WHITE OILS MAX 160 MIN. liquid cst

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CHAPTER 24 WHITE MINERAL OILS

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WHITE OIL 8 0.812 0.845 0.810 0.842 0.819 0.816 7 10 cst 5 cst 476 6 MAX 39 150 MIN 154 WHITE OIL 12 0.818 0.858 0.815 0.855 0.824 0.821 10 14 cst 19 cst 6 MAX 24 160 MIN 166 476 The above data is indicated of recent average values only. Minor variations which do not affect product performance or quality may be Specific requirements shall be custommade on request. White Oils are manufactured in compliance with I.P., U.S.P., B.P. and E.Ph specifications and conform to the requirement of U.S. FDA 21 CFR 17878 (a) and (b).

WHITE OIL 15 0.823 0.863 0.820 0.860 0.838 0.835 14 18 cst 15 cst 4764 6 MAX 24 165 MIN 174 WHITE OIL 20 0.826 0.863 0.821 0.860 0.830 0.827 19 22 cst 20 cst 6 MAX 15 180 MIN 186 4765 The above data is indicated of recent average values only. Minor variations which do not affect product performance or quality may be Specific requirements shall be custommade on request. White Oils are manufactured in compliance with I.P., U.S.P., B.P. and E.Ph specifications and conform to the requirement of U.S. FDA 21 CFR 17878 (a) and (b).

WHITE OIL 32 0.828 0.868 0.825 0.865 0.850 0.847 30 33 cst 32 cst 4765 6 MAX 18 200 MIN 210 WHITE OIL 50 Density @ 25 ºC,g/ml 0.828 0.873 0.825 0.870 0.838 0.835 48 54 cst 49 cst 6 MAX 18 220 MIN 240 477 The above data is indicated of recent average values only. Minor variations which do not affect product performance or quality may be Specific requirements shall be custommade on request. White Oils are manufactured in compliance with I.P., U.S.P., B.P. and E.Ph specifications and conform to the requirement of U.S. FDA 21 CFR 17878 (a) and (b).

WHITE OIL 68 0.848 0.880 0.845 0.880 0.856 0.853 65 75 cst 70 cst 6 MAX 15 220 246 4775 WHITE OIL 100 0.853 0.880 0.850 0.880 0.857 0.854 95 105 cst 100 cst 6 MAX 12 240 248 4775 The above data is indicated of recent average values only. Minor variations which do not affect product performance or quality may be Specific requirements shall be custommade on request. White Oils are manufactured in compliance with I.P., U.S.P., B.P. and E.Ph specifications and conform to the requirement of U.S. FDA 21 CFR 17878 (a) and (b).

WHITE OIL LIGHT Transparent Oily Liquid Solubility Insoluble in water & alcohol, soluble in ether and chloroform 0.810 to 0.860 @ 40ºC 7 cst to 40 cst Cloud Point ºC Below zero 9 MAX 150 MIN WHITE OIL HEAVY Transparent Oily Liquid Solubility Insoluble in water & alcohol, soluble in ether and chloroform 0.845 to 0.880 @ 40ºC 40 cst to 120 cst Cloud Point ºC Below zero 9 MAX 180 MIN REPORT The sample complies with the prescribed standards of quality. The methods used were ASTM.

VISCOSITY GRADE Range Density Typical, cst at 40 ºC 8, SUS at 100 ºF ASTM D 2161 15 12 20 32 50 68 100 0.8100.842 0.8150.855 0.8200.860 0.8260.863 0.8250.865 0.8250.870 0.8450.880 0.8500.880 0.821 0.835 0.827 0.847 0.835 0.853 0.854 0.816 19 49 15 70 5 20 32 100 56 72 85 104 152 245 340 500 476 476 4764 4765 4765 477 4775 4775 Cloud Point ºC 12 9 9 9 6 6 6 6 39 24 24 15 18 18 15 12 154 166 174 186 210 240 246 248 TE: 1) All oils above are colourless (Saybolt ), odourless, tasteless and meet requirements of U.S. FDA and USP, B.P. and Eph Pharmacpeia standard for Neutrality, s, Solid Paraffins and Carbonizable substances. All the above oils have nil arsenic and lead content. 2) The above data is indicated of recent average values only. Minor variations which do not affect product performance or quality may be 3) Specific requirements can be custommade on request. ISO 90012008 CERTIFIED ISO 140012004 CERTIFIED

