Bar type baffle for 1000 ml reactor Alloy C-22 Ø 10 mm, width 15 mm, length 249 mm Optional Accessories 51192218 O-ring for 1000/500 ml reactor FFKM Temperature up to 275 C Ø 107.5 mm x 3.53 mm, AS No. 244 15
OptiMax Cover Set OptiMax Cover Set For 1000 ml and 500 ml Reactors 30090540 OptiMax cover set This reactor cover is an extremely robust alternative for the standard glass cover 51162671. It is the perfect choice if the reactor is equipped with heavy inserts and probes which bears the risk to break the glass version of the cover. The cover comes as full set with all the required adapters to accommodate typical combinations of probes and inserts. OptiMax cover set consisting of The cover can be used in combination with the standard O-rings and reactor clamp as used for the glass cover. COWIE part number Product Description Quantity cover for 1000 ml and 500 ml reactors 1 OptiMax standard stirrer adapter, ST24/32 x 3/4 NPT 1 PC711.1919 ST19/38 x 3/4 NPT 3 PC711.2925 ST29/42 x 1 NPT 2 PC711.1413 ST14/35 x 1/2 NPT 1 PC701.100.19 1 NPT x 19 mm compression fitting 1 PC701.100.625 1 NPT x 5/8 15.875 mm compression fitting 1 PC701.075.14 3/4 NPT x 14 mm compression fitting 1 PC701.075.12 3/4 NPT x 12 mm compression fitting 1 PC701.075.08 3/4 NPT x 8 mm compression fitting 1 PC701.075.375 3/4 NPT x 3/8 9.525 mm compression fitting 1 PC701.075.250 3/4 NPT x 1/4 6.35 mm compression fitting 1 PC701.050.06 1/2 NPT x 6 mm compression fitting 1 PC701.050.250 1/2 NPT x 1/4 6.35 mm compression fitting 1 Note: All the contained threaded adapters are standard parts from COWIE. In case replacement or additional adapters are required, please refer to www.cowie.com. All the COWIE part numbers are indicated with a PC as prefix. 16
OptiMax Cover Set The cover is mainly used to run crystallization experiments. Special care needs to be taken when the cover is used for reflux experiments since absolute solvent tightness cannot be guaranteed under all circumstances. 3/4 NPT ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm, calibration heater Ø 8 mm 3/4 NPT Overhead stirrer 3/4 NPT ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm, calibration heater Ø 8 mm 1 NPT ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/8 15.875 mm, ParticleTrack G400 probe Ø 19 mm 1 NPT ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/8 15.875 mm, ParticleTrack G400 probe Ø 19 mm 1/2 NPT Tr probe glass Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/4 6.35 mm, Tr probe Alloy C-22 Ø 1/4 6.35 mm 3/4 NPT ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm, calibration heater Ø 8 mm cover for 1000 ml and 500 ml reactors, seven ports 2 x 1 NPT, 4 x 3/4 NPT, 1 x 1/2 NPT Temperature 40 C to 180 C OptiMax standard stirrer adapter ST24/32 x 3/4 NPT Inner Ø ST24/32, 3/4 NPT PC711.2925 ST29/42 x 1 NPT Inner Ø ST29/42, 1 NPT, height 60 mm PC711.1919 ST19/38 x 3/4 NPT Inner Ø ST19/38, 3/4 NPT, height 57 mm PC711.1413 ST14/30 x 1/2 NPT Inner Ø ST14/35, 1/2 NPT, height 45 mm PC701.100.19 1 NPT x 19 mm compression fitting Inner Ø 19 mm, 1 NPT 17
OptiMax Cover Set PC701.100.625 1 NPT x 5/8 compression fitting, PEEK Inner Ø 5/8 15.875 mm, 1 NPT PC701.075.14 3/4 NPT x 14 mm compression fitting, PEEK Inner Ø 14 mm, 3/4 NPT PC701.075.12 3/4 NPT x 12 mm compression fitting, PEEK Inner Ø 12 mm, 3/4 NPT PC701.075.08 3/4 NPT x 8 mm compression fitting, PEEK Inner Ø 8 mm, 3/4 NPT PC701.075.375 3/4 NPT x 3/8 compression fitting, PEEK Inner Ø 3/8 9.525 mm, 3/4 NPT PC701.075.250 3/4 NPT x 1/4 compression fitting, PEEK Inner Ø 1/4 6.35 mm, 3/4 NPT PC701.050.250 1/2 NPT x 1/4 compression fitting, PEEK Inner Ø 1/4 6.35 mm, 1/2 NPT PC701.050.06 1/2 NPT x 6 mm compression fitting, PEEK Inner Ø 6 mm, 1/2 NPT 18
