pro-k Fluoropolymergroup Technical Brochure 06: Tolerances for the machining of PTFE-parts

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pro-k Fluoropolymergroup Technical Brochure 06: Tolerances for the machining of PTFE-parts Status: January 2014

2 Fluoropolymergroup Preamble The fully fluorinated polymer PTFE is the most widely used fluoropolymer and based on its unique properties is established as an undispensible construction material in modern industries. The main extraordinary properties of PTFE are resistance to most chemicals, a broad service temperature range, the excellent electrical properties, resistance to embrittlement, ageing resistance and very high purity. This technical brochure provides information about the tolerances for the machining of PTFE parts, which are essential for high quality PTFE products. This brochure replaces and in parts respectively augments the brochure quality requirements, test guidelines and tolerances for PTFE products edited in 1993 by the Gesamtverband Kunststoffverarbeitende Produkte (GKV). Important note: This brochure is provided for information only. The information given herein has been prepared according to our best knowledge at this time. The author and pro-k do not provide any warranty for its correctness and completeness. Each reader has to make sure that the information is suitable and appropriate for his purpose. Picture credits (front-page): Heute+Comp GmbH Fluoropolymergroup The Fluoropolymergroup is a product group of pro-k Industrieverband Halbzeuge und Konsumprodukte aus Kunststoff e.v, Städelstraße 10, D-60596 Frankfurt am Main; Tel.: 069-2 71 05-31; Fax 069-23 98 37; Trägerverband von und

3 Fluoropolymergroup Content 1. PTFE-turned parts 1.1 Area of application 1.2 Selection of tolerances 1.3 Admissable deviance for the length 2. PTFE-milled parts 2.1 Area of application 2.2 Selection of tolerances 3. PTFE-Stamped parts 3.1 Area of application 3.2 Selection of tolerances 3.3 Admissable deviance for the thickness 4. Admissable tolerances for the deviances of dimensions of PTFE rotation symmetrical parts made by chipping 4.1 Diameter and length 4.2 Radius and slope 4.3 Angular dimension 4.4 Deviances from the shape 5. Surfac quality 5.1 Test method 5.2 Requirements 6. Measurement equipment and methods for the surface testing

4 Fluoropolymergroup 1. PTFE-turned parts 1.1 Area of application Chapter 1 deals with the maintainable tolerances that can be achieved with chipping of a length 5 d, maximum 50 mm machined length ( d = outer diameter to be machined). The measurement is done at a normal climate 1. The samples have to be in a thermal equilibrium. 1.2 Selection of tolerances The following table is consistent with the geometric product specification (GPS) ISO tolerance system for lengths part 1. Basics for tolerances, deviances and fits (ISO/DIS 286-1:2007); German Version EN ISO 286-1:2007 Following tolerances apply (in µm): Up to 50 mm: for the wall thickness IT 10 for the diameter IT 11 above 50 to 180 mm: for the wall thickness IT 11 for the diameter IT 12 above 180 to 500 mm: for the wall thickness IT 12 for the diameter IT 12 1 According to DIN EN ISO 291 there are different normal climates. First normal climate 23/50 (for non tropic countries) and the normal climate 27/65 (for tropic countries). For both climates there are two classes 1 and 2. Class 1 iequires a temperature tolerance of +- 1 C and a moisture tolerance of +- 5%. Class 2 requires a temperature tolerance of +- 2 C and a moisture tolerance of +- 10 %.