TRANSFORMER OILS TYPICAL TEST RESULTS CHARACTERISTICS Appearance Density @ 29.5 ºC AS PER IS:335 AS AMENDED MIN MAX TEST A representative sample of the The oil shall be clear and oil shall be examined in 100 mm transparent & free from thick layer at 27 ºC suspended matter or sediment 0.89 IS : 1448 (P16) NEW INSULATING OIL Transparent, clear and light 0.840 g/cm³ at 27 ºC, cst IS : 1448 (P25) Interfacial Tension N/m @27ºC IS : 6104 0.04 0.048 N/m Flash Point PMCC ºC IS : 1448 (P21) 160 ºC IS : 1448 (P10) 140 6 15 ºC Neutralisation value a) Total Acidity, mg KOH/gm (Max) b) Inorganic acidity/alkalinity IS : 1448 (P2) 0.03 Nil 0.0009 mg KOH/g Nil Corrosive Sulphur Annex B 27 14 cst Non Corrosive Non Corrosive Electrical Strength (Breakdown Voltage) KV(rms) a) New Unfiltered Oil IS 6792 b) After Filteration 30 68 60 72 0.002 0.0003 Dielectric Dissipation factor, (Tan Delta) at 90 ºC IS : 6262 Specific Resistance (Resisitivity) Ohmcm a) At 90 ºC b) At 27 ºC IS : 6103 35 x 10¹² 1500 X 10¹² Oxidation Stability 164 Hours @ 100 ºC a) Neutralisation Value after Oxidation b) Total Sludge Annex C Accelerated Ageing test 96 hrs @ 115 ºC (open Beaker Method) IS : 12177 a) Sp. Resistance (Resistivity) ohmcm @ 27 ºC b) Sp. Resistance (Resistivity) ohmcm @ 90 ºC c) Dielectric Dissipation Factor @ 90 ºC d) Total Acidity, mg/koh/gm e) Total sludge value, % Wt 300 x 10¹² 13200 X 10¹² 0.40 0.10 0.091 0.0087 IS : 6103 IS : 6103 IS : 6262 IS : 1448 (P2) Annex. A of IS 12177 5 X 10¹² 0.2 X 10¹² 0.20 0.05 0.05 641 X 10¹² 87 X 10¹² 0.034 0.035 0.006 Presence of oxidation inhibitor % wt IS : 13631 Not present Water Content ppm Max IS : 13567 The oil shall not contain antioxidant additives 50 ppm S.K.Value, % (Max) Annex D, IS : 335 8 Max 1 15 ppm Our product conforms to IS 335 : 1993 The above data is indicated of recent average values only. Minor variations which do not affect product performance or quality may be Specific requirements shall be custommade on request.

TRANSFORMER OILS NEW INSULATING OIL / TRANSFORMER OIL New Insulating Oil is a premium grade uninhibited Mineral Insulating Oil for Transformers and Switchgears TEST DESCRIPTION TEST SPECIFICATION LIMITS Appearance BS 1481998 Transparent, clear, bright, odourless free from suspended impurities Transparent, clear, bright, odourless free from suspended impurities ASTM D 1500 L 0.5 0.5 At 40ºC ISO 3104 11 9.0 At 30ºC ISO 3104 1800 298,(Min), PMCC ISO 2719 130 150 ISO 3016 45 45 Density kg/dm³, @ 20ºC (Max) BS EN ISO 3675 0.895 0.88 Neutralisation Value mg KOH/g (Max) IEC 62021 0.01 Nil Interfacial Tension @ 25ºC ISO 6295 0.04 Max 0.045 Corrosive Sulphur DIN 51353/BS 5680 Non corrosive Non corrosive Water Content, Max mg/kg IEC 60814 a) Bulk 20 14 b) Drum 30 22 Anti oxidant Additives (Sub Clause 5) IEC 60666/BS 5984 Not detectable Not detectable Oxidation Stability, 164 h Total acidity, mg KOH/g of oil (Max) Sludge, % by mass (Max) DDF @ 90 ºC IEC 61125 : 1993 (Method C) IEC 60247 2 0.8 0.5 0 0.68 0.36 Break down Voltage, Min IEC 60156 As Delivered (Kv), min 30 50 After Treatment (Kv), min 70 70 Dielectric Dissipation factor at 90 ºC and 40 to 60 Hz (Max) IEC 60247/61620 0.005 0.0005 Gassing tendency at 50 Hz after 120 min, mm³/min Method A (Max) BS 5797/IEC60628A +5 +1 Total PCB content mg/kg IEC 61619 Non detectable Non detectable Total Furans mg/kg, Max BS EN 61698 00 Nil Polycyclic Aromatics % mass, Max BS 2000 00 0.5, mm²/s (max) Our product conforms to IEC 60296:2003/BS148:1998 The above data is indicated of recent average values only. Minor variations which do not affect product performance or quality may be Specific requirements shall be custommade on request.