OptiMax 500 ml Two-Piece Glass Reactor Set OptiMax 500 ml Glass Reactor Set Two-Piece 51162832 500 ml two-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 500 ml two-piece glass reactor set consisting of The 500 ml two-piece glass reactor is equipped with a bottom drain valve and has a working volume of 500 ml, a nominal volume of 830 ml and a starting volume of 70 ml. Order Number Product Description Quantity 51162632 Glass reactor, 500 ml 1 51162783 Reactor holder for 500 ml reactor 1 51162671 Glass cover, for 1000/500 ml reactor, 7 ports 1 51162780 Cover holder for 1000/500 ml reactor cover 1 51162670 Receptacle for 500 ml reactor 1 51162673 Reactor clamp for 1000/500 ml reactor 1 51192205 O-ring for 1000/500 ml reactor 1 51162722 Stirrer shaft for 1000/500 ml reactor, Alloy C-22 1 103504 Pitched stirrer blade, Alloy C-22, downward 1 51162638 Bar type baffle for 500 ml reactor, Alloy C-22 1 51104154 adapter for baffle 1 51162685 Drain union, bended 1 51192169 Pinch clamp S19 1 71518 Glass stopper ST29/32 2 71517 Glass stopper ST19/26 3 51190878 Glass stopper ST14/23 1 51192168 Keck clamp ST29 2 51192167 Keck clamp ST24 1 51191429 Keck clamp ST19 3 51191505 Keck clamp ST14 1 19
OptiMax 500 ml Two-Piece Glass Reactor Set ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST24/29 Overhead stirrer ST29/32 ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/8 15.875 mm ST29/32 ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/8 15.875 mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/4 6.35 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm 51162632 500 ml glass reactor Borosilicate glass,, PEEK, silicone Working Volume Max. 500 ml Nominal Volume 830 ml Temperature 40 C to 180 C Inner Ø 77 mm, height 172 mm, wall 2.5 mm 51162671 Glass cover for 1000/500 ml reactor, seven ports 1 x ST14/23, 3 x ST19/26, 2 x ST29/32, center ST24/29 Borosilicate glass Temperature 40 C to 180 C Inner Ø 98 mm 51162783 Reactor holder for 500 ml reactor Stainless steel 1.4404, PE 51162780 Cover holder for 1000/500 ml reactor cover Stainless steel 1.4404, PE Inner Ø 121 mm x 22 mm 51162670 Receptacle for 500 ml reactor Thermostat sleeve Aluminium anodized 20
OptiMax 500 ml Two-Piece Glass Reactor Set 51162673 Reactor clamp for 1000/500 ml reactor Stainless steel 1.4404, Glastherm HT 220 (Thermalite 220M) 51192205 O-ring for 1000/500 ml reactor Elastomer Vollkern Silicone VQM, FEP-coated Temperature 60 C to 200 C Ø 107.5 mm x 3.53 mm, AS No. 244 51162685 Drain union, bended Borosilicate glass Inner Ø 9 mm, spherical joint S19 51192169 Pinch clamp S19 drain union clamp Stainless steel 71518 Glass stopper ST29/32 Glass 71517 Glass stopper ST19/26 Glass 51190878 Glass stopper ST14/23 Glass 51192168 Keck clamp ST29 POM 51192167 Keck clamp ST24 POM 21
OptiMax 500 ml Two-Piece Glass Reactor Set 51191429 Keck clamp ST19 POM 51191505 Keck clamp ST14 POM 51162722 Stirrer shaft for 1000/500 ml reactor M8 thread Alloy C-22 Ø 10 mm, length 400 mm 103504 Pitched stirrer blade for 1000/500 ml reactor downward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm 51104154 adapter for baffle, eccentric for baffle, including 103047 sealing ring Inner Ø 10 mm, ST19 51162638 Bar type baffle for 500 ml reactor Alloy C-22 Ø 10 mm, width 15 mm, length 237 mm Optional Accessories 51192218 O-ring for 1000/500 ml reactor FFKM Temperature up to 275 C Ø 107.5 mm x 3.53 mm, AS No. 244 22
OptiMax 250 ml Two-Piece Glass Reactor Set OptiMax 250 ml Glass Reactor Set Two-Piece 51162833 250 ml two-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 250 ml two-piece glass reactor set consisting of The 250 ml two-piece glass reactor has no bottom drain valve and has a working volume of 250 ml, a nominal volume of 370 ml and a starting volume of 50 ml. Order Number Product Description Quantity 51162635 Glass reactor, 250 ml 1 51162758 Reactor stand for 250 ml reactor 1 51162699 Glass cover for 250 ml reactor, 7 ports 1 51162781 Cover holder for 250 ml reactor cover 1 51162698 Receptacle for 250 ml reactor 1 51162703 Reactor clamp for 250 ml reactor 1 51192170 O-ring for 250 ml reactor 1 51162417 Stirrer shaft for 250 ml reactor, Alloy C-22 1 51162418 Pitched stirrer blade, Alloy C-22, downward 1 71517 Glass stopper ST19/26 4 51190878 Glass stopper ST14/23 2 51192167 Keck clamp ST24 1 51191429 Keck clamp ST19 4 51191505 Keck clamp ST14 2 23