5 Fluoropolymergroup Nominalmeasurement range mm from 1 to 3 from 3 To 6 From 6 To 10 From 10 To 18 From 18 To 30 From 30 To 50 From 50 To 80 From 80 To 20 From 20 To 80 From 80 To 50 From 50 To 15 From 15 To 400 From 400 To 500 Radial wall thickness Diameter 8 9 10 11 12 13 14 8 9 10 11 12 13 14 1 4 25 40 60 100 140 250 14 25 40 60 100 140 250 1 8 30 48 75 120 180 300 18 30 48 75 120 180 300 2 2 36 58 90 150 220 360 22 36 58 90 150 220 360 2 7 43 70 110 180 270 430 27 43 70 110 180 270 430 3 3 52 84 130 210 330 520 33 52 84 130 210 330 520 3 9 62 100 160 250 390 620 39 62 100 160 250 390 620 4 6 74 120 190 300 460 740 46 74 120 190 300 460 740 5 4 87 140 220 350 540 870 54 87 140 220 350 540 870 6 3 100 160 250 400 630 1000 63 100 160 250 400 630 1000 7 2 115 185 290 460 720 1150 72 115 185 290 460 720 1150 8 1 130 210 320 520 810 1300 81 130 210 320 520 810 1300 8 9 140 230 360 570 890 1400 89 140 230 360 570 890 1400 9 7 155 250 400 630 970 1550 97 155 250 400 630 970 1550

6 Fluoropolymergroup 1.3 Admissable deviations for length According to ISO 2768 (Page 1), Table 1: upper and lower limit for length, exactness grade fine Exactness Measurement range (mm) 0,5 to 6 above 6 to 30 above 30 to 120 Fine ± 0,05 ± 0,1 ± 0,15 The measurements are performed at normal climate 23/50 according to DIN 50014. In case it is necessary for the correct operation to have a lower tolerance, which would require higher efforts, a product related commitment has to be agreed on between the customer and the PTFEsupplier. Chipless formed turned parts require bigger tolerances than machined ones. They have to be agreed on between customer and PTFE supplier. 2 PTFE-milled parts 2.1 Area of application Chapter 2 deals with the tolerances that can be achieved with normal production efforts. The peculiar behaviour of the face machining of PTFE often requires higher tolerances for complicated shaped parts or forms. 2.2 Selection of tolerances The table of tolerances is consistent with the ISO tolerance (IT) according to ISO 286-1. It contains a limitation of the fineness with respect to the basic tolerances of the IT chapters 13, 14 and 15.

7 Fluoropolymergroup Machining dimension mm From 1 To 3 Above 3 To 6 Above 6 To 10 Above 10 To 18 Above 18 To 30 Above 30 To 50 Above 50 To 80 Above 80 To 120 Above 120 To 180 Above 180 To 250 Above 250 To 315 Above 315 To 400 Above 400 To 500 IT 8 9 10 11 12 13 14 15 16 17 18 14 25 40 60 100 140 250 400 600 --- --- 18 30 48 75 120 180 300 480 750 --- --- 22 36 58 90 150 220 360 580 900 1500 --- 27 43 70 110 180 270 430 700 1100 1800 2700 33 52 84 130 210 330 520 840 1300 2100 3300 39 62 100 160 250 390 620 1000 1600 2500 3900 46 74 120 190 300 460 740 1200 1900 3000 4600 54 87 140 220 350 540 870 1400 2200 3500 5400 63 100 160 250 400 630 1000 1600 2500 4000 6300 72 115 185 290 460 720 1150 1850 2900 4600 7200 81 130 210 320 520 810 1300 2100 3200 5200 8100 89 140 230 360 570 890 1400 2300 3600 5700 8900 97 155 250 400 630 970 1550 2500 4000 6300 9700 In case it is necessary for the correct operation to have a lower tolerance, which would require higher efforts, a product related commitment has to be agreed on between the customer and the PTFEsupplier. 3 PTFE-blanked parts 3.1 Area of application The specified tolerances are valid for one side of the blanked part, the opposite side may differ by the conical shape of the cut face. For this reason the reference dimension for the tolerance is for the inside dimension the smallest size and for the outside dimension is the biggest size.