TRANSFORMER OILS DESCRIPTION OF TEST UNIT TEST AS PER IEC296 1 PHYSICAL Appearance IEC : 296 2 3 Density @ 20 ºC, Max g/cm³ Cst. ISO : 3675 ISO : 3104 4 5 6 Interfacial Tension, at 25 ºC Flash Point Water Content Bulk Water Content Drum Pour Point N/m ºC Mg/Kg ISO : 6295 ISO : 733 IEC : 60814 ºC ISO : 3016 kvrms IEC : 60156 7 1 2 1 2 3 1 2 6 ELECTRICAL Electrical Strength BDV As Delivered After treatment Dielectric Dissipation factor (tan delta) at 50Hz, Max ICAL Neutralization Value (Total Acidity) Corrosive Sulphur Oxidation Stability for 164 hrs at 100 ºC Neutralization value Total Sludge by mass Presence of Oxidation Inhibitor REQUIRED VALUE MEASURED VALUE Clear, transparent & free from sediment & suspended matter 0.895 Max 10 at 40 ºC 800 at 15 ºC 0.04 Min 140 Min 30 Max 40 Max 30 Max Clear, transparent & free from sediment & suspended matter 0.822 6 400 0.052 160 9.2 10 36 62 0.0003 IEC : 60247 30 min 50 min 0.005 Mg.KOH/gm IEC : 296 ISO : 5662 0.03 Max NonCorrosive 0.002 NonCorrosive Mg.KOH/gm % IEC : 61125 IEC : 666 0.4 Max 0.1 Max Not detectable 0.07 0.001 Not detected REMARKS: Conforms to IEC296/1982, Class I (UNINHIBITED OIL) DESCRIPTION OF TEST UNIT TEST AS PER IEC296 1 PHYSICAL Appearance IEC : 296 2 3 Density @ 20 ºC, Max g/cm³ Cst. ISO : 3675 ISO : 3104 4 5 6 Interfacial Tension, at 25 ºC Flash Point Water Content Bulk Water Content Drum Pour Point N/m ºC Mg/Kg ISO : 6295 ISO : 2719 IEC : 60814 ºC ISO : 3016 kvrms IEC : 60156 7 1 2 1 2 3 1 2 6 ELECTRICAL Electrical Strength BDV As Delivered After treatment Dielectric Dissipation factor (tan delta) at 50Hz, Max ICAL Neutralization Value (Total Acidity) Corrosive Sulphur Oxidation Stability for 164 hrs at 100 ºC Neutralization value Total Sludge by mass Presence of Oxidation Inhibitor REQUIRED VALUE MEASURED VALUE Clear, transparent & free from sediment & suspended matter 0.895 Max 10 at 40 ºC 1800 at 30 ºC 0.04 Min 130 Min 30 Max 40 Max 45 Max Clear, transparent & free from sediment & suspended matter 0.870 0 900 0.050 148 1 10.0 45 60 0.0002 IEC : 60247 30 min 50 min 0.005 at 90 ºC Mg.KOH/gm IEC : 296 ISO : 5662 0.03 Max NonCorrosive 0.003 NonCorrosive Mg.KOH/gm % IEC : 61125 IEC : 666 0.4 Max 0.1 Max Not detectable 0.08 0.002 Not detected REMARKS: Conforms to IEC296/1982, Class II (UNINHIBITED OIL)