OptiMax 250 ml Two-Piece Glass Reactor Set ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/4 6.35 mm ST24/29 Overhead stirrer ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/4 6.35 mm 51162635 Glass reactor, 250 ml Borosilicate glass Working Volume Max. 250 ml Nominal Volume 370 ml Temperature 40 C to 180 C Inner Ø 62 mm, height 127 mm, wall 2.2 mm 51162699 Glass cover for 250 ml reactor, seven ports 2 x ST14/23, 4 x ST19/26, center ST24/29 Borosilicate glass Temperature 40 C to 180 C Inner Ø 68 mm 51162758 Reactor stand for 250 ml reactor PE Ø 108 mm x 105 mm 51162781 Cover holder for 250 ml reactor cover Stainless steel 1.4404, PE Inner Ø 88 mm x 22 mm 51162698 Receptacle for 250 ml reactor Thermostat sleeve Aluminium anodized 51162703 Reactor clamp for 250 ml reactor Stainless steel 1.4404, Glastherm HT 220 (Thermalite 220M) 24
OptiMax 250 ml Two-Piece Glass Reactor Set 51192170 O-ring for 250 ml reactor Elastomer Vollkern Silicone VQM, FEP-coated Temperature 60 C to 200 C Ø 69.44 mm x 3.53 mm, AS No. 232 51162417 Stirrer shaft for 250 ml reactor M3 thread Alloy C-22 Ø 10/8 mm, length 400 mm 51162418 Pitched stirrer blade for 250 ml reactor downward, four impellers, 45, M3 thread Alloy C-22 Outer Ø 38 mm 71517 Glass stopper ST19/26 Glass 51190878 Glass stopper ST14/23 Glass 51192167 Keck clamp ST24 POM 51191429 Keck clamp ST19 POM 51191505 Keck clamp ST14 POM Optional Accessories 51192219 O-ring for 250 ml reactor FFKM Temperature up to 275 C Ø 69.44 mm x 3.53 mm, AS No. 244 25
OptiMax 1000 ml One-Piece Glass Reactor Set OptiMax 1000 ml Glass Reactor Set One-Piece 51162834 1000 ml one-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 1000 ml one-piece glass reactor set consisting of The 1000 ml one-piece glass reactor has a working volume of 1000 ml, a nominal volume of 1150 ml and a starting volume of 200 ml. Order Number Product Description Quantity 51162732 One-piece glass reactor, 1000 ml 1 51162760 Reactor stand for 1000 ml reactor 1 51162681 Glass stirrer shaft for 1000/500/250 ml one-piece reactor 1 51162682 Half-moon stirrer blade, 71 mm 1 51162637 Bar type baffle for 1000 ml reactor, Alloy C-22 1 51104154 adapter for baffle 1 71518 Glass stopper ST29/32 1 71517 Glass stopper ST19/26 4 51190878 Glass stopper ST14/23 1 51192168 Keck clamp ST29 1 51192167 Keck clamp ST24 1 51191429 Keck clamp ST19 4 51191505 Keck clamp ST14 1 26
OptiMax 1000 ml One-Piece Glass Reactor Set ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST24/29 Overhead stirrer ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST29/32 ParticleTrack D/G600 probe Ø 19 mm, PVM V819 probe Ø 19 mm, ReactIR probe Ø 5/8 15.875 mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/4 6.35 mm 51162732 1000 ml one-piece glass reactor, seven ports 1 x ST14/23, 4 x ST19/26, 1 x ST29/32, center ST24/29 Borosilicate glass Working Volume Max. 1000 ml Nominal Volume 1150 ml Temperature 40 C to 180 C Inner Ø 101 mm, height 230 mm, wall 3 mm 51162760 Reactor stand for 1000 ml one-piece reactor PE Ø 148 mm x 120 mm 51162681 Glass stirrer shaft for 1000/500/250 ml reactor Borosilicate glass Ø 10 mm, length 380 mm 51162637 Bar type baffle for 1000 ml reactor Alloy C-22 Ø 10 mm, width 15 mm, length 249 mm 51162682 Half-moon stirrer blade for 1000 ml reactor 19 mm x 71 mm 51104154 adapter for baffle, eccentric for baffle, including 103047 sealing ring Inner Ø 10 mm, ST19 27
OptiMax 1000 ml One-Piece Glass Reactor Set 71518 Glass stopper ST29/32 Glass 71517 Glass stopper ST19/26 Glass 51190878 Glass stopper ST14/23 Glass 51192168 Keck clamp ST29 POM 51192167 Keck clamp ST24 POM 51191429 Keck clamp ST19 POM 51191505 Keck clamp ST14 POM 28
OptiMax 500 ml One-Piece Glass Reactor Set OptiMax 500 ml Glass Reactor Set One-Piece 51162835 500 ml one-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 500 ml one-piece glass reactor set consisting of The 500 ml one-piece glass reactor has a working volume of 500 ml, a nominal volume of 700 ml and a starting volume of 70 ml. Order Number Product Description Quantity 51162733 One-piece glass reactor, 500 ml 1 51162670 Receptacle for 500 ml reactor 1 51162681 Glass stirrer shaft for 1000/500/250 ml one-piece reactor 1 51162683 Half-moon stirrer blade, 54 mm 1 51162759 Reactor stand for 500 ml reactor 1 51162638 Bar type baffle for 500 ml reactor, Alloy C-22 1 51104154 adapter for baffle 1 71517 Glass stopper ST19/26 4 51190878 Glass stopper ST14/23 2 51192168 Keck clamp ST29 1 51192167 Keck clamp ST24 1 51191429 Keck clamp ST19 4 51191505 Keck clamp ST14 2 29
