SUMMARY: DETAIL DESIGN REVIEW

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March 2, 2015 [Type here] - 1 - SUMMARY: DETAIL DESIGN REVIEW Biodiesel Reactor Improvements University of Idaho Team Liquid Gold Meeting: BAE Conference Room, 3:30, 02/26/2015 Present: Jon Van Gerpen, Ph.D., BAE Chair, Client Dev Shrestha, Ph.D., BAE Faculty, Client Keegan Duff, BAE Staff, Client Steve Beyerlein, Ph.D., ME Faculty, Adviser Andrew Engel, Team Member Brian Hanson, Team Member Connor Saxe, Team Member Gene Staggs, Team Member Summary: On February 26, 2015, members of Team Liquid Gold met with members of the BAE faculty to present a design proposal for improving the biodiesel reactor located in BAE experimental facilities. Approval to go ahead with the design was obtained, with suggestions for additional validation of design choices. On February 26, 2015 the above-listed met to review the detail design proposed by Team Liquid Gold for enclosing the biodiesel reactor operated by the BAE department. During previous meetings, the scope of the project, originally a full redesign and automation of mixing, heating, and reacting of biodiesel, had been reduced to designing a lid to enclose the existing reactor. Additional modifications were not approved based on cost limitations. During previous meetings, the clients expressed concerns that the tank lid could develop harmonics from resonant frequencies similar to those of a drum surface. The team presented that experts consider FEA frequency modal analysis of mixers mounted on vessels only essential for mixers over 100 HP. As the system motors are much less than 100 HP, the team elected to consider such an analysis as not necessary. The clients accepted the team s analysis, but requested that the team treat the lid as a drum surface and find a resonant frequency to avoid during operation. The team presented a finite analysis of four iterations of lid structural design, representing possible combinations of lid sheet thickness and the presence or absence of reinforcing webs. The design as proposed offered minimal stress loading and deflection with 100 pounds force applied at the center of the lid. The client requested that we increase the central loading to 200 pounds force or more in order to reflect upper limit design considerations. Because of this refined scope, the problem statement, goals, and design specifications were revised to focus on this narrower design. These revisions were accepted by the clients. The team presented the proposed lid layout and fabrication methods. The clients approved the

March 2, 2015 [Type here] - 2 - general design, but requested further engineering proof of analysis on the quantity and type of bolt specified to fasten the lid to the existing tank, citing concerns about edge of tank sealing. The clients noted incompatibilities between the proposed sealant (Buna-N) and recommended use of Viton sealants instead. The team is following up on the questions of bolt specification, drum head resonance, and improved FEA analysis. Viton sealant will be researched, and if appropriate, specified for tank sealing. Further research is being done into design of a system to condense methanol vapors venting from the reaction. The team is currently working to analyze concerns about the regularity of the tank diameter. Observations have indicated that the current tank is out of round when filled with biodiesel and with equipment braces mounted on it. It will be necessary to measure the tank in a completely relaxed state to define the effect of filling and bracing the tank on the roundness of the tank. If effects are noted that will impair mounting of the current design to the tank flange, these will be accounted for by revisions to the design. The delay until these measurements can be taken is not yet known, and will impact the date for parts ordering. Budget needs are well within available constraints, allowing some stretching of expenses in case revisions add cost to the project. The clients reviewed the budget plan and approved the scope of the team s expenses. The schedule proposed by the team estimates that assembly can begin on or around April 1, with the caveats of necessary redesign or parts unavailability not withstanding. The clients approved the proposed schedule. For further questions, please contact the team at engr-liquidgold@uidaho.edu or review the powerpoint attached in this document.

TEAM LIQUID GOLD 2014-15 BIODIESEL REACTOR

Updated Problem Statement SUMMARY The BAE Department at the University of Idaho operates a reactor for the production of biodiesel. The system has several needs: Reduce methanol exposure levels Enclose transesterification process Provide explosion safety with enclosure

Updated Project Goals SUMMARY The goals of the project are: Provide a stainless lid for the reactor Incorporate a hinged access hatch Provide viewports, mixer mounts, and fixtures for plumbing Include enclosure venting and methanol condensing Control potential explosion paths

Design specifications SUMMARY No materials used will react with the chemical process The design shall be cleanable without disassembly The design shall prevent methanol escape from the enclosure The design shall channel explosion hazards away from areas of use The design shall provide an illumination source to the tank interior

Overview/Functionality DESIGN DETAILS Plumbing Ports Bracing Ribs Pyrex Viewport Gear Motor Support Strut Gear Motor Facing Hatch Clamps Hinged Lid Hydraulic Motor Mount Continuous Lid Bolt Pattern Methanol Condensing Ports

Vibration Concerns DESIGN DETAILS "The possibility of any coincident frequencies between the operating speed and its harmonics and the tank structure needs to be addressed. While this is not normally a problem for smaller mixers and tanks a finite element modal analysis of the mixer-vessel-mounting structure is recommended for mixers over 100 hp." Mixer Mechanical Design Fluid Forces Weetman & Gigas 2002

