INLINE MONITORING OF FREE WATER AND PARTICULATE CONTAMINATION OF JET A FUEL

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INLINE MONITORING OF FREE WATER AND PARTICULATE CONTAMINATION OF JET A FUEL INTERIM REPORT TFLRF No. 466 ADA by Keri M. Petersen U.S. Army TARDEC Fuels and Lubricants Research Facility Southwest Research Institute (SwRI ) San Antonio, TX for Joel A. Schmitigal U.S. Army TARDEC Force Projection Technologies Warren, Michigan Contract No. W56HZV-09-C-0100 (WD27) : Distribution Statement A. Approved for public release April 2015

Disclaimers Reference herein to any specific commercial company, product, process, or service by trade name, trademark, manufacturer, or otherwise, does not necessarily constitute or imply its endorsement, recommendation, or favoring by the United States Government or the Department of the Army (DoA). The opinions of the authors expressed herein do not necessarily state or reflect those of the United States Government or the DoA, and shall not be used for advertising or product endorsement purposes. Contracted Author As the author(s) is(are) not a Government employee(s), this document was only reviewed for export controls, and improper Army association or emblem usage considerations. All other legal considerations are the responsibility of the author and his/her/their employer(s). DTIC Availability Notice Qualified requestors may obtain copies of this report from the Defense Technical Information Center, Attn: DTIC-OCC, 8725 John J. Kingman Road, Suite 0944, Fort Belvoir, Virginia 22060-6218. Disposition Instructions Destroy this report when no longer needed. Do not return it to the originator.

INLINE MONITORING OF FREE WATER AND PARTICULATE CONTAMINATION OF JET A FUEL INTERIM REPORT TFLRF No. 466 by Keri M. Petersen U.S. Army TARDEC Fuels and Lubricants Research Facility Southwest Research Institute (SwRI ) San Antonio, TX for Joel A. Schmitigal U.S. Army TARDEC Force Projection Technologies Warren, Michigan Contract No. W56HZV-09-C-0100 (WD27) SwRI Project No. 08.19648 : Distribution Statement A. Approved for public release April 2015 Approved by: Gary B. Bessee, Director U.S. Army TARDEC Fuels and Lubricants Research Facility (SwRI )

REPORT DOCUMENTATION PAGE Form Approved OMB No. 0704-0188 Public reporting burden for this collection of information is estimated to average 1 hour per response, including the time for reviewing instructions, searching existing data sources, gathering and maintaining the data needed, and completing and reviewing this collection of information. Send comments regarding this burden estimate or any other aspect of this collection of information, including suggestions for reducing this burden to Department of Defense, Washington Headquarters Services, Directorate for Information Operations and Reports (0704-0188), 1215 Jefferson Davis Highway, Suite 1204, Arlington, VA 22202-4302. Respondents should be aware that notwithstanding any other provision of law, no person shall be subject to any penalty for failing to comply with a collection of information if it does not display a currently valid OMB control number. PLEASE DO NOT RETURN YOUR FORM TO THE ABOVE ADDRESS. 1. REPORT DATE (DD-MM-YYYY) 10-04-2015 2. REPORT TYPE Interim Report 4. TITLE AND SUBTITLE Inline Monitoring of Free Water and Particulate Contamination of Jet A Fuel 3. DATES COVERED (From - To) September 2013 April 2015 5a. CONTRACT NUMBER W56HZV-09-C-0100 5b. GRANT NUMBER 5c. PROGRAM ELEMENT NUMBER 6. AUTHOR(S) Petersen, Keri M. 5d. PROJECT NUMBER SwRI 08.19648 5e. TASK NUMBER WD 27 5f. WORK UNIT NUMBER 7. PERFORMING ORGANIZATION NAME(S) AND ADDRESS(ES) 8. PERFORMING ORGANIZATION REPORT NUMBER U.S. Army TARDEC Fuels and Lubricants Research Facility (SwRI ) TFLRF No. 466 Southwest Research Institute P.O. Drawer 28510 San Antonio, TX 78228-0510 9. SPONSORING / MONITORING AGENCY NAME(S) AND ADDRESS(ES) 10. SPONSOR/MONITOR S ACRONYM(S) U.S. Army RDECOM U.S. Army TARDEC Force Projection Technologies Warren, MI 48397-5000 12. DISTRIBUTION / AVAILABILITY STATEMENT : Dist A Approved for public release; distribution unlimited 13. SUPPLEMENTARY NOTES 11. SPONSOR/MONITOR S REPORT NUMBER(S) 14. ABSTRACT The U.S. Army is actively pursuing advanced technologies that can monitor aviation fuel cleanliness by detecting and quantifying water and particulate matter. There are several viable options but the preference is to have sensors that are in-line and can perform measurements in near real-time. Although present day particle counting technology may be sufficient for measuring solid contaminants in real time, they can not sufficiently differentiate water droplets or entrained air. The objective of this effort was to conduct an operational test of two developmental, in-line fuel sensors under real-world flow conditions. The sensors were subjected to a range of water and particulate contamination and the results were compared to standard laboratory/field methods. 15. SUBJECT TERMS Particle counting, sensor, fuel, water, particulate 16. SECURITY CLASSIFICATION OF: 17. LIMITATION OF ABSTRACT a. REPORT Unclassified b. ABSTRACT Unclassified c. THIS PAGE 18. NUMBER OF PAGES Unclassified Unclassified 11 19a. NAME OF RESPONSIBLE PERSON 19b. TELEPHONE NUMBER (include area code) Standard Form 298 (Rev. 8-98) Prescribed by ANSI Std. Z39.18 iv