OptiMax 500 ml One-Piece Glass Reactor Set ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST24/29 Overhead stirrer ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/4 6.35 mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/4 6.35 mm 51162733 500 ml one-piece glass reactor, seven ports 2 x ST14/23, 4 x ST19/26, center ST24/29 Borosilicate glass Working Volume Max. 500 ml Nominal Volume 700 ml Temperature 40 C to 180 C Inner Ø 77 mm, height 225 mm, wall 2.5 mm 51162670 Receptacle for 500 ml one-piece reactor Thermostat sleeve Aluminium anodized 51162681 Glass stirrer shaft for 1000/500/250 ml reactor Borosilicate glass Ø 10 mm, length 380 mm 51162759 Reactor stand for 500 ml one-piece reactor PE Ø 123 mm x 120 mm 51162683 Half-moon stirrer blade for 500 ml reactor 19 mm x 54 mm 30
OptiMax 500 ml One-Piece Glass Reactor Set 51104154 adapter for baffle, eccentric for baffle, including 103047 sealing ring Inner Ø 10 mm, ST19 51162638 Bar type baffle for 500 ml reactor Alloy C-22 Ø 10 mm, width 15 mm, length 237 mm 71517 Glass stopper ST19/26 Glass 51190878 Glass stopper ST14/23 Glass 51192168 Keck clamp ST29 POM 51192167 Keck clamp ST24 POM 51191429 Keck clamp ST19 POM 51191505 Keck clamp ST14 POM 31
OptiMax 250 ml One-Piece Glass Reactor Set OptiMax 250 ml Glass Reactor Set One-Piece 51162836 250 ml one-piece glass reactor set The different OptiMax reactor sets combine all the available parts for a particular reactor type and volume in just one part number. This simplifies the evaluation and ordering process and makes it error-free. OptiMax 250 ml one-piece glass reactor set consisting of The 250 ml one-piece glass reactor has a working volume of 250 ml, a nominal volume of 400 ml and a starting volume of 50 ml. Order Number Product Description Quantity 51162734 One-piece glass reactor, 250 ml 1 51162758 Reactor stand for 250 ml reactor 1 51162698 Receptacle for 250 ml reactor 1 51162681 Glass stirrer shaft for 1000/500/250 ml one-piece reactor 1 51162684 Half-moon stirrer blade, 43 mm 1 71517 Glass stopper ST19/26 4 51190878 Glass stopper ST14/23 2 51192167 Keck clamp ST24 1 51191429 Keck clamp ST19 4 51191505 Keck clamp ST14 2 32
OptiMax 250 ml One-Piece Glass Reactor Set ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/4 6.35 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST24/29 Overhead stirrer ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm ST14/23 Tr probe Ø 6 mm, turbidity probe Ø 6 mm, ReactIR probe Ø 1/4 6.35 mm ST19/26 Bar type baffle, ParticleTrack S/G400 Ø 14 mm, ph probe Ø 12 mm, turbidity probe Ø 12 mm, ReactIR probe Ø 3/8 9.525 mm 51162734 250 ml one-piece glass reactor, seven ports 2 x ST14/23, 4 x ST19/26, center ST24/29 Borosilicate glass Working Volume Max. 250 ml Nominal Volume 400 ml Temperature 40 C to 180 C Inner Ø 62 mm, height 205 mm, wall 2.5 mm 51162698 Receptacle for 250 ml one-piece reactor Thermostat sleeve Aluminium anodized 51162681 Glass stirrer shaft for 1000/500/250 ml reactor Borosilicate glass Ø 10 mm, length 380 mm 51162758 Reactor stand for 250 ml one-piece reactor PE Ø 108 mm x 105 mm 51162684 Half-moon stirrer blade, 43 mm 19 mm x 43 mm 33
OptiMax 250 ml One-Piece Glass Reactor 71517 Glass stopper ST19/26 Glass 51190878 Glass stopper ST14/23 Glass 51192167 Keck clamp ST24 POM 51191429 Keck clamp ST19 POM 51191505 Keck clamp ST14 POM 34