LIQUID PARAFFINS DESCRIPTION Columbia's Light Liquid Paraffin/White Mineral Oil is suitable for Pharmaceutical, Cosmetics & Food industries for direct & indirect food contact. PROPERTIES For specific uses these oils must be less Odourless Tasteless Conforming to the standards of pharmaceutical purity I.P., B.P. & U.S.P. Conforming to the standards of oils in contact with edible substances They are therefore, subjected to a higher refinement so as to be able to conform to particular specifications, (different specifications) in different countries and the standard FDA (Food & Drugs Administrative U.S.A.) The range of Columbia Liquid Paraffins has the following gradations: Light grade Heavy Grade APPLICATIONS Chemical Industry The inert oils for the fabrications of metallic hydrides and catalysts Absorbent oils (e.g. in the extraction of the natural essence of perfumeries, the impregnated paper of white oil is used.) Cosmetic Industry Preparation of solid and brilliantine Preparation of detergent creams, cold creams and beauty lotions Preparation of hydrated creams Preparation of bronzed oils Preparation of oil for hygiene of children Preparation of makeup products Pharmaceutical Industry Antifoaming for the production of penicillin Internal lubricants as laxatives Additive in the machining of the ingredients for the fabrication of the compressed Basis for ointments and emollients Vehicle of transport of medical spray Packaging Industry for edible products Components for the lubricants of the tin band intended to be used for the tinned food Oiling of the cart and cartons for fruits and vegetables The Plastic Material Industry Additive for the production of polyethylene Additive for extrusion of Polyvinyl Chloride Dispersant for production of polyethylene Plasticizer for ethyl cellulose Plasticizer for coumaroneindene (resin) Plasticizer for EPDM (Ethylenepropylenediene monomer) Plasticizer for polyethylene Plasticizer for polypropylene Plasticizer for polystyrene Plasticizer for Annealing of the printed objects in nylon Hardening and annealing Textile Industry Oil components for spinning Oils for weaving and mesh Lubrication for sewing machines & hosiery Various other industries Components for insecticide in agriculture Compressors for reactive gases like chlorine and sulphur dioxide (lubrication of cylinders) Lubrication of paper cutter knives in paper mill Air filters for conditioning systems and underwater works

LIQUID PARAFFINS LIGHT LIQUID PARAFFINS TYPICAL PARAMETER LIGHT LIQUID PARAFFIN I.P. LIGHT LIQUID PARAFFIN B.P./EPh LIGHT LIQUID PARAFFIN U.S.P Saybolt colour Odour and taste Dynamic Viscosity @ 20ºC, mpa s 25 to 80 25 to 80 @ 40ºC Not less than 35 Specific Gravity @ 25ºC 0.820 to 0.880 0.810 to 0.875 0.818 to 0.880 Acidity / Alkalinity (Neutrality) Solid Paraffin Readily Carbonisable Substance Light absorption in the range 240 to 280 nm <0.1 Polynucleur Aromatics Compound HEAVY LIQUID PARAFFINS HEAVY LIQUID PARAFFIN I.P. HEAVY LIQUID PARAFFIN B.P./EPh HEAVY LIQUID PARAFFIN U.S.P Saybolt colour Odour and taste Dynamic Viscosity @ 20ºC, mpa s 110 to 230 110 to 230 @ 40ºC Not less than 35 Specific Gravity @ 25ºC 0.860 to 0.904 0.827 to 0.890 0.845 to 0.905 Acidity / Alkalinity (Neutrality) Solid Paraffin Readily Carbonisable Substance Light absorption in the range 240 to 280 nm <0.1 Polynucleur Aromatics Compound TYPICAL PARAMETER The above data is indicated of recent average values only. Minor variations which do not affect performance or quality may be expected in manufacture. Specific requirements shall be custommade on request Light Liquid Paraffins / White Mineral Oils are manufactured in compliance with I.P., U.S.P., B.P. and Eph specifications and conforms to the requirement of US FDA 21 CFR 17878 (a) & (b)