VARIOUS COATING TECHNIQUES AN OVERVIEW. John A. Pasquale, III Senior Vice President P.O. Box 377 Hawthorne, NJ 07507

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VARIOUS COATING TECHNIQUES AN OVERVIEW John A. Pasquale, III Senior Vice President P.O. Box 377 Hawthorne, NJ 07507

AGENDA Features of the following Coaters Direct, Reverse and Offset Gravure Kiss Direct and Reverse Roll Slot Die Curtain Knife Over Roll Air Knife Saturation/Dip and Squeeze Similarities and Differences Preferred Applications for Use

Selection There is no universally superior coating method, only the best type for a given application Know the coating properties, coat weight or thickness requirements, and desired accuracy Analyze the substrate properties tension limitations, finish and caliper uniformity Look at the operating range and speed limitations of different coating methods Consider the cost to manufacture your products using any of the various methods Select a coater that enables you to manufacture the majority of your products successfully

Direct, Reverse and Offset Gravure Coaters Direct Both rolls run opposed to each other at same speed Reverse Anilox roll runs opposite direction of web Offset Anilox roll runs in either direction to effect film split BACKING BACKING BACKING TRANSFER ANILOX ANILOX ANILOX Direct Gravure Reverse Gravure Offset Gravure

Gravure Coaters Factors That Affect Coating Weight and Quality Applicator roll pattern, cell volume and shape Impression roll covering thickness and durometer Applicator/impression roll nip pressure Doctor blade type and position Coating viscosity and flow properties Material and finish of web being coated Web speed and operating environment

Direct Gravure Coater Rolls rotate at same speed opposed to each other Coating transferred by nip force between rolls Coating metered by engraved cell pattern BACKING ANILOX Direct Gravure Useful for applying low to medium solids at moderate to high speed Typical Coating Properties Viscosity: 10 2000 cps Wet thickness:.0001 -.003 Web speed: 25 2300 fpm Uniformity: 2%

Reverse Gravure Coater Applicator roll rotates opposite the direction of the web Coating is metered and transferred by reverse action of applicator roll, removes cell pattern Film split between applicator roll and web affects coat weight BACKING ANILOX Reverse Gravure Useful for applying low to medium solids at moderate to high speeds Typical Coating Properties Viscosity: 10 2000 cps Wet thickness:.0001 -.003 Web speed: 25 2300 fpm Uniformity: 2%

Offset Gravure Coater Transfer and Anilox rolls rotate at different speeds, affecting coating weight Two film splits further reduces coat weight Anilox roll operates in forward or reverse direction BACKING TRANSFER ANILOX Offset Gravure Useful for applying low to medium solids at moderate to high speeds Typical Coating Properties Viscosity: 50 12000 cps Wet thickness:.0001 -.005 Web speed: 25 2500 fpm Uniformity: 2%

Kiss Coater Applicator roll can be smooth or lightly engraved Coat weight based on web tension, wrap angle and roll speed This method has limited viscosity and speed range Coat weight can be further controlled by Mayer Rod unit MAYER ROD SMOOTH OR ANILOX LIFT OFF Kiss Coater with Mayer Rod Useful for applying low solids at low to moderate speeds Typical Coating Properties Viscosity: 50 1000 cps Wet thickness:.0002 -.003 Web speed: 100 1000 fpm Uniformity: 10%

Reverse Roll Coaters Applicator roll operates at 1.2-2.5 times web speed to vary coating weight Metering roll operates from zero to web speed, based on coating rheology Useful for a wide range of coating thicknesses, viscosities and speeds Typical Coating Properties Viscosity: 200 50,000 cps Wet thickness:.0008 -.018 Web speed: 25 1750 fpm Uniformity: 1% with precision rolls and bearings BACKING APPLICATOR METERING Nip Fed Reverse Roll Coater

Reverse Roll Coaters Coating applied and precisely metered onto applicator roll by gap between metering roll and applicator roll Gap determines initial coating application Gap set controlled manually or by the use of servomotors Closed loop system using thickness gauge monitoring equipment can be added Speed of metering roll with respect to applicator roll Controls coating quality Allows small changes in coating thickness

