PERRY JOHNSON LABORATORY ACCREDITATION, INC. Certificate of Accreditation Perry Johnson Laboratory Accreditation, Inc. has assessed the Laboratory of: (Hereinafter called the Organization) and hereby declares that Organization is accredited in accordance with the recognized International Standard: ISO/IEC 17025:2005 This accreditation demonstrates technical competence for a defined scope and the operation of a laboratory quality management system (as outlined by the joint ISO-ILAC-IAF Communiqué dated January 2009): Chemical Testing of Petroleum Products (As detailed in the supplement) Accreditation claims for such testing and/or calibration services shall only be made from addresses referenced within this certificate. This Accreditation is granted subject to the system rules governing the Accreditation referred to above, and the Organization hereby covenants with the Accreditation body s duty to observe and comply with the said rules. For PJLA: Initial Accreditation Date: Issue Date: Expiration Date: April 28, 2010 August 10, 2014 August 10, 2016 Tracy Szerszen President/Operations Manager Perry Johnson Laboratory Accreditation, Inc. (PJLA) 755 W. Big Beaver, Suite 1325 Troy, Michigan 48084 Accreditation No.: Certificate No.: 66166 L14-206-1 The validity of this certificate is maintained through ongoing assessments based on a continuous accreditation cycle. The validity of this certificate should be confirmed through the PJLA website: www.pjlabs.com Page 1 of 5
Chemical F Fuels Distillation of Petroleum Products ASTM D86 Herzog Automated Distillation Unit Heat of Combustion ASTM D240 Parr Bomb Calorimeter Lube s Cetane Index Oxidation Stability of Fuel Sediment and Water Free Water and Particulates Cetane Index (Calculated) Heat of Combustion - Precision Method High Frequency Reciprocating Rig Bio-diesel present by FTIR Cleveland Open Cup Flash Point Testing Water by Distillation Ash Ramsbottom Residue Rust and Corrosion Sulfated Ash Foam Test Pentane/Toluene Insolubles Water Separability Rotating Pressure Vessel Oxidation Stability Air Release Properties Fuel Dilution by GC Automatic Titration - TAN/TBN Direct Reading Ferrography ASTM D976 Calculation ASTM D2274 Apparatus ASTM D2276 ASTM D2709 Centrifuge ASTM D4176 ASTM D4737 ASTM D4809 Parr Bomb Calorimeter ASTM D5452 ASTM D6079 HFRR Instrument D6217 HL-0102 HL-1141A FTIR ASTM D92 Herzog Automated Flash Point Manual Flash Point Apparatus ASTM D95 ASTM D482 Muffle Furnace ASTM D524 ASTM D664 Automated Titration Unit ASTM D665 Rust Apparatus ASTM D874 Muffle Furnace ASTM D892 Foam Apparatus ASTM D893 Centrifuge ASTM D1401 Apparatus ASTM D2272 Apparatus ASTM D2896 Automated Titration Unit ASTM D3427 Apparatus ASTM D3524 Varian GC ASTM D4739 Automated Titration Unit HL-1118 Automated Titration Unit HL-1131 Predict DR-III Issue 4/14 This supplement is in conjunction with certificate #L14-206-1 Page 2 of 5
Chemical F Lube s Analytical Ferrography HL-1132 Microscope Grease Fuels and Lube s Infrared Analysis (Integra) Infrared Analysis (Omnic) - Scans Cone Penetration of Grease - Full Scale Cone Penetration of Grease - 1/2 & Dropping Point Pensky Martin closed Cup Flash Point Pour Point Copper Corrosion Conradson Carbon Residue API Gravity Kinematic Viscosity API, Specific Gravity & Density Color ASTM Sediment and Water Viscosity Index Cloud Point Sulfur Digital Densiometer Sulfur by X-Ray Fluorescence Water by Karl Fisher Apparatus Appearance HL-1140 FTIR HL-1141 FTIR ASTM D217 Penetrometer, Cone and Attachments ASTM D1403 Penetrometer, Cone and Attachments ASTM D2265 Apparatus ASTM D93 Herzog Automated Flash Point - Manual Flash Point Apparatus ASTM D97 Lawler Automated Cloud/Pour Point ASTM D130 ASTM D189 ASTM D287 Hydrometers ASTM D445 Cannon Automated Viscometers ASTM D974 ASTM D1298 Hydrometers ASTM D1500 Colorimeter ASTM D1796 Centrifuge ASTM D2270 ASTM D2500 Lawler Automated Cloud/Pour Point ASTM D3120 Mitsubishi TOX- 100 Microcoulometer ASTM D4052 Anton Parr Digital Densiometer ASTM D4294 Horiba Sulfur Analyzer ASTM D6304 KF Instruments HL-1121 Particle Count by APC HL-1185 Hiac Royko Automatic Particle Counters Transformer Dielectric Strength HL-0887 ASTM D877 Viscosity Ag Al B ASTM D445 Issue 4/14 This supplement is in conjunction with certificate #L14-206-1 Page 3 of 5
Chemical F Ba Ca Cd Cr Cu Fe K Mg Mn Mo Na Ni P Pb S Sb Si Sn Ti V Zn Chemical Properties by Infrared Spectroscopy Soot Nitration Oxidation Nitration Sulfate Anti-wear (ZnDTP) depletion of material Diesel Fuel HL-1158, HL1976 HL-1158, HL1976 HL-1140 (Quantitative), Issue 4/14 This supplement is in conjunction with certificate #L14-206-1 Page 4 of 5
Chemical Gasoline Glycol Water Water by Karl Fisher Automatic Particle Count Ferrographic Analysis Ferrographic Analysis ASTM D6304 HL-1118, D664, D4739 and D2896 HL-1118, D664, D4739 and D2896 HL-1185 HL-1131 HL-1132 (qualitative, subjective) 1. The presence of a superscript F means that the laboratory performs testing of the indicated parameter at its fixed location. Example: Outside Micrometer F would mean that the laboratory performs this testing at its fixed location. Issue 4/14 This supplement is in conjunction with certificate #L14-206-1 Page 5 of 5