EXECUTIVE SUMMARY The U.S. Army is actively pursuing advanced technologies that can monitor aviation fuel cleanliness by detecting and quantifying water and particulate matter. There are several viable options but the preference is to have sensors that are in-line and can perform measurements in near real-time. Although present-day particle counting technology may be sufficient for measuring solid contaminants in real-time, they cannot sufficiently differentiate between water droplets and solids. The objective of this effort was to conduct an operational test of two developmental, in-line fuel sensors under real-world flow conditions. The sensors were subjected to a range of water and particulate contamination and the results were compared to standard laboratory/field methods. The testing yielded some promising results but further research will be needed to move the technology forward. v

FOREWORD/ACKNOWLEDGMENTS The U.S. Army TARDEC Fuel and Lubricants Research Facility (TFLRF) located at Southwest Research Institute (SwRI), San Antonio, Texas, performed this work during the period of September 2013 through April 2015 under Contract No. W56HZV-09-C-0100. The U.S. Army Tank Automotive RD&E Center, Force Projection Technologies, Warren, Michigan administered the project. Mr. Eric Sattler (RDTA-SIE-ES-FPT) served as the TARDEC contracting officer s technical representative. Joel Schmitigal of TARDEC served as project technical monitor. The authors would like to acknowledge the contribution of the TFLRF technical support staff along with the administrative and report-processing support provided by the TFLRF administrative staff. vi

TABLE OF CONTENTS Section Page EXECUTIVE SUMMARY...v FOREWORD/ACKNOWLEDGMENTS... vi ACRONYMS AND ABBREVIATIONS... viii 1.0 OBJECTIVE AND BACKGROUND...1 2.0 TESTING PROCEDURE...1 2.1 TEST SENSORS...1 2.2 TEST CONDITIONS...1 2.3 TEST MEASUREMENTS...2 3.0 Results of Testing...2 3.1 PROGENY...2 3.2 CANTY...3 4.0 Conclusion...3 vii

ACRONYMS AND ABBREVIATIONS GPM L/m mg/l ppm RIO SwRI TARDEC gallons per minute liter per minute milligrams per liter parts per million red iron oxide Southwest Research Institute Tank Automotive Research Development and Engineering Center viii

