Irving Oil Whitegate Refinery Limited

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Irving Oil Whitegate Refinery Limited Whitegate, Midleton, Co. Cork Testing Laboratory Registration number: 258T is accredited by the Irish National Board (INAB) to undertake testing as detailed in the Schedule bearing the Registration Number detailed above, in compliance with the International Standard ISO/IEC 17025:2005 2 nd Edition General Requirements for the Competence of Testing and Calibration Laboratories (This Certificate must be read in conjunction with the Annexed Schedule of ) Date of award of accreditation: 13:04:2010 Date of last renewal of accreditation: 10:11:2014 Expiry date of this certificate of accreditation: 10:11:2019 This shall remain in force until further notice subject to continuing compliance with INAB accreditation criteria, ISO/IEC 17025 and any further requirements specified by the Irish National Board. Manager: Dr Adrienne Duff Chairperson: Issued on 10 November 2014 Mr Tom O Neill Organisations are subject to annual surveillance and are re-assessed every five years. The renewal date on this Certificate confirms the latest date of renewal of accreditation. To confirm the validity of this Certificate, please contact the Irish National Board. The INAB is a signatory of the European co-operation for (EA) Testing Multilateral Agreement (MLA) and the International Laboratory Cooperation (ILAC) Mutual Recognition Arrangement. Edition 7, 24/10/2016 258T Page 1 of 8

Schedule of Wilton Park House, Wilton Place, Dublin 2, Ireland Tel +353 1 607 3003 Fax +353 1 607 3109 E-mail inab@inab.ie Web www.inab.ie (Annex to Certificate) IRVING OIL WHITEGATE REFINERY LTD Initial Registration Date : 13-April-2010 Postal Address: (Address of other locations as they apply) Whitegate, Midleton, Co. Cork Telephone: +353 (21) 4622200 Fax: +353 (21) 4661029 E-mail: kieran.murphy@irvingoil.com Contact Name: Kieran Murphy Facilities: Normally not available for Public testing Edition 7, 24/10/2016 258T Page 2 of 8

Wilton Park House, Wilton Place, Dublin 2, Ireland Tel +353 1 607 3003 Fax +353 1 607 3109 E-mail inab@inab.ie Web www.inab.ie Schedule of THE IRISH NATIONAL ACCREDITATION BOARD (INAB) is the Irish body for the accreditation of organisations including laboratories. Laboratory accreditation is available to testing and calibration facilities operated by manufacturing organisations, government departments, educational institutions and commercial testing/calibration services. Indeed, any organisation involved in testing, measurement or calibration in any area of technology can seek accreditation for the work it is undertaking. Each accredited laboratory has been assessed by skilled specialist assessors and found to meet criteria which are in compliance with ISO/IEC 17025 or ISO/IEC 15189 (medical laboratories). Frequent audits, together with periodic inter-laboratory test programmes, ensure that these standards of operation are maintained. Testing and Calibration Categories: : Permanent laboratory calibration and testing where the laboratory is erected on a fixed location for a period expected to be greater than three years. Category B: Category C: Category D: Site calibration and testing that is performed by staff sent out on site by a permanent laboratory that is accredited by the Irish National Board. Site calibration and testing that is performed in a site/mobile laboratory or by staff sent out by such a laboratory, the operation of which is the responsibility of a permanent laboratory accredited by the Irish National Board. Site calibration and testing that is performed on site by individuals and organisations that do not have a permanent calibration/testing laboratory. Testing may be performed using (a) (b) (c) (d) portable test equipment a site laboratory a mobile laboratory or equipment from a mobile or site laboratory Standard Specification or Test Procedure Used: The standard specification or test procedure that is accredited is the issue that is current on the date of the most recent visit, unless otherwise stated. Glossary of Terms Facilities: Public calibration/testing service: Conditionally available for public calibration/testing: Normally not available for public calibration/testing: Commercial operations which actively seek work from others. Established for another primary purpose but, more commonly than not, is available for outside work. Unavailable for public calibration/testing more often than not. Laboratory users wishing to obtain assurance that calibration or test results are reliable and carried out to the Irish National Board criteria should insist on receiving an accredited calibration certificate or test report. Users should contact the laboratory directly to ensure that this scope of accreditation is current. INAB will, on request, verify the status and scope. Edition 7, 24/10/2016 258T Page 3 of 8

Analysing Heating Gases Constituents produced or used as energy sources in refineries. Hydrogen I.S. EN 15984:2011 0.1 > 100.0 Mole % Petroleum industry and products - Carbon Dioxide Determination of 0.1 > 3.0 Mole % composition of refinery heating gas and calculation of carbon content and Nitrogen calorific value - Gas 0.1 > 59.8 Mole % chromatography method. Carbon Monoxide Refinery Gas Analyser's use 0.064 > 1.5 Mole % F.I.D & T.C.D./A.I.B. Detectors Methane 0.1 > 100 Mole % Ethane 0.1 > 45 Mole % Edition 7, 24/10/2016 258T Page 4 of 8

Ethylene 0.1 > 12.5 Mole % Acetylene 0.1 > 5.0 Mole % Propane 0.1 > 100.0 Mole % Propylene 0.1 > 15.0 Mole % Propadiene 0.1 > 5.0 Mole % n-butane 0.1 > 100.0 Mole % t-2-butane 0.1 > 15.5 Mole % Edition 7, 24/10/2016 258T Page 5 of 8

C-2-Butene 0.1 > 5.0 Mole % i - Butene 0.1 > 100.0 Mole % 1 - Butene 0.1 > 10.0 Mole % ISO > Butylene 0.1 > 5.0 Mole % 1.3 > Butadiene 0.1 > 15.5 Mole % n- Pentane 0.1 > 10.0 Mole % iso > Pentane 0.1 > 10.0 Mole % Edition 7, 24/10/2016 258T Page 6 of 8

Cyclopropane 0.033 > 0.165 Mole % 1 - Pentene 0.1 > 2.0 Mole % trans -2-Pentene 0.1 > 1.0 Mole % GS -2- Pentene 0.1 > 1.5 Mole % 2-Methyl-2-Butene 0.1 > 1.0 Mole % C6 + ( C6) Included are all gaseous components containing six or more carbon molecules. n-hexane is a common example of such a component. 0.05 > 0.5 Mole % Edition 7, 24/10/2016 258T Page 7 of 8

Carbon Content & Calorific I.S. EN 15984:2011 (Heating) Value by calculation Petroleum industry and Carbon content units of g/100g products - of gas Calorific (Heating) Value units Determination of are KJ/100g of gas @ 15ºC composition of refinery heating gas and calculation of carbon content and calorific value - Gas chromatography method. Refinery Gas Analyser's use F.I.D & T.C.D./A.I.B. Detectors Edition 7, 24/10/2016 258T Page 8 of 8