OptiMax Spare Parts, Adapters, and Stirrers OptiMax Reactor Spare Parts and Adapters 51162633 Glass vessel for two-piece 1000 ml reactor without parts for bottom drain valve Borosilicate glass Working Volume Nominal Volume Max. 1000 ml 1300 ml Temperature 40 C to 180 C Inner Ø 101 mm, height 172 mm, wall 3 mm 51162631 Glass vessel for two-piece 500 ml reactor without parts for bottom drain valve Borosilicate glass Working Volume Nominal Volume Max. 500 ml 700 ml Temperature 40 C to 180 C Inner Ø 77 mm, height 172 mm, wall 2.5 mm 51162730 Bottom drain connect set for bottom drain valve PEEK, Ø 52 mm 71540 Sealing ring for bottom drain FEP Inner Ø 22 mm, 14 mm 51191774 Spindle, bottom drain valve 115 mm, with spring Ø 14 mm x 115 mm 51160970 adapter, eccentric for PVM/D600 probe, including 51160973 sealing ring Inner Ø 19 mm, ST29 51160973 Sealing ring for 51160970 adapter cord Inner Ø 19 mm Quantity 5 pcs in a set 35
OptiMax Spare Parts, Adapters, and Stirrers 51104154 adapter for baffle, eccentric for baffle, including 103547 sealing ring Inner Ø 10 mm, ST19 103547 Sealing ring for 51104154 adapter cord Inner Ø 10 mm Quantity 5 pcs in a set 51162880 adapter for G400, including 51162879 sealing ring Inner Ø 14 mm, ST19 51162879 Sealing ring for 51162880 adapter Inner Ø 14 mm 51162717 adapter, eccentric for ph and turbidity probe, including 51162765 sealing ring Inner Ø 12 mm, ST19 51162765 Sealing ring for 51162717 adapter Inner Ø 12 mm 51162713 adapter, eccentric for turbidity probe, including 51162716 sealing ring Inner Ø 6 mm, ST19 Can also be used for Ø 1/4 6.35 mm inserts 51162716 Sealing ring for 51162713 and 51162720 adapters Inner Ø 6 mm Can also be used for Ø 1/4 6.35 mm inserts 36 51162720 adapter, eccentric for Tr and turbidity probe, including 51162716 sealing ring Inner Ø 6 mm, ST14 Can also be used for Ø 1/4 6.35 mm inserts
OptiMax Spare Parts, Adapters, and Stirrers OptiMax Mixing Device Available Stirrers For 1000 ml two-piece reactor 51162722 Stirrer shaft for 1000/500 ml reactor M8 thread Alloy C-22 Ø 10 mm, length 400 mm 103507 Anchor blade for 1000 ml reactor M8 thread Alloy C-22 Outer Ø 90 mm, height 100 mm 51160025 Pitched stirrer blade for 1000/500 ml reactor upward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm 103504 Pitched stirrer blade for 1000/500 ml reactor downward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm 51162826 Pitched-blade glass stirrer for 1000/500 ml reactor upward, four impellers, 45 Borosilicate glass Outer Ø 45 mm, length 400 mm 51162825 Pitched-blade glass stirrer for 1000/500 ml reactors downward, four impellers, 45 Borosilicate glass Outer Ø 45 mm, length 400 mm 37
OptiMax Spare Parts, Adapters, and Stirrers For 500 ml two-piece reactor 51162722 Stirrer shaft for 1000/500 ml reactor M8 thread Alloy C-22 Ø 10 mm, length 400 mm 51162677 Anchor blade for 500 ml reactor M8 thread Alloy C-22 Outer Ø 69 mm, height 100 mm 51160025 Pitched stirrer blade for 1000/500 ml reactor upward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm 103504 Pitched stirrer blade for 1000/500 ml reactor downward, four impellers, 45, M8 thread Alloy C-22 Outer Ø 45 mm 51162826 Pitched-blade glass stirrer for 1000/500 ml reactor upward, four impellers, 45 Borosilicate glass Outer Ø 45 mm, length 400 mm 51162825 Pitched-blade glass stirrer for 1000/500 ml reactor downward, four impellers, 45 Borosilicate glass Outer Ø 45 mm, length 400 mm 38
OptiMax Spare Parts, Adapters, and Stirrers For 250 ml two-piece reactor 51162417 Stirrer shaft for 250 ml reactor M3 thread Alloy C-22 Ø 10/8 mm, length 400 mm 51162678 Anchor stirrer for 250 ml reactor M3 thread Alloy C-22 Outer Ø 55 mm, height 80 mm 51162442 Pitched stirrer blade for 250 ml reactor upward, four impellers, 45, M3 thread Alloy C-22 Outer Ø 38 mm 51162418 Pitched stirrer blade for 250 ml reactor downward, four impellers, 45, M3 thread Alloy C-22 Outer Ø 38 mm 51162424 Pitched-blade glass stirrer for 250 ml reactor upward, four impellers, 45 Borosilicate glass Outer Ø 38 mm, length 400 mm 51162423 Pitched-blade glass stirrer for 250 ml reactor downward, four impellers, 45 Borosilicate glass Outer Ø 38 mm, length 400 mm 39