Reverse Roll Coater

Direct (Forward) Roll Coaters Much more limited in its use compared to reverse roll coater Operates over a narrow low viscosity range Ribbing may easily occur due to roll speed and gap limitations Useful for applying low to medium solids at moderate speeds Typical Coating Properties Viscosity: 20 2000 cps Wet thickness:.0005 -.008 Web speed: 100 1500 fpm Uniformity: 7% - 10%

Ribbing Defect Ribbing develops when the flow in the coating zone becomes unstable It is a function of the hydrodynamic pressure gradient and surface tension that develops in the coating zone Gap and roll speed variation are the prime variants when applying a coating of specific viscosity at a given speed When gap is the major (or only) variant (forward roll, slot die, knife, etc) the onset of ribbing occurs more readily When gap and roll speed variation can be altered (as in differential offset gravure, reverse roll, etc) ribbing is more readily eliminated Shows an example of a ribbing pattern that occurs in a roll coater - caused by small gap/low roll speed

Slot Die Coating Delivers a pre-metered amount of coating to the die Wide viscosity range vacuum box used for low viscosity coatings Die to backing roll gap and die operating angle affect coat weight Wide range of products No recirculation Operating Conditions: Viscosity: 5 20000 cps Wet thickness:.002 -.015 Line speed: 20-1750 fpm Accuracy: 2% vacuum source Coating Roll web direction vacuum box solution to scrap coating bead top die plate bottom die plate distribution manifold solution pump process measurements

Used in paper coatings, photographic films, ink jet paper, and adhesives. Operating Conditions: Viscosity: 5 5000 cps Wet thickness:.0003 -.012 Line speed: 250-1250 fpm Accuracy: 2% - 5% Curtain Coater Pre-metered amount of coating applied - dependent on flow rate, width, surface tension and coating rheology Curtain height, impingement and edge guides affect coating quality

Knife Over Roll Applies heaviest coatings over a wide viscosity range Coating speed limited by shear forces at the blade Entry contour of the blade controls penetration into the web COATING SOLUTION KNIFE COATING SUBSTRATE COATED SUBSTRATE Typical Coating Properties Viscosity: 100 50000 cps Wet thickness:.001 -.030 Web speed: 10 350fpm Uniformity: 3% - 10%

Air Knife Coating Useful for low viscosity water based coatings; knife pressure controls coverage. Coverage increases with speed & viscosity; decreases with air knife pressure. Susceptible to streaks & chatter Operates in metering and squeegee modes Operating Conditions: Viscosity: 1 500 cps Wet thickness:.0001 -.005 Line speed: 50-400 fpm - metering 125 2000 fpm - squeegee Accuracy: 5% Uncoated Web Coated Web Coating Roll Air Knife Coating Solution in Overflow Coating Pan

Saturation/Dip and Squeeze Self-metering system - uses free meniscus to apply coating Web exposure, viscosity and surface tension dependent Nip pressure can saturate or impregnate the web Typical Coating Properties Viscosity: 10 3000cps Wet thickness:.002 -.016 Web speed: 50 1000 fpm Uniformity: 7% - 10%

Summary of Coaters Coater Type Viscosity Range (cps) Wet Thickness (in.) Line Speed Range (fpm) Uniformity (%) Direct Gravure 10-2000.0001-.003 25-2300 2 Reverse Gravure 10-2000.0001-.003 25-2300 2 Offset Gravure 50-12000.0001-.005 25-2500 2 Kiss 50-1000.0002-.003 100-1000 10 Reverse Roll 200-50000.0008-.018 25-1750 1 - w/precision rolls & bearings Direct (Forward) Roll 20-2000.0005-.008 100-1500 7-10 Slot Die 5-20000.002-.015 20-1750 2 Curtain 5-5000.0003-.012 250-1250 2-5 Knife Over Roll 100-50000.001-.030 10-350 3-10 Air Knife 1-500.0001-.005 50-400 metering 125-2000 squeegee 5 Saturation/Dip & Squeeze 10-3000.002-.016 50-1000 7-10

REFERENCES The following references were used, with permission of the authors: 1. Principles of Roll Coating Equipment, by John A. Pasquale III 2. Coating Methods: Selecting the Right Coating Methods, by Dr. Edward D. Cohen Special thanks are extended to Dr. Edward D. Cohen who generously provided some of the data and visual materials he has compiled over many years of service to the industry.

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