" VALVES IN MOTION..." SAMPLING VALVES
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1 " VALVES IN MOTION..." SAMPLING VALVES SWISS QUALITY ISO 9001 / 2008
2 SAMPLING VALVES DESCRIPTION OF OPERATIONS 4 PATENTED PISTON 5 STANDARD DN50 DN50 / PN10 125A 6 TRI-CLAMP EASY CLEAN DN50 / PN10 125TC 7 CRUST BREAKING DN50 / PN10 125CC 8 SECURITY DN50 / PN10 125S 9 AUTOMATIC TYPE DN50 / PN10 125AUT 10 NEAR INFRA RED DN50 / PN10 125NIR 11 HIGH-CONTAINMENT DN50 / PN10 125OEL 12 METALLIC DN50 / PN10 135A 14 STANDARD DN25 DN25 / PN10 130C 15 STANDARD DN15 DN15 / PN10 115A 16 TECHNICAL DATA 18 DIMENSIONS 19 CLEANING / PURGING STERILISATION 20 FLANGE CONNECTION 21 OUTLET COUPLING 22 BOTTLE (CONTAINER) 23 PISTON / POLISHING 25 ACCESSORIES 26 CERTIFICATIONS / CONTACT 27 2
3 FAMAT SA is a Swiss engineering company for more than 30 years in the development and manufacturing of valves applications for projects in : Water Works Power Generation PetroChemical Oil and Gas Pharmaceutical and Chemical FAMAT SA has today offices or Agents in most major countries in Europe, Middle-East, Asia and America. This global network allows us a close cooperation with our customers and endusers, to guarantee a full satisfaction at all levels of the supply chain. Founded in 1974, FAMAT SA is certified ISO Its procedures guarantee the best Services in compliance and on-time deliveries with most industries standard For the Pharmaceutical and Chemical, FAMAT SA supplies a complete range of products and services allowing the sampling of products in the best conditions of efficiency in terms of representativity of the samples, security, cleanliness. With its impressive references in the Pharmaceutical and Chemical production business (SANDOZ, NOVARTIS, MERCK, BIO-MERIEUX, PFIZER, BASF, GLAXO...) FAMAT is able to provide you the sampling solution you need... FAMAT SA Chemin des Jordils St-Sulpice Switzerland 3
4 DESCRIPTION OF OPERATIONS CLOSED POSITION 9 The piston is a flush fit to the reactor or dryer leaving no dead space (FIG. 1). A perfect seal is formed directly by the piston (9) against the body of the valve. 2 1 FIG. 1 SAMPLING PROCEDURE Turn the handwheel counter clockwise to lower the piston (9) to its open position. While the product flows down into the sampling bottle (2), the operator can check the desired quantity of the product through the sight glass (1) (FIG. 2 ). 9 Turn the handwheel clockwise to bring back the piston (9) in its closed position. A firm final turn of the handwheel will give reliable sealing and no dead space. 2 1 FIG. 2 Equalise the pressure (or vacuum) in chamber (V) by opening the valve (25). Remove the sampling bottle (2) on its quick coupling connection (FIG. 3 ) V 2 1 FIG. 3 4
5 PATENTED PISTON In closed position, sealing is formed directly by the piston on the inside wall of the valve, without the need of a gasket. The patented system inside this piston allows the PTFE to expand and insure a perfect tightness from vacuum up to 10 bar (145 psi). The advantage of having an expendable piston inside the valve is to eliminate the need for O-rings that can be damaged during valve operation. In this position, the piston will be flush with the connection point, leaving no dead space. 5
6 STANDARD DN50 / PN10 125A Type 125A is the standard DN50 sampling valve by Famat (FIG. 1 ). Used for sampling applications of powders, granules, pastes and liquids under process conditions in the pharmaceutical, chemical and food industries. Pressure from full vacuum up to 10 bar (145 psi). Temperature from -20 C (-4 F) up to 180 C (360 F). FIG. 1 In standard configuration, the internal roughtness is Ra 0.8 µm and the external is Ra 3.2 µm. 6
7 TRI-CLAMP EASY CLEAN DN50 / PN10 125TC For cleaning internals between batches This sampling valve has one Tri-Clamp (TC) 2.5 near the handwheel (FIG. 1 ). Called " EasyClean ", the piston can be removed from the valve housing with the minimum of effort allowing full cleaning as shown on the picture (FIG. 2 ). Please note, the dryer or the vessel has to be empty for this procedure. For CIP options (Cleaning In Place), please refer to page 20. FIG. 1 FIG
8 CRUST BREAKING 125CC DN50 / PN10 This valve is used for products which could clug inside the dryer or vessel and block the piston. To eliminate the risk of this impeding product flow in to the sampling valve, Famat has developped the 125CC (FIG. 1). With this kind of valve type, the crust will be broken by the piston before the sample is taken. security device 1. Remove the security device. 2. Turn the red handwheel clockwise to move the piston into the dryer to break the crust as shown on the picture (FIG. 2 ). 3. Once the crust has been broken. Proceed with the standard sampling (page 4) with the black handwheel to get the sample inside the bottle. FIG. 1 Caution : Make sure to engage the security device in the red handwheel and as soon as possible to secure it with the lock to avoid any contact with the mixer or blades when bringing back the piston in its closed position. The outlet length can be adapted on request. FIG. 2 8
