MagneDrives. Agitation

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MagneDrives Agitation Parker Autoclave Engineers MagneDrive is a magnetically coupled, packless rotary impeller system designed to provide continuous high speed mixing without leakage or contamination. Utilizing the rare earth magnetic technology which Parker Autoclave Engineers developed and was the first to market in 1958, the packless MagneDrive eliminates the process contamination, lubrication, packing friction, shaft cooling and maintenance problems common with other forms of mixing. MagneDrive is a completely sealed, closed sytem with metal-to-metal or O-ring seals. The incorporation of a leak-free mixing system enables researchers to process hazardous/toxic fluids without fear of fugitive emissions. Parker Autoclave Engineers has continually improved the magnetics of the MagneDrive to provide increased horsepower and torque in a smaller package. These improvements have extended the capacities, speeds and viscosity handling capabilities for the MagneDrive, allowing more applications to utilize this environmentally safe mixing system. MagneDrives are available with the Dispersimax Gas Dispersion Impeller System (and others) which utilizes a hollow shaft to draw gases into the impeller and propel them into the liquid for maximum gas dispersion. MagneDrives are available in four (4) magnet diameters and several models which can be retrofitted for existing vessels or customer supplied vessels. For high temperature applications, air and water cooling are available. Parker Autoclave Engineers will custom design a MagneDrive for individual mixing requirements.

Applications High speed mixing Low to moderate torque High pressure service Lethal service Contaminant sensitive process Gas Dispersion Hydrogenation Blending Suspension of particles * Consult factory for other applications The MagneDrive Principle: N MagneDrive agitators use rare earth magnets, permitting packless mixing at higher speeds in larger vessels and with higher viscosity fluids. Outer drive magnets, rotated by a motor-driven belt, exert powerful attraction on the encapsulated inner magnet assembly. As the outer drive magnets are rotated, the inner magnets are actuated, resulting in rotation of the agitator shaft. External Driver Magnets N Encapsulated Driver Magnet Assembly and Sealed Rotor Shaft S Outer magnets are rotated by motor-driven belts thus rotating inner magnets and rotor shaft. MagneDrives for containment-free packless agitation MAG075 Belt Drive Parker Autoclave Engineers MAG075 Series MagneDrive with enhanced design provides improved bearing life and the ability to increase the MagneDrive torque capacity with the substitution of a high torque stator module. This module allows the user to easily convert between 7 in-lbs (.8Nm) and 16 in-lbs (1.8Nm) static mixing torque. The MAG075 utilizes a solid state magnetically sensitive pickup for general purpose or explosion proof (requires Intrinsic Safety Barriers) applications. For more information, refer to bulletin MAG075 Series MagneDrive or consult factory. imag075 Inline Drive Parker Autoclave Engineers imag075 Inline Series MagneDrive uses a direct inline motor to elimanate belts, reduce size and create nearly silent operation. The unit has a compact design with up to 7 in-lbs. (791 N-mm) at static torque. The unit is desinged for simple disassembly and maintenance. Bearings can be replaced with minimal effort. Upper Bearing Holder Driver Magnets Cooling Jacket Drive Shaft Purge Connection Cover Lower Bearing Ball Bearings Encapsulation Housing Tach Pickup MAG075 SERIES imag075 SERIES 2

