ICA Bremen Cotton Round Test

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1 ICA Bremen Cotton Round Test in Cooperation with Bremer Baumwollboerse carried out by Bremen Fibre Institute (FIBRE) Evaluation of the Test Results 1 / Bremen, Tested Cotton: Cameroun Number of Laboratories: 15 Cotton Number: RM Argentina 1 Australia 1 Bangladesh 1 Brazil China, PR 15 Czech Republic 3 Egypt 3 France 1 Germany 11 Greece 5 Hungary 1 India Iran 1 Israel 1 Italy - Japan 1 Kazakhstan 1 Korea, R 1 Latvia 1 Mali 1 Mauritius, Rep of - Mozambique - The Netherlands 1 Pakistan Poland Russia 1 Serbia 1 Slovenia South Africa - Spain 3 Sudan 1 Switzerland 3 Tanzania - Thailand Turkey Uganda 1 United Kingdom - United States Uzbekistan 1 Vietnam, SR Zimbabwe - For any questions, please mail to gerardi@faserinstitut.de [Type text] ICA Bremen GmbH Wachtstrasse 17-, 8195 Bremen, Germany t: +9 () f: +9 () e: info@ica-bremen.org V1 Draft FB 31_TestReport-Cotton_ICA_Bremen_v1

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3 ICA Bremen Cotton Round Test 1- in Cooperation with Bremer Baumwollboerse carried out by Bremen Fibre Institute (FIBRE) Explanations: test material The sample material is generally unprocessed cotton lint without additional homogenisation from varying origins with a wide spectrum of properties. The Bremen Fibre Institute (FIBRE) usually avoids origins with high result variations. In this Round Test the cotton is: Cameroun (RM ) The variation of the utilized cotton was measured at the Bremen Fibre Institute (FIBRE) with an Uster HVI 1 with 1 tests on samples from 1 different layers with the following results: HVI HVICCS SD between bale layers (based on 1 tests per layer) SD between single tests (based on 1 times 1 tests) Mic,1,3 Strength, g/tex,197,78 Length, UHM, inch,5,15 Length, UHM, mm,17,391 The test material is not suitable as a reference for calibration. result evaluation The results of the participating laboratories for one test method and one parameter are grouped in one table implying that the used instruments yield comparable results despite different instrument types or different national standard test methods. The results are partitioned in different tables as soon as significant differences appear. Based on the compilation of the results, an identification of outliers is carried out, which is according to Grubbs Test for Outliers described in ISO 575 with one slight modification: the algorithm is applied repeatedly to ensure that all outliers are excluded. All outliers are marked by putting the result in brackets. The statistical parameters for all tables and characteristics are calculated after the exclusion of outliers. For the usage of the statistical data, the different numbers of repetitions in each lab have to be considered. [Type text] ICA Bremen GmbH Wachtstrasse 17-, 8195 Bremen, Germany t: +9 () f: +9 () e: info@ica-bremen.org V1 Draft FB 31_TestReport-Cotton_ICA_Bremen_v1

4 assessment of the laboratory performance From the results, the bias of each laboratory can be calculated. Stability and repeatability cannot be assessed. The ICA Bremen Cotton Round Test does not include any benchmarking or rating of the laboratories and their results. Rather the results can be used by each laboratory to evaluate its own performance. For estimating a bias to results of other laboratories, please calculate the difference between your result and either the average or the median of all laboratories (after exclusion of outliers). For evaluating the bias, the z-score calculation may be applied: z your value average( or median) StdDev If the z-score is between -1 and 1 your lab belongs to the better 8% of all labs and no measures are necessary. In the z-score range of - to are 95 % of all values. The closer your z-score is to (-) the more urgently it is to take measures to improve performance. If your z-score is above (below -) a basic revision of all conditions will be necessary. For assessing permanent deviations, please monitor all deviations in subsequent ICA Bremen Round Tests or in comparison to other round trial programmes like the CSITC Round Trials or the USDA HVI Checktest. laboratory numbers The laboratory numbers for each laboratory are confident. The numbers are usually kept constant for subsequent Round Tests. In case that any laboratory has doubts in the anonymity of its number, a new laboratory number should be requested. In case of more than one instruments of the same type, an adjunct number or character is given (e.g and 13-). In order to distinguish between your instruments, please provide specific adjunct characters for each of your instruments with your data sheet. registration and participation To register a new laboratory to the ICA Bremen Round Test, please send the laboratory s contact details to Mrs Hannelore Gerardi contact details provided below In the case that a laboratory does not send any results back for a whole year s period, we have to exclude it from the participants. [Type text] ICA Bremen GmbH Wachtstrasse 17-, 8195 Bremen, Germany t: +9 () f: +9 () e: info@ica-bremen.org V1 Draft FB 31_TestReport-Cotton_ICA_Bremen_v1

