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Richter Sampling Valves PA/F, PA/S Body ductile iron with PFA lining or investment cast stainless steel Bellows-sealed Safety packing gland Representative sampling

Richter sampling valves Fields of application Representative and safe sampling of pure and slightly solids-laden media in the chemical, pharmaceutical and other industries. The Richter series PA/F (fluoroplastic lining PFA) and PA/S (stainless steel version) are specially suitable for taking samples of corrosive and pure media, also slightly solids-laden media during the ongoing process prior to filling into other containers/further transport prior to feeding into the process for the regular monitoring of stocks in the piping and from containers Operating ranges from -75 to 400 F (-0 to 00 C) from vacuum to max. 35 psi (1 bar) Product features Top-entry design for very easy maintenance, the valve body can remain installed in the system Valve actuation: safety hand lever, removable. Pneumatic or electric actuator on request. Long plug tip: Counteracts clogging, e.g. caking media. Anti-adhesive, wetted surfaces thanks to PFA/PTFE (PA/F), can be steam-sterilised (must be checked on a case-to-case basis) External corrosion protection: Epoxy coating (PA/F), stainless steel valve bonnet and screws On request with stainless steel protective cabinet (see page 5) Type codes, materials Sampling valve manual actuation remote actuation perfluoroalkoxy (PFA) lined stainless steel version PA/... PAP/....../F.../S Differenciation to sampling ball valves Conventional sampling ball valves are not cavity-free: Residues remain in the area between the ball and the body lining and therefore, before a representative sample can be taken, rinsing must be performed several times and troublesome disposal of the initial samples is necessary promote an undesirable increase in the sedimentation of solids in the dead leg above the ball are usually not self-closing, no dead man s handle have a normal not self-adjusting packing gland seal, have no bellows sealing a Travel stop, adjustable from outside finely metered sampling closing force can be increased at any time if the sealing action in the seat/plug area is insufficient (e.g. if sealing surfaces damaged) b Safety spring return by means of a central spring suitable for all pressure ranges ( dead man s handle ) c Safety packing gland acts independently re-adjustable from outside d a: Lining virgin PFA wall thickness 0.1-0.14 (3-3.5 mm) high permeation resistance vacuum-proof anchored b: Alternatively stainless steel 31 L (1.4435) investment cast body without lining e Glandless due to heavy-duty PTFE bellows hermetic sealing of the product chamber bellows wall 0.1 (.5 mm) thick, can also be used for highly permeating media f Cavity-free tapered valve bottom representative sampling: only fresh medium is taken no prior rinsing necessary no formation of residue in entire valve g Standard bottle connection with thread GL to DIN 18 modified pure PTFE secured against turning possibility of side connection for venting or overflow for PA/F: integrated FKM O-ring (Viton or equivalent) is not wetted further connection possibilities (see page ) h Removable safety hand lever disengages after actuation on request firmly installed with split pin in central bore lockable with lock or split pin alternative position: lever upwards i Highly viscous media or applications with low operating pressure: Special plug and seat option (see page ). j For solids-laden media: Inclined or vertical position of the valve and, as a result, possibly special bottle connection is recommended (see page ).

disengaged engaged 1 8 5 3 k D DN 4a H 1 optional 7 1 disengaged engaged F H nxd Sampling valve PA/F with thick-walled PFA lining L 8 3 E optional 5 4b D k DN nxd H 1 H 7 L Sampling valve PA/S of stainless steel design (without lining) 3

