2 Pine Trees, Chertsey Lane, Staines-upon-Thames, TW18 3HR, UK ITS Testing Services (UK) Limited (Caleb Brett - Downstream) Caleb Brett House Unit A 734 London Road West Thurrock Grays Essex RM20 3NL Contact: Mrs Claire Johnson Tel: +44 (0)1708 680200 Fax: +44 (0)1708 680247 E-Mail: Claire.johnson@intertek.com Website: www.intertek.com Laboratory locations: below s covered by the organisation and their relevant activities details Activity code Address Caleb Brett House Unit A 734 London Road West Thurrock Grays Essex RM20 3NL Local contact Mr Gary Ogborn Tel: +44(0)1708 680200 E-mail: gary.ogborn@intertek.com Petroleum and Petroleum Products A Address Unit 15 Waterston Industrial Estate Main Road Waterston Milford Haven SA73 1DP Local contact Mr A J Walsh Tel: +44 (0)1646 697675 E-Mail: adrian.walsh@intertek.com Petroleum and Petroleum Products (Aviation fuel) B Address Lakeside Shellway Raod Ellesmere Port Cheshire CH65 4LQ Local contact Mr Tony Kavanagh Tel: +44 (0)151 705 1902 E-Mail: Tony.Kavanagh@Intertek.com Petroleum and Petroleum Products C Address West Jetty Immingham Docks Immingham NE Lincolnshire DN40 2NT Local contact Ms Susan Swan Tel: +44 (0)1469 572353 E-Mail: susan.swan@intertek.com Petroleum and Petroleum Products Environmental Samples D Assessment Manager: DC1 Page 1 of 25
details Activity code Address Seal Sands Middlesbrough Cleveland TS2 1UB Local contact Dr Mike McGravey Tel: +44 (0)1642 546669 E-Mail: mike.mcgravey@intertek.com Petroleum and Petroleum Products Environmental Samples E Address South Hook LNG Terminal Company Ltd Dale Road Herbrandston Milford Haven Pembrokeshire SA73 3SU Local contact Mr A J Walsh Tel: +44 (0)1646 697675 E-Mail: adrian.walsh@intertek.com Natural Gas Environmental Samples F Address Carron Dock North Grangemouth Falkirk Stirling FK3 8UD Local contact Mr Ash Morgan Tel: +44 (0) 01324 472332. E-Mail: ashley.morgan@intertek.com Petroleum and Petroleum Products G Assessment Manager: DC1 Page 2 of 25
DETAIL OF ACCREDITATION WEST THURROCK Aviation and distillate fuels Conductivity IP 274 ASTM D2624 A Aviation turbine fuel, kerosene Burning characteristics - 24 hour Cleanliness Estimation of net heat of combustion Existent gum content - jet evaporation Fatty acid methyl esters (FAME) content IP 10 IP 565 by portable automatic particle counter ASTM D3338 IP 540 IP 585 by GC-MS with selective ion monitoring/scan detection IP 590 (HPLC) Freezing point IP 529 ASTM D7153 By automatic laser Freezing point - manual Fuel System Icing Inhibitors (FSII) Knock characteristics - supercharge ASTM D2386 IP 16 ASTM D5006 IP 119 ASTM D909 Assessment Manager: DC1 Page 3 of 25
Aviation turbine fuel, kerosene Naphthalene hydrocarbons ASTM D1840 By ultraviolet spectrophotometry A Oxidation stability - potential residue IP 138 ASTM D873 Particulate contaminant (line sampling) IP 216 ASTM D2276 Particulate contamination - laboratory filtration ASTM D5452 MIL-DTL-83133 Smoke point (manual ) IP 57, IP 598 ASTM D1322 ISO 3014 Thermal oxidation stability - jet fuel thermal oxidation tester (JFTOT) IP 323 ASTM D3241 Total acidity IP 354 ASTM D3242 By colour indicator titration Water reaction IP 289 ASTM D1094 Water separation characteristics ASTM D3948 Using a portable separometer Burner fuels derived from waste mineral oils (PFO) Sulphated ash IP 550 Assessment Manager: DC1 Page 4 of 25
Crude oil and fuel oil Sediment content - extraction IP 53 ASTM D473 EN ISO 3735 A Crude petroleum and liquid or solid petroleum products Density IP 189 IP 190 EN ISO 3838 By pyknometer Diesel and domestic heating fuels Diesel fuel Cold filter plugging point (CFPP) Ignition quality - cetane engine IP 309 EN 116 IP 41 ASTM D613 EN ISO 5165 Lubricity assessment ISO 12156-1 IP 450 Using high frequency reciprocating rig (HFRR) Manganese BS EN 16576 by ICP Fatty Acid Methyl Esters (FAME) and FAME/Diesel blends Oxidation stability IP 574, BS EN 15751 Accelerated oxidation Fuel oil Aluminium and Silicon content IP 377 ISO 10478 By inductively coupled plasma emission (ICP) and atomic absorption spectroscopy (AAS) Assessment Manager: DC1 Page 5 of 25