5 choice of test methods included in the round test The ICA Bremen Round Test strives to include every commonly used test method. Test methods will remain included as long as sufficient participant numbers are given, although the Bremen Fibre Institute (FIBRE) maintains the right to exclude methods. Proposals for the inclusion of new methods/instruments/parameters are appreciated. For this, an adequate number of long term participants should be given. Test methods for stickiness are excluded due to difficulties in sample provision. improvement of the ica bremen cotton round test Any proposals for improving the Round Test are highly appreciated. For this, please contact Mr Axel Drieling contact details provided below. important notes Please take care to fill in all the necessary information on the test forms (e.g. the test methods, the instrument types and the number of repetitions for each test). Please provide one or two reliable addresses to Mrs Gerardi - contact details are provided in the last section. Contact For any questions regarding the ICA Bremen Cotton Round Test, please contact: Mr Axel Drieling for general questions relating to the Round Test and cotton testing, Tel , axel@ica-bremen.org Mrs Hannelore Gerardi for questions relating to the realization of the current tests, Tel , gerardi@faserinstitut.de With kind regards, Axel Drieling Hannelore Gerardi [Type text] ICA Bremen GmbH Wachtstrasse 17-, 8195 Bremen, Germany t: +9 () f: +9 () e: info@ica-bremen.org V1 Draft FB 31_TestReport-Cotton_ICA_Bremen_v1

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7 1 MICRONAIRE Lab. Rep. Mic. Instrument Standard Test Method GB/T Fibronaire Sheffield ISO Fibronaire JIS MK.1 ASTMD RM Sheffield ASTMD DigiMic XT ASTMD ASTMD Fibronaire ICCS 115. Kaisokki ASTM STATEX IIC Shirley ISO Fibronaire ASTM Sheffield BS ASTM DIN internal ISO WIRA Sheffield DPM DIN Fibronaire ASTMD FMT Average 3.9 Median 3.7 StdDev.1 CV 3.78 Min 3.3 Max. n 35

8 PRESSLEY, STELOMETER Pressley Tester Stelometer Lab. Standard Test Bundle Tenacity Elongation Standard Test Rep. PI () PI (3.) Rep. Method gf/tex % Method ISO JIS ASTMD ASTM ASTMD ASTM ICCS ASTM.3.5 ASTM ASTM (.1).3 ASTM DIN ISO3 13 (9.1) internal TPPSI DIN 539 Average Median StdDev CV Min Max n Pressley PI() Av., gf/tex 1.9 StdDev, gf/tex.7 CV, % 11.1 (3.) Av., gf/tex. StdDev, gf/tex CV, %

9 3 DIGITAL - FIBROGRAPH (further information see page "Multiple Devices") Span Length Lab. Rep..5 % SL 5 % SL UR SFC (N) SFC (W) SFI mm inch mm inch % % % (3.) (.9) (81) Average Median StdDev CV Min Max n