Richter sampling valves Components and materials Item Designation Material 100 Body PA/F: ductile cast iron ASTM A395/ EN-JS 1049 with PFA lining PA/S: investm. cast stainl. steel 31 L/1.4435 104 Transition flange stainless steel (only DN 1 1 / +3 / 40+80, not shown) 10 Cover stainless steel 03 Lever stainless steel 05 Seat PA/F: ductile cast iron ASTM A395/ EN-JS 1049 with PFA lining DN 1 1 / +3 / 40+80: stainless steel PA/S: investm. cast stainl. steel 31 L/1.4435 0 Bellows w. plug modified pure PTFE Bottle connection modified pure PTFE 30/1 Guide ring PTFE carbon 400/1 O-ring, not wetted FKM (Viton or equivalent) 40/1 Packing ring PTFE 405/1 Thrust ring stainless steel 503 Packing gland stainless steel follower 509/1 Groove nut stainless steel 513 Spring bonnet stainless steel 514 Spring bush stainless steel 515 Actuation stainless steel 550/1 Disc stainless steel 51/1 Grooved pin stainless steel 855 Stem stainless steel 90/1 Stud screw stainless steel 904/1 Setscrew stainless steel 90/3 Hex. check nut stainless steel 95 Pressure spring stainless steel 93 Star knob plastic/stainless steel 94 Ball head plastic Temperature/pressure ranges Temperature F ( C) 70 (0) 300 (150) 400 (00) Pressure psi (bar) 35 (1) 0 (15) 05 (14) Cv values (US gpm), k v100 values (m 3 /h) Cv (k v100) Cv (k v100) Valve Sampling flow rate at max. stroke inch DN flow rate Tapered plug Flat plug 1 5 17.5 (15) 1 1 / 40 54.8 (47) 50 75.7 (5) 0.448 (0.385).98 (.5) 3 80 33 (00) Other valve sizes on request 514 515 51/1 10 100 03 94 PA/F + PA/S Viscosity/operating pressure diagram p (bar) 1 14 1 10 8 4 0.4 0.001 Standard design with tapered plug Design for viscous media (see page ) 1 0.1 1 5 10 50 100 500 1000 1.8 1.5 Density 1 (g/cm 3 ) 0.7 0.0050.01 0.05 0.1 0.5 1 p (psi) 35 05 175 145 115 85 93 90/3 513 95 509/1 904/1 90/1 503 405/1 40/1 30/1 855 0 05 400/1 550/1 Kinematic viscosity (mm /s) Dynamic viscosity (Pas) Installation and connecting dimensions and weights for series PA/F and PA/S Face-to-face ISO 575 series 1 (DIN EN 558-1 series 1, formerly DIN 30/F1) Flanges drilled to ASME/ANSI B 1.5 Cl.150, on request to ISO 7005-1 PN1 (formerly DIN 53/33), JIS 10 K DN D k n x d H H 1 E L F approx. weight PA/F PA/S (appr.) PA/F* PA/S* inch mm inch mm inch mm inch mm inch mm inch mm inch mm inch mm inch mm inch mm lbs kg lbs kg 1 5 4.5 115 3.35 85 4x 5 /8 4x14 7.48 190 4.84 13 4.17 10 7.87 00.3 10 9.5 35 10 0 9 1 1 / 40 5.9 150 4.33 110 4x 5 /8 4x19 9.84 50 5 17 7.87 00 7.87 00.89 175 40 18 ** ** 50.5 15 4.9 15 4x 3 /4 4x19 7.8 195 5.1 131 4.8 1 7.87 00 9.05 30 9.0 30 40 18 31 14 3 80 7.9 00.3 10 8x 3 /4 8x19 1. 310.8 173 8.3 11 1. 310 3.8 97 40 18 ** ** * manually actuated, ** availability on request Other valve sizes on requst 4

Options Sampling valves with stainless steel protective cabinet Sampling valves with actuator Septum bottle adapter for high-purity media NEW: Needle and adapter made of stainless steel With this new option sampling in a septum bottle is even possible with the stainless steel series PA/S. The protective cabinets are produced in standard sizes and with various accessories, also custom-made. Fig.: Option with spring-loaded bottle holder. Pneumatic and electric actuators. Makes as per customer s choice. For design details, see page Body heating Handwheel instead of lever actuation Flat plug for slightly solids-laden media e.g. for crystallising media, heating jacket made of stainless steel, mounted (PA/F) or welded on (PA/S) Permits particularly finely metered sampling over the entire flow range of the valve. No automatic spring return. The integrated FFKM O-ring still seals if small solid particles are jammed in the sealing surface area. 5

Special versions of the models PA/F and PA/S Special design for highly viscous media or applications with low operating pressure The standard version of the PA valve with a tapered plug has a travel of 0.1 (3 mm), producing an angular gap of 0.0 (0.5 mm) over a length of 3 /4 (0 mm). However, taking samples of higher viscous media and media with a low operating pressure requires an enlarged passage cross section. Choice of connection possibilities for sampling bottles Twin adapter for two different bottle sizes Presented by: Adapter for standard horizontal valve installation A spring-loaded threadless bottle clamping feature can also be provided in conjunction with a protective cabinet; see page 5. Bottle connections: Standard GL to DIN 18 and customised special versions. Adapter for hose nozzle With a travel of 0.1 (3 mm) the special flat plug produces a full cross section of the outlet opening of 0.4 (10 mm). The suitable valve plug is selected according to the viscosity/operating pressure diagram (see page 4). Richter should be consulted in the case of different application parameters. Adapter for vertical valve installation Adapter with O-ring, prevents the ingress of ambient atmosphere Venting bore Flat plug Adapter for septum bottle (see picture page 5) Richter Inc. A Unit of IDEX Corporation 40 State Street, Cedar Falls, 5013 IA, USA Tel. +1(319) 8-8038, Fax +1(803) 1-770 Sampling bore Integrated needle for perforating the septum Headquarter: Richter Chemie-Technik GmbH Otto- Schott- Str., D-4790 Kempen, Germany Tel. +49(0) 1 5/14-0, Fax +49(0) 1 5/14-190 www.richter-ct.com, richter-info@idexcorp.com Publication No. 10us 08.13 Richter Chemie-Technik GmbH. Subject to change without notice. Printed in Germany. Richter = TM Richter Chemie-Technik GmbH; IDEX = TM IDEX Corporation; Viton = Trademark of DuPont