Fuel oil Hydrogen Sulphide IP 570 procedure A Rapid liquid phase extraction A Water and sediment content ASTM D1796 by centrifuge Gasoline, petrol Benzene content IP 429 BS EN 238 By infra red spectrometry Lead content ASTM D3237 By atomic absorption spectroscopy (AAS) Lead content IP 270 EN ISO 3830 Manganese content IP 588 EN 16135 ASTM D3831 by AAS Organic oxygenate compounds and total organically bound oxygen content Oxidation stability - induction period Phosphorus content IP 466 EN 13132 by Gas Chromatography IP 40 ASTM D525 EN ISO 7536 ASTM D3231 Assessment Manager: DC1 Page 6 of 25
Lubricating oils () Insolubles (pentane and toluene insolubles) ASTM D893 A Lubricating oils (), base oils Additive and selected elements, wear metals, and contaminants ASTM D5185 by ICP-AES Lubricating oils and additives Sulphated ash IP 163 ISO 3987 Motor and aviation-type fuels Motor fuels Petroleum distillates and aliphatic olefins Petroleum oils and synthetic Fluids Sulphated ash content Knock characteristics - octane number by motor (MON) Knock characteristics - octane number by research (RON) Bromine number - electrometric Water separability ASTM D874 IP 236 ASTM D2700 EN ISO 5163 IP 237 ASTM D2699 EN ISO 5164 IP 130 ASTM D1159 ISO 3839 ASTM D1401 Petroleum products Ash content IP 4 ASTM D482 ISO 6245 Asphaltenes IP 143 ASTM D6560 Assessment Manager: DC1 Page 7 of 25
Petroleum products Base number - Perchloric acid potentiometric titration ASTM D2896 By perchloric acid potentiometric titration A Carbon residue - Conradson IP 13 ISO 6615 ASTM D189 Carbon residue - micro IP 398 ASTM D4530 Carbon residue - Ramsbottom IP 14 ASTM D524 ISO 4262 Cloud point IP 219 EN 23015 ISO 3015 ASTM D2500 Colour - ASTM colour scale IP 196 ASTM D1500 ISO 2049 Colour - Lovibond tintometer Colour - Saybolt by automatic tristimulus Colour - Saybolt chronometer Colour of clear liquids - Platinum-Cobalt scale IP 17 ASTM D6045 ASTM D156 ASTM D1209 Assessment Manager: DC1 Page 8 of 25
Petroleum products Corrosiveness to Copper IP 154 ASTM D130 EN ISO 2160 A Coumarin content Density - oscillating U-tube Distillation (at atmospheric pressure) Distillation (at reduced pressure) IP 374 by fluorimetric and high performance liquid chromatography (HPLC) s ASTM D4052 IP 365 EN ISO 12185 ASTM D86 IP 123 EN ISO 3405 ASTM D1160 Doctor test IP 30 Dry vapour pressure equivalent (calculated) Elemental Analysis: Carbon, Hydrogen and Nitrogen IP 394 EN 13016-1 ASTM D5291 Filter blocking tendency IP 387 ASTM D2068 Flash and Fire points - Cleveland open cup IP 36 EN ISO 2592 ASTM D92 Assessment Manager: DC1 Page 9 of 25
Petroleum products Flash point - Pensky-Martens closed cup IP 34 ASTM D93 EN ISO 2719 A Flash/no Flash and Flash point - rapid equilibrium closed cup IP 523 EN ISO 3679 Hydrocarbon types - fluorescent indicator adsorption (FIA) IP 156 ASTM D1319 Low lead concentration IP 428, BS EN 237 Atomic Absorption Spectroscopy (AAS) Nitrogen ASTM D5762 by boat-inlet chemiluminescence Pour point IP 15 ASTM D97 ISO 3016 Quinizarin content - extraction spectrophotometric Specific energy (calorific value) IP 298 IP 12 Sulphur content IP 336 ISO 8754 ASTM D4294 by energy-dispersive X-ray fluorescence (ED-XRF) Assessment Manager: DC1 Page 10 of 25