OptiMax Spare Parts, Adapters, and Stirrers For 1000 ml one-piece reactor 51162681 Glass stirrer shaft for 1000/500/250 ml one-piece reactor Borosilicate glass Ø 10 mm, length 380 mm 51162682 Half-moon stirrer blade for 1000 ml one-piece reactor 19 mm x 71 mm For 500 ml one-piece reactor 51162681 Glass stirrer shaft for 1000/500/250 ml one-piece reactor Borosilicate glass Ø 10 mm, length 380 mm 51 162 683 Half-moon stirrer blade for 500 ml one-piece reactor 19 mm x 54 mm For 250 ml one-piece reactor 51162681 Glass stirrer shaft for 1000/500/250 ml one-piece reactor Borosilicate glass Ø 10 mm, length 380 mm 51162684 Half-moon stirrer blade for 250 ml one-piece reactor 19 mm x 43 mm 40
OptiMax Accessories and Probes OptiMax Accessories Reflux Condenser, Tr and ph Probes 51192166 Reflux condenser glass, ST19 Borosilicate glass 250 mm x 40 mm 51162827 Glass temp. sensor, including chip Glass Ø 6 mm, 300 mm 51162839 Alloy C-22 temp. sensor, including chip Alloy C-22 Ø 1/4 6.35 mm, 300 mm 51162829 ph sensor OptiMax, incl. chip without cable Lead-free glass (shaft), high alkaline glass (membrane) Ø 12 mm, 325 mm (glass body only) 51162888 Cable for 51162829 ph sensor Length 100 cm 41
OptiMax Accessories and Probes Dosing Unit SP-50 Set 51161770 Dosing unit SP-50 set This unit will allow you to dose one reagent in two reactors completely independent and in parallel via touchscreen or PC software. Only available in the set. Dosing unit SP-50 set consisting of Order Number Product Description Quantity Dosing Unit SP-50, only available in the set 1 51191988 CAN cable 100 cm 1 51191306 dosing tube Ø 3.2 mm 3 51191304 dosing tube Ø 1.6 mm 2 51191515 Nut for UNF 1/4 28 threads, outer Ø max. 3.2 mm, 4 pcs in a set 1 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm, 4 pcs in a set 1 51191204 Plug for UNF 1/4 28 threads, 4 pcs in a set 1 51191203 Nut for UNF 1/4 28 threads, outer Ø max. 1.6 mm, 4 pcs in a set 1 51191202 Ferrule for tubing and sensors of outer Ø 1.6 mm, 4 pcs in a set 1 51191267 Glass adapter ST14/23-GL14 2 51190318 Screw cap GL14, closed 3 51191170 Silicone rubber seal (septum), 10 pcs in a set 1 51191972 Distributor cap GL45 2 x GL14 1 51191591 Bottle GL45 250 ml with cap 1 51161558 Adapter GL14-UNF 3 51190317 Screw cap GL14, with aperture 3 51103947 Silicone rubber sealing ring, outer Ø 12 mm, aperture 6 mm 6 51191687 Assorted heat-shrink tubings, 8 pcs in a set 1 42
OptiMax Accessories and Probes 51191515 Nut for UNF 1/4 28 threads ETFE Outer Ø max. 3.2 mm Quantity 4 pcs in a set only available in the set Dosing unit SP-50 51191514 Ferrule for tubing and sensors of outer Ø 3.2 mm Quantity ETFE Outer Ø max. 3.2 mm 4 pcs in a set 51191988 CAN cable 100 cm Length 100 cm 51191204 Plug for UNF 1/4 28 threads ETFE Outer Ø max. 1.6 mm Quantity 4 pcs in a set 51191306 dosing tube Ø 3.2 mm Ø 3.2 mm, length 2.5 m 51191203 Nut for UNF 1/4 28 threads ETFE Outer Ø max. 1.6 mm Quantity 4 pcs in a set 51191304 dosing tube Ø 1.6 mm Ø 1.6 mm, length 2.5 m 51191202 Ferrule for tubing and sensors of outer Ø 1.6 mm Quantity ETFE Outer Ø max. 1.6 mm 4 pcs in a set 43
OptiMax Accessories and Probes 51191267 Glass adapter ST14/23-GL14 Glass Height 54 mm 51161558 Adapter GL14-UNF GF25 36.14 mm x 2.62 mm 51190318 Screw cap GL14, closed with sealing PBT Temperature Max. 200 C 51190317 Screw cap GL14, with aperture PBT Temperature Max. 200 C Aperture Ø 9.5 mm 51191170 Silicone rubber seal (septum) for screw cap GL14 Quantity Silicone rubber VQM Ø 12 mm, thickness 2 mm 10 pcs in a set 51103947 Sealing ring with vulcanized-on washers for GL14 cap Silicone rubber VQM, -coated Ø 12 mm, aperture 6 mm 51191972 Distributor cap GL45 2x GL14 PP 51191687 Assorted heat-shrink tubings 8 pcs in a set Polyolefin 51191591 Bottle GL45 250 ml with cap Glass, PP 44
OptiMax Accessories and Probes Dosing Unit SP-50 Syringes Flexible volumes from 1 ml, 10 ml, 25 ml, and 50 ml syringes Automatic refill of syringes possible with Dosing Unit SP-50 Interchangeable at all times during an experiment 51191793 Syringe 1 ml Glass,, metal Volume 1 ml 51191794 Syringe 25 ml Glass,, metal Volume 25 ml 51191792 Syringe 10 ml Glass,, metal Volume 10 ml 51191987 Syringe 50 ml Glass,, metal Volume 50 ml 45