10 COMB SORTER (further information see page "Multiple Devices") Staple Length N W Lab. Rep. Instrument ML CV < 1.5 mm ML CV <1.5 mm mm % % mm % % 131 Keisokki ALMETER (further information see page "Multiple Devices") Staple Length N W Lab. Rep. ML CV < 1.5 mm ML CV <1.5 mm mm % % mm % % Maturity, Fineness (further information see page "Multiple Devices") Fibrograph Causticaire (18 % NaOH) Microscopic Test Lab % % ASTM, % BS, % Gravimetric Fineness dtex

11 5 IIC/SHIRLEY FM-TESTER (further information see page "Multiple Devices") Maturity, Fineness Lab. Rep. PM, % MAT FIN, mtex Average Median StdDev CV Min Max n

12 HVI (table is divided into 3 pages) General Each rep. consisting of Lab. Manufacturer Instrument Std. Test Method Rep. Combs for Color Mic. meas. length/strength readings USTER USTER 1 Line USTER 1 Line USTER USTER Spectrum I ASTMD USTER Spectrum I SN/T USTER Spectrum internal USTER Spectrum SN/T USTER 1 SN/T USTER 9 A ASTMD Textechno Fibrotest 1 31 USTER USTER 9 A internal Premier HFT ICC Premier HFT HVI Test Method USTER USTER USTER Spectrum 5 3 USTER USTER 1 USTER Spectrum Manufacturer Premier HFT ASTMD USTER USTER 1 internal 1 5- USTER 1 internal USTER 1 internal 1 5 USTER 1 ASTM 5 USTER Spectrum USDA 1 5 USTER Spectrum I HVI Test Method USTER 1 internal 1 1 USTER 1M7 ASTM 1 - USTER 1 ASTM 1 1 USTER 9 ASTMD Premier ART ASTM 71 USTER Spectrum SN/T USTER 1 SN/T USTER USTER Spectrum I 1 79 USTER USTER USTER Spectrum I SN/T USTER 1 USDA USTER Spectrum ASTMD USTER 1 ASTMD USTER USTER USTER 1 ASTMD USTER MAG HVT Expert 11 ASTMD USTER 1 GB/T USTER 1 USDA. ASTM USTER 1 ASTMD USTER 9 B ASTMD USTER Spectrum 1 ASTMD USTER SW7V ASTMD

13 7 HVI (table is divided into 3 pages) General Each rep. consisting of Lab. Manufacturer Instrument Std. Test Method Rep. Combs for Color Mic. meas. length/strength readings 1 USTER 1 USDA 1 15 USTER Spectrum Manufacturer 1 17 Premier ART ASTMD USTER 1 ASTMD USTER Statex Fibrotex ASTM USTER Spectrum SN/T USTER 1M7 ASTMD USTER 9 SA ASTM USTER 1 SN/T USTER USTER Spectrum ASTMD USTER 1 ASTM 1 Premier HFT ASTM 1 18 USTER ASTMD USTER 9 SA ASTMD Premier ART ICC USTER 9 A USDA 13 Textechno Fibrotest 1 13 USTER Spectrum I ASTMD USTER Spectrum I ASTMD Premier ART USTER Spectrum 1 1 USTER Spectrum 1 18 USTER USTER 9 A USTER Spectrum USDA. ASTM USTER USTER USTER 9 A HVI Mode 1 17 USTER 1 HVICC USTER 1 SN/T USTER 1 ASTMD USTER USTER 9 1 Premier ART HVI Mode USTER 9 1 Premier HFT GB/T USTER 1 GB/T USTER Spectrum I GB/T USTER 1 ASTMD USTER 1 ASTMD USTER 1 ASTMD USTER 1 ASTMD USTER 1 ASTMD Premier ART ASTM MAG HVT Expert 11 ASTMD Premier ART ICC MAG HVT Expert 11 ASTMD MAG HVT Expert 11 ASTMD MAG HVT Expert 11 ASTMD MAG HVT Expert 11 ASTMD MAG HVT Expert 11 ASTMD Premier HFT Premier ART ICC 1