9 SECURITY 125S DN50 / PN10 A B The mechanical locking device secures the sampling procedure. 1. The sampling bottle (container) can only be removed if the piston is completly closed and if the purging valve is opened. 2. The piston can only be opened if the sampling bottle (container) is coupled on the outlet and if the purging valve is closed. The sample is taken in the same way as the standard Famat sample valve. The indicator (A) shows the position of the piston. This indicator has to show " closed " to allow the security lock (B) to be moved to the open position. Only then, the sampling bottle can be removed from its bayonet coupling. The piston is locked inside the valve until the sample bottle is refitted and the security lock (B) is moved to " closed ". 9
10 AUTOMATIC 125AUT DN50 / PN10 Standard sampling valve with a double acting actuator (FIG. 1 ). ACTUATOR Operating pressure : 4 to 10 bar (58 to 145 psi) Mode of operation : Double-acting Pneumatic connection : G 1 / 8 PROXIMITY SENSOR Measuring principal : Inductive FIG. 1 10
11 NEAR INFRA RED 125NIR DN50 / PN10 At the top of the piston, the 125NIR valve (FIG. 1 ) has a scraper which allows installation of a fiberoptic probe (FIG. 2 ). This probe, ideally located, will measure several parameters such as temperature, ph, humidity and / or composition of the product before taking physically the sample, transmitted by fiberoptic to the connector. A second hole, on the scraper (FIG. 2 ), is made nearby the fiberoptic probe for the cleaning system (Nitrogen) as shown on the picture. The measuring probe (not shown on picture) is cleaned through a nozzle with Nitrogen. FIG. 1 FIG
12 HIGH CONTAINMENT 125OEL DN50 / PN10 Toxic products This new compact OEL High-Containment sampling device (FIG. 1 ) allows the removal of a product sampled under contained conditions. The OEL (Operator Exposure Limit) describes the maximum concentration of a drug substance which can be tolerated in the air of the production room without any negative effect to the health of the operators. The (OEL) level range : 1-10µg / m 3 Container capacity : 290 ml (# 18 cu in) Tri-clamp connection : DN FIG. 1 The bottle (container) has a piston which includes 2 separating parts : (FIG. 3, page 15) The front plug isolates the outlet of the sampling valve. The body of the piston (inside the bottle) isolates and seals the sampling bottle. The container includes a locking system and a purging valve (Tri-clamp, ¼ G). The handwheel allows a precise sampling of the product (FIG. 2 ). ADVANTAGES FIG. 2 Quick dismantling for cleaning (without tools) - incl. a cleaning device Compact dimensions No dead volumes Sight glass for visual sample check Competitive quality-price 12
13 DESCRIPTION OF OPERATIONS 2 V 1 IN CLOSED POSITION The High-Containment device remains closed (seals without dead volume), assembled with the intermediate unit (1) and fixed to the Famat sampling valve (2). The plug (3) and the piston (4) are joined together via a bayonet and magnets. The indicator (5) shows the position «closed» of the bottle. FIG. 1 SAMPLING A sample can be taken by lowering the piston (3 and 4). On opening the sampling valve, the product flows down into the sample bottle. The quantity can be controlled by the operator through the sight glass (caution do not overfill ). Close the piston when the required quantity is reached. 5 3 REMOVING THE SAMPLING BOTTLE FIG. 2 4 Adjust compartment (V) to atmospheric pressure. Bring back the piston to its closed position. A firm final turn of the handwheel will ensure sealing of the valve and no dead volume. Remove the sample bottle unit by its quick coupling connection. This action will disconnect the front plug of the piston. The sampling valve outlet is closed by the plug (3) and the sample bottle sealed with the piston (FIG. 3 ). Under secure conditions in a laboratory, the sample can be extracted from the sample bottle by retracting the piston or by removing the Tri-Clamp connection. FIG. 3 CLEANING (process to be approved by customer) Reconnect the empty sample bottle with its closed piston, (FIG. 4 ) onto the unit. A cleaning can be carried out throughout the valve via various cleaning ports placed on the sample valve and the sample bottle (defined on request). Before further sampling, all ports must be closed. FIG