OptiMax Accessories and Probes OptiMax HFCal Kit 30 050 150 OptiMax HFCal Kit A calorimetry Upgrade Kit for OptiMax. It is Plug&Play and contains all necessary parts to convert the workstation into a fully functional calorimeter. icontrol software is not included. No service call is required for installation. OptiMax HFCal kit consisting of Order Number Product Description Quantity 30050151 OptiMax HFCal box 1 30050155 Calibration heater, 300 mm 1 30064131 Adapter ST19,, with sealing ring 1 51191988 CAN cable 100 cm 1 30050157 icontrol HeatFlow License 1 46
OptiMax Accessories and Probes 51191988 CAN cable 100 cm Length 100 cm 30050151 OptiMax HFCal box can be attached on the left or right side of the OptiMax 120 mm x 40 mm x 170 mm (w, d, h) 30050155 Calibration heater Alloy C-22 Ø 8 mm, 300 mm 30064131 adapter, eccentric for calibration heater, including 30064134 sealing ring Inner Ø 8 mm, ST19 30064134 Sealing ring for 30064131 adapter Inner Ø 8 mm OptiMax Calorimetry Starter Kit 30064130 OptiMax Calorimetry Starter Kit The OptiMax HFCal Starter Kit is a heat flow based, ready-to-use system to quickly obtain heat data of any chemical or physical reaction in a 1 L scale. The kit includes all parts required in just one single part number. The icontrol software and the HFCal license are included too. OptiMax Calorimetry Starter kit consisting of Order Number Product Description Quantity 51162830 OptiMax Startet Kit for details see page 5 1 30050150 OptiMax HFCal Kit 1 51161893 icontrol Single Instrument License for details see page 49 1 47
48 Notes
icontrol Software for OptiMax icontrol Software for OptiMax Optional Accessories The software for experiment preparation, instrument control and data evaluation icontrol for single or multiple instruments icontrol for Office icare software maintenance icontrol provides the maximum amount of information from a single experiment. It uses a simple-tooperate user interface enabling EasyMax to be operated by either the PC software or in combination with the touchscreen. icontrol enables scientists to gain a comprehensive understanding of the chemical reaction under study. The combination of reactor data with information from METTLER TOLEDO analytical tools helps chemists in research and development reach appropriate con-clusions from each experiment, enabling them to make better decisions and complete projects faster. icontrol Software for OptiMax Order Number License type Description 51161893 icontrol Single Instrument License Software license for experiment preparation, control and data evaluation for one instrument 51162612 icontrol Multiple Instrument License Software license for experiment preparation, control and data evaluation for up to three instruments 51162613 icontrol Office License Software license for experiment preparation and experiment evaluation 51162629 icare for icontrol Instrument Software maintenance for instrument license 51162630 icare for icontrol Office Software maintenance for office license 49
Compatibility List 1000 ml glass reactor and cover 1000 ml glass reactor and cover 500 ml glass reactor and cover 500 ml glass reactor and cover 51160025 Pitched stirrer blade, upward, four impellers, Ø 45 mm, Alloy C-22 103504 Pitched stirrer blade, downward four impellers, Ø 45 mm, Alloy C-22 1 1 1 1 1 1 1 1 103507 Anchor blade, Ø 90 mm, Alloy C-22 1 1 51162677 Anchor blade, Ø 69 mm, Alloy C-22 1 1 51162826 Pitched-blade stirrer, upward four impellers, Ø 45 mm, glass 51162825 Pitched-blade stirrer, downward four impellers, Ø 45 mm, glass 1 1 1 1 1 1 1 1 51162442 Pitched stirrer blade, upward four impellers, Ø 38 mm, Alloy C-22 51162418 Pitched stirrer blade, downward four impellers, Ø 38 mm, Alloy C-22 51162678 Anchor blade, Ø 55 mm, Alloy C-22 51162424 Pitched-blade stirrer, upward four impellers, Ø 38 mm, glass 51162423 Pitched-blade stirrer, downward four impellers, Ø 38 mm, glass 51162637 Bar type baffle, 15 mm x 249 mm, Alloy C-22 3 51162638 Bar type baffle, 15 mm x 237 mm, Alloy C-22 51162839 Temp. sensor, Alloy C-22, 1/4 6.35 mm x 300 mm, incl. chip 51162827 Temp. sensor, glass, 6 mm x 300 mm, incl. chip 4 4 4 4 4 4 4 4 3 51162829 ph sensor OptiMax, incl. chip 4 4 4 4 51192166 Reflux condenser glass, ST19, 250 mm x 40 mm Needed items 1) 51162722 Stirrer shaft 2) 51162417 Stirrer shaft 3) 51104154 adapter for baffle 4) 51162720 adapter, ST14 5) 51162681 Stirrer shaft 51162634 1000 ml glass reactor 51162671 Glass cover 51162634 1000 ml glass reactor 30083877 cover 51162632 500 ml glass reactor 51162671 Glass cover 51162632 500 ml glass reactor 30083877 cover 50