14 8 HVI (table is divided into 3 pages) General Each rep. consisting of Lab. Manufacturer Instrument Std. Test Method Rep. Combs for Color Mic. meas. length/strength readings 38 Premier ART ICC Premier ART ICC Premier ART HVI Mode 1 71 Premier ART internal USTER 9 internal Premier ART Premier ART USDA Premier ART Manufacturer Premier HFT 1 3 Premier ART ASTM Premier HFT HVI User's Guide Premier ART ASTMD MAG HVT Expert 11 ASTM

15 9 Micronaire, Tenacity, Elongation HVI (table is divided into 3 pages) Lab. Micronaire Tenacity Elongation ICCS, gf/tex HVICCS, gf/tex ICCS, % HVICCS, % (.)

16 1 Micronaire, Tenacity, Elongation HVI (table is divided into 3 pages) Lab. Micronaire Tenacity Elongation ICCS, gf/tex HVICCS, gf/tex ICCS, % HVICCS, % (1.8) (8.3)

17 11 Micronaire, Tenacity, Elongation HVI (table is divided into 3 pages) Lab. Micronaire Tenacity Elongation ICCS, gf/tex HVICCS, gf/tex ICCS, % HVICCS, % (3.3) (.) (.) (3.1) Average Median StdDev CV Min Max n

18 1 HVI (table is divided into 3 pages) ICCS HVICCS Length Lab..5 % SL UR UHM UI mm inch % mm inch % (.) (1.5) (78.)

19 13 HVI (table is divided into 3 pages) ICCS HVICCS Length Lab..5 % SL UR UHM UI mm inch % mm inch % (13.5)

20 1 HVI (table is divided into 3 pages) ICCS HVICCS Length Lab..5 % SL UR UHM UI mm inch % mm inch % Average Median StdDev CV Min Max n

21 15 Color, Trash HVI (table is divided into 3 pages) Lab. Color Trash Rd +b CG leaf area cnt (1.) (15.5) (7) (1.7) (11.) (1.3) (.3)

22 1 Color, Trash HVI (table is divided into 3 pages) Lab. Color Trash Rd +b CG leaf area cnt (13.8) (59) (7) (1.3) (.5) (33)

23 17 Color, Trash HVI (table is divided into 3 pages) Lab. Color Trash Rd +b CG leaf area cnt (71) Average Median StdDev CV Min Max n

24 18 Short Fibre Index, Maturity HVI (table is divided into 3 pages) Lab. ICCS SFI HVICCS SFI PM % Maturity Ratio (3.1) (13.7)

25 19 Short Fibre Index, Maturity HVI (table is divided into 3 pages) Lab. ICCS SFI HVICCS SFI PM % Maturity Ratio (.78) 1 8. (.78) (.78) (.77)

26 Short Fibre Index, Maturity HVI (table is divided into 3 pages) Lab. ICCS SFI HVICCS SFI PM % Maturity Ratio (.77) Average Median StdDev CV Min Max n

27 1 AFIS General Lab. Manufacturer Instrument Std. Test Method Repetitions 7 USTER 1 USTER Autojet 1 7 USTER 31 USTER 5 3 USTER AFIS Pro 1 38 USTER 39 USTER 1 USTER 3 USTER 5 USTER AFIS Pro internal 1 51 USTER ISO USTER internal 1 8 USTER 1 9 USTER Manufacturer 1 91 USTER AFIS Pro USTER MN USTER 935 B-PA F USTER AFIS Pro B-PA F 5 1 USTER ICCS 3 15 USTER Manufacturer USTER AFIS Pro USTER MD USTER ASTMD USTER AFIS Pro ASTM 8 13 USTER ASTMD USTER AFIS Pro ASTMD USTER AFIS Pro ASTMD USTER ASTM 19 USTER AFIS Pro ASTMD USTER 13 USTER AFIS Pro ASTMD USTER 5 13 USTER ASTM USTER AFIS Pro USTER AFIS Pro 1 15 USTER USTER 5 17 USTER USTER AFIS Pro ASTMD USTER Manufacturer USTER AFIS Pro Manufacturer 1 7 USTER AFIS Pro ASTMD USTER 71 USTER internal 1 7 USTER 88 USTER Manufacturer