MAG3050 Inline Drive The MAG3050, used in the Mini-Reactor product, is also available as an individiual unit. In-line motor eliminates belts, reduces size and creates nearly silent operation. It has a compact design with up to 5 in-lbs. (565 N-mm) of static torque. Designed for simple disassembly and maintenance. Bearings can be replaced in seconds from top or bottom. MAG3050 SERIES MagneDrive Specifications: SERIES Shaft Coupling Shaft Diameter inches (mm) Pressure PSI (Bar) Maximum Speed RPM 1 Average Static Torque inch-lbs (N-m) HP @ Maximum Speed RPM 2,3 imag075 Tapered Thread 1/2 (12.7) 6000 (414) 2500 7 (0.8) 0.28 @ 2500 MAG07501 Tapered Thread 1/2 (12.7) 6000 (414) 3300 7 (0.8) 0.36 @ 3300 MAG07502 Tapered Thread 1/2 (12.7) 6000 (414) 3300 16 (1.8) 0.86 @ 3300 MAG3050 None 5/16 (7.5) 6000 (414) 3600 5 (.56) 0.24 @ 3000 1.5001AS*_A&C Pinned 3/8 (9.53) 6000 (414) 2500 27 (3.0) 1.07 @ 2500 1.5001AS*_CBD Pinned 5/8 (15.88) 6000 (414) 2500 27 (3.0) 1.07 @ 2500 1.5001SS* Pinned 5/8 (15.88) 4400 (304) 2500 27 (3.0) 1.07 @ 2500 1.5002AS* Threaded 3/4 (19.05) 6000 (414) 2000 60 (6.6) 1.90 @ 2000 1.5002SR* Threaded 3/4 (19.05) 3300 (229) 2000 60 (6.6) 1.90 @ 2000 1.5004 In-Tank Coupling 7/8 (22.22) 3000 (207) 3250 120 (14) 6.19 @ 3250 1.5006 In-Tank Coupling 7/8 (22.22) 3000 (207) 3000 180 (20) 8.57 @ 3000 1.5008 In-Tank Coupling 7/8 (22.22) 3000 (207) 3000 240 (27) 11.42 @ 3000 1.5010 In-Tank Coupling 7/8 (22.22) 3000 (207) 2750 300 (34) 13.09 @ 2750 2.7504 In-Tank Coupling 1-1/2 (38.1) 3000 (207) 1700 284 (32) 7.66 @ 1700 2.7506 In-Tank Coupling 1-1/2 (38.1) 3000 (207) 1500 426 (47) 10.14 @ 1500 2.7508 In-Tank Coupling 1-1/2 (38.1) 3000 (207) 1400 568 (63) 12.62 @ 1400 2.7510 In-Tank Coupling 1-1/2 (38.1) 3000 (207) 1300 710 (80) 14.64 @ 1300 * NOTE: SS = 316SS, AS = A286, and SR = 304SS 1 2 3 Maximum speeds may be limited by mixing requirements and shaft vibration, including critical speed. Motor horsepower should be sized at least 25% higher than the intended application requirement. To determine horsepower at a certain speed, use the formula: hp = T x n where: T= torque in inch-lbs 63,025 n= speed in rpm 4 5 Purebon is a registered Trademark of Pure Carbon Company, Inc. The magnets are stabilized at 300 o F (149 o C). When the temperature of the magnets exceeds the stabilizing temperature for an extended period, loss of magnetic torque will occur. Some of this loss is reversible and torque will regenerate; however, the problem is avoided by using adequate cooling to limit the magnet temperature to 300 o F (149 o C). A cooling jacket with two NPT connections is provided for water cooling, if necessary. Additional information on cooling requirements can be obtained in the Operation and Maintenance Manual. 3

Material of Construction: 316, 304, or A-286 Stainless Steel. Optional materials include Hastelloy C-276, Hastelloy B-2, and Titanium. Please consult factory for additional materials. Bearing Material: Standard bearing material is Purebon 658RCH 4. Please consult factory for other bearing requirements. Maximum Temperature @ Connection: 650 o F (343 o C) Maximum Temperature @ Magnet Zone: 300 o F (149 o C) 5 Cover Connection: Threaded, collar and gland, or flanged. Refer to individual bulletins for specific MagneDrives. Purge Connection: MagneDrives are provided with gas purge connection. The imag075 inline does not have purge connection. Shaft and Impeller: MagneDrives are supplied without shafts or impellers, allowing for the customization of the shaft length and impeller style. Parker Autoclave Engineers offers a wide ` selection of impellers in a variety of materials, including the Dispersimax TM Gas Dispersion System. Please consult factory for more information. Test Reports: Parker Autoclave Engineers will provide computer analysis of many of the variables which impact your mixing system. These computer projections enable us to properly size and engineer an agitation system to meet your specific requirements. Shown below are typical graphs illustrating the relationship between several critical parameters. These graphs are approximate and represent a sample of our capabilities. For a detailed evaluation of your mixing application, call your Parker Autoclave Engineers representative. Mixing Horsepower (in water) 12 10 8 6 4 2 0 Mixing HP vs Impeller Diameter AE Dispersimax TM Impeller 6"Dia. 5"Dia. 4"Dia. 3"Dia. 2"Dia. 100 500 1000 1500 2000 Impeller Speed (RPM) Mixing Horsepower 12 10 8 6 4 2 0 Mixing HP vs Viscosity AE Dispersimax TM Impeller @ 1500 RPM 6"Dia. 5"Dia. 4"Dia. 3"Dia. 2"Dia. 1000 5000 10000 20000 50000 Viscosity (centipoise) Mixing Horsepower (in water) 30 25 20 15 10 5 0 Mixing HP vs Impeller Style Impeller Diameter 6" AE Dispersimax Rushton 4 Blade A-310 Marine Prop 100 500 1000 1500 2000 Impeller Speed (RPM) Liquid Level above Impeller (in water) 16 14 12 10 8 6 4 Gas Dispersion vs Liquid Level Maximum Level to Initiate Dispersion 6" Dia. 5" Dia. 4" Dia. 3" Dia. 2" Dia. 2 500 600 660 700 775 835 900 1100 1400 1900 Impeller Speed (RPM) 4