Compatibility List 250 ml glass reactor and cover 1000 ml one-piece glass reactor 500 ml one-piece glass reactor 250 ml one-piece glass reactor 51162442 Pitched stirrer blade, upward four impellers, Ø 38 mm, Alloy C-22 51162418 Pitched stirrer blade, downward four impellers, Ø 38 mm, Alloy C-22 2 2 51162678 Anchor blade, Ø 55 mm, Alloy C-22 2 51162424 Pitched-blade stirrer, upward four impellers, Ø 38 mm, glass 51162423 Pitched-blade stirrer, downward four impellers, Ø 38 mm, glass 2 2 51162682 Half-moon stirrer blade, 19 mm x 71 mm, 5 51162683 Half-moon stirrer blade, 19 mm x 54 mm, 5 51162684 Half-moon stirrer blade, 19 mm x 43 mm, 5 51162637 Bar type baffle, 15 mm x 249 mm, Alloy C-22 3 51162638 Bar type baffle, 15 mm x 237 mm, Alloy C-22 51162839 Temp. sensor, Alloy C-22, 1/4 6.35 mm x 300 mm, incl. chip 51162827 Temp. sensor, glass, 6 mm x 300 mm, incl. chip 4 4 4 4 4 4 4 4 3 51162829 ph sensor OptiMax, incl. chip 4 4 4 4 51192166 Reflux condenser glass, ST19, 250 mm x 40 mm Needed items 1) 51162722 Stirrer shaft 2) 51162417 Stirrer shaft 3) 51104154 adapter for baffle 4) 51162720 adapter, ST14 5) 51162681 Stirrer shaft 51162635 250 ml glass reactor 51162699 Glass cover 51162732 1000 ml one-piece glass reactor 51162733 500 ml one-piece glass reactor 51162734 250 ml one-piece glass reactor 51
Characterize the Process While Optimizing the Chemistry In chemical and process development, experiment quality is key. METTLER TOLEDO s OptiMax is designed to help make better decisions faster. It executes experiments with great accuracy, providing critical and information-rich data. Often, chemistry can be understood only when additional information, such as the reaction mechanism or the kinetics, is available. Key reaction species including intermediates and by-products are easily monitored in real-time with ReactIR, an FTIR-based in-situ reaction analysis tool. The analysis is conducted in the reaction mixture itself, eliminating errors associated by taking samples, and allowing organic chemists to quickly understand if the correct reaction occurred and to observe its start- and endpoint. The precise temperature control and the high reproducibility of an experiment makes the OptiMax the ideal workstation to optimize crystallization processes when combined with the particle characterization system ParticleTrack. It provides immediate insight into the particle system, enabling chemists and chemical engineers to quickly screen experimental parameters and develop a scalable process in early process development. The ic software suite allows scientists and engineers within the pharmaceutical, chemical and specialty chemical industries to convert the data collected in their experiments into important process knowledge. It provides a unique perspective when it comes to integration of data sets from other equipment, and shares a common design, so users learn the software once and use many instruments. The seamless integration of complementary data sets contributes to the faster understanding of the process under investigation. www.mt.com/optimax For more information Mettler-Toledo AG, AutoChem Sonnenbergstrasse 74 CH-8603 Schwerzenbach, Switzerland Phone +41 44 806 7711 Fax +41 44 806 7290 Email autochem@mt.com Internet www.mt.com/autochem Subject to technical changes 11/2013 Mettler-Toledo AG, AutoChem Printed in Switzerland, 51727001B Quality certificate. Development, production and testing according to ISO 9001. Environmental man agement system according to ISO 14001. European conformity. The CE conformity mark provides you with the assurance that our products comply with the EU directives.