14 METALLIC 135A DN50 / PN10 The 135A sampling valve (FIG. 1 ) is equipped with a metallic piston (Stainless Steel, Hastelloy) for sampling process up to 300 C (572 F). Unlike the PTFE or PEEK piston, the metal piston has a high temperature gasket around it. To avoid any damage when closing the piston, the gasket is recessed into the piston and seals against the valve cylinder wall making contact only after the final sealing turn of the handwheel. Tightness from vacuum up to 10 bar (145 psi). FIG. 1 14
15 STANDARD 130C DN25 / PN10 The design is similar to the DN50 range with, as always, the patented expansion system for perfect sealing tightness. Pressure from full vacuum up to 10 bar (145 psi). Temperature from -20 C (-4 F) up to 180 C (360 F). In standard configuration, the internal roughtness is Ra 0.8 µm and the external is Ra 1.6 µm. 15
16 STANDARD 115A DN15 / PN10 For small reactors or dryers, the DN 15 sampling valve by Famat (FIG. 1 ) is usually used for liquid product. The design is similar to the DN 25 range with, as always, the patented expansion system for a perfect tightness. Pressure from full vacuum up to 10 bar (145 psi). Temperature from -20 C (-4 F) up to 180 C (360 F). In standard configuration, the internal roughtness is Ra 0.8 µm and the external is Ra 1.6 µm. FIG. 1 16
17 NOTES 17
18 TECHNICAL DATA MATERIAL STANDARD Stainless Steel Hastelloy PTFE (reinforced with glassfibers) FDA white PEEK (PolyEther EtherKetone) FDA beige Perfluoroelastomer FFKM Viton (FEP) FDA Borosilicate 3.3 Sampling Valve Bottle (container) Body / Flange / Coupling Piston Gaskets * Sight Glass HCB High-Containment (p. 12) Body / Coupling Piston Gasket Sight Glass All valves are equipped with Purging Valve ¼ G or ½ Ferrule and Handwheel in Aluminium or Thermoplast * Only 135A WEIGHT 125A 125TC 125CC 125S 125AUT 125NIR 125OEL B OEL B A 130C DN25 115A DN15 HCB B103 HCB B104 kg lbs PRESSURE / TEMPERATURE Full vacuum, up to 10 bar (145 psi ) for all valves. -20 C / -4 F, up to 180 C / 360 F for all valves, except type 135A : up to 300 C / 572 F 18
19 DIMENSIONS TC DN 50 Type 125 DN 25 Type 130 Type [millimeters] A B C NB D E F FD (Famat-DIN, standard) ND (DIN PN10 - DN50) DN50 Type 125 FA (FAMAT ANSI) NA ( lbs ANSI ISO) TC (TRI-CLAMP 2½ ISO 2852) DN25 Type 130 FD (PN10 - DN25) NA (ANSI 150 lbs) TC (TRI-CLAMP 1½ ISO 2852) Remark : 1 inch = 25.4 mm On request : The valve and flange dimensions can be adapted (if possible attach a drawing with your enquiry). 19
20 CLEANING / PURGING STERILISATION By placing 2 cleaning valves on the body, the solvent will clean / sterilise around the piston, the outlet and the bottle which is also equipped with a valve. Once flushing is complete, the chamber is dried by nitrogen through the same cleaning valves. Purging / cleaning valve ¼ G in stainless steel Purging / cleaning valve Tri-Clamp in stainless steel Standard 0.5 ISO
21 FLANGE CONNECTION DIN / ANSI Norm as requested Tri-clamp connection Standard Without nozzle The piston will tighten and will expand directly connexion on itself inside the reactor housing. O-ring on the connection point For dimensions of the nozzle (page 19) length and diameter of the nozzle can be customized. 21
22 OUTLET COUPLING Bayonet coupling Tri-clamp coupling Standard 2.0 ISO 2852 Food coupling Standard DN 50 GL 45 coupling DIN / ANSI Flange (if used as a tank bottom valve) 22
23 BOTTLE (CONTAINER) Type B101 Bottle with bayonet coupling Type B101 - TC Bottle with Tri-Clamp coupling Standard 2.0 ISO 2852 Type B101 - RL Bottle with food coupling Standard DN 50 Type B105 - Glass Bottle Bayonet - GL 45 A Metallic protection can be added. Size : 50 ml (3 cu in ), 100 ml (7 cu in ), 250 ml (15 cu in ), 500 ml (30 cu in ). 23
24 BOTTLE (CONTAINER) Type B102 Bottle with bayonet coupling Shock resistant cleaning system. Type B102 - TC Bottle with Tri-Clamp coupling Standard 2.0 ISO 2852 Shock resistant cleaning system. Type B109 Sight glass Standard 2.0 ISO 2852 Security lock available in option on all bottles Short deliveries. All bottles on stock. 24
25 PISTON Type P925 Piston in PTFE reinforced with glassfibers The material is available as well in PEEK. Type P922 Piston in GFK-reinforced PTFE with metallic scraper. Recommended for abrasiv or sticky products. Type P909 Metallic piston for hightemperature up to 300 C (# 572 F) Sampling valve 135A, (page 14). POLISHING Internal polishing External polishing 25
26 ACCESSORIES Handwheel in aluminium Handwheel in stainless steel Handwheel in thermoplast with number of turns indicator Limit switch Bottle cover Valve Body cover Short deliveries. All accessories on stock. 26
27 CERTIFICATIONS 27
28 NOVEMBER 2010 FAMAT SA Chemin des Jordils St-Sulpice Switzerland T. +41 (0)
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