8 Fluoropolymergroup 3.2 Selection of tolerances for the diameter and other dimensions ( except thickness) For blanked parts, that have been machined with precision tools ( combination die, knife cut) the basic tolerances of the IT row 15 according to EN ISO 286-1: 2007 apply. The values of tolerance are valid up to a thickness of max. 3 mm. 3.3 Admissable deviations for the thickness Up to a nominal thickness of 2 mm: ± 10 %; For a thickness above 2mm the defined tolerances for thickness of PTFE plates described in pro-k guidelines apply. 4. Admissable deviations for dimensions without defined tolerance of faced or rotation symmetric PTFE-parts 4.1 Diameter and length According to ISO 2768 General tolerances: Length and angles, shape and position, not for new constructions, edition 4. 1991 (page 1) Table 1 upper and lower limits for lengths, exactness grade medium and coarse, identical to ISO 2768-1 general tolerances. Limit dimensions in mm for the nominal measurement range Exactness 0,5 Above 3 Above 6 Above 30 Above 120 Above 400 Above 1000 grade to 3 to 6 to 30 to 120 to 400 to 1000 to 2000 medium ± 0,1 ± 0,1 ± 0,2 ± 0,3 0,5 0,8 1,2 coarse ± 0,2 ± 0,3 ± 0,5 ± 0,8 ± 1,2 ± 2,0 ± 3 For the nominal measurement range of 0,5 to 120 mm the exactness grade medium applies. For measurement ranges above 120-2000 mm as well as for complicated (thin walled) parts the exactness grade coarse has to be applied, provided there is no specific agreement ion place.

9 Fluoropolymergroup 4.2 Radius of curvature and cant (heel) According to ISO 2768 (Page 1), Table 2, upper and lower limit for radius of curvature and heel hight the exactness grade fine/medium identical with DIN ISO 2768-1 general tolerances applies. Limit dimension in mm for the nominal measurement range Exactness grade 0,5 Above 3 Above 6 Above 30 Above 120 to 3 to 6 to 30 to 120 to 315 Fine/ medium ± 0,2 ± 0,5 ± 1,0 ± 2,0 ± 4,0 4.3 Angular dimension According to ISO 2768 (Page 1), Table 3: Exactness grade fine/medium Limit of angular dimensions for the nominal measurement range of the short arm in mm to 10 Above 10 to 50 Above 50 to 120 Exactness grade Grad mm per 100 Grad mm per 100 Grad mm jper100 mm mm mm Fine medium ± 1 1,8 ± 30 0,9 ± 20 ± 0,6 4.4 Deviations in shape PTFE hollow articles - especially those with thin walls - are difficult to measure with respect to deviations in shape. The following tolerances are valid only for massive shaped pieces or hollow articles with a diameter/thickness ratio < 5. These parts may utilize the tolerances of the particular nominal dimension given in table 4.1 to 4.3

10 Fluoropolymergroup 5. Surface quality 5.1 Test method DIN EB USI 3274 Geometric product specifications (GPS) surface quality: Code procedere Nominal properties of code tools (ISO 3274:1996); German Edition EN ISO 3274:1998. It is recommended to use the reference area code system with a code radius of 0,005 mm. Because of the softness of PTFE a very low measuring force of (0,7 mn) should be applied. 5.2 Requirements The guidance levels for the acceptable roughness of face machined surfaces are as follows: PTFE-grade Roughness R z Virginal < 16 µm Filled* 2 < 25 µm Please ensure the necessary test length. The surface quality can be improved by increased manufacturing effort. 6. Measuring equipment and test method for the surface measureent It is recommended to use a spring loaded scanning system. The probe type is carried out as a cone with a rounded peak. The curve radius should amount maximum 5 µm. Especially when testing filled PTFE products a diamond needle is recommended. 2 Is affected by the character and amount of filler as well as its particle size, fibre length e.g glass fibre typical values L 50 = 60 µm, maximum fibre length about 150 µm.

11 Fluoropolymergroup Members of the Fluoropolymergroup: www.dyneon.com www.elringklinger.de www.fietz.com www.heutecomp.de www.kudernak.de www.lenzing-plastics.com www.kudernak.de www.sglgroup.de www.teadit.at www.teku-gmbh.de www.3p-plastiquesperformants.com www.solvaysolexis.com www.ptfe-nuenchritz.com