1.0 OBJECTIVE AND BACKGROUND The objective of this effort was to conduct an operational test of in-line fuel sensors provided by the government. The sensors were designed to detect, differentiate, and quantify free water (0-30 ppm) and sediment (0-5 mg/l) independently. The testing included a comparative analysis of the sensors to standard test methods for water content and particulates. 2.0 TESTING PROCEDURE 2.1 TEST SENSORS Two sensor systems, from the following companies, were selected by TARDEC for testing in the Southwest Research Institute aviation filtration test facility: Progeny Systems Corporation J.M. Canty Inc. 2.2 TEST CONDITIONS Both sets of testing were witnessed by Joel Schmitigal (TARDEC) and a representative from the respective instrument company. Both sensors were installed in-line and subjected to the following nominal conditions: System Flow Rate: 105.7 gpm (400 L/m) Neat Jet A Baseline A-1 Test Dust at 1.0, 0.5 and 0.25 mg/l A-2 Test Dust at 1.0, 0.5 and 0.25 mg/l A-3 Test Dust at 1.0, 0.5 and 0.25 mg/l Water Challenges at 5, 10, 20, and 40 ppm Red Iron Oxide (RIO) at 1.0, 0.5 and 0.25 mg/l Lowest water detected with RIO Lowest water detected with A-1 Test Dust at 0.25mg/L 1

2.3 TEST MEASUREMENTS The following measurements were taken during each test: gravimetric samples at 5 and 20 minutes per ASTM D2276 Aqua-Glo to measure free water per ASTM D3240 particle counts by: o Parker ACM 20 o Parker IOS o Stanhope-Seta AvCount fuel flow rate differential pressure fuel temperature voltage response of in-line optical sensors. 3.0 RESULTS OF TESTING 3.1 PROGENY Joel Schmitigal (TARDEC) and Mike Strong and David Beers (Progeny Systems Corporation) visited SwRI the week of 04 November 2013 to witness testing of the Progeny instrumentation. The Progeny instrumentation was installed in-line and the following tests were performed: Neat Jet A Baseline followed by A-1 Test Dust at 1.0, 0.5, 0.25 mg/l Neat Jet A Baseline followed by A-2 Test Dust at 1.0, 0.5, 0.25 mg/l Neat Jet A Baseline followed by A-3 Test Dust at 1.0, 0.5, 0.25 mg/l Neat Jet A Baseline followed by water challenge at 5, 10, 20, 40 ppm Neat Jet A Baseline followed by Red Iron Oxide (RIO) at 1.0, 0.5, 0.25 mg/l Neat Jet A Baseline, Baseline of A-2 Test Dust at 0.25 mg/l, followed by water challenge at 5, 10, 20 ppm All data was collected and tabulated and, per TARDEC s request, submitted independently of the final report. A detailed report was to be prepared by TARDEC. 2

3.2 CANTY Joel Schmitigal (TARDEC) and Justin Halbach (J.M. Canty Inc.) visited SwRI the week of 03 November 2014 to witness testing of the Canty instrumentation. The Canty instrumentation was installed in-line and completed the following tests: Neat Jet A Baseline followed by A-1 Test Dust at 1.0, 0.5, 0.25 mg/l Neat Jet A Baseline followed by A-2 Test Dust at 1.0, 0.5, 0.25 mg/l Neat Jet A Baseline followed by A-3 Test Dust at 1.0, 0.5, 0.25 mg/l Neat Jet A Baseline followed by water challenge at 5, 10, 20, 40 ppm Neat Jet A Baseline followed by Red Iron Oxide (RIO) at 1.0, 0.5, 0.25 mg/l Neat Jet A Baseline, Baseline of A-2 Test Dust at 0.25 mg/l, followed by water challenge at 5 ppm All data was collected and tabulated and, per TARDEC s request, submitted independently of the final report. A detailed report was to be prepared by TARDEC. Overall, the Canty instrumentation was unable to operate under higher flow rates. The flow rate was limited to 29 GPM, but the desired flow rate was 105.7 GPM. There were several cases where a particle was classified as both a water droplet and dirt particulate. The sample size was also very small compared to standard particle counters. The Canty instrument was, however, able to detect and distinguish between water and dirt passing by the lens. 4.0 CONCLUSION Overall, both systems showed positive results. However, each system would require additional research and development to enhance its ability to differentiate between dirt particles and water droplets. The fuel sample size needs to be more comparable to that of the standard particle counters and results will likely need to be presented in ISO 4406 codes in order to be accepted by the industry. A more extensive discussion about each sensor will be provided in the forthcoming reports from TARDEC. 3