Petroleum products Sulphur content IP 490 ISO 20846 ASTM D5453 By ultraviolet fluorescence A Vapour Pressure - mini ASTM D5191 Viscosity kinematic IP 71, Section 1 ASTM D445 EN ISO 3104 Water content IP 438 EN ISO 12937 by coulometric Karl Fischer titration Weak and strong acid number IP 177 ASTM D664 By potentiometric titration Petroleum products - distillate fuels Petroleum products - light and middle distillates Free Water and particulate contamination Gum content - jet evaporation Hydroperoxide number Thiol (mercaptan) sulphur content - potentiometric ASTM D4176 By visual inspection IP 131 EN ISO 6246 ASTM D381 ASTM D3703 IP 342 ASTM D3227 ISO 3012 Assessment Manager: DC1 Page 11 of 25
Petroleum products - middle distillate fuels Ignition delay and derived cetane number IP 498 EN 15195 ASTM D6890 By combustion in a constant volume chamber A Oxidation stability - accelerated IP 388 ASTM D2274 EN ISO 12205 Particulate content - laboratory filtration IP 415 Water and sediment content - centrifuge ASTM D2709 Petroleum products - middle distillates Aromatic hydrocarbons - high performance liquid chromatography (HPLC) with refractive index detection IP 391 EN 12916 By HPLC with refractive index detection Cetane index - calculation by the four-variable equation IP 380 ISO 4264 ASTM D4737 Fatty acid methyl ester (FAME) content IP579 EN 14078 By infrared spectrometry Petroleum products- middle distillates, diesel fuels and FAME Total contamination IP 440 EN 12662 By vacuum and weighing Assessment Manager: DC1 Page 12 of 25
Petroleum products and bituminous materials Petroleum products and hydrocarbon solvents Petroleum products and lubricants Water content IP 74 ASTM D95 ISO 3733 By Dean and Stark Aniline point IP 2 ASTM D611 ISO 2977 Acid or base number IP 139 ASTM D974 ISO 6618 Colour indicator titration A Petroleum products and other liquids Residual fuel oil Flash point - Abel closed cup Aluminium, silicon, vanadium, nickel, iron, sodium, calcium, zinc and phosphorous Total sediment content - hot filtration IP 170 EN ISO 13736 IP 501 By ashing, fusion and ICP- ES IP 375 ASTM D4870 ISO 10307-1 Residual fuel oil Total sediment content - thermal ageing, chemical ageing Residual fuels Cleanliness and compatibility - spot test IP 390 ASTM D4870 ISO 10307-2 ASTM D4740 Bitumen and bituminous binders Determination of solubility EN 12592IP 47 Bitumen and asphalt Kinematic viscosity EN 12595IP 319 ASTM D2170 Assessment Manager: DC1 Page 13 of 25
MILFORD HAVEN Aviation Turbine Fuel Total acidity IP354, ASTM D3242 B Corrosiveness to copper Colour Saybolt Density and relative density Distillation characteristics at atmospheric pressure Doctor test Existent gum - gum extent of aviation turbine fuel Estimation of net heat of combustion Flash point by Abel closed cup Freezing point of aviation fuels Hydrocarbon types by FIA IP154, ASTM D130 ASTM D156 ASTM D4052, IP365 IP123, ASTM D86 IP30, ASTM D4952 IP540 ASTM D3338 IP170 IP16, ASTM D2386 (manual) IP 529, ASTM D7153 (automatic) IP156, ASTM D1319 Assessment Manager: DC1 Page 14 of 25
Aviation Turbine Fuel Jet Fuel Thermal Oxidation Tester (JFTOT) - Thermal oxidation stability of gas turbine fuels IP323, ASTM D3241 B Mercaptan sulphur IP342, ASTM D3227 Naphthalene hydrocarbons in aviation turbine fuels ASTM D1840 Smoke point manual only ASTMD1322, IP 598 Sulphur content Viscosity kinematic Water separation characteristics of aviation fuels (MSEP) IP336 IP71 Section 1, ASTM D445 ASTM D3948 Assessment Manager: DC1 Page 15 of 25
ELLESMERE PORT, LUBE OILS Colour ASTM D1500 C Density IP 365 Distillation (automatic only) Elemental Analysis C, H, N ASTM D86 ASTM D5291 Flash Point (COC) IP 36 Heat of combustion (gross and net) IP 12 ASTM D240 Pour Point IP 15 ASTM D97 Refractive Index RVP (minivap) ASTM D1218 ASTM D5191 Sulphur Content IP 336 Viscosity IP 71 ASTM D445 Water Content IP 438 LUBE OILS Apparent viscosity (Cold Cranking Simulator) Evaporative Loss (Noack) ASTM D5293 ASTM D5800 SOLVENTS Distillation (automatic only) ASTM D1078 Assessment Manager: DC1 Page 16 of 25