Finite Element Analysis DESIGN DETAILS Four designs tested using FEA Design 1: 0.1875 Stainless Steel Plate Design 2: 0.135 Stainless Steel Plate Design 3: 0.1875 Stainless Steel Plate with ¼ -1 Double Stainless Steel Flat Bar Bracing Design 4: 0.135 Stainless Steel Plate with ¼ -1 Double Stainless Steel Flat Bar Bracing

Finite Element Analysis DESIGN DETAILS FEA Experiment Design Force Applied: 100 lbf concentrated load applied to center of tank enclosure Boundary Condition: Fixed static geometry along perimeter of the tank lid

Finite Element Analysis DESIGN 1

Finite Element Analysis DESIGN 2

Finite Element Analysis DESIGN 3

Finite Element Analysis DESIGN 4

Finite Element Analysis FEA SUMMARY Design 1: Displacement: 0.3106 Stress: 9.123 (ksi) Design 2: Displacement: 0.8067 Stress: 16.94 (ksi) Design 3: Displacement: 0.04104 Stress: 6.245 (ksi) Design 4: Displacement: 0.0572 Stress: 8.048 (ksi)

Key features DESIGN DETAILS Stainless construction Combined vent and condenser In-lid viewports and connections Sealed, fastened access hatch

Manufacturing process MANUFACTURING 1. Water jet stainless components (Bay Shore Systems) Cost: Free 2. UI Facilities Welding Cost: $129.00 3. Tank Flange Drilling Cost: Unknown 4. Assembly w/ purchased parts

Manufacturing Process TANK ENCLOSURE

Manufacturing Process TANK ENCLOSURE

Manufacturing Process TANK VIEWPORT

Manufacturing Process AGITATOR BRACE

Manufacturing Process ENCLOSURE ASSEMBLY

Manufacturing Process ENCLOSURE ASSEMBLY

Manufacturing Process DYNAMIC ENCLOSURE

Bill of Materials MANUFACTURING Part Name Quantity Manufacturer Part Number Description # of Units Unit Cost Cost Clamp 1McMaster Carr 5126A64 Hold-Down Toggle Clamp, Steel, Standard, 200 lb. Maximum Hold Capacity, 1-3/8" Long Arm 6 $ 11.15 $ 66.90 Tank Fitting 1McMaster Carr 1145K55 Weld-on Fitting for Flat Tanks, Easy-Weld Steel, 1 Pipe Size, 2-3/8" OD 4 $ 36.82 $ 147.28 Stainless Steel Plate 1Metals Depot S410 10 GA. (.135+/-) thick T304 Stainless Steel Sheet - Dull Mill Finish 1 $751.04 $ 751.04 Stainless Steel Flat Bar 1Metals Depot F5141 1/4 X 1 304 Stainless Steel Flat 2 $ 22.80 $ 45.60 Type 316 Stainless Steel Hex Head Cap Screw, 1/4"-20 Thread, 1" 1/4-1" Bolts 2McMaster Carr 93190A542 Long, Fully Threade 2 $ 6.40 $ 12.80 1/4" Nuts 1McMaster Carr 94804A029 Type 316 Stainless Steel Hex Nut, 1/4"-20 Thread Size, 7/16" Wide, 7/32" High 1 $ 9.05 $ 9.05 1/4" Washer 1McMaster Carr 90107A013 Type 316 Stainless Steel Flat Washer, Oversized, Number 12 Screw Size, 0.250" ID, 0.562" OD 1 $ 7.72 $ 7.72 1/4" Seal Washer 5McMaster Carr 93781A029 Pressure-Sealing Washer for Nuts and Washers, Zinc-Plated Steel, 1/4" Screw Size, 0.255" ID, 0.562" OD 5 $ 8.16 $ 40.80 1/16" Buna-N Rubber Ultra-Strength Oil-Resistant Buna-N Rubber, Plain Back, 1/16" Sheet 1McMaster Carr 8969K73 Thick, 12" x 24" 2 $ 17.85 $ 35.70 Silicon Sealent 1McMaster Carr 7587A3 Dow Corning Silicone Sealant, Number 732, 10.1-Ounce Cartridge 2 $ 6.47 $ 12.94 Expanded-PTFE Value Seal Gasket Tape, 0.020" Thick, 1/2" Gasket Tape 1McMaster Carr 95705K121 Wide, 50 Feet Long Roll 1 $ 41.00 $ 41.00 Pyrex Glass 1McMaster Carr 8476K21 Heat-Resistant Borosilicate Glass, Square, 10" x 10"-1/4" 1 $ 33.63 $ 33.63 Steel Sheet 1Metals Depot S110 10 GA. (.135 thick) Steel Sheet Hot Rolled Steel Sheet 1 $ 38.76 $ 38.76 Handle 1McMaster Carr 5187A2 Weld-on Stamped 304 Stainless Steel Oval-Grip Pull Handle, Dull Finish, 6-5/16" Overall Length, 1-1/2" Projection 1 $ 8.97 $ 8.97 Grand Total $1,252.19

Milestones and Tasks SCHEDULE March 1: Quoting Completed March 15: Orders to Suppliers April 1: All Parts Procured