28 AFIS L Length N Lab. ML CV.5 % 5% SFC mm inch % mm inch mm inch % (39.) (.3) (.9) Average Median StdDev CV Min Max n

29 3 AFIS L Length W Lab. ML CV UQL SFC mm inch % mm inch % (53.9) (18.3) (.7) (5.1) (1.7) Average Median StdDev CV Min Max n

30 AFIS D / M Diameter, Maturity Lab. D (N) CV (D(N)) Fineness IFC µm % mtex % Mat. Ratio (11) (5.) (.) (.73) Average Median StdDev.7.1. CV Min Max n

31 5 AFIS T Lab. Mean Diam. Trash Dust V. F. M. µm Cnt/g Cnt/g % (117) (15) Average Median StdDev CV Min Max n 3 3 Trash

32 AFIS N Neps Neps SCN Lab. Mean Diameter Mean Diameter Cnt/g µm µm Cnt/g () (8) (87) () Average Median StdDev CV Min Max n

33 7 aqura Length, Neps (further information see page "Multiple Devices") SFC (n) SFC (w) 5. % L (n) 5 % L (n) Lab. Repetitions <1.7 mm <1.7 mm Fibre Neps SCN mm mm % % Cnt/g Cnt/g (3.1) Average Median StdDev CV Min Max n

34 8 Multiple Devices (information not provided in the respective table) General Lab. Device Manufacturer Instrument Std. Test Method Repetitions 8 DigitalFibrograph Textechno Fibrotest 1 35 DigitalFibrograph USTER FMT 5 Causticaire Micronaire JIS 58 ALMeter internal 3 7 GravFineness SDL MK.1 ISO FMT SDL MK.1 ASTMD GravFineness RSTUz-9 9 DigitalFibrograph DigiLen ASTMD DigitalFibrograph ASTM17 93 FMT WIRA ISO 1 DigitalFibrograph 53 ICCS 5 1 FMT SDL FMT 3 ICCS 11 DigitalFibrograph Bitra 11 aqura Premier 17 aqura Premier 18 FMT Micromat ASTM 8 19 Causticaire Microscope IS 3 13 aqura Premier 131 DigitalFibrograph 53 ASTM 131 CombSorter Keisokki ASTM 131 Causticaire Fibroscope British 13 ALMeter Peyer AL1 DIN DigitalFibrograph 3 internal 1 13 DigitalFibrograph USTER 33 ABNTNBR aqura Premier 15 ALMeter Peyer Causticaire DIN GravFineness ASTMD FMT SDL FMT USDA 13 aqura Premier 5 51 aqura Premier 77 aqura Premier 3 aqura Premier

35 BCRT 1-9 Graphics of selected round test data 1 1 Micronaire Pressley-Index () HVI Micronaire HVI Tenacity ICCS gf/tex HVI Tenacity HVICCS HVI Elongation ICCS gf/tex %

36 BCRT 1-3 Graphics of selected round test data HVI Elongation HVICCS HVI.5 % SL ICCS % mm HVI UR ICCS HVI UHM HVICCS % mm HVI UI HVICCS AFIS ML N % mm

37 BCRT 1-31 Graphics of selected round test data AFIS.5 % SL N AFIS SFC N mm % AFIS ML W AFIS UQL W mm mm AFIS SFC W AFIS Fineness % mtex

38 BCRT 1-3 Graphics of selected round test data AFIS Maturity Ratio AFIS Trash Mean Diameter µm AFIS Trash Cnt/g AFIS Dust Cnt/g Cnt/g Cnt/g AFIS V.F.M. AFIS Neps Mean Diameter % µm

39 BCRT 1-33 Graphics of selected round test data AFIS Nep Cnt/g AFIS SCN Cnt/g Cnt/g Cnt/g

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