IMMINGHAM BIODIESEL, PETROLEUM and PETROLEUM PRODUCTS Density IP 365 EN ISO 12185 ASTM D4052 D Methanol Content EN ISO 14110 Cold Filter Plugging Point IP 309 BS EN 116 Viscosity IP 71 ASTM D445 EN ISO 3104 Calcium and Magnesium EN ISO 14538 Phosphorus EN ISO 14107 Sulphur Content IP 490 EN ISO 20846 Iodine Number EN ISO 14111 Acid Value EN ISO 14104 Oxidation Stability EN ISO 14112 Water Content IP 438 EN ISO 12937 Ester Content EN ISO 14103 Assessment Manager: DC1 Page 17 of 25
BIODIESEL, PETROLEUM and PETROLEUM PRODUCTS HYDROCARBON SOLVENTS Appearance In-house IMM-LAB-SWI-146 based on client EC- A_A01 D Acidity ASTM D1613 Aromatics content In-house IMM-LAB-SWI-144 based on client UV 1 by UV/Vis Colour - Platinum cobalt Saybolt ASTM D1209 ASTM D6045 Distillation at atmospheric pressure ASTM D86 Distillation range of volatile organic liquids ASTM D1078 Flash point ASTM D93 ASTM D56 Non-volatile matter ASTM D1353 Refractive index ASTM D1218 Solvent composition In-house IMM-LAB-SWI-126 based on client GC 3 by GC-FID Water content of volatile solvents ASTM D1364 Water miscibility ASTM D1722 Assessment Manager: DC1 Page 18 of 25
TRADE EFFLUENT (to controlled water) ph In-house IMM- LAB-SWI-100 based on APHA 4500-H+ D Suspended solids In-house IMM- LAB-SWI-101 based on BS EN 872 Assessment Manager: DC1 Page 19 of 25
TEESSIDE PETROLEUM and Cold Filter Plugging Point IP 309 BS EN 116 E Colour Pt-Co (Hazen) Density Distillation ASTM D5386 ASTM D4052 IP 365 EN ISO 12185 ASTM D86 IP 123 EN ISO 3405 Ester Content EN ISO 14103 E Flash Point ASTM D93 IP 34 EN ISO 2719 Pensky Martens Closed Cup Lubricity IP 450 ISO 12156-1:2006 Motor Octane Number (MON) ASTM D2700 IP 236 EN ISO 5163 Oxidation Stability BS EN 14112 Assessment Manager: DC1 Page 20 of 25
PETROLEUM and Petroleum Distillates Paraffin, naphthene and aromatic hydrocarbon types (PNA) ASTM 5443 E Research Octane Number (RON) ASTM D2699 IP 237 EN ISO 5164 Sulphur ASTM D5453 IP 490 EN ISO 20846 Vapour Pressure ASTM D5191 IP 394 EN 13016 Viscosity ASTM D445 IP 71 ISO 3104 Assessment Manager: DC1 Page 21 of 25
PETROLEUM and Petroleum Products Water Content IP 438 EN ISO 12937 E Volatile Solvents Water Content ASTM D1364 Petroleum and Petroleum Products Water Content ASTM E203 Organic Liquids Water Content ASTM E1064 FATTY ACID METHYL ESTERS Chemical Testing Sodium BS EN 14108 E Potassium BS EN 14109 ENVIRONMENTAL SAMPLES Chemical Testing Surface water Chemical Oxygen Demand BS ISO 15705 E Suspended Solids BS EN 872 Biochemical Oxygen Demand BS EN 1899 E Assessment Manager: DC1 Page 22 of 25
SOUTH HOOK NATURAL GAS In house s in the series SHT-LAB-SOP-xx and SHT-LAB-TP-xx Composition GPA 2261:13 by GC F Incomplete combustion factor and soot index Moisture dew point Molecular weight, vapour density, relative vapour density, gross heating value, net heating value, Wobbe Index Determination of oxygen present Determination and speciation of sulphur compounds Calculation from statutory instrument 1996 number 551 gas safety regulations ASTM D5454: 11e1 SHT-LAB-SOP-06 ISO 6976:2016 and ISO 6976:2005 (superseded) by calculation SHT-LAB-TP-02 by oxygen meter ISO 19739:04 by GC NATURAL GAS Sampling Spot and composite sampling of Natural Gas during vessel discharges at South Hook LNG Terminal SHT-LAB-SOP-15 F TRADE EFFLUENT TO CONTROLLED WATERS Sampling Sampling SHT-LAB-SOP-07 F Assessment Manager: DC1 Page 23 of 25
TRADE EFFLUENT TO CONTROLLED WATERS In house s in the series SHT-LAB-SOP-xx and SHT-LAB-TP-xx Free chlorine SHT-LAB-TP-01 by Hach Test Kit F Nitrates APHA 4500-NO3-B by UV ph BS EN ISO 10523: 2012 Total suspended solids BS 6068-2.54:05 Turbidity BS EN ISO 7027-1:2016 Assessment Manager: DC1 Page 24 of 25
GRANGEMOUTH PETROLEUM and Crude Oil Water Content IP 386 G DVPE ASTM D5191 (mod) Reid Vapour Pressure (RVP) IP 69 END Assessment Manager: DC1 Page 25 of 25