AGITATORS Parker Autoclave Engineers offers a broad variety of agitator impeller systems which can be used in processes involving gas dispersion, liquid blending and motion, and solids suspension from low to very high viscosities with variable mixing intensity requirements. Illustrated are only four of the many standard agitators offered. For additional types, write or call for our Parker Autoclave Agitator/Mixer Bulletin. Dispersimax TM Turbine Pitched Blade Turbine Anchor Helical Supporting Information: imag075 Series Bulletin AGT-MAG075 Inline MAG075 Series Bulletin AGT-MAG075 MAG3050 Series Bulletin AGT-MAG3050 1.5001 Series Bulletin AGT-1.5001MD 1.5002 Series Bulletin AGT-1.5002MD 1.5004-1.5010 Series Bulletin AGT-1.50MD 2.7504-2.7510 Series Bulletin AGT-2.75MD Autoclave Agitator/Mixer Bulletin 1201 MagneDrive Application Data Sheet Bulletin AGT-ADSMD Please see Page 9-10 for the MagneDrive Application Data Sheet 5

Notes: 6

Notes: 7

Notes: 8

MagneDrive Application Data Sheet To allow us to select a MagneDrive that best fits your application, please provide the following information. The information that must be supplied is marked with an asterisk(*). This information can also be submitted electronically through our website. PLEASE INCLUDE UNITS WHERE APPLICABLE. Name*: Company Name*: Address: Fax*: Phone*: City: State: Zip Code: Country or Province: Please check the items you require a quote on*: o MagneDrive o Shaft o Impeller o Motor APPLICATION: MODEL (if known): DESIGN PRESSURE: DESIGN TEMPERATURE: MAX MIN* MAX. WORKING PRESSURE*: MATERIAL OF CONSTRUCTION*: MAX. WORKING TEMPERATURE*: (Note - On some non-stainless Steel MagneDrives, material of construction of some components such as retaining rings and screws may not be available in the requested material. See bulletins for list of standard materials.) BEARING MATERIAL: o Standard o Other: O-RING SEAL MATERIAL: o Standard o Other: IN-TANK COUPLING: o Yes o No o SHAFT DIAMETER MOTOR TO DRIVE CONNECTION*: o In-line o Belt-driven (In-line is not available on all MagneDrives ) MIXING REQUIREMENTS MAXIMUM SPECIFIC GRAVITY*: MAXIMUM VISCOSITY*: ARE SOLIDS PRESENT? o No o Yes SIZE: % SOLIDS: REACTOR INSIDE DIAMETER*: SHAFT LENGTH FROM TOP OF COVER*: REACTOR INSIDE LENGTH: LIQUID HEIGHT ABOVE IMPELLER: (required for dispersion)* IMPELLER*: o Dispersimax TM (gas dispersion) Diameter: Qty: o Fixed o Straight 6-blade turbine Diameter: Qty: o Adjustable o Fixed o 45 deg pitched 4-blade (up) Diameter: Qty: o Adjustable o Fixed o 45 deg pitched 4-blade (down) Diameter: Qty: o Adjustable o Fixed o Marine Impeller (Propeller) Diameter: Qty: o Adjustable o Fixed o Helix Diameter: Number of outer flights: Number of inner flights: o Anchor Diameter: o Other:

SPACING OF IMPELLERS ON SHAFT*: MAXIMUM REQUIRED SPEED (RPM)*: NORMAL OPERATING SPEED (RPM): MINIMUM REQUIRED SPEED (RPM): LIQUID LEVEL ABOVE BOTTOM IMPELLER: IS DISPERSION REQUIRED?* o Yes o No ARE MIXING BAFFLES PRESENT: o Yes o No IS A FOOT BEARING AVAILABLE OR ACCEPTABLE: o Yes o No DRIVE MOTOR REQUIREMENTS: o DC motor o AC motor ELECTRIC MOTOR VOLTAGE REQUIREMENTS: o o General Purpose Explosion-Proof ELECTRICAL CLASSIFICATION: CLASS DIV GROUP(S) OTHER o Air motor AIR SUPPLY PRESSURE AND FLOW RATE AVAILABLE: MOTOR MOUNTING REQUIRED (Foot mount, Face mount, etc.): MOTOR / MAGNEDRIVE CENTER TO CENTER DISTANCE: MISCELLANEOUS REQUIREMENTS: Please provide any additional information on a separate sheet. FAILURE, IMPROPER SELECTION OR IMPROPER USE OF THE PRODUCTS AND/OR SYSTEMS DESCRIBED HEREIN OR RELATED ITEMS CAN CAUSE DEATH, PERSONAL INJURY AND PROPERTY DAMAGE. WARNING This document and other information from Parker Hannifin Corporation, its subsidiaries and authorized distributors provide product and/or system options for further investigation by users having technical expertise. It is important that you analyze all aspects of your application and review the information concerning the product or system in the current product catalog. Due to the variety of operating conditions and applications for these products or systems, the user, through its own analysis and testing, is solely responsible for making the final selection of the products and systems and assuring that all performance, safety and warning requirements of the application are met. The products described herein, including without limitation, product features, specifications, designs, availability and pricing, are subject to change by Parker Hannifin Corporation and its subsidiaries at any time without notice. Offer of Sale The items described in this document are available for sale by Parker Hannifin Corporation, its subsidiaries or its authorized distributors. Any sale contract entered by Parker will be governed by the provisions stated in Parker's standard terms and conditions of sale (copy available upon request). 2013 Parker Hannifin Corporation Autoclave Engineers is a registered trademark of the Parker Hannifin Corporation May2013 Instrumentation Products Division Autoclave Engineers Operation 8325 Hessinger Drive Erie, Pennsylvania 16509-4679 USA PH: 814-860-5700 FAX: 814-866-7748 www.autoclaveengineers.com

FAILURE, IMPROPER SELECTION OR IMPROPER USE OF THE PRODUCTS AND/OR SYSTEMS DESCRIBED HEREIN OR RELATED ITEMS CAN CAUSE DEATH, PERSONAL INJURY AND PROPERTY DAMAGE. WARNING This document and other information from Parker Hannifin Corporation, its subsidiaries and authorized distributors provide product and/or system options for further investigation by users having technical expertise. It is important that you analyze all aspects of your application and review the information concerning the product or system in the current product catalog. Due to the variety of operating conditions and applications for these products or systems, the user, through its own analysis and testing, is solely responsible for making the final selection of the products and systems and assuring that all performance, safety and warning requirements of the application are met. The products described herein, including without limitation, product features, specifications, designs, availability and pricing, are subject to change by Parker Hannifin Corporation and its subsidiaries at any time without notice. Offer of Sale The items described in this document are available for sale by Parker Hannifin Corporation, its subsidiaries or its authorized distributors. Any sale contract entered by Parker will be governed by the provisions stated in Parker's standard terms and conditions of sale (copy available upon request). 2013 Parker Hannifin Corporation Autoclave Engineers is a registered trademark of the Parker Hannifin Corporation 06-0067BE May2013 Instrumentation Products Division Autoclave Engineers Operation 8325 Hessinger Drive Erie, Pennsylvania 16509-4679 USA PH: 814-860-5700 FAX: 814-866-7748 www.